CN1390623A - Microporous ceramic filter plate and its preparing process - Google Patents

Microporous ceramic filter plate and its preparing process Download PDF

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Publication number
CN1390623A
CN1390623A CN 01114048 CN01114048A CN1390623A CN 1390623 A CN1390623 A CN 1390623A CN 01114048 CN01114048 CN 01114048 CN 01114048 A CN01114048 A CN 01114048A CN 1390623 A CN1390623 A CN 1390623A
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major ingredient
ceramic filter
layer
filter plate
soil
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CN1236840C (en
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高斌
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Liaoning ring Hi Tech Co., Ltd.
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高斌
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Abstract

A microporous ceramic filter plate for solid-liquid separation of slurry material is composed of two microporous ceramic filter sheets. Each filter sheet consists of the base layer prepared from ceramic particles containing corundum particles (40-500 microns), and the surficial layer prepared from ceramic microparticles containing corundum particles (0.5-25 microns). Its advantages are high strength, high filter performance, low flow resistance, high resistance to acid corrosion, low cost and long service life.

Description

Microporous Ceramic Filter Plate And Preparation Method
The present invention relates to a kind of Microporous Ceramic Filter Plate And Preparation Method that is used for slurry material solid-liquid separation, the Microporous Ceramic Filter Plate And Preparation Method of using in particular for black, nonferrous mine beneficiation concentrate dewatering and filtering.
Present capillary ceramic plate has two types, a kind of is to adopt one-time cast-forming, and micropore is uniform isometrical hole on thickness direction, and another kind is the second pouring moulding, pour into the hollow layer structure earlier, sinter into behind hollow layer with big ceramic particle pouring filling again; Capillary ceramic plate is to use the wicking action principle, and under the water-wet state, capillary action can be passed through water, gas and solid particulate can not pass through, and the quality of screen plate filter effect is relevant with the micro-pore diameter size, and the more little filter effect of micro-pore diameter is good more, but micropore is more little, and flow resistance is then big more.One-time cast-forming, micropore is uniform isometrical hole on thickness direction, be not suitable for separating the concentrate material of the above granularity of 200 orders, because this capillary ceramic plate will satisfy filter effect, need make very little micropore, will satisfy requirement of strength simultaneously also will increase thickness, and thickness increases, flow resistance is big, and discharge capacity is low; In addition, one-time cast-forming, defectives such as pin hole, tiny crack appear in screen plate surface easily, cause strength degradation; The second pouring moulding, can overcome above-mentioned shortcoming, satisfying filter effect and do not increasing under the prerequisite of flow resistance, improve screen plate intensity, as Chinese patent: a kind of ceramic filtering board for separating solid from liquid and preparation method (patent No. 98111184) adopt aggregate and base-material to mix, aggregate is selected corundum and/or mullite and/or flint clay and/or carborundum, base-material is aluminum oxide and/or clay and/or feldspar, burn earlier and form the hollow layer structure, the big ceramic particle made from above-mentioned aggregate and base-material again, filling sinters supporter in hollow layer, and the supporter outside surface adsorbs one deck mud sintering again under negative pressure, though this capillary ceramic plate can form the hole gradient, but the hollow layer structural walls of this method cast earlier is thin to be difficult for reaching requirement, and tamp the centre, do not have the drainage passage, flow resistance is also bigger.Present capillary ceramic plate base material adopts high temperature agglomerated materials such as lime carbonate more, and lime carbonate is corroded in acidic medium easily, causes screen plate working strength in acidic medium to reduce, and phenomenons such as easy explosion occur.
The purpose of this invention is to provide a kind of slurry material solid-liquid separation that can be used in, good filtration effect, filter plate intensity height, the Microporous Ceramic Filter Plate And Preparation Method that flow resistance is little, manufacture craft is simple and direct.
The object of the present invention is achieved like this:
A kind of microporous ceramic filter plate, form by two micropore ceramic filter sheets, every micropore ceramic filter sheet comprises by granularity 40~500 μ m corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material and is the base layer formed of the ceramic particle of major ingredient and is the upper layer that the ceramic particle of major ingredient is formed by granularity 0.5~25 μ m corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material, upper layer is sprayed on the outside surface of base layer, and upper layer is one or more layers.
Above-mentioned microporous ceramic filter plate, upper layer are two-layer, and internal layer is the middle layer, and skin is an extexine, and middle layer major ingredient granularity is at 1.5~25 μ m, and extexine major ingredient granularity is at 0.5~15 μ m.
Above-mentioned microporous ceramic filter plate, base layer is a major ingredient with corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material, with clay and/or wilkinite and/or feldspar and/or Jiepai soil and/or ancient smelting soil is auxiliary material, with yellow starch gum solution and/or caking agent is the liquid bonding material, its weight proportion is: major ingredient 60~95%, auxiliary material 4~30%, liquid bonding material 1~10%, the thickness of every sheet matrix layer is at 4~25mm.
Above-mentioned microporous ceramic filter plate, the middle layer is a major ingredient with corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material, mud with clay and/or wilkinite and/or feldspar and/or Jiepai soil and/or ancient smelting soil is auxiliary material, its weight proportion is: major ingredient 50~98%, auxiliary material 2~50%, every intermediate layer thickness 0.3~0.7mm.
Above-mentioned microporous ceramic filter plate, extexine is a major ingredient with corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material, mud with clay and/or wilkinite and/or feldspar and/or Jiepai soil and/or ancient smelting soil is auxiliary material, its weight proportion is: major ingredient 55~99%, auxiliary material 1~45%, every extexine thickness 0.1~0.3mm.
Above-mentioned microporous ceramic filter plate, the matrix internal surface has groove, and groove is connected.
The preparation method of above-mentioned microporous ceramic filter plate is:
1) body material is molded into sheet after mixing stirring;
2) dry down at 10~200 ℃;
3) at 800~1400 ℃ of left and right sides sintering;
4) surface layer material is stirred be sprayed on the outside surface of matrix;
5) dry below 100 ℃;
6) at 800~1400 ℃ of left and right sides sintering;
Benefit of the present invention is:
The intensity height, drainability is good, and flow resistance is little, it is good that the selection brown corundum abrasive is done body material, the white fused alumina abrasive material is done the surface layer material acid-resistant corrosion, and manufacture craft is simple and direct, is difficult for explosion during back flushing, low cost of manufacture, life-span is long, screen plate utilization coefficient height, and energy-saving effect is remarkable, adaptability is strong, improve the concentrate product recovery rate, filtrate is limpid can avoid environmental pollution directly as industrial circulating water.
Further specify below in conjunction with drawings and Examples:
Fig. 1 capillary ceramic plate section structure synoptic diagram
Fig. 2 micropore ceramics sheet section structural representation
Fig. 3 micropore ceramics sheet matrix internal surface synoptic diagram
Embodiment 1:
As shown in Figure 1, a kind of microporous ceramic filter plate that is used for slurry material solid-liquid separation is made up of two micropore ceramic filter sheets 1.
As shown in Figure 2, a kind of microporous ceramic filter plate that is used for slurry material solid-liquid separation, wherein micropore ceramic filter sheet 1 comprises by granularity 100 μ m brown corundum abrasives and is the base layer 2 formed of the ceramic particle of major ingredient, is the middle layer 3 formed of the ceramic particle of major ingredient and is the extexine 4 that the ceramic particle of major ingredient is formed by granularity 1 μ m white fused alumina abrasive material by granularity 5 μ m white fused alumina abrasive materials.
Base layer 2 is a major ingredient with the brown corundum abrasive, is auxiliary material with the wilkinite, is the liquid bonding material with yellow starch gum solution, and its weight proportion is: major ingredient 70%, auxiliary material 20%, liquid bonding material 10%, the thickness of matrix is at 10mm.
Middle layer 3 is a major ingredient with the white fused alumina abrasive material, is auxiliary material with the bentonite slurry, and its weight proportion is: major ingredient 80%, auxiliary material 20%, intermediate layer thickness 0.3mm.
Extexine 4 is a major ingredient with the white fused alumina abrasive material, is auxiliary material with the bentonite slurry, and its weight proportion is: major ingredient 80%, auxiliary material 20%, extexine thickness 0.2mm.
As shown in Figure 3, base layer is by compression molding, and the internal surface of base layer 1 suppresses groove 6, projection 5 when compacting, and groove 6 is connected.Two were docking together when the micropore ceramics sheet used, and the part of projection is bonding, and groove forms the drainage passage.
Embodiment 2:
A kind of microporous ceramic filter plate that is used for slurry material solid-liquid separation, wherein micropore ceramic filter sheet 1 comprises by the quartzy abrasive material of granularity 200 μ m and is the base layer 2 formed of the ceramic particle of major ingredient, is the middle layer 3 formed of the ceramic particle of major ingredient and is the extexine 4 that the ceramic particle of major ingredient is formed by granularity 5 μ m white fused alumina abrasive materials by granularity 10 μ m white fused alumina abrasive materials.
Base layer 2 is a major ingredient with the brown corundum abrasive, is auxiliary material with clay and wilkinite, is the liquid bonding material with yellow starch gum solution, and its weight proportion is: major ingredient 80%, auxiliary material 15%, liquid bonding material 5%, the thickness of matrix is at 15mm.
Middle layer 3 is a major ingredient with the white fused alumina abrasive material, is auxiliary material with clay and bentonite slurry, and its weight proportion is: major ingredient 70%, auxiliary material 30%, intermediate layer thickness 0.6mm.
Extexine 4 is a major ingredient with the white fused alumina abrasive material, is auxiliary material with clay and bentonite slurry, and its weight proportion is: major ingredient 70%, auxiliary material 30%, extexine thickness 0.25mm.
The making method of above-mentioned ceramic filter is:
1) body material is molded into sheet after mixing stirring;
2) dry down at 100 ℃;
3) at 1200 ℃ of left and right sides sintering;
4) surface layer material is stirred be sprayed on the outside surface of matrix;
5) dry below 100 ℃;
6) at 1200 ℃ of left and right sides sintering;
Above-mentioned base layer is to constitute the intensity height by the big particle of granularity, resistance is little, the skeleton that discharge capacity is strong, mainly play a supportive role, outside surface sprayed surface layer at base layer, from base layer, the middle layer forms interporal lacuna hole gradient from big to small to extexine, extexine is one deck tight zone, can make ultra-thin, flow resistance is little, extexine plays main filteration, be filtered thing and be blocked on the extexine outside, can make back flushing easy like this, select brown corundum abrasive to do body material, it is good to do the surface layer material acid-resistant corrosion from corundum abrasive, carry out the high supporter of intensity earlier, spray the low upper layer of ultra-thin intensity again, technology realizes easily, is difficult for explosion during back flushing, low cost of manufacture increases the service life.Show that through actual measurement microporous ceramic filter plate of the present invention has the filtration efficiency height, screen plate utilization coefficient height, energy-saving effect is remarkable, and adaptability is strong, improves the concentrate product recovery rate, and filtrate is limpid can avoid environmental pollution directly as industrial circulating water.

Claims (7)

1. microporous ceramic filter plate, it is characterized in that: form by two micropore ceramic filter sheets, every micropore ceramic filter sheet comprises by granularity 40~500 μ m corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material and is the base layer formed of the ceramic particle of major ingredient and is the upper layer that the ceramic particle of major ingredient is formed by granularity 0.5~25 μ m corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material, upper layer is sprayed on the outside surface of base layer, and upper layer is one or more layers.
2. microporous ceramic filter plate according to claim 1 is characterized in that: upper layer is two-layer, and internal layer is the middle layer, and skin is an extexine, and middle layer major ingredient granularity is at 1.5~25 μ m, and extexine major ingredient granularity is at 0.5~15 μ m.
3. microporous ceramic filter plate according to claim 1 and 2, it is characterized in that: base layer is a major ingredient with corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material, with clay and/or wilkinite and/or feldspar and/or Jiepai soil and/or ancient smelting soil is auxiliary material, with yellow starch gum solution and/or caking agent is the liquid bonding material, its weight proportion is: major ingredient 60~95%, auxiliary material 4~30%, liquid bonding material 1~10%, the thickness of every sheet matrix layer is at 4~25mm.
4. microporous ceramic filter plate according to claim 1 and 2, it is characterized in that: the middle layer is a major ingredient with corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material, mud with clay and/or wilkinite and/or feldspar and/or Jiepai soil and/or ancient smelting soil is auxiliary material, its weight proportion is: major ingredient 50~98%, auxiliary material 2~50%, every intermediate layer thickness 0.3~0.7mm.
5. microporous ceramic filter plate according to claim 1 and 2, it is characterized in that: extexine is a major ingredient with corundum and/or mullite and/or flint clay and/or carborundum and/or quartzy abrasive material, mud with clay and/or wilkinite and/or feldspar and/or Jiepai soil and/or ancient smelting soil is auxiliary material, its weight proportion is: major ingredient 55~99%, auxiliary material 1~45%, extexine thickness 0.1~0.3mm.
6. ceramic filter plate according to claim 1 and 2 is characterized in that: the base layer internal surface has groove, and groove is connected.
7. the making method of ceramic filter plate according to claim 1 is characterized in that:
1) body material is molded into sheet after mixing stirring;
2) dry down at 10~200 ℃;
3) at 800~1400 ℃ of left and right sides sintering;
4) surface layer material is stirred be sprayed on the outside surface of matrix;
5) dry below 100 ℃;
6) at 800~1400 ℃ of left and right sides sintering.
CN 01114048 2001-06-08 2001-06-08 Microporous ceramic filter plate and its preparing process Expired - Lifetime CN1236840C (en)

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CN1236840C CN1236840C (en) 2006-01-18

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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101773746A (en) * 2010-03-05 2010-07-14 江苏势坤矿山机械有限公司 Vacuum ceramic filter plate and manufacture method thereof
CN101816859A (en) * 2010-04-09 2010-09-01 扬中市荣鑫磨具磨料有限公司 Method for forming ceramic vacuum filter plate
CN102350134A (en) * 2011-07-29 2012-02-15 王建忠 Multilayer casting filter
CN103191606A (en) * 2013-05-02 2013-07-10 张家港市金邦铝业有限公司 Ceramic filter
CN103381324A (en) * 2013-06-25 2013-11-06 蚌埠凤凰滤清器有限责任公司 Tourmaline functional ceramic filter core and preparation method thereof
CN103382126A (en) * 2013-06-25 2013-11-06 蚌埠凤凰滤清器有限责任公司 Porous ceramic filter core and preparation method thereof
CN107715574A (en) * 2017-12-08 2018-02-23 烟台核晶陶瓷新材料有限公司 Ceramic filter plate and its production technology
CN109603308A (en) * 2019-01-28 2019-04-12 常州市日臣艺术装饰材料有限公司 A kind of preparation method of ceramic filter plate
CN112473246A (en) * 2020-10-21 2021-03-12 安徽金安矿业有限公司 Efficient filtering method
CN113248238A (en) * 2021-06-04 2021-08-13 佛山市东鹏陶瓷有限公司 Dark brick with high modulus of rupture and preparation method thereof
CN113372126A (en) * 2021-06-29 2021-09-10 潍坊荣洁铸造材料有限公司 Special composite ceramic filter disc for wind power and production process thereof
CN113651633A (en) * 2021-07-27 2021-11-16 武汉工程大学 Mullite fiber reinforced silicon carbide ceramic filter tube and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN101480544B (en) * 2009-01-14 2012-05-02 黄樟焱 Double-face filter board-shaped micropore ceramic and method for producing the same

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101773746A (en) * 2010-03-05 2010-07-14 江苏势坤矿山机械有限公司 Vacuum ceramic filter plate and manufacture method thereof
CN101816859A (en) * 2010-04-09 2010-09-01 扬中市荣鑫磨具磨料有限公司 Method for forming ceramic vacuum filter plate
CN102350134B (en) * 2011-07-29 2014-12-17 江西宝安新材料科技有限公司 Multilayer casting filter
CN102350134A (en) * 2011-07-29 2012-02-15 王建忠 Multilayer casting filter
CN103191606A (en) * 2013-05-02 2013-07-10 张家港市金邦铝业有限公司 Ceramic filter
CN103382126A (en) * 2013-06-25 2013-11-06 蚌埠凤凰滤清器有限责任公司 Porous ceramic filter core and preparation method thereof
CN103381324A (en) * 2013-06-25 2013-11-06 蚌埠凤凰滤清器有限责任公司 Tourmaline functional ceramic filter core and preparation method thereof
CN103382126B (en) * 2013-06-25 2015-05-20 安徽凤凰滤清器股份有限公司 Porous ceramic filter core and preparation method thereof
CN107715574A (en) * 2017-12-08 2018-02-23 烟台核晶陶瓷新材料有限公司 Ceramic filter plate and its production technology
CN109603308A (en) * 2019-01-28 2019-04-12 常州市日臣艺术装饰材料有限公司 A kind of preparation method of ceramic filter plate
CN109603308B (en) * 2019-01-28 2021-05-14 蔡盼 Preparation method of ceramic filter plate
CN112473246A (en) * 2020-10-21 2021-03-12 安徽金安矿业有限公司 Efficient filtering method
CN113248238A (en) * 2021-06-04 2021-08-13 佛山市东鹏陶瓷有限公司 Dark brick with high modulus of rupture and preparation method thereof
CN113372126A (en) * 2021-06-29 2021-09-10 潍坊荣洁铸造材料有限公司 Special composite ceramic filter disc for wind power and production process thereof
CN113651633A (en) * 2021-07-27 2021-11-16 武汉工程大学 Mullite fiber reinforced silicon carbide ceramic filter tube and preparation method thereof

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Assignee: ANSHAN SPECIAL WEAR-RESISTING EQUIPMENT FACTORY

Assignor: Gao Bin

Contract fulfillment period: 2009.3.19 to 2011.6.8

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Denomination of invention: Microporous ceramic filter plate and its preparing process

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Assignor: Gao Bin

Contract fulfillment period: 2007.6.8 to 2021.6.8

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Denomination of invention: Microporous ceramic filter plate and its preparing process

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Address after: 114048 Anshan city of Liaoning Province Qianshan District Tanggangzi Zhen Dian Chi Gou Cun

Patentee after: Liaoning ring Hi Tech Co., Ltd.

Address before: 114048 Anshan city of Liaoning Province Qianshan District Tanggangzi Zhen Dian Chi Gou Cun Anshan special wear-resistant equipment factory

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