CN1318845C - Solid phase extraction sample bottle and thermal analysis apparatus - Google Patents
Solid phase extraction sample bottle and thermal analysis apparatus Download PDFInfo
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- CN1318845C CN1318845C CNB2004100692047A CN200410069204A CN1318845C CN 1318845 C CN1318845 C CN 1318845C CN B2004100692047 A CNB2004100692047 A CN B2004100692047A CN 200410069204 A CN200410069204 A CN 200410069204A CN 1318845 C CN1318845 C CN 1318845C
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- sample bottle
- gas
- extraction sample
- extraction
- bottle
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- 238000002414 normal-phase solid-phase extraction Methods 0.000 title claims abstract description 20
- 238000002076 thermal analysis method Methods 0.000 title claims abstract description 16
- 238000000605 extraction Methods 0.000 claims abstract description 98
- 239000007787 solid Substances 0.000 claims abstract description 7
- 239000007789 gas Substances 0.000 claims description 101
- 238000003795 desorption Methods 0.000 claims description 36
- 238000010926 purge Methods 0.000 claims description 28
- 230000005526 G1 to G0 transition Effects 0.000 claims description 25
- 239000012159 carrier gas Substances 0.000 claims description 15
- 239000000284 extract Substances 0.000 claims description 12
- 239000010453 quartz Substances 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- 125000006850 spacer group Chemical group 0.000 claims description 8
- 239000000084 colloidal system Substances 0.000 claims description 6
- 229920000620 organic polymer Polymers 0.000 claims description 6
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 6
- 102000029749 Microtubule Human genes 0.000 claims description 5
- 108091022875 Microtubule Proteins 0.000 claims description 5
- 210000004688 microtubule Anatomy 0.000 claims description 5
- 239000003463 adsorbent Substances 0.000 claims description 4
- 238000000576 coating method Methods 0.000 claims description 3
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical group C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 claims description 3
- 239000011521 glass Substances 0.000 claims description 3
- 229910052697 platinum Inorganic materials 0.000 claims description 3
- 239000004793 Polystyrene Substances 0.000 claims description 2
- 239000011248 coating agent Substances 0.000 claims description 2
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims description 2
- 239000002808 molecular sieve Substances 0.000 claims description 2
- 229920002223 polystyrene Polymers 0.000 claims description 2
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 2
- 238000004458 analytical method Methods 0.000 abstract description 11
- 238000005516 engineering process Methods 0.000 abstract description 9
- 239000007788 liquid Substances 0.000 abstract description 8
- 238000001179 sorption measurement Methods 0.000 abstract description 6
- 238000004587 chromatography analysis Methods 0.000 abstract description 3
- 238000001172 liquid--solid extraction Methods 0.000 abstract description 3
- 238000005070 sampling Methods 0.000 abstract description 3
- 238000001514 detection method Methods 0.000 abstract description 2
- 238000004321 preservation Methods 0.000 abstract description 2
- 239000007790 solid phase Substances 0.000 abstract 1
- 238000010408 sweeping Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 238000010586 diagram Methods 0.000 description 6
- 239000012530 fluid Substances 0.000 description 6
- 238000007789 sealing Methods 0.000 description 6
- 238000000197 pyrolysis Methods 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 238000002470 solid-phase micro-extraction Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 238000001228 spectrum Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 239000011261 inert gas Substances 0.000 description 3
- 230000003068 static effect Effects 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- 230000032683 aging Effects 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000000575 pesticide Substances 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- 230000005477 standard model Effects 0.000 description 2
- 239000002352 surface water Substances 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 235000013618 yogurt Nutrition 0.000 description 2
- 241001270131 Agaricus moelleri Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000004794 expanded polystyrene Substances 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000004853 microextraction Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- -1 polytetrafluoroethylene Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000004451 qualitative analysis Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000004454 trace mineral analysis Methods 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
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Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2004100692047A CN1318845C (en) | 2004-07-14 | 2004-07-14 | Solid phase extraction sample bottle and thermal analysis apparatus |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2004100692047A CN1318845C (en) | 2004-07-14 | 2004-07-14 | Solid phase extraction sample bottle and thermal analysis apparatus |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1721850A CN1721850A (en) | 2006-01-18 |
CN1318845C true CN1318845C (en) | 2007-05-30 |
Family
ID=35912317
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2004100692047A Active CN1318845C (en) | 2004-07-14 | 2004-07-14 | Solid phase extraction sample bottle and thermal analysis apparatus |
Country Status (1)
Country | Link |
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CN (1) | CN1318845C (en) |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102009003429B3 (en) | 2009-02-04 | 2010-07-01 | Joint Analytical Systems Gmbh | Apparatus and method for preparing samples for gas chromatography |
US8490466B2 (en) * | 2009-12-20 | 2013-07-23 | Agilent Technologies, Inc. | Capsule injection system for gas chromatography |
CN101852692A (en) * | 2010-04-30 | 2010-10-06 | 清华大学 | Passive filling adsorption sampling device for air volatile contaminant concentration detection |
CN102207433B (en) * | 2011-03-10 | 2012-09-26 | 长沙开元仪器股份有限公司 | Device for sealing sample |
CN103649712B (en) * | 2011-07-08 | 2015-09-02 | 株式会社日立高新技术 | Solid-phase extraction device and viscosimeter |
CN103091387A (en) * | 2011-11-02 | 2013-05-08 | 中国科学院大连化学物理研究所 | Solid sample rapid thermal desorption mass spectrometry sampling device |
CN103163013B (en) * | 2011-12-15 | 2015-04-08 | 中国科学院大连化学物理研究所 | Thermal analysis and permeable membrane compound device for solid and liquid sample injection |
CN103675082A (en) * | 2012-09-13 | 2014-03-26 | 中国科学院大连化学物理研究所 | Sample introduction device for improving detection sensitivity of ion mobility spectrometry (IMS) |
CN104458970B (en) * | 2013-09-13 | 2016-04-27 | 中国科学院大连化学物理研究所 | A kind of thermal desorption device |
CN104931623A (en) * | 2014-03-20 | 2015-09-23 | 常州仪盟核芯仪器有限公司 | Capillary column switching device |
CN105606745A (en) * | 2015-11-27 | 2016-05-25 | 中山大学惠州研究院 | Detection method for odor substances in exhaust gas of perfume and essence industry |
CN105911197B (en) * | 2016-05-25 | 2018-06-29 | 延边大学 | Automatic sample thermal desorption and liquid phase microemulsion preconcentrate device |
US9913924B2 (en) * | 2016-05-25 | 2018-03-13 | S. C. Johnson & Son, Inc. | Dispensing device |
CN106053288B (en) * | 2016-08-11 | 2018-11-30 | 北京市环境保护科学研究院 | Using the method for spherical passive sample devices measurement soil gas volatilization flux |
CN108072720A (en) * | 2016-11-11 | 2018-05-25 | 成都青山利康药业有限公司 | A kind of device for keeping sample injection bottle cleaning dry |
CN109839295A (en) * | 2017-11-27 | 2019-06-04 | 中国科学院大连化学物理研究所 | One kind being enriched with absorption-thermal desorption device for trace samplings |
CN111141858B (en) * | 2018-11-06 | 2021-07-27 | 中国科学院大连化学物理研究所 | Device of thermal analyzer interface |
CN109350995A (en) * | 2018-12-26 | 2019-02-19 | 济南大学 | A kind of solid-phase extraction column and preparation method thereof loading SBA-15 adsorbent |
CN110411800B (en) * | 2019-08-02 | 2021-09-14 | 河北大学 | Integrated dispersed solid phase extraction device and sample pretreatment method |
CN110988009B (en) * | 2019-11-22 | 2021-03-09 | 浙江大学 | Pyrolysis reaction resonant cavity for EPR spectrometer and EPR spectrometer |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001081912A1 (en) * | 2000-04-27 | 2001-11-01 | Sofia Softwareentwicklung Und Intelligente Analytik Gmbh | Metal cannula for extracting organic substances |
CN1405560A (en) * | 2002-10-31 | 2003-03-26 | 上海交通大学 | Active-carbon-fiber type solid-phase adsorption method for gas-phase chromatogram |
-
2004
- 2004-07-14 CN CNB2004100692047A patent/CN1318845C/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001081912A1 (en) * | 2000-04-27 | 2001-11-01 | Sofia Softwareentwicklung Und Intelligente Analytik Gmbh | Metal cannula for extracting organic substances |
CN1405560A (en) * | 2002-10-31 | 2003-03-26 | 上海交通大学 | Active-carbon-fiber type solid-phase adsorption method for gas-phase chromatogram |
Non-Patent Citations (2)
Title |
---|
固相微萃取新技术 马继平等,色谱,第20卷第1期 2002 * |
热解析GC用的大容量固相萃取器的开发及其基本特征的探讨 王丽丽等,浙江科技学院学报,第15卷 2003 * |
Also Published As
Publication number | Publication date |
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CN1721850A (en) | 2006-01-18 |
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Effective date of registration: 20160303 Address after: 266101 building 10, building 2, Zhuzhou Road, Laoshan District, Qingdao District, Shandong, Patentee after: Qingdao Shenghan Chromatography Technology Co., Ltd. Address before: 116023 Zhongshan Road, Liaoning, No. 457, Patentee before: Dalian Institute of Chemical Physics, Chinese Academy of Sciences |
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Denomination of invention: Solid phase extraction sample bottle and thermal analysis apparatus Effective date of registration: 20161115 Granted publication date: 20070530 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: Qingdao Shenghan Chromatography Technology Co., Ltd. Registration number: 2016990000975 |
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Date of cancellation: 20171205 Granted publication date: 20070530 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: Qingdao Shenghan Chromatography Technology Co., Ltd. Registration number: 2016990000975 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Solid phase extraction sample bottle and thermal analysis apparatus Effective date of registration: 20171211 Granted publication date: 20070530 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: Qingdao Shenghan Chromatography Technology Co., Ltd. Registration number: 2017370010091 |
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Date of cancellation: 20180823 Granted publication date: 20070530 Pledgee: Qingdao high technology financing Company limited by guarantee Pledgor: Qingdao Shenghan Chromatography Technology Co., Ltd. Registration number: 2017370010091 |
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Denomination of invention: Solid phase extraction sample bottle and thermal analysis apparatus Effective date of registration: 20200623 Granted publication date: 20070530 Pledgee: Qingdao high tech Cci Capital Ltd. Pledgor: QINGDAO SHENGHAN CHROMATOGRAPHY TECHNOLOGY Co.,Ltd. Registration number: Y2020990000662 |
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Date of cancellation: 20210601 Granted publication date: 20070530 Pledgee: Qingdao high tech Cci Capital Ltd. Pledgor: QINGDAO SHENGHAN CHROMATOGRAPHY TECHNOLOGY Co.,Ltd. Registration number: Y2020990000662 |
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