CN1314155A - Mampalon perfume and its producing method - Google Patents
Mampalon perfume and its producing method Download PDFInfo
- Publication number
- CN1314155A CN1314155A CN00113332A CN00113332A CN1314155A CN 1314155 A CN1314155 A CN 1314155A CN 00113332 A CN00113332 A CN 00113332A CN 00113332 A CN00113332 A CN 00113332A CN 1314155 A CN1314155 A CN 1314155A
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- otter
- mampalon
- essence
- perfume
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- Cosmetics (AREA)
Abstract
Mampalon perfume is extractive of mampalon perfume gland secretion, which is inducing secreted by adult male mempalon after intramuscular injection of external hormone, such as HCG in 50-100 IU, PMSG in 200-300 Iu or propionic testosterone 1-2 g continuously for 6-8 days. The secretion is taken from live mampalon and extracted. THe prepared mampalon perfume can be used to replace musk as medicine material and perfume owing to easy cultivation of mampalon and easy extraction of mampalon perfume.
Description
The present invention relates to a kind of otter essence and preparation method thereof.
Moschus is a kind of well-known famous and precious raw material, and it is the glandular sac secretions of male Moschus moschiferous, can make spice, also can be used as medicine, and purposes is very extensive, but because output is limited, thereby seem very precious, cost an arm and a leg.Developing with Moschus the material that has identical and analogous components, has a similar functions effect is the target that many scientific research personnel pursue.
The objective of the invention is to provide a kind of has similar functions with Moschus, has the pharmic function of antiinflammatory, anoxia enduring, blood pressure lowering, can make the otter essence and the preparation method thereof of fixastive again.
The objective of the invention is to realize with the following methods.Otter essence of the present invention is that grow up male mampalon intramuscular injection exogenous hormone such as HCG 50-100IU or PMSG 200-300IU or androlin 1-2 are restrained continuous 6-8 days, the product that extracts behind the fragrant liquid of the otter essence glandular secretion of induced development.
The method that otter essence of the present invention is produced is: 1, the artificial induction secretes perfume (or spice): bull mampalon intramuscular injection exogenous hormone such as HCG 50-100IU or PMSG 200-300IU or androlin 1-2 are restrained continuous 6-8 days, the fragrant liquid of the otter essence glandular secretion of induced development, sustainable 20 days.2, artificial live body is got perfume (or spice): mampalon is put into a cage, this cage make mampalon headfirst, and can then with finger touch and massage scent gland capsule, gradually to the lower edge extruding, make its row fragrant in mampalon head and middle part, afterbody Baoding from the scent gland upper end, access fragrant liquid with container.3, otter essence extracts: the crude product otter essence of taking is put into the steam distillation device, add entry 150-250 milliliter, steam distillation.In receiving bottle, add a little ether, prevent that volatile material runs off, distillate extracted with diethyl ether 5-7 time, the extract ether moiety is controlled at 35 ℃, rotation is changeed evaporation and is reclaimed ether, uses the anhydrous sodium sulfate dehydration drying then, and gained white grease is the refine otter essence.
The otter essence that the present invention produced has 28 kinds of compositions through the experiment Preliminary Identification, and wherein cyclopentadecanone accounts for 16.82%, and heptadecanone 18.04% (percentage by weight) is the main fragrance component of otter essence.Be made into 0.1% (percentage by weight) otter essence solution with normal saline, it has inhibitory action to escherichia coli, meningitis bacillus, the golden Fructus Vitis viniferae coccobacillus.To anesthetized dog intravenous injection 24mg/kg otter essence, having increases Coronary vein blood oxygen amount very significantly, reduces the arterial blood oxygen amount, reduces myocardial oxygen consumption and reduces the coefficient of oxygen utilization effect.Give into mice by intraperitoneal injection otter essence 120mg/kg in age, the white mice weightening finish is obviously grown rapidly.In emollient cream, add otter essence, make emollient cream have the soft delicate fragrance of abnormal smells from the patient and attack people and persistent characteristics.
The otter essence that the present invention produces can replace Moschus, can be widely used as medical material, can be used as spice again since mampalon be easy to culture, make otter essence to produce raw material sources guaranteed, and it is simple to produce process, has improved the added value that mampalon is cultured greatly.
Embodiment: the producing of otter essence
1, the artificial induction secretes perfume (or spice): to continuous 7 days of the male mampalon intramuscular injection of healthy adult exogenous hormone HCG 50IU, and the fragrant liquid of the otter essence glandular secretion of induced development, sustainable 20 days.2, artificial live body is got perfume (or spice): make cage type restrainer structure with No. 16 electrowelding netes, and lengthwise 25cm, point diameter 6.5cm, rear end diameter 8cm, middle-end diameter 7.5cm with mampalon headfirst, makes it climb into restrainer Baoding voluntarily.Touch and massage scent gland capsule with thumb and forefinger behind mampalon Baoding, gradually to the lower edge extruding, make its row fragrant, access fragrant liquid with 50ml tool plug vial from the scent gland upper end.3, otter essence extracts: the crude product otter essence of taking is put into the steam distillation device, add 200 milliliters of entry, steam distillation.In receiving bottle, add a little ether, prevent that volatile material runs off, distillate extracted with diethyl ether 6 times, the extract ether moiety is controlled at 35 ℃, and rotary evaporation reclaims ether, uses the anhydrous sodium sulfate dehydration drying then, and gained white grease is the refine otter essence.
Claims (4)
1, a kind of otter essence, it is characterized in that this otter essence is to growing up male mampalon intramuscular injection exogenous hormone continuous 6-8 days, the product that extracts behind the fragrant liquid of the otter essence glandular secretion of induced development, its main component cyclopentadecanone accounts for 16.82%, heptadecanone 18.04% (percentage by weight).
2, a kind of method of producing otter essence, it is characterized in that may further comprise the steps: (1), the artificial induction secreted perfume (or spice): to bull mampalon intramuscular injection exogenous hormone continuous 6-8 days, the fragrant liquid of the otter essence glandular secretion of induced development, sustainable 20 days, (2), artificial live body is got perfume (or spice): mampalon is put into a cage, this cage makes mampalon headfirst, and can be with mampalon head and middle part, afterbody Baoding, then with finger touch and massage scent gland capsule, push to lower edge gradually from the scent gland upper end, make its row fragrant, access fragrant liquid with container, (3), otter essence extracts: the crude product otter essence of taking is put into the steam distillation device, add entry 150-250 milliliter, steam distillation, in receiving bottle, add a little ether, prevent that volatile material runs off, distillate extracted with diethyl ether 5-7 time, the extract ether moiety is controlled at 35 ℃, rotation is changeed evaporation and is reclaimed ether, uses the anhydrous sodium sulfate dehydration drying then, and gained white grease is the refine otter essence.
3, the method for producing otter essence according to claim 2, when it is characterized in that artificial live body is got perfume (or spice), make cage type restrainer structure with No. 16 electrowelding netes, lengthwise 25cm, point diameter 6.5cm, rear end diameter 8cm, middle-end diameter 7.5cm, with mampalon headfirst, make it climb into restrainer Baoding voluntarily.
4, the method for producing otter essence according to claim 2 is characterized in that to bull mampalon intramuscular injection exogenous hormone be HCG 50-100IU or PMSG 200-300IU or androlin 1-2 gram.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001133322A CN1138549C (en) | 2000-03-20 | 2000-03-20 | Mampalon perfume and its producing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB001133322A CN1138549C (en) | 2000-03-20 | 2000-03-20 | Mampalon perfume and its producing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1314155A true CN1314155A (en) | 2001-09-26 |
| CN1138549C CN1138549C (en) | 2004-02-18 |
Family
ID=4583126
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB001133322A Expired - Fee Related CN1138549C (en) | 2000-03-20 | 2000-03-20 | Mampalon perfume and its producing method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1138549C (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103417576A (en) * | 2013-07-22 | 2013-12-04 | 王振英 | Method for extracting musk from musk rat sweetly |
| CN103777020A (en) * | 2014-01-24 | 2014-05-07 | 北京林业大学 | Method for determining fragrance secretion action time of forest musk deer by measuring testosterone content in excrement |
| CN104839092A (en) * | 2015-06-09 | 2015-08-19 | 重庆市药物种植研究所 | Method for manually taking musk |
-
2000
- 2000-03-20 CN CNB001133322A patent/CN1138549C/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103417576A (en) * | 2013-07-22 | 2013-12-04 | 王振英 | Method for extracting musk from musk rat sweetly |
| CN103777020A (en) * | 2014-01-24 | 2014-05-07 | 北京林业大学 | Method for determining fragrance secretion action time of forest musk deer by measuring testosterone content in excrement |
| CN103777020B (en) * | 2014-01-24 | 2016-01-20 | 北京林业大学 | A kind of method of being secreted the fragrant activity time by ight soil testosterone concentration judgement woods musk deer |
| CN104839092A (en) * | 2015-06-09 | 2015-08-19 | 重庆市药物种植研究所 | Method for manually taking musk |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1138549C (en) | 2004-02-18 |
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