Summary of the invention
Technical matters to be solved by this invention provide a kind of can realistic simulation pressure sensitive adhesive tape 180 ° and 90 ° of two kinds of forms commonly used when using, detect the method and the proving installation thereof of the pressure-sensitive class encapsulant of the test sealing property of pressure sensitive adhesive or pressure sensitive adhesive tape quality index more intuitively, accurately and effectively.
Technical scheme of the present invention is: a kind of method of testing pressure-sensitive class encapsulant sealing property is provided, it is characterized in that under steady temperature and relative humidity environment, lie in a horizontal plane on two vertical support frames respectively and sticking the combining as a whole of test board that can rotate around its vertical support frame fulcrum respectively with tested sample with two, symmetry such as is mounted with at the counterweight of weight between the outboard end of two test boards and itself and the vertical support frame contact position, under the effect of two counterweights, first and second test boards are axle with separately vertical support frame fulcrum respectively, lateral rotation takes place, timing is measured tested sample and is sealed the time of being drawn back, and is the sealing-strength index of tested sample.
The invention provides a kind of multi-functional sealing-strength proving installation of realizing technique scheme, comprise support, first test board and second test board through the sticking connection of tested sample, the counterweight that connects with test board, be used to detect the counterweight position near switch and with the time set that is electrically connected near switch, it is characterized in that on support, being provided with two vertical support frames and contour with it fixed mount, two vertical support frames are a near symmetrical setting with fixed mount, described first test board and the second test board equal in length, lie in a horizontal plane in respectively on two vertical support frames, two test boards are located in the same horizontal plane, by the sticking connection of tested sample, the end that first test board is close with second test board is placed on the fixed mount, below at least one counterweight, be provided with near switch, be electrically connected with time set near switch.
Technical scheme of the present invention also provides the method for the pressure-sensitive class encapsulant of another kind of test sealing property, it is characterized in that under steady temperature and relative humidity environment, a horizontal checkout plate and one are positioned at sticking the combining as a whole of vertical checkout plate of horizontal checkout plate one end with tested sample, wherein the horizontal checkout plate is placed on the vertical support frame and can rotates around its vertical support frame fulcrum, the vertical checkout plate is fixed on the support fixed mount, be mounted with counterweight between the outboard end of horizontal checkout plate and itself and the vertical support frame contact position, under the effect of counterweight, the horizontal checkout plate is an axle with the vertical support frame fulcrum, lateral rotation takes place, timing is measured tested sample and is sealed the time of being drawn back, and is the sealing-strength index of tested sample.
The invention provides but a kind of multi-functional sealing-strength proving installation of realizing technique scheme, comprise support, first test board and second test board through the sticking connection of tested sample, the counterweight that connects with test board, be used to detect the counterweight position near switch and with the time set that is electrically connected near switch, it is characterized in that on support, being provided with vertical support frame and contour with it fixed mount, horizontal positioned first test board on the vertical support frame, the end that first test board is adjacent with second test board is placed on the fixed mount, length is to become 90 ° of angle settings between half second test board and first test board of the first test board length, be fixed on by securing member on the fixed mount of support, join by tested sample is sticking between two test boards, be connected with counterweight on the position of lengthwise dimension 1/2nd between the first test board outboard end and itself and the vertical support frame contact position, the below of counterweight is provided with near switch, is electrically connected with time set near switch.
Aforesaid vertical support frame is the vertical support frame that has the edge of a knife, horizontal positioned test board on its edge of a knife; The osculatory of described vertical support frame and test board is positioned at 1/2nd positions of test board lengthwise dimension; Described tested sample is pressure sensitive adhesive tape or pressure-sensitive label.
Aforementioned stationary temperature is 23 ± 2 ℃; Described relative humidity is 65 ± 5%.
Compared with the prior art, advantage of the present invention is:
1. can select different method of testings according to the different using method or the use occasion of pressure sensitive adhesive tape or pressure-sensitive label.
2. when test, only consider that tested sample drawn back the employed time, the test result comparability is strong.
3. the force-bearing situation when selected method of testing is used near pressure sensitive adhesive tape or pressure-sensitive label are actual very much, therefore, the data that test obtains more can reflect the inherent quality index of pressure sensitive adhesive tape or pressure-sensitive label truly, exactly.
Embodiment
Below in conjunction with drawings and Examples the present invention is further elaborated.
Among Fig. 1, the existing support 1 of holding the viscosity tester is provided with door type frame formula test stand 2, test stand is fixedly connected by securing member 9 and vertically disposed second test board 3, same vertically disposed first test board 4 glues connection with second test board and the other end connects with counterweight 6 through tested sample 5, the below of counterweight be provided for detecting the counterweight position near switch 7.First and second test boards that post tested sample are vertically hung on door type frame formula test stand, the lower end hangs the counterweight of predetermined weight, breaks away from the required time fully with sticking displacement that takes off of tested sample behind the certain hour or tested sample and measures the ability that the tested sample opposing pulls.
Owing to hold viscosity when test doing, first and second test boards are on a vertical plane, only depend on counterweight to apply downward acting force (to tested sample and the simple shearing force of Yan Weiyi) in vertical direction, the force direction that this and pressure sensitive adhesive tape or pressure-sensitive label are actual to be born when using is not inconsistent, measure like this to hold the viscosity data directly perceived inadequately to the quality situation reflection of pressure sensitive adhesive tape or pressure-sensitive label, accurately.
Embodiment 1:
The structure of a sealing-strength proving installation embodiment as shown in Figure 2.
Among Fig. 2, vertical support frame 28-1 is set on support 21,28-2 and contour with it fixed mount 22, to be that axle is approximate with the fixed mount be symmetrical arranged equidistantly for two vertical support frames, first test board 24 and the second test board 23-1 equal in length, lie in a horizontal plane in respectively on two vertical support frames, two test boards are located in the same horizontal plane, by tested sample 25 sticking connection, wherein the end that first test board is adjacent with second test board is placed on the fixed mount, the counterweight 26-1 and the 26-2 of weight such as be mounted with between the outboard end of two test boards and itself and the vertical support frame contact position on the position of lengthwise dimension 1/2nd respectively, at least be provided with near switch 27 in the below of a counterweight (being counterweight 26-1 among the figure), be electrically connected (not shown) with time set near switch.
Wherein vertical support frame is the vertical support frame that has the edge of a knife, the osculatory of its vertical support frame edge of a knife and test board is positioned at 1/2nd positions of test board lengthwise dimension, the position of the coupled position of the counterweight and second test board lengthwise dimension 1/2nd between test board outboard end and vertical support frame contact position (in detail can referring to shown in Fig. 4); First test board and second test board all are 180 ° of settings of level.
Among Fig. 4, if the length of test board is 2L, then its osculatory 24-1 with vertical support frame is positioned at lengthwise dimension L place, for the ease of with the support edge of a knife contacting partly, on the osculatory position shallow grooves can be set; On the position (i.e. 1/2nd L places) of lengthwise dimension 1/2nd between test board outboard end and the vertical support frame osculatory place, counterweight hook 20 is set is used to articulate counterweight.
The manufactured materials of above-mentioned test board is 1Cr18Ni9Ti, and first test board and the second test board length are 160mm, and width is 80mm, and thickness is 2mm, pastes the surface of sample and handles through polishing, requires roughness to be not more than 0.4.
The counterweight of test usefulness comprises that hook highly is 75mm, and quality is two kinds of 500 ± 10g and 1000 ± 20g.
The horizontal width of vertical support frame is identical with the width dimensions of test board.
Represented the paste position of tested sample on test board in the present embodiment among Fig. 5, if the width of test board is L, then the width of tested sample is 1/2nd L, its length is two L, wherein the stickup length of tested sample 25 on first test board 24 and the second test board 23-1 is a L, leaves the space about 2mm between first and second test boards.
The method of its test is:
(1) specimen preparation: cut long 120mm with sampling knife, the sample of wide 40mm 23 ± 2 ℃ of temperature, is placed standby more than 2 hours under the condition of relative humidity 65 ± 5%.
(2) testing procedure:
A. dip in Wiping material and get clean-out system and clean first test board and second test board, with clean gauze it is carefully dried then, clean so repeatedly more than three times, until on the workplace of test board through visual reach cleaning till.
B. 23 ± 2 ℃ of temperature, under the condition of relative humidity 65 ± 5%, having on the experiment porch of vertical edges, the support of first test board is close to the vertical edges of platform, again second test board is placed on the platform and align with first test board, sample pasted according to position shown in Figure 5 be placed on first test board and second test board that aligns on the platform, leave the space about 2mm between two plates.With rubber roller [with the about 84cm of diameter (not comprising rubber) that rubber coats, steel wheel of the about 45cm of width.Rubber hardness (Shao Er A type) is (80 ± 5) °, and thickness is about 6mm; Quality is (2000 ± 50) g, during roll extrusion, can only put on the sample with the power that results from the pressure roller quality] roll extrusion, the number of times of roll extrusion is generally reciprocal three times.
C. sample is after pasting on the test board, placed 20 minutes, test board is transferred on the sealing-strength proving installation, first and second test boards are lain in a horizontal plane on the vertical support frame naturally, require the edge of a knife of vertical support frame to aim at the osculatory at the first and second test board back sides; With hook the counterweight chosen is hanging on the test board then, openhandedly presses the timing button when driving counterweight, time set is connected timing signal loop, opening entry test duration.
D. drawn back when tested sample, when counterweight fell, near switch motion, time set disconnected the timing signal loop, stops timing.
Present embodiment is used for the situation that the actual face of sealing of simulation test is a plane (180 °) (as common employed commodity extranal packing box), under the action of gravity of weight counterweights such as two, first and second test boards are divided into axle with the blade portion of separately vertical support frame respectively, lateral rotation takes place (among the figure for being axle with two edges of a knife, two test boards are respectively and rotate from right to left and rotate from left to right), actual loading situation with the sealing tape of imitation commodity extranal packing box, timing is measured tested sample and is sealed the time of being drawn back, and is the sealing-strength index of tested sample.
Because during the present embodiment test, very near the practical application force-bearing situation of pressure sensitive adhesive tape or pressure-sensitive label, therefore, the data that test obtains more can reflect the inherent quality situation of pressure sensitive adhesive tape or pressure-sensitive label series products to the method for testing of selection intuitively, exactly.
Embodiment 2:
The structure of another sealing-strength proving installation embodiment as shown in Figure 3.
Among Fig. 3, length that different with Fig. 2 is is to become 90 ° of angle settings between half the second test board 23-2 and first test board of first test board, 24 length, second test board is fixed on the fixed mount 22 of support by securing member 29, vertical support frame 28-1 goes up horizontal positioned first test board 24, the contiguous end of first test board and second test board is placed on the fixed mount 22, glue connection by tested sample 25 between two test boards, be connected with counterweight 26 on the position of lengthwise dimension 1/2nd between the first test board outboard end and itself and the vertical support frame contact position, the below of counterweight is provided with near switch 27, is electrically connected (not shown) near switch with time set.All the other same Fig. 2.
Wherein first test board is a square, and the length of side is 80cm, and thickness is 2mm; The second test board length is 160mm, and width is 80mm, thickness 2mm, the position of the osculatory of second test board and counterweight hitch point as shown in Figure 4, all the other are with embodiment 1.
Represented the paste position of tested sample on test board in the present embodiment among Fig. 6, if the width of test board is L, then the width of tested sample is 1/2nd L, its length is one and 1/2nd L, wherein the stickup length of tested sample 25 on first test board 24 is a L, stickup length on the second test board 23-2 is 1/2nd L, leaves the space about 2mm between first and second test boards.
Specimen preparation and testing procedure in the present embodiment method of testing are substantially the same manner as Example 1, and difference is second test board
Be fixed on by securing member on the fixed mount of support, the paste position of tested sample on test board undertaken by position shown in Figure 6, and all the other processes are identical with embodiment 1 with step, no longer repeat at this.
Present embodiment is used for the situation that the actual face of sealing of simulation test is a right angle (90 °) (as common employed commodity inner packaging box), under the action of gravity of counterweight, second test board is divided into axle with the blade portion of vertical support frame, lateral rotation takes place (among the figure for being axle with the edge of a knife, rotate from right to left), seal the actual loading situation of pressure sensitive adhesive tape or pressure-sensitive label with imitation commodity inner packaging box, timing is measured tested sample and is sealed the time of being drawn back, and is the sealing-strength of tested sample.
When adopting the present invention to test the sealing-strength of pressure sensitive adhesive tape or pressure-sensitive label, can select different method of testings according to the different using method of pressure sensitive adhesive tape or pressure-sensitive label.If the actual face of sealing is a plane, can select embodiment 2 described 180 ° of sealing-strength method of testings; If the actual face of sealing is a right angle, can select embodiment 3 described 90 ° of sealing-strength method of testings.During actual test, the employed time when only considering that pasting a sample is drawn back, survey suitable timer range by choosing, the test selectable range is extremely wide, and short tested several seconds, and the long hundreds of tested hour does not wait.
Because the present invention is when testing tested sample, the method of testing of selecting is very near the actual use stressing conditions of pressure sensitive adhesive tape or pressure-sensitive label product, therefore, test the inherent quality that the data that obtain more can reflect pressure sensitive adhesive tape or pressure-sensitive label product efficiently and accurately.
The present invention can be widely used in the sealing-strength test that various pressure sensitive adhesives seal adhesive product (as the joint sealing pressure sensitive adhesive tape or seal label etc.).