CN1183449A - Preparation method of antifogging cleaning liquid for glass - Google Patents
Preparation method of antifogging cleaning liquid for glass Download PDFInfo
- Publication number
- CN1183449A CN1183449A CN 97106187 CN97106187A CN1183449A CN 1183449 A CN1183449 A CN 1183449A CN 97106187 CN97106187 CN 97106187 CN 97106187 A CN97106187 A CN 97106187A CN 1183449 A CN1183449 A CN 1183449A
- Authority
- CN
- China
- Prior art keywords
- preparation
- glass
- essence
- cleaning cream
- resistant cleaning
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000011521 glass Substances 0.000 title claims abstract description 40
- 238000004140 cleaning Methods 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000007788 liquid Substances 0.000 title abstract 2
- 239000000203 mixture Substances 0.000 claims abstract description 12
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000011347 resin Substances 0.000 claims abstract description 10
- 229920005989 resin Polymers 0.000 claims abstract description 10
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 10
- 239000010703 silicon Substances 0.000 claims abstract description 10
- 239000004094 surface-active agent Substances 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical group O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000008367 deionised water Substances 0.000 claims abstract description 3
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 3
- 229910052731 fluorine Inorganic materials 0.000 claims abstract description 3
- 239000011737 fluorine Substances 0.000 claims abstract description 3
- 239000002994 raw material Substances 0.000 claims abstract description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 27
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 15
- 239000006071 cream Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 10
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 7
- -1 polysiloxane Polymers 0.000 claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 125000000217 alkyl group Chemical group 0.000 claims description 5
- 229920001296 polysiloxane Polymers 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000006210 lotion Substances 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 238000010792 warming Methods 0.000 claims description 4
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 238000005660 chlorination reaction Methods 0.000 claims description 3
- FWDBOZPQNFPOLF-UHFFFAOYSA-N ethenyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)C=C FWDBOZPQNFPOLF-UHFFFAOYSA-N 0.000 claims description 2
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 claims description 2
- 239000000428 dust Substances 0.000 abstract description 3
- 229920005862 polyol Polymers 0.000 abstract description 2
- 150000003077 polyols Chemical class 0.000 abstract description 2
- 230000003068 static effect Effects 0.000 abstract description 2
- 230000000855 fungicidal effect Effects 0.000 abstract 1
- 239000000417 fungicide Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000009413 insulation Methods 0.000 description 4
- 239000003595 mist Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 230000002688 persistence Effects 0.000 description 3
- 125000001153 fluoro group Chemical group F* 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 229920005479 Lucite® Polymers 0.000 description 1
- 206010039203 Road traffic accident Diseases 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
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- Detergent Compositions (AREA)
Abstract
The present invention provides a preparation method of antifog cleaning liquor for glass, its raw material composition includes (wt%) 1-5% of polyol, 1-10% of fluorine-containing resin, 30-55% of silicon surfactant, 0.1-0.05% of essence, 0.3-5% of fungicide and the rest is deionized water. Compared with the prior art, the preparation method of the glass antifogging cleaning liquid has the characteristics of scientific formula, easy processing, convenient use, multiple purposes and the like, can be used for surface antifogging cleaning of various organic glass and inorganic glass products, and has the functions of static resistance, dust resistance and the like, thereby having good popularization and use values.
Description
The present invention relates to a kind of preparation method of sanitising agent, specifically a kind of preparation method of glass fogging-resistant cleaning cream.
The windshield glass of common glasses lens, the glass vision panel of motorcycle helmet, automobile and the glazed door of dwelling house etc. are easy to tie mist in cold season and the transparency that reduces glass.If on the glass vision panel of the windshield glass of automobile, motorcycle helmet, tie the sight line that mist will block the officer, influence the normal driving of officer to vehicle, its harm is very serious.In order to solve the cold season moisture at various knot mists on glass, reduce because of the knot mist blocks sight line because of a various traffic accident, people have developed various glass antidimmers, to prevent or to reduce moisture at formation mist film on glass.The kind of the glass antidimmer of selling on market at present is a lot, its Chemical Composition mostly is the polyol blends of ethylene glycol, glycerol or Virahol, the deficiency that the glass antidimmer that is mixed with above-mentioned chemical substance in use exists is that anti-fog performance is relatively poor, persistence is low, and the effect of not keeping a public place clean.
It is strong and have a preparation method of the glass fogging-resistant cleaning cream of the effect of keeping a public place clean to the purpose of this invention is to provide a kind of anti-fog performance height, persistence.
The objective of the invention is to realize in the following manner, in the mixture of the polyvalent alcohol that has antifogging agent now, fluoro containing polymers resin and silicon-containing surfactant have been added, thereby improved anti-fog effect, increased elimination electrostatic function, overcome because of the glass surface static electrification and adsorbed the defective that dust influences the glass transparent degree.In addition because fluoro containing polymers resin the adhering in the antifogging agent at glass surface; thereby the surface of glass also played the certain protection effect; not only can prevent the scuffing of glass; and the fine vestige that glass surface has scratched remedied; eliminate the trickle cut of glass surface to ray refraction, thereby can increase the smooth finish and the transparency of glass.
The preparation method of glass fogging-resistant cleaning cream, its raw material percentage composition is that polyvalent alcohol 1-5%, fluorine resin 1-10%, Silicon surfactant 30-55%, essence 0.1-0.05%, sterilant 0.3-5%, surplus are deionized water.
Polyvalent alcohol can be ethylene glycol, glycerol, Virahol one or more a mixture wherein, is preferably ethylene glycol.
Silicon-containing surfactant can be one or more the mixture in alkyl polysiloxane, vinyltriethoxysilane, r-aminopropyl triethoxysilane, the rare acyloxy Trimethoxy silane of r-methyl-prop, the r-r-chloropropyl trimethoxyl silane, is preferably alkyl polysiloxane.The alkyl polysiloxane chemical molecular formula is: RSi (CH
3)
2[Si (CH
3)
2] m (CH
2)
3O (CH
2CH
2O) nHm=3 n=4-12 R=CH
3Or
The chemical molecular formula of fluoro-resin is:
What sterilant adopted is tetradecyl xylylene chlorination ammonia.
Essence is common makeup essence.
The preparation method of glass fogging-resistant cleaning cream is: mix in the reactor with ethylene glycol and water adding belt stirrer and heating jacket in proportion, be warming up to 85 ℃, the adding Silicon surfactant stirs and is incubated 30 minutes, be cooled to 50 ℃ again, add Virahol, fluoro-resin, essence and sterilant while stirring, continue to stir 5-10 minute, and material is emitted be cooled to after the room temperature to such an extent that transparent lotion be product of the present invention.
What sterilant adopted is tetradecyl xylylene chlorination ammonia.
Essence is common makeup essence.
Embodiment one:
Taking by weighing 48 kilograms of 1 kilogram of ethylene glycol, 0.5 kilogram of glycerol, water adds in the reactor of belt stirrer and heating jacket and mixes, be warming up to 85 ℃, add 45 kilograms of Silicon surfactants, insulation insulation 30 minutes stirs, be cooled to 50 ℃ and add each 0.002 kilogram in 0.5 kilogram of Virahol, 5 kilograms of fluoro-resin, essence and sterilant, continue to stir 10 minutes, and material is emitted be cooled to after the room temperature to such an extent that transparent lotion be product of the present invention.
Embodiment two:
Taking by weighing 36 kilograms of 5 kilograms of ethylene glycol, 0.5 kilogram of glycerol, water adds in the reactor of belt stirrer and heating jacket and mixes, be warming up to 85 ℃, add 50 kilograms of drawing together property of silicon face agent, insulation insulation 30 minutes stirs, be cooled to 50 ℃ and add each 0.002 kilogram in 0.5 kilogram of Virahol, 8 kilograms of fluoro-resin, essence and sterilant, continue to stir 10 minutes, and material is emitted be cooled to after the room temperature to such an extent that transparent lotion be product of the present invention.
The operating position contrast of glass fogging-resistant cleaning cream of the present invention and existing polyalcohol antifoggant:
The antifog persistence cleaning action of the name of an article
2 hours left and right differences of the product of prior art
Product of the present invention is good about 2 days
Glass fogging-resistant cleaning cream of the present invention can be used for the table of various lucite and unorganic glass goods The face fog-proof cleaning has the functions such as antistatic dust protection.
Using method is identical with the simple glass antifoggant.
The preparation method of glass fogging-resistant cleaning cream of the present invention is compared with existing technology, and has prescription section Learn, be easy to the characteristics such as processing, easy to use, one-object-many-purposes, thereby, have good popularization and make Use value.
Claims (6)
1. the preparation method of glass fogging-resistant cleaning cream is characterized in that the raw material percentage composition is that polyvalent alcohol 1-5%, fluorine resin 1-10%, Silicon surfactant 30-55%, essence 0.1-0.05%, sterilant 0.3-5%, surplus are deionized water.
2. the preparation method of glass fogging-resistant cleaning cream according to claim 1 is characterized in that polyvalent alcohol can be ethylene glycol, glycerol, Virahol one or more a mixture wherein, is preferably ethylene glycol.
3. the preparation method of glass fogging-resistant cleaning cream according to claim 1, it is characterized in that silicon-containing surfactant can be one or more the mixture in alkyl polysiloxane, vinyltriethoxysilane, r-aminopropyl triethoxysilane, the rare acyloxy Trimethoxy silane of r-methyl-prop, the r-r-chloropropyl trimethoxyl silane, is preferably alkyl polysiloxane.
4. the preparation method of glass fogging-resistant cleaning cream according to claim 1, what it is characterized in that the sterilant employing is tetradecyl xylylene chlorination ammonia.
5. the preparation method of glass fogging-resistant cleaning cream according to claim 1 is characterized in that essence is common makeup essence.
6. the preparation method of glass fogging-resistant cleaning cream according to claim 1, it is characterized in that the preparation method is: mix in the reactor with ethylene glycol and water adding belt stirrer and heating jacket in proportion, be warming up to 85 ℃, the adding Silicon surfactant stirs and is incubated 30 minutes, be cooled to 50 ℃ again, add Virahol, fluoro-resin, essence and sterilant while stirring, continue to stir 5-10 minute, material is emitted be cooled to after the room temperature to such an extent that transparent lotion be product of the present invention.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 97106187 CN1183449A (en) | 1997-11-06 | 1997-11-06 | Preparation method of antifogging cleaning liquid for glass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 97106187 CN1183449A (en) | 1997-11-06 | 1997-11-06 | Preparation method of antifogging cleaning liquid for glass |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1183449A true CN1183449A (en) | 1998-06-03 |
Family
ID=5168452
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 97106187 Pending CN1183449A (en) | 1997-11-06 | 1997-11-06 | Preparation method of antifogging cleaning liquid for glass |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1183449A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100354222C (en) * | 2002-08-01 | 2007-12-12 | 中央硝子株式会社 | Coating agent for forming antifogging film and method for forming antifogging film using same |
| CN103740333A (en) * | 2013-11-27 | 2014-04-23 | 南通晶鑫光学玻璃有限公司 | Long-acting decontamination anti-fog agent for glass, and preparation method thereof |
| CN106350237A (en) * | 2016-08-30 | 2017-01-25 | 东兴华鸿光学科技有限公司 | Decontaminating and fog remover of spectacle lens |
| CN106833524A (en) * | 2016-12-28 | 2017-06-13 | 于文 | Glass pane antifoggant and preparation method thereof in automobile |
| CN109852492A (en) * | 2018-12-26 | 2019-06-07 | 李沛泽 | A kind of automotive glass water |
-
1997
- 1997-11-06 CN CN 97106187 patent/CN1183449A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100354222C (en) * | 2002-08-01 | 2007-12-12 | 中央硝子株式会社 | Coating agent for forming antifogging film and method for forming antifogging film using same |
| CN103740333A (en) * | 2013-11-27 | 2014-04-23 | 南通晶鑫光学玻璃有限公司 | Long-acting decontamination anti-fog agent for glass, and preparation method thereof |
| CN106350237A (en) * | 2016-08-30 | 2017-01-25 | 东兴华鸿光学科技有限公司 | Decontaminating and fog remover of spectacle lens |
| CN106833524A (en) * | 2016-12-28 | 2017-06-13 | 于文 | Glass pane antifoggant and preparation method thereof in automobile |
| CN109852492A (en) * | 2018-12-26 | 2019-06-07 | 李沛泽 | A kind of automotive glass water |
| CN109852492B (en) * | 2018-12-26 | 2020-12-15 | 李沛泽 | Glass water for automobile |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |