CN118014589A - Sample management method, device and system and nonvolatile storage medium - Google Patents
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- 238000007726 management method Methods 0.000 title claims abstract description 49
- 238000001514 detection method Methods 0.000 claims abstract description 130
- 238000004458 analytical method Methods 0.000 claims abstract description 26
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- 238000004806 packaging method and process Methods 0.000 claims 1
- 239000000523 sample Substances 0.000 description 128
- 238000007689 inspection Methods 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
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Abstract
The invention discloses a sample management method, a device, a system and a nonvolatile storage medium. Wherein the method comprises the following steps: acquiring information of all samples including the comparison sample, wherein all the samples are planted with electronic tags with safety mechanisms, and the electronic tag serial numbers, answer results of the comparison sample and whether three pieces of information belonging to the comparison sample are not opened to a monitored detector; uniformly numbering all samples including the comparison sample; obtaining detection results and detection numbers of all samples including the comparison sample; judging whether the detection error of the sample for comparison is within a preset error threshold, if so, determining the batch detection analysis specification, and if not, determining that the batch detection analysis is not enough. The invention solves the problem that the supervision side is difficult to discover the nonstandard laboratory analysis of the detection side in time.
Description
Technical Field
The invention relates to the technical field of sample inspection, in particular to a sample management method, a device, a system and a nonvolatile storage medium.
Background
With the development of the economic society, the inspection and detection mechanism in China is rapidly developed, and 2021, china shares 51949 inspection and detection mechanism and sends out 6.84 parts per million inspection and detection reports. But the phenomenon of nonstandard inspection and detection behaviors is quite remarkable, and in 2018, the national accumulated inspection and detection institutions exceed 4.5 ten thousand times, and nearly three-component institutions are subjected to administrative treatment and punishment in different degrees.
At present, as the supervisory side, including the government supervisory department or the internal supervisory department of the inspection and detection mechanism, mainly relies on management means such as random spot check and account checking to check, lacks effective technical means support, the supervisory side is difficult to discover that laboratory analysis of the detection side is not standard in time, and the problem that data distortion occurs and even the detection result is directly forged without detection, and phenomena such as sample exchange by a collusion detector are caused.
In view of the above problems, no effective solution has been proposed at present.
Disclosure of Invention
The embodiment of the invention provides a sample management method, a device, a system and a nonvolatile storage medium, which at least solve the problems that a supervision party is difficult to find out that laboratory analysis of a detection party is not standard in time, data distortion occurs, even a detection result is directly forged without detection, and samples are exchanged by a collusion detection personnel.
According to an aspect of an embodiment of the present invention, there is provided a sample management method including: acquiring information of all samples including the comparison sample, wherein all samples are planted with electronic tags with a safety mechanism, the information at least comprises an electronic tag serial number, and at least the electronic tag serial number, an answer result of the comparison sample and whether three pieces of information belonging to the comparison sample are not opened to a monitored detection party; uniformly detecting all samples including the comparison samples, wherein the detection numbers are in one-to-one correspondence with the serial numbers of the electronic tags; obtaining detection results and detection numbers of all samples including the comparison sample; judging whether the detection error of the comparison sample is within a preset error threshold according to the one-to-one correspondence between the detection serial number and the electronic tag serial number, if so, determining that the batch detection analysis is standard, and if not, determining that the batch detection analysis is not standard.
Optionally, the method further comprises: all samples, including the alignment samples, are partially or fully reordered.
Optionally, the sample for alignment comprises: samples of the same container package or no container package, the detection result of which is mastered by a supervisory party; when the sample is liquid or gas, selecting partial or all parallel samples, and quantitatively adding substances containing analysis items.
According to another aspect of an embodiment of the present invention, there is also provided a sample management apparatus including: the first acquisition module is used for acquiring information of all samples including the comparison sample, wherein all the samples are planted with electronic tags with a safety mechanism, the information at least comprises an electronic tag serial number, and at least the electronic tag serial number, an answer result of the comparison sample and whether three pieces of information belonging to the comparison sample are not opened to a monitored detection party; the execution module is used for uniformly carrying out detection numbers on all samples including comparison samples, wherein the detection numbers are in one-to-one correspondence with the serial numbers of the electronic tags; the second acquisition module is used for acquiring detection results and detection numbers of all samples including the comparison sample; the judging module is used for judging whether the detection error of the sample for comparison is within a preset error threshold according to the one-to-one correspondence between the serial numbers of the detection and the electronic tag, if so, determining the batch detection analysis specification, and if not, determining that the batch detection analysis is not enough.
According to yet another aspect of an embodiment of the present invention, there is also provided a sample management system including: the sample management device, the electronic tag and the labeling unit, wherein the electronic tag is a data carrier for detecting sample information and is used for sample identification, tracking and information acquisition; the labeling unit is connected with the sample management device and is used for printing a label containing a detection number and adhering the label on the sample container.
Optionally, the above system further comprises a sorting unit connected to the sample management device for reordering all samples, including the alignment samples, partially or fully.
According to yet another aspect of an embodiment of the present invention, there is also provided a nonvolatile storage medium storing a plurality of instructions adapted to be loaded by a processor and to perform the sample management method of any one of the above.
According to still another aspect of the embodiment of the present invention, there is also provided an electronic device including: one or more processors and memory for storing one or more programs, wherein the one or more programs, when executed by the one or more processors, cause the one or more processors to implement the sample management method of any of the claims.
In the embodiment of the invention, information of all samples including the comparison sample is obtained, wherein all samples are planted with electronic tags with a safety mechanism, the sample information at least comprises an electronic tag serial number, and at least the electronic tag serial number, an answer result of the comparison sample and whether three pieces of information belonging to the comparison sample are not opened to a monitored detector; uniformly numbering all samples including the comparison samples for detection, wherein the detection numbers are in one-to-one correspondence with the serial numbers of the electronic tags; obtaining detection results and detection numbers of all samples including the comparison sample; according to the one-to-one correspondence between the serial numbers of the detection and the serial numbers of the electronic tags, judging whether the detection errors of the samples for comparison are in a preset error threshold, if so, determining that the batch detection analysis is standard, if not, determining that the batch detection analysis is not standard enough, and achieving the purpose of evaluating the detection standardization of the samples in the same batch by comparing the detection accuracy of the samples, thereby realizing the technical effect of timely finding out the nonstandard detection behaviors by technical means, and further solving the problems that a supervisor is difficult to timely find out the laboratory analysis nonstandard of the detection party, data distortion even direct counterfeiting detection results without detection occurs, and phenomena such as sample exchange by a series-connection detection personnel are solved.
Drawings
The accompanying drawings, which are included to provide a further understanding of the application and are incorporated in and constitute a part of this specification, illustrate embodiments of the application and together with the description serve to explain the application and should not be taken as limiting the application. In the drawings:
FIG. 1 is a flow chart of a sample management method according to an embodiment of the present invention;
FIG. 2 is a schematic view of a sample management apparatus according to an embodiment of the present invention;
FIG. 3 is a schematic diagram of a sample management system provided according to an embodiment of the present invention;
Detailed Description
In order that those skilled in the art will better understand the present invention, a technical solution in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in which it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the present invention without making any inventive effort, shall fall within the scope of the present invention.
Example 1
In this embodiment, water quality sample detection is taken as an example, and the sample management method provided by the invention is explained.
In accordance with an embodiment of the present invention, there is provided an embodiment of a sample management method, it being noted that the steps shown in the flowchart of the figures may be performed in a computer system, such as a set of computer executable instructions, and, although a logical order is shown in the flowchart, in some cases, the steps shown or described may be performed in an order other than that shown or described herein.
Fig. 1 is a flow chart of a sample management method according to an embodiment of the present invention, as shown in fig. 1, the method includes the following steps:
Step S102, information of all samples including the comparison sample is obtained, wherein all samples are planted with electronic tags with a safety mechanism, the sample information at least comprises an electronic tag serial number, and at least the electronic tag serial number, an answer result of the comparison sample and whether three pieces of information belonging to the comparison sample are not open to a monitored detector.
Specifically, the sample information acquisition mode can be input by a sampling person during on-site sampling, and also can be input at a sample collection place, and the sample information acquisition device is a handheld PDA (Personal DIGITAL ASSISTANT) device. The sample information comprises an electronic tag serial number, a consignment unit, sampling point information, an index to be measured, a storage and transportation condition and the like; further sample point information may include geographic location (e.g., latitude and longitude), sample location, and the like. The sample information for comparison is input by a supervisor, and the sample information for comparison comprises answer results of the sample for comparison besides other sample information. The samples in the same batch adopt the same appearance and material and sample bottles without artificial marks so as to prevent the samples from being identified by people, and all the sample bottles are attached with waterproof electronic labels. The detection party refers to a unit or department that takes on the task of detecting a sample.
Specifically, the electronic tag is RFID (Radio Frequency Identification) tag, and the target object is identified by the radio frequency signal and related data is obtained. The invention requires at least electronic tag serial number, answer result of comparison sample and whether three information of comparison sample is supervisor privacy data, not open to the detecting party, if there is no information, such as whether the information is of comparison sample, the information is equivalent to supervisor privacy data, not open to the detecting party. The invention mainly guarantees the data privacy through a safety mechanism, and prevents the supervised detecting party from violating the authority to acquire the private data such as the electronic tag serial number, the answer result of the comparison sample, whether the private data belongs to the comparison sample or not. The security mechanism of the electronic tag mainly comprises: a method for changing the uniqueness of the serial number of the electronic tag based on a tag renaming technology and based on a cryptography technology (such as a Hash-Lock protocol, a randomized Hash-Lock protocol, a Hash chain protocol and the like); hidden information methods based on proxy technology, distance measurement technology, blocking technology and the like for avoiding or preventing a reader from acquiring tag data; a synchronization method; a sleep method for letting the tag enter a temporary disabled state; and adopting a central processing unit to encrypt the CPU type electronic tag.
Step S104, carrying out unified detection numbers on all samples including comparison samples, wherein the detection numbers are in one-to-one correspondence with the serial numbers of the electronic tags.
Specifically, the detection number is a number used by the detection party in laboratory sample detection management, and is open to the detection party. The detection number can be two-dimensional codes, bar codes, characters and the like, further the characters can be numerals, letters, chinese characters and the like, the detection number is compiled by a supervision party according to the coding rules of the detection party or the supervision party, and each sample in the same batch uses a unique detection number. Although different electronic tag serial numbers are returned to the visitor each time through the security mechanism, the supervision side locks the electronic tag serial numbers through the corresponding relation before and after the electronic tag serial numbers are changed, so that the one-to-one correspondence between the detection serial numbers and the electronic tag serial numbers is realized.
Step S106, obtaining detection results and detection numbers of all samples including comparison samples;
Specifically, after the detection is completed by the detection party, the detection results of all samples and corresponding numbers for detection are input by the personnel of the detection party.
Step S108, judging whether the detection error of the comparison sample is within a preset error threshold according to the one-to-one correspondence between the detection serial number and the electronic tag serial number, if so, determining the batch detection analysis specification, and if not, determining that the batch detection analysis is not enough.
Specifically, the preset error threshold is set by the supervisory side according to the sample property, the analysis method, and the like, for example, the preset error threshold of the colorimetric determination content is set to 2%.
The sample is not limited to the water sample, but may be various test samples such as a gas sample, a soil sample, a product sample, a raw material sample, etc., and the sample may be packaged in a container (for example, a water sample bottle), may not be packaged in a container (for example, a cement test block), and the electronic sample tag packaged in the container may be attached to the container.
According to the sample management method provided by the embodiment of the invention, information of all samples including the comparison sample is obtained, wherein all samples are planted with electronic tags with a safety mechanism, the sample information at least comprises an electronic tag serial number, at least the electronic tag serial number, a comparison sample answer result and whether three pieces of information belonging to the comparison sample are not opened to a monitored detection party; uniformly numbering all samples including the comparison samples for detection, wherein the detection numbers are in one-to-one correspondence with the serial numbers of the electronic tags; obtaining detection results and detection numbers of all samples including the comparison sample; according to the one-to-one correspondence between the serial numbers of the detection and the serial numbers of the electronic tags, judging whether the detection errors of the samples for comparison are in a preset error threshold, if so, determining that the batch detection analysis is standard, if not, determining that the batch detection analysis is not standard enough, and achieving the purpose of evaluating the detection standardization of the samples in the same batch by comparing the detection accuracy of the samples, thereby realizing the technical effect of timely finding out the nonstandard detection behaviors by technical means, and further solving the problems that a supervisor is difficult to timely find out the laboratory analysis nonstandard of the detection party, data distortion even direct counterfeiting detection results without detection occurs, and phenomena such as sample exchange by a series-connection detection personnel are solved.
As an alternative embodiment, reordering all or part of the samples, including the alignment samples, prevents the alignment sample position from being inferred by the sample alignment order. The samples are typically reordered prior to numbering for detection. If the numbers for detection are not in the order of the numbers for detection, the numbers for detection can be reordered first.
As an alternative embodiment, the sample for comparison may be a sample packaged in the same container or packaged without a container, such as a water sample prepared by a supervisor, for which the supervisor grasps the answer. The detection sample contains parallel samples, and part or all of the parallel samples can be directly selected as comparison samples; when the parallel samples are liquid or gas, part or all of the parallel samples can be selected, and substances containing analysis items can be quantitatively added to prepare a sample for comparison. If the sample for comparison is a parallel sample or a sample for comparison prepared by using the parallel sample, the information of the sample can be the information of the parallel sample or can be adjusted; if the comparison sample is not the case, it is written with similar sample information.
Example 2
According to an embodiment of the present invention, there is further provided an apparatus for implementing the above sample management method, and fig. 2 is a schematic structural diagram of a sample management apparatus according to an embodiment of the present invention, and as shown in fig. 2, the sample management apparatus 200 includes: the first acquisition module 202, the execution module 204, the second acquisition module 206, and the determination module 208 are described in detail below with respect to the sample management apparatus 200.
A first obtaining module 202, configured to obtain information of all samples including the sample for comparison, where all samples are planted with electronic tags having a security mechanism, where the information includes at least an electronic tag serial number, an answer result of the sample for comparison, and whether three pieces of information belonging to the sample for comparison are not open to a monitored detecting party; the execution module 204 is connected to the first acquisition module 202, and is configured to uniformly perform a detection number on all samples including the comparison sample, where the detection number corresponds to the serial number of the electronic tag one by one; a second obtaining module 206, connected to the executing module 204, for obtaining the detection results and the detection numbers of all samples including the comparison sample; the judging module 208 is connected to the second obtaining module 206, and is configured to judge whether the detection error of the sample for comparison is within a preset error threshold according to the one-to-one correspondence between the detection number and the serial number of the electronic tag, if yes, determine that the batch detection analysis specification is not enough, and if not, determine that the batch detection analysis is not enough.
It should be noted that, the first obtaining module 202, the executing module 204, the second obtaining module 206, and the determining module 208 correspond to steps S102 to S108 in implementing the sample management method, and the plurality of modules are the same as the examples and application scenarios implemented by the corresponding steps, but are not limited to those disclosed in the foregoing embodiment 1.
Example 3
According to another aspect of the embodiment of the present invention, there is provided a sample management system, fig. 3 is a schematic structural diagram of the sample management system according to the embodiment of the present invention, and as shown in fig. 3, the sample management system 300 includes: the sample management apparatus 200, the electronic tag 302, and the labeling unit 304 are described below with respect to the sample management system 300.
The electronic tag 302 is a data carrier for detecting sample information, and is used for identifying, tracking and collecting the sample, and transmitting related information to the sample management device 200;
The sample management device 200 is configured to implement sample management by acquiring sample information, performing a number for detection, acquiring a detection result, and determining a detection error of a sample for comparison, and transmit the generated number for sample detection to the labeling unit 304;
And a labeling unit 304 connected with the sample management device and used for printing a label containing a detection number and adhering the label on the sample container.
As an alternative embodiment, the sample management system further comprises a sorting unit, connected to the sample management device, for reordering all samples, including the alignment samples, partially or fully.
Example 4
According to another aspect of embodiments of the present invention, there is also provided a computer-readable storage medium, which when executed by a processor of an electronic device, causes the electronic device to perform the sample management method of any one of the above.
Example 5
According to another aspect of the embodiment of the present invention, there is also provided an electronic device including: a processor; a memory for storing processor-executable instructions, wherein the processor is configured to execute the instructions to implement the sample management method of any of the above.
Example 6
According to a further aspect of embodiments of the present invention, there is provided a computer program product comprising a computer program, characterized in that the computer program, when executed by a processor, implements the sample management method of any of the above.
The foregoing embodiment numbers of the present invention are merely for the purpose of description, and do not represent the advantages or disadvantages of the embodiments.
From the above description of the method embodiments, it will be clear to those skilled in the art that the present invention may be implemented by means of software plus necessary general hardware platform, but of course also by means of hardware, but in many cases the former is a preferred embodiment. Based on this understanding, the technical solution of the present invention may be embodied essentially or in part in the form of a software product stored in a storage medium, including instructions for causing a computer device (which may be a personal computer, a server, or a network device, etc.) to perform all or part of the steps of the method according to the embodiments of the present invention. And the aforementioned storage medium includes: read Only Memory (ROM), random Access Memory (RAM), magnetic or optical disks, and the like.
In the foregoing embodiments of the present invention, the descriptions of the embodiments are emphasized, and for a portion of this disclosure that is not described in detail in this embodiment, reference is made to the related descriptions of other embodiments. In particular, for apparatus or system embodiments, since they are substantially similar to method embodiments, the description is relatively simple, with reference to the description of method embodiments in part. The apparatus and system embodiments described above are merely illustrative, wherein the elements illustrated as separate elements may or may not be physically separate, and the elements shown as elements may or may not be physical elements, may be located in one place, or may be distributed over a plurality of network elements. Some or all of the modules may be selected according to actual needs to achieve the purpose of the solution of this embodiment. Those of ordinary skill in the art will understand and implement the present invention without undue burden.
It is to be understood that the invention is operational with numerous general purpose or special purpose computing system environments or configurations. For example: personal computers, server computers, hand-held or portable devices, tablet devices, multiprocessor systems, microprocessor-based systems, set top boxes, programmable consumer electronics, network PCs, minicomputers, mainframe computers, distributed computing environments that include any of the above systems or devices, and the like.
The invention may be described in the general context of computer-executable instructions, such as program modules, being executed by a computer. Generally, program modules include routines, programs, objects, components, data structures, etc. that perform particular tasks or implement particular abstract data types. The invention may also be practiced in distributed computing environments where tasks are performed by remote processing devices that are linked through a communications network. In a distributed computing environment, program modules may be located in both local and remote computer storage media including memory storage devices.
It should be noted that in this document, relational terms such as "first" and "second" and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising one … …" does not exclude the presence of other like elements in a process, method, article, or apparatus that comprises the element.
The foregoing is merely illustrative of the embodiments of this invention and it will be appreciated by those skilled in the art that variations and modifications may be made without departing from the principles of the invention, and it is intended to cover all modifications and variations as fall within the scope of the invention.
Claims (8)
1. A method of sample management comprising:
Acquiring information of all samples including the comparison sample, wherein all samples are planted with electronic tags with a safety mechanism, the information at least comprises an electronic tag serial number, and at least the electronic tag serial number, an answer result of the comparison sample and whether three pieces of information belonging to the comparison sample are not opened to a monitored detection party;
uniformly detecting all samples including the comparison samples, wherein the detection numbers are in one-to-one correspondence with the serial numbers of the electronic tags;
obtaining detection results and detection numbers of all samples including the comparison sample;
Judging whether the detection error of the comparison sample is within a preset error threshold according to the one-to-one correspondence between the detection serial number and the electronic tag serial number, if so, determining that the batch detection analysis is standard, and if not, determining that the batch detection analysis is not standard.
2. The method as recited in claim 1, further comprising:
all samples, including the alignment samples, are partially or fully reordered.
3. The method of claim 1, wherein the sample for alignment comprises:
Samples of answer results held by the supervisor, either packaged in the same container or without container packaging;
When the sample is liquid or gas, selecting partial or all parallel samples, and quantitatively adding substances containing detection items.
4. A sample management apparatus, comprising:
The first acquisition module is used for acquiring information of all samples including the comparison sample, wherein all the samples are planted with electronic tags with a safety mechanism, the information at least comprises an electronic tag serial number, and at least the electronic tag serial number, an answer result of the comparison sample and whether three pieces of information belonging to the comparison sample are not opened to a monitored detection party;
the execution module is used for uniformly carrying out detection numbers on all samples including comparison samples, wherein the detection numbers are in one-to-one correspondence with the serial numbers of the electronic tags;
the second acquisition module is used for acquiring detection results and detection numbers of all samples including the comparison sample;
The judging module is used for judging whether the detection error of the sample for comparison is within a preset error threshold according to the one-to-one correspondence between the serial numbers of the detection and the electronic tag, if so, determining the batch detection analysis specification, and if not, determining that the batch detection analysis is not enough.
5. A sample management system, characterized in that the system comprises the sample management device, an electronic tag and a labeling unit according to claim 4, wherein the electronic tag is a data carrier for detecting sample information and is used for sample identification, tracking and information acquisition; the labeling unit is connected with the sample management device and is used for printing a label containing a detection number and pasting the label on a sample or a sample container.
6. The system of claim 5, further comprising a ranking unit coupled to the sample management device for reordering all or part of the samples, including the alignment samples.
7. A non-volatile storage medium storing a plurality of instructions adapted to be loaded by a processor and to perform the sample management method of any one of claims 1 to 3.
8. An electronic device, comprising: one or more processors and memory for storing one or more programs, wherein the one or more programs, when executed by the one or more processors, cause the one or more processors to implement the sample management method of any of claims 1-3.
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