CN117866689A - Environment-friendly water-based cold extrusion lubricant and preparation method and application thereof - Google Patents
Environment-friendly water-based cold extrusion lubricant and preparation method and application thereof Download PDFInfo
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- CN117866689A CN117866689A CN202410054015.XA CN202410054015A CN117866689A CN 117866689 A CN117866689 A CN 117866689A CN 202410054015 A CN202410054015 A CN 202410054015A CN 117866689 A CN117866689 A CN 117866689A
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- 239000000314 lubricant Substances 0.000 title claims abstract description 65
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 46
- 238000000641 cold extrusion Methods 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title abstract description 9
- -1 polytetrafluoroethylene Polymers 0.000 claims abstract description 35
- 239000004810 polytetrafluoroethylene Substances 0.000 claims abstract description 17
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims abstract description 17
- ITRNXVSDJBHYNJ-UHFFFAOYSA-N tungsten disulfide Chemical compound S=[W]=S ITRNXVSDJBHYNJ-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 16
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 13
- 239000002270 dispersing agent Substances 0.000 claims abstract description 13
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 13
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 10
- 238000005461 lubrication Methods 0.000 claims description 17
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 12
- 230000001050 lubricating effect Effects 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 6
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 4
- 229920002367 Polyisobutene Polymers 0.000 claims description 4
- 229920002675 Polyoxyl Polymers 0.000 claims description 4
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 4
- 150000001336 alkenes Chemical class 0.000 claims description 4
- WGQKYBSKWIADBV-UHFFFAOYSA-N benzylamine Chemical compound NCC1=CC=CC=C1 WGQKYBSKWIADBV-UHFFFAOYSA-N 0.000 claims description 4
- 239000004359 castor oil Substances 0.000 claims description 4
- 235000019438 castor oil Nutrition 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 150000004665 fatty acids Chemical class 0.000 claims description 4
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims description 4
- 229920002503 polyoxyethylene-polyoxypropylene Polymers 0.000 claims description 4
- 239000001384 succinic acid Substances 0.000 claims description 4
- KZNICNPSHKQLFF-UHFFFAOYSA-N succinimide Chemical compound O=C1CCC(=O)N1 KZNICNPSHKQLFF-UHFFFAOYSA-N 0.000 claims description 4
- 239000013530 defoamer Substances 0.000 claims description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 2
- 150000001412 amines Chemical class 0.000 claims description 2
- AGXUVMPSUKZYDT-UHFFFAOYSA-L barium(2+);octadecanoate Chemical compound [Ba+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O AGXUVMPSUKZYDT-UHFFFAOYSA-L 0.000 claims description 2
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 claims description 2
- 239000008116 calcium stearate Substances 0.000 claims description 2
- 235000013539 calcium stearate Nutrition 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N isopropyl alcohol Natural products CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- HGPXWXLYXNVULB-UHFFFAOYSA-M lithium stearate Chemical compound [Li+].CCCCCCCCCCCCCCCCCC([O-])=O HGPXWXLYXNVULB-UHFFFAOYSA-M 0.000 claims description 2
- 229920000259 polyoxyethylene lauryl ether Polymers 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 claims description 2
- 229960002317 succinimide Drugs 0.000 claims description 2
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 238000005260 corrosion Methods 0.000 abstract description 3
- 230000007797 corrosion Effects 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 10
- 229910052751 metal Inorganic materials 0.000 description 10
- 239000002184 metal Substances 0.000 description 10
- 230000000694 effects Effects 0.000 description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- 229910002804 graphite Inorganic materials 0.000 description 5
- 239000010439 graphite Substances 0.000 description 5
- 238000005406 washing Methods 0.000 description 5
- 238000004140 cleaning Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
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- 238000007127 saponification reaction Methods 0.000 description 4
- 238000003912 environmental pollution Methods 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
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- 230000002195 synergetic effect Effects 0.000 description 2
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- 239000002253 acid Substances 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000013556 antirust agent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005536 corrosion prevention Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
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- 239000003921 oil Substances 0.000 description 1
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- 230000002035 prolonged effect Effects 0.000 description 1
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- 238000011160 research Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
The scheme discloses an environment-friendly water-based cold extrusion lubricant, and a preparation method and application thereof, and belongs to the technical field of water-based lubricants. The invention discloses an environment-friendly water-based cold extrusion lubricant which comprises the following components in parts by weight: 5-15 parts of water-based stearate, 5-15 parts of nano tungsten disulfide, 5-15 parts of polyethylene glycol, 20-30 parts of polytetrafluoroethylene, 1-10 parts of nonionic surfactant, 10-20 parts of water-based interface lubricant, 0.1-2 parts of dispersing agent, 0.1-1 part of defoaming agent and 50-80 parts of water. The aqueous cold extrusion lubricant disclosed by the invention has the advantages of wear resistance, corrosion resistance, high temperature resistance, environmental protection and no pollution, and can reduce the wear of machinery and prolong the service life of the machinery.
Description
Technical Field
The invention relates to the technical field of aqueous lubricants, in particular to an environment-friendly aqueous cold extrusion lubricant, and a preparation method and application thereof.
Background
In the cold extrusion processing technology of metal, the use of a lubricant is critical, the contact surface can generate resistance for preventing tangential movement, namely external friction force when the processed metal moves relative to a die in the cold molding process of the metal, the external friction force can increase the force and energy required by processing, so that the metal surface is subjected to lubrication treatment, the lubricant is a lubrication medium for reducing the friction resistance of a friction pair and slowing down the abrasion of the friction pair, a firm and tough lubrication film is formed between a workpiece and the die, the purpose of reducing the friction is achieved, if the lubrication of the surface of the lubrication film cannot meet the requirement, the phenomena of die abrasion, adhesion, scratch and the like on the surface of the workpiece can be aggravated, and the development of lubrication technology can promote the development of cold molding processing of the metal.
In the cold molding process of metal, the application of the phosphating-saponification lubrication technology is quite common, but the phosphating-saponification needs to be subjected to seven working procedures of alkali washing oil removal, water washing, acid washing rust removal, water washing, phosphating, water washing, saponification and the like, and the problems of high consumption of raw materials and energy sources, poor total working environment, easiness in causing environmental pollution and the like exist. In recent years, the use of phosphating-saponification lubrication technology has gradually stopped. Therefore, finding an environment-friendly lubricant suitable for metal cold forming is a hot spot of research.
At present, most of novel water-based lubricants on the market are high-molecular graphite type lubricants, and the lubricants have a certain lubricating effect on metal cold molding, but the graphite type lubricants also have a plurality of hidden dangers, such as poor lubricating performance, electric conduction, difficult cleaning, heavy pollution and the like, and have higher cost, and the black dust pollution in the production environment is serious, so that the method is unfavorable for the physical health of workers.
Therefore, how to provide an aqueous lubricant with good lubrication effect and safe and environment-friendly preparation process is a problem to be solved in the field.
Disclosure of Invention
The invention aims to provide an environment-friendly water-based cold extrusion lubricant, and a preparation method and application thereof, so as to solve the problems of poor lubrication effect, unsafe preparation process and the like of the common lubricant in the prior art, which are easy to cause environmental pollution.
The environment-friendly water-based cold extrusion lubricant in the scheme comprises the following components in parts by weight:
5-15 parts of water-based stearate, 5-15 parts of nano tungsten disulfide, 5-15 parts of polyethylene glycol, 20-30 parts of polytetrafluoroethylene, 1-10 parts of nonionic surfactant, 10-20 parts of water-based interface lubricant, 0.1-2 parts of dispersing agent, 0.1-1 part of defoaming agent and 50-80 parts of water.
The beneficial effects of the technical scheme are that:
the water-based stearate has the characteristics of lubricity, waterproofness, ductility and high melting point, and can play roles in gelling, improving pour point and increasing thickening;
the nano tungsten disulfide can play a role in antifriction and antiwear. When the load is higher and the friction is aggravated, tungsten disulfide and a metal substrate are subjected to chemical action to produce a FeS film with a lower melting point, so that the contact between metal friction pairs can be effectively reduced, and the service life of the instrument is prolonged;
the polyethylene glycol has adjustable solubility and chain length, and the viscosity and fluidity of the lubricant are adjusted by changing the molecular weight and the content of the polyethylene glycol;
polytetrafluoroethylene has the advantages of no oxidation, hardening or softening leakage at high temperature, and corrosion prevention in a humid environment, and can enhance the physical and chemical properties of the lubricant;
the nonionic surfactant can prevent rust, corrosion and foam, can regulate the viscosity of the lubricant and can reduce the viscosity-temperature performance;
the water-based interface lubricant has the characteristics of cooling, cleaning and pollution prevention, and can reduce the friction resistance of friction pairs and slow down wear.
Further, the aqueous stearate is aqueous zinc stearate, aqueous calcium stearate, aqueous barium stearate or aqueous lithium stearate.
Further, the friction coefficient of the nano tungsten disulfide is 0.1-0.3, and the particle size is 0.5-0.9 mu m.
Further, the nonionic surfactant comprises one or more of alkyl alcohol amide, alkylphenol polyoxyethylene, higher fatty alcohol polyoxyethylene and C13 isopropanol amide;
the aqueous interface lubricant is prepared from alcohol ether carboxylic acid, polyoxyl castor oil, olefin and chlorinated fatty acid; the weight percentages of the components are 12.5 percent of alcohol ether carboxylic acid, 27.5 percent of polyoxyl castor oil, 10 percent of olefin and 50 percent of chlorinated fatty acid.
Further, the dispersing agent comprises one or more of polyisobutylene succinimide, polyisobutylene succinate and benzylamine;
the defoamer comprises one or more of polyoxyethylene polyoxypropylene pentaerythritol ether, polyoxyethylene polyoxypropylene alcohol amine ether, polyoxyethylene lauryl ether, alkenyl succinic acid and alkenyl succinic acid half ester.
The preparation method of the environment-friendly water-based cold extrusion lubricant comprises the following steps:
s1: adding water and a nonionic surfactant into a reaction kettle until the nonionic surfactant is completely dissolved;
s2: adding water-based stearate and nano tungsten disulfide into the solution prepared in the step S1, heating, continuously stirring, and continuously heating at 60 ℃ for 1h;
s3: and (3) after the solution is cooled, adding an aqueous interface lubricant, polyethylene glycol, polytetrafluoroethylene, a dispersing agent and a defoaming agent into the solution obtained in the step (S2) to obtain the lubricating liquid.
The environment-friendly water-based cold extrusion lubricant prepared by the method is applied to mechanical lubrication.
The beneficial effects of the technical scheme are that:
1) The invention solves the problems of poor lubricating performance, electric conduction, difficult cleaning and the like of the conventional lubricant and the conventional graphite lubricant in the environment-friendly field, improves the problem of high friction coefficient of the graphite-free lubricant, and provides an environment-friendly water-based cold extrusion lubricant which is uniform in dispersion, good in lubricating effect, pollution-free, safe and environment-friendly in preparation process for the water-based lubricant.
2) The polytetrafluoroethylene has the same structure as graphite, the melting temperature is 327-342 ℃, the working temperature can reach 250 ℃, and the polytetrafluoroethylene is the material with the lowest friction coefficient in all lubricating materials, and the polytetrafluoroethylene does not cause the problems of difficult cleaning and environmental pollution like graphite.
The nanometer tungsten disulfide lamellar structure is easy to dissociate, and has very low friction coefficient, high extreme pressure resistance and high oxidation resistance. The lubricant is suitable for lubrication under various severe conditions such as high temperature, high pressure, high vacuum, high load, high rotation speed, high radiation, strong corrosion, ultralow temperature and the like, and can increase the application scene of the lubricant.
The two are combined, the synergistic effect can be achieved, the lubrication effect of the lubricant is improved, and the lubricant belongs to clean raw materials and is not easy to cause pollution.
Detailed Description
The invention is described in further detail below by way of specific embodiments:
example 1 an environmentally friendly aqueous Cold extrusion Lubricant
5 parts of water-based stearate, 5 parts of nano tungsten disulfide, 5 parts of polyethylene glycol, 20 parts of polytetrafluoroethylene, 1 part of nonionic surfactant, 10 parts of water-based interface lubricant, 0.2 part of dispersing agent, 0.1 part of defoaming agent and 50 parts of water.
Example 2 an environmentally friendly aqueous Cold extrusion Lubricant
10 parts of water-based stearate, 10 parts of nano tungsten disulfide, 10 parts of polyethylene glycol, 25 parts of polytetrafluoroethylene, 5 parts of nonionic surfactant, 15 parts of water-based interface lubricant, 1 part of dispersing agent, 0.5 part of defoaming agent and 60 parts of water.
Example 3 an environmentally friendly aqueous Cold extrusion Lubricant
15 parts of water-based stearate, 15 parts of nano tungsten disulfide, 15 parts of polyethylene glycol, 30 parts of polytetrafluoroethylene, 10 parts of nonionic surfactant, 20 parts of water-based interface lubricant, 2 parts of dispersing agent, 1 part of defoaming agent and 80 parts of water.
Comparative example 1 an environmentally friendly aqueous cold extrusion lubricant
10 parts of water-based stearate, 10 parts of nano tungsten disulfide, 5 parts of nonionic surfactant, 15 parts of water-based interface lubricant, 1 part of dispersing agent, 1 part of antirust agent, 0.5 part of defoaming agent and 60 parts of water.
Comparative example 2 an environmentally friendly aqueous Cold extrusion Lubricant
10 parts of aqueous stearate, 10 parts of polyethylene glycol, 25 parts of polytetrafluoroethylene, 5 parts of nonionic surfactant, 15 parts of aqueous interface lubricant, 1 part of dispersing agent, 0.5 part of defoaming agent and 60 parts of water.
Comparative example 3 an environmentally friendly aqueous cold extrusion lubricant
10 parts of aqueous stearate, 10 parts of polyethylene glycol, 5 parts of nonionic surfactant, 15 parts of aqueous interface lubricant, 1 part of dispersing agent, 0.5 part of defoamer and 60 parts of water.
Effect verification
1. Determination of the coefficient of Friction
The coefficient of friction of the environment-friendly aqueous cold extrusion lubricants prepared in examples 1 to 3 and comparative examples 1 to 3 was measured by using a four-ball friction tester, and the average coefficient of friction was measured at 30℃under a relative humidity of 30%, a load of 500N, a rotation speed of 1200r/min and a wear of 60min, and the results are shown in Table 1.
Example 1 | Example 2 | Example 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | |
Coefficient of friction | 0.079 | 0.073 | 0.082 | 0.095 | 0.103 | 0.112 |
As can be seen from Table 1, the friction coefficient of the lubricant prepared by the invention can be as low as 0.073, thus achieving the ideal lubrication effect; after polyethylene glycol and polytetrafluoroethylene components are removed, the friction coefficient is increased; after removing the nano tungsten disulfide component, the friction coefficient is increased; after removing the nano tungsten disulfide and polytetrafluoroethylene components, the friction coefficient is increased to 0.112, so that the lubricating effect of the aqueous lubricant is improved through the synergistic effect of the nano sulfur dioxide and polytetrafluoroethylene.
The lubricants of examples 1 to 3 and comparative examples 1 to 3 were subjected to physical and chemical property tests, and the results are shown in Table 2.
TABLE 2 physicochemical property test results of examples 1-3 and comparative examples 1-3
As shown in Table 2, the lubricant prepared by the invention has high kinematic viscosity, high viscosity index, up to 962N maximum seizure-free load and good cutting stability, and has good lubrication effect, stable performance and high bearing capacity. After the nano tungsten disulfide and polytetrafluoroethylene are removed in the comparative example 3, the maximum non-biting load is only 876N, the stability is as high as 0.3%, and the lubrication effect, the stability and the bearing capacity of the product are all reduced.
The foregoing is merely exemplary embodiments of the present invention, and specific structures and features that are well known in the art are not described in detail herein. It should be noted that modifications and improvements can be made by those skilled in the art without departing from the structure of the present invention, and these should also be considered as the scope of the present invention, which does not affect the effect of the implementation of the present invention and the utility of the patent. The protection scope of the present application shall be subject to the content of the claims, and the description of the specific embodiments and the like in the specification can be used for explaining the content of the claims.
Claims (7)
1. An environment-friendly water-based cold extrusion lubricant is characterized by comprising the following components in parts by weight:
5-15 parts of water-based stearate, 5-15 parts of nano tungsten disulfide, 5-15 parts of polyethylene glycol, 20-30 parts of polytetrafluoroethylene, 1-10 parts of nonionic surfactant, 10-20 parts of water-based interface lubricant, 0.1-2 parts of dispersing agent, 0.1-1 part of defoaming agent and 50-80 parts of water.
2. An environmentally friendly aqueous cold extrusion lubricant as claimed in claim 1, wherein:
the aqueous stearate is any one or a combination of more of aqueous zinc stearate, aqueous calcium stearate, aqueous barium stearate or aqueous lithium stearate.
3. An environmentally friendly aqueous cold extrusion lubricant as claimed in claim 1, wherein:
the friction coefficient of the nano tungsten disulfide is 0.1-0.3, and the grain diameter is 0.5-0.9 mu m.
4. An environmentally friendly aqueous cold extrusion lubricant as claimed in claim 1, wherein:
the nonionic surfactant comprises one or more of alkyl alcohol amide, alkylphenol polyoxyethylene, high-carbon fatty alcohol polyoxyethylene and C13 isopropanol amide;
the aqueous interface lubricant is prepared from alcohol ether carboxylic acid, polyoxyl castor oil, olefin and chlorinated fatty acid; the weight percentages of the components are 12.5 percent of alcohol ether carboxylic acid, 27.5 percent of polyoxyl castor oil, 10 percent of olefin and 50 percent of chlorinated fatty acid.
5. An environmentally friendly aqueous cold extrusion lubricant as claimed in claim 1, wherein:
the dispersing agent is one or more of polyisobutylene succinimide, polyisobutylene succinate and benzylamine;
the defoamer comprises one or more of polyoxyethylene polyoxypropylene pentaerythritol ether, polyoxyethylene polyoxypropylene alcohol amine ether, polyoxyethylene lauryl ether, alkenyl succinic acid and alkenyl succinic acid half ester.
6. The method for preparing the environment-friendly water-based cold extrusion lubricant as claimed in any one of claims 1 to 5, comprising the following steps:
s1: adding water and a nonionic surfactant into a reaction kettle until the nonionic surfactant is completely dissolved;
s2: adding water-based stearate and nano tungsten disulfide into the solution prepared in the step S1, heating, continuously stirring, and continuously heating at 60 ℃ for 1h;
s3: and (3) after the solution is cooled, adding an aqueous interface lubricant, polyethylene glycol, polytetrafluoroethylene, a dispersing agent and a defoaming agent into the solution obtained in the step (S2) to obtain the lubricating liquid.
7. Use of the environmentally friendly aqueous cold extrusion lubricant prepared according to claim 6 in mechanical lubrication.
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