CN117847831A - Adiabatic demagnetization refrigerating system capable of running without vibration and refrigerating method - Google Patents
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- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
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Abstract
Description
技术领域Technical Field
本发明涉及低温制冷技术领域,尤其涉及一种可无振动运行的绝热去磁制冷系统及制冷方法。The present invention relates to the technical field of low-temperature refrigeration, and in particular to an adiabatic demagnetization refrigeration system and a refrigeration method capable of operating without vibration.
背景技术Background technique
随着凝聚态物理、空间测量、两只技术等前沿科学领域的发展,极低温制冷需求日益增加,极低温制冷技术通常是至获取低于1K温度并提供一定冷量的制冷技术,目前常用的极低温制冷技术主要由吸附制冷、稀释制冷和绝热去磁制冷。With the development of cutting-edge scientific fields such as condensed matter physics, space measurement, and two-phase technology, the demand for ultra-low temperature refrigeration is increasing. Ultra-low temperature refrigeration technology is usually a refrigeration technology that can obtain a temperature below 1K and provide a certain amount of cooling. Currently, the commonly used ultra-low temperature refrigeration technologies mainly consist of adsorption refrigeration, dilution refrigeration, and adiabatic demagnetization refrigeration.
ADR即绝热去磁制冷作为最早出现的极低温温制冷技术之一,具有高效、不依赖重力条件和稀缺资源氦3气体等优点,成为空间应用中最具有发展潜力的极低温制冷技术,绝缘去磁制冷基于顺磁材料随外界磁场变化产生的磁热效应进行制冷,其基本构成包括磁热模块、磁体、热开关、热沉和冷头,理想ADR在热沉温度和制冷温度间由等温磁化、绝热去磁、等温去磁和绝热磁化四个过程进行逆卡诺循环,磁热模块被磁化至高于热沉温度一定程度后,闭合热沉和磁热模块之间的热开关,磁热模块进行等温磁化,释放磁化热给热沉,直至达到目标磁场上限;断开热沉与磁热模块之间的热开关,磁热模块绝热去磁并降温至制冷温度,在由热负荷状态下,控制去磁速率,使磁热模块进行等温去磁并产生冷量维持热负荷温度恒定;当磁场温度降低至目标磁场下限时,保持热开关断开,使磁热模块在绝热条件下磁化再生,升温至热沉温度后,重复上述步骤。但在某些实际应用中,需要严格安静的极低温环境,例如空间分辨率达到纳米级甚至皮米级的现代显微镜对外部振动及其敏感,而机械式4K制冷机的压缩机单元和冷头都会产生较大的振动。ADR, or adiabatic demagnetization refrigeration, is one of the earliest cryogenic refrigeration technologies. It has the advantages of high efficiency, independence from gravity and scarce helium-3 gas, making it the most promising cryogenic refrigeration technology in space applications. Adiabatic demagnetization refrigeration is based on the magnetocaloric effect of paramagnetic materials as the external magnetic field changes. Its basic structure includes a magnetocaloric module, a magnet, a thermal switch, a heat sink and a cold head. The ideal ADR performs a reverse Carnot cycle between the heat sink temperature and the refrigeration temperature through four processes: isothermal magnetization, adiabatic demagnetization, isothermal demagnetization and adiabatic magnetization. The magnetocaloric module is magnetized to a high temperature. When the temperature of the heat sink reaches a certain level, the thermal switch between the heat sink and the magnetothermal module is closed, the magnetothermal module is isothermally magnetized, and the magnetization heat is released to the heat sink until the upper limit of the target magnetic field is reached; the thermal switch between the heat sink and the magnetothermal module is disconnected, the magnetothermal module is adiabatically demagnetized and cooled to the cooling temperature, and under the heat load state, the demagnetization rate is controlled so that the magnetothermal module is isothermally demagnetized and generates cold to maintain the constant heat load temperature; when the magnetic field temperature drops to the lower limit of the target magnetic field, the thermal switch is kept disconnected so that the magnetothermal module is magnetized and regenerated under adiabatic conditions, and the above steps are repeated after the temperature is raised to the heat sink temperature. However, in some practical applications, a strictly quiet ultra-low temperature environment is required. For example, modern microscopes with spatial resolutions of nanometers or even picometers are extremely sensitive to external vibrations, and the compressor unit and cold head of a mechanical 4K refrigerator will produce large vibrations.
发明内容Summary of the invention
为了解决制冷单元在进行制冷时产生振动的问题,本发明提出一种可无振动运行的绝热去磁制冷系统及制冷方法。In order to solve the problem of vibration of the refrigeration unit during refrigeration, the present invention provides an adiabatic demagnetization refrigeration system and a refrigeration method that can operate without vibration.
本发明通过以下技术方案实现的:The present invention is achieved through the following technical solutions:
本发明提出可无振动运行的绝热去磁制冷系统包括绝热去磁模块,构架模块和预冷模块,其中:The present invention proposes an adiabatic demagnetization refrigeration system capable of operating without vibration, comprising an adiabatic demagnetization module, a frame module and a precooling module, wherein:
所述构架模块包括套在所述绝热去磁模块外侧的二级冷屏;The frame module includes a secondary cold shield sleeved on the outside of the adiabatic demagnetization module;
所述绝热去磁模块包括磁热模块,所述磁热模块底部连接有负荷,所述磁热模块通过第二热开关与热沉连接;The adiabatic demagnetization module includes a magnetocaloric module, a load is connected to the bottom of the magnetocaloric module, and the magnetocaloric module is connected to a heat sink via a second thermal switch;
所述磁热模块上下两侧与悬挂结构连接,所述悬挂结构外沿固定在磁屏蔽的上下端面,所述磁热模块通过所述悬挂结构固定在环形超导磁体的中间,所述磁热模块与所述超导磁体不接触;The upper and lower sides of the magnetocaloric module are connected to the suspension structure, the outer edge of the suspension structure is fixed to the upper and lower end surfaces of the magnetic shield, the magnetocaloric module is fixed in the middle of the annular superconducting magnet through the suspension structure, and the magnetocaloric module is not in contact with the superconducting magnet;
所述绝热去磁模块包括所述磁屏蔽,所述磁屏蔽顶部一侧通过铜棒与所述热沉连接;The adiabatic demagnetization module includes the magnetic shield, and one side of the top of the magnetic shield is connected to the heat sink through a copper rod;
所述热沉顶部一侧设有第一热开关,所述二级冷屏顶部还设有二级冷盘,所述二级冷盘与所述二级冷屏固定连接,所述热沉通过所述第一热开关与所述二级冷盘连接,所述热沉通过低导热支撑柱与所述二级冷盘固定;A first thermal switch is provided on one side of the top of the heat sink, a secondary cold plate is also provided on the top of the secondary cold screen, the secondary cold plate is fixedly connected to the secondary cold screen, the heat sink is connected to the secondary cold plate via the first thermal switch, and the heat sink is fixed to the secondary cold plate via a low thermal conductivity support column;
所述预冷模块位于所述二级冷盘顶部与所述二级冷盘连接。The pre-cooling module is located on the top of the secondary cold plate and is connected to the secondary cold plate.
进一步的,还包括一级冷屏和一级冷盘,所述一级冷屏套在所述二级冷屏外侧,所述一级冷屏与所述一级冷盘固定连接。Furthermore, it also includes a primary cold screen and a primary cold plate, wherein the primary cold screen is sleeved on the outside of the secondary cold screen, and the primary cold screen is fixedly connected to the primary cold plate.
进一步的,所述一级冷盘底部通过低导热支撑柱与所述二级冷盘顶部固定连接。Furthermore, the bottom of the first-stage cold plate is fixedly connected to the top of the second-stage cold plate via a low thermal conductivity support column.
进一步的,所述一级冷盘底部一侧设有二级冷头,所述二级冷头顶部一侧与所述一级冷盘连接,所述二级冷头底部一侧设有柔性连接件,所述二级冷头底部通过所述柔性连接件与所述二级冷盘固定连接。Furthermore, a secondary cold head is provided on one side of the bottom of the first-level cold plate, the top side of the secondary cold head is connected to the first-level cold plate, a flexible connector is provided on one side of the bottom of the secondary cold head, and the bottom of the secondary cold head is fixedly connected to the secondary cold plate through the flexible connector.
进一步的,还包括真空罩和密封盘,所述真空罩套于所述一级冷屏的外侧,所述真空罩与所述密封盘固定连接。Furthermore, it also includes a vacuum cover and a sealing disk. The vacuum cover is sleeved on the outer side of the primary cold screen, and the vacuum cover is fixedly connected to the sealing disk.
进一步的,所述密封盘底部通过低导热支撑柱与所述一级冷盘固定连接。Furthermore, the bottom of the sealing plate is fixedly connected to the primary cold plate via a low thermal conductivity support column.
进一步的,所述密封盘底部还设有一级冷头,所述一级冷头位于所述密封盘底部靠近所述二级冷头一侧,所述一级冷头顶部与所述密封盘连接,所述一级冷头底部与所述一级冷盘连接。Furthermore, a first-level cold head is provided at the bottom of the sealing disk, and the first-level cold head is located on the bottom of the sealing disk close to the second-level cold head. The top of the first-level cold head is connected to the sealing disk, and the bottom of the first-level cold head is connected to the first-level cold disk.
进一步的,还包括预冷制冷机,所述预冷制冷机的室温部分位于所述密封盘靠近所述一级冷头一侧,所述预冷制冷机的室温部分与所述密封盘连接。Furthermore, it also includes a pre-cooling refrigerator, the room temperature part of the pre-cooling refrigerator is located on the side of the sealing disk close to the first-level cold head, and the room temperature part of the pre-cooling refrigerator is connected to the sealing disk.
进一步的,所述预冷制冷机与所述真空罩之间设有减震波纹管。Furthermore, a shock-absorbing bellows is provided between the pre-cooling refrigerator and the vacuum cover.
进一步的,一种可无振动运行的绝热去磁制冷系统的制冷方法包括正常制冷模式和无振动制冷模式,其中,所述正常制冷模式包括以下步骤:Furthermore, a refrigeration method of an adiabatic demagnetization refrigeration system capable of operating without vibration includes a normal refrigeration mode and a vibration-free refrigeration mode, wherein the normal refrigeration mode includes the following steps:
预冷制冷机启动进行制冷,闭合第一热开关和第二热开关,通过预冷模块对绝热去磁模块进行预冷;The precooling refrigerator is started to perform cooling, the first thermal switch and the second thermal switch are closed, and the adiabatic demagnetization module is precooled through the precooling module;
预冷到热沉温度之后,绝热去磁模块进行运作,磁热模块被磁化的同时被冷却,达到目标磁场后,断开第二热开关,随后进行绝热去磁,等温去磁制冷,绝热磁化,然后闭合第二热开关,进行等温磁化,进入周期性制冷。此模式中预冷制冷机一直保持运行状态,第一热开关始终处于闭合状态,为正常制冷模式;After precooling to the heat sink temperature, the adiabatic demagnetization module operates, the magnetocaloric module is magnetized and cooled at the same time, and after reaching the target magnetic field, the second thermal switch is disconnected, followed by adiabatic demagnetization, isothermal demagnetization refrigeration, adiabatic magnetization, and then the second thermal switch is closed for isothermal magnetization to enter periodic refrigeration. In this mode, the precooling refrigerator is always in operation, and the first thermal switch is always in the closed state, which is the normal refrigeration mode;
所述无振动制冷模式包括以下步骤:The vibration-free refrigeration mode comprises the following steps:
预冷制冷机启动进行制冷,闭合第一热开关和第二热开关,通过预冷模块对绝热去磁模块进行预冷;The precooling refrigerator is started to perform cooling, the first thermal switch and the second thermal switch are closed, and the adiabatic demagnetization module is precooled through the precooling module;
预冷到热沉温度之后,绝热去磁模块进行运作,磁热模块被磁化的同时被冷却,达到目标磁场后,断开第二热开关和第一热开关,同时预冷制冷机停止运行,预冷模块与绝热去磁模块处于传热断开状态,磁热模块进行绝热去磁和等温去磁制冷,此模式中预冷制冷机一直处于停止运行状态,第一热开关始终处于断开状态,为无振动制冷模式;After precooling to the heat sink temperature, the adiabatic demagnetization module operates, the magnetocaloric module is magnetized and cooled at the same time, and after reaching the target magnetic field, the second thermal switch and the first thermal switch are disconnected, and the precooling refrigerator stops running at the same time. The precooling module and the adiabatic demagnetization module are in a heat transfer disconnection state, and the magnetocaloric module performs adiabatic demagnetization and isothermal demagnetization refrigeration. In this mode, the precooling refrigerator is always in a stopped state, and the first thermal switch is always in a disconnected state, which is a vibration-free refrigeration mode;
预冷制冷机重新启动进行制冷,闭合第一热开关和第二热开关,绝热去磁模块进行运作,磁热模块被磁化的同时被冷却,达到目标磁场后,断开第二热开关和第一热开关,同时预冷制冷机停止运行,开启新一轮无振动制冷模式。The pre-cooling refrigerator restarts to cool, closes the first thermal switch and the second thermal switch, and the adiabatic demagnetization module operates. The magnetocaloric module is magnetized and cooled at the same time. After reaching the target magnetic field, the second thermal switch and the first thermal switch are disconnected, and the pre-cooling refrigerator stops running at the same time, starting a new round of vibration-free cooling mode.
附图说明BRIEF DESCRIPTION OF THE DRAWINGS
图1为本发明的可无振动运行的绝热去磁制冷系统的结构图;FIG1 is a structural diagram of an adiabatic demagnetization refrigeration system capable of operating without vibration according to the present invention;
图2为传统绝热去磁制冷系统的结构图;FIG2 is a structural diagram of a conventional adiabatic demagnetization refrigeration system;
图中,绝热去磁模块1,磁热模块11,负荷12,第二热开关13,热沉14,悬挂结构15,磁屏蔽16,超导磁体17,高导热铜棒18,构架模块2,二级冷屏21,二级冷盘22,一级冷盘23,一级冷屏24,真空罩25,密封盘26,低导热支撑柱27,预冷模块3,预冷制冷机31,一级冷头32,二级冷头33,柔性连接件34,第一热开关4。In the figure, an adiabatic demagnetization module 1, a magnetocaloric module 11, a load 12, a second thermal switch 13, a heat sink 14, a suspension structure 15, a magnetic shield 16, a superconducting magnet 17, a high thermal conductivity copper rod 18, a frame module 2, a secondary cold screen 21, a secondary cold plate 22, a primary cold plate 23, a primary cold screen 24, a vacuum cover 25, a sealing plate 26, a low thermal conductivity support column 27, a pre-cooling module 3, a pre-cooling refrigerator 31, a primary cold head 32, a secondary cold head 33, a flexible connector 34, and a first thermal switch 4.
本发明为目的的实现、功能特点及优点将结合实施例,参照附图做进一步说明。The purpose, features and advantages of the present invention will be further described with reference to the accompanying drawings in conjunction with the embodiments.
具体实施方式Detailed ways
为了更加清楚完整的说明本发明的技术方案,下面结合附图对本发明作进一步说明。In order to more clearly and completely illustrate the technical solution of the present invention, the present invention is further described below in conjunction with the accompanying drawings.
请参考图1-图2,本发明提出一种可无振动运行的绝热去磁制冷系统包括绝热去磁模块1、构架模块2和预冷模块3,其中:Please refer to FIG. 1-FIG. 2, the present invention proposes an adiabatic demagnetization refrigeration system capable of operating without vibration, comprising an adiabatic demagnetization module 1, a frame module 2 and a precooling module 3, wherein:
构架模块2包括套在绝热去磁模块1外侧的二级冷屏21;The frame module 2 includes a secondary cold shield 21 which is sleeved on the outside of the adiabatic demagnetization module 1;
所述绝热去磁模块1包括磁热模块11,所述磁热模块11底部连接有负荷12,所述磁热模块11通过第二热开关13与热沉14连接。The adiabatic demagnetization module 1 includes a magnetocaloric module 11 , a load 12 is connected to the bottom of the magnetocaloric module 11 , and the magnetocaloric module 11 is connected to a heat sink 14 via a second thermal switch 13 .
所述磁热模块11上下两侧与悬挂结构15连接,所述悬挂结构15外沿固定在磁屏蔽16的上下端面,所述磁热模块11通过所述悬挂结构15固定在环形超导磁体17的中间,所述磁热模块11与所述超导磁体17不接触;The upper and lower sides of the magnetocaloric module 11 are connected to the suspension structure 15, the outer edge of the suspension structure 15 is fixed to the upper and lower end surfaces of the magnetic shield 16, and the magnetocaloric module 11 is fixed in the middle of the annular superconducting magnet 17 through the suspension structure 15, and the magnetocaloric module 11 is not in contact with the superconducting magnet 17;
所述绝热去磁模块1包括所述磁屏蔽16,所述磁屏蔽16顶部一侧通过高导热铜棒18与所述热沉14连接;The adiabatic demagnetization module 1 includes the magnetic shield 16, and one side of the top of the magnetic shield 16 is connected to the heat sink 14 through a high thermal conductivity copper rod 18;
热沉14顶部一侧设有第一热开关4,二级冷屏21与顶部的二级冷盘22固定,热沉14通过第一热开关4与二级冷盘22连接,热沉14通过低导热支撑柱27与二级冷盘22固定;A first thermal switch 4 is provided on one side of the top of the heat sink 14, a secondary cold shield 21 is fixed to the secondary cold plate 22 on the top, the heat sink 14 is connected to the secondary cold plate 22 through the first thermal switch 4, and the heat sink 14 is fixed to the secondary cold plate 22 through a low thermal conductivity support column 27;
预冷模块3位于二级冷盘22顶部与二级冷盘22连接。The pre-cooling module 3 is located on the top of the secondary cold plate 22 and is connected to the secondary cold plate 22 .
具体的,第二热开关13和第一热开关4用于控制热传递导通和断开。预冷模块3进行制冷,闭合第一热开关4和第二热开关13,通过预冷模块3对绝热去磁模块1进行预冷,当预冷到要求的热沉14温度后,绝热去磁模块1进行运作,磁热模块11被磁化的同时被冷却,达到目标磁场后,进入绝热去磁过程。Specifically, the second thermal switch 13 and the first thermal switch 4 are used to control the conduction and disconnection of heat transfer. The precooling module 3 performs cooling, closes the first thermal switch 4 and the second thermal switch 13, and precools the adiabatic demagnetization module 1 through the precooling module 3. After precooling to the required temperature of the heat sink 14, the adiabatic demagnetization module 1 operates, and the magnetocaloric module 11 is magnetized and cooled at the same time. After reaching the target magnetic field, the adiabatic demagnetization process begins.
在正常制冷模式中,预冷制冷机31一直保持运行状态,第一热开关4始终处于闭合状态。在绝热去磁过程,当磁热模块11温度降低至制冷温度时,保持第二热开关13断开,进入等温去磁制冷过程,并施加一定负荷12,当等温去磁至磁场为零时,首次制冷结束,保持第二热开关13断开,进入绝热磁化过程,当磁热模块11升温至略高于热沉14温度时,闭合第二热开关13,磁热模块11等温磁化,产生磁化热,并通过第二热开关13释放磁化热给热沉14;当磁热模块11磁化至最大磁场时,进入周期性制冷过程;In the normal cooling mode, the precooling refrigerator 31 is always kept in operation, and the first thermal switch 4 is always in a closed state. In the adiabatic demagnetization process, when the temperature of the magnetocaloric module 11 drops to the cooling temperature, the second thermal switch 13 is kept disconnected, and the isothermal demagnetization cooling process is entered, and a certain load 12 is applied. When the isothermal demagnetization reaches zero magnetic field, the first cooling is completed, and the second thermal switch 13 is kept disconnected, and the adiabatic magnetization process is entered. When the magnetocaloric module 11 is heated to a temperature slightly higher than the temperature of the heat sink 14, the second thermal switch 13 is closed, the magnetocaloric module 11 isothermally magnetized, generates magnetization heat, and releases the magnetization heat to the heat sink 14 through the second thermal switch 13; when the magnetocaloric module 11 is magnetized to the maximum magnetic field, it enters a periodic cooling process;
在某些实际应用中,要求严格安静的极低温环境,需要停止运行预冷制冷机31,进行无振动制冷,若预冷模块3和绝热去磁模块1之间没有设置热开关进行连接,由于预冷模块3中包含很多金属部件,此时预冷模块3可以是为一个热导体,来自高温区的大量漏热导致热沉14迅速升温,超导磁体17将会因为失超无法正常工作,从而无法进行绝热去磁制冷;In some practical applications, a strictly quiet and extremely low temperature environment is required, and the precooling refrigerator 31 needs to be stopped to perform vibration-free cooling. If no thermal switch is provided between the precooling module 3 and the adiabatic demagnetization module 1 for connection, since the precooling module 3 contains many metal parts, the precooling module 3 can be a thermal conductor at this time. A large amount of heat leakage from the high temperature area causes the heat sink 14 to heat up rapidly, and the superconducting magnet 17 will not be able to work normally due to quenching, thereby failing to perform adiabatic demagnetization cooling;
本申请通过在预冷模块3和绝热去磁模块1之间增加第一热开关4连接,预冷制冷机31停止运行,并断开第一热开关4,切断预冷模块3和绝热去磁模块1之间的传热,使得绝热去磁模块1能在较长时间内维持负荷12在制冷温度下并提供无振动环境,同时预冷制冷机中的压缩机和旋转阀等大功率的部件停止运行,大幅度降低了电磁干扰。The present application adds a first thermal switch 4 connection between the precooling module 3 and the adiabatic demagnetization module 1, the precooling refrigerator 31 stops running, and the first thermal switch 4 is disconnected to cut off the heat transfer between the precooling module 3 and the adiabatic demagnetization module 1, so that the adiabatic demagnetization module 1 can maintain the load 12 at the refrigeration temperature for a long time and provide a vibration-free environment. At the same time, high-power components such as the compressor and rotary valve in the precooling refrigerator stop running, which greatly reduces electromagnetic interference.
预冷模块3进行制冷,闭合第一热开关4和第二热开关13,通过预冷模块3对绝热去磁模块1进行预冷,当预冷到要求的热沉14温度后,绝热去磁模块1进行运作,磁热模块11被磁化的同时被冷却,达到目标磁场后,进入无振动制冷模式。The precooling module 3 performs cooling, closes the first thermal switch 4 and the second thermal switch 13, and precools the adiabatic demagnetization module 1 through the precooling module 3. After precooling to the required temperature of the heat sink 14, the adiabatic demagnetization module 1 operates, and the magnetocaloric module 11 is magnetized and cooled at the same time. After reaching the target magnetic field, it enters the vibration-free cooling mode.
在无振动运行模式中,预冷制冷机31一直停止运行,第一热开关4始终处于断开状态。当磁热模块11被冷却同时磁化至目标磁场后,断开第二热开关13和第一热开关4,同时预冷制冷机31停止运行,预冷模块3与绝热去磁模块1处于传热断开状态,磁热模块11进行绝热去磁;当磁热模块11温度降低至制冷温度时,保持第二热开关13断开,进入等温去磁制冷过程,对负荷12实施无振动制冷;当等温去磁至磁场为零时,预冷制冷机31重新启动进行制冷,闭合第一热开关4和第二热开关13,绝热去磁模块1进行运作,磁热模块11被磁化的同时被冷却,达到目标磁场后,断开第二热开关13和第一热开关4,同时预冷制冷机31停止运行,开启新一轮无振动制冷模式。In the vibration-free operation mode, the precooling refrigerator 31 is always stopped, and the first thermal switch 4 is always in the disconnected state. When the magnetocaloric module 11 is cooled and magnetized to the target magnetic field, the second thermal switch 13 and the first thermal switch 4 are disconnected, and the precooling refrigerator 31 stops running at the same time. The precooling module 3 and the adiabatic demagnetization module 1 are in the heat transfer disconnected state, and the magnetocaloric module 11 performs adiabatic demagnetization; when the temperature of the magnetocaloric module 11 drops to the refrigeration temperature, the second thermal switch 13 is kept disconnected, and the isothermal demagnetization refrigeration process is entered, and vibration-free refrigeration is performed on the load 12; when the isothermal demagnetization reaches zero magnetic field, the precooling refrigerator 31 restarts to perform refrigeration, closes the first thermal switch 4 and the second thermal switch 13, and the adiabatic demagnetization module 1 operates, and the magnetocaloric module 11 is magnetized and cooled at the same time. After reaching the target magnetic field, the second thermal switch 13 and the first thermal switch 4 are disconnected, and the precooling refrigerator 31 stops running at the same time, and a new round of vibration-free refrigeration mode is started.
在一个实施例中,图2为传统绝热去磁制冷系统的结构设计,本申请通过在预冷模块3和绝热去磁模块1之间增加了第一热开关4连接,整个系统结构简单,可操作性强,满足了更严格的极低温制冷需求,同时第一热开关4和第二热开关13还可以加快降温速率。In one embodiment, Figure 2 is a structural design of a traditional adiabatic demagnetization refrigeration system. The present application adds a first thermal switch 4 between the pre-cooling module 3 and the adiabatic demagnetization module 1. The entire system has a simple structure and strong operability, meeting more stringent ultra-low temperature refrigeration requirements. At the same time, the first thermal switch 4 and the second thermal switch 13 can also accelerate the cooling rate.
进一步的,还包括一级冷屏24和一级冷盘23,一级冷屏24套在二级冷屏21外侧,一级冷屏24与一级冷盘23固定连接;Furthermore, it also includes a primary cold screen 24 and a primary cold plate 23, the primary cold screen 24 is sleeved on the outside of the secondary cold screen 21, and the primary cold screen 24 is fixedly connected to the primary cold plate 23;
一级冷盘23底部通过低导热支撑柱27与二级冷盘22顶部固定连接;The bottom of the primary cold plate 23 is fixedly connected to the top of the secondary cold plate 22 via a low thermal conductivity support column 27;
一级冷盘23底部一侧设有二级冷头33,二级冷头33顶部一侧与一级冷盘23固定连接,二级冷头33底部一侧设有柔性连接件34,二级冷头33底部通过柔性连接件34与二级冷盘22连接。A secondary cold head 33 is provided on one side of the bottom of the primary cold plate 23, and a top side of the secondary cold head 33 is fixedly connected to the primary cold plate 23. A flexible connector 34 is provided on one side of the bottom of the secondary cold head 33, and the bottom of the secondary cold head 33 is connected to the secondary cold plate 22 through the flexible connector 34.
具体的,柔性连接件34可以减少振动,柔性连接件34采用高纯度铜箔或铜辫,第二冷头底部和二级冷盘22通过柔性连接件34进行柔性热连接,一级冷盘23和二级冷盘22都是采用无氧高纯铜材质,其中二级冷盘22表面镀金处理,通过镀金处理加强4K温区部件的热接触和防止氧化,一级冷屏24和二级冷屏21为表面抛光铝制,并包裹多层隔热材料来降低辐射漏热,低导热支撑柱27进行支撑和连接一级冷盘23、二级冷盘22和热沉11,此处的低导热支撑柱27采用薄壁不锈钢管进行支撑。Specifically, the flexible connector 34 can reduce vibration. The flexible connector 34 is made of high-purity copper foil or copper braid. The bottom of the second cold head and the secondary cold plate 22 are flexibly thermally connected through the flexible connector 34. The primary cold plate 23 and the secondary cold plate 22 are both made of oxygen-free high-purity copper. The surface of the secondary cold plate 22 is gold-plated. The gold plating treatment is used to strengthen the thermal contact of the 4K temperature zone components and prevent oxidation. The primary cold screen 24 and the secondary cold screen 21 are made of polished aluminum and are wrapped with multiple layers of thermal insulation materials to reduce radiation heat leakage. The low thermal conductivity support column 27 supports and connects the primary cold plate 23, the secondary cold plate 22 and the heat sink 11. The low thermal conductivity support column 27 here is supported by a thin-walled stainless steel tube.
进一步的,还包括真空罩25和密封盘26,真空罩25套于一级冷屏24的外侧,真空罩25与密封盘26固定连接。Furthermore, it also includes a vacuum cover 25 and a sealing disk 26 . The vacuum cover 25 is sleeved on the outer side of the primary cold shield 24 , and the vacuum cover 25 is fixedly connected to the sealing disk 26 .
密封盘26底部通过低导热支撑柱4与一级冷盘23固定连接。密封盘26底部还设有一级冷头32,一级冷头32位于密封盘26底部靠近二级冷头33一侧,一级冷头32顶部与密封盘26连接,一级冷头32底部与一级冷盘23连接。The bottom of the sealing plate 26 is fixedly connected to the primary cold plate 23 through the low thermal conductivity support column 4. A primary cold head 32 is also provided at the bottom of the sealing plate 26. The primary cold head 32 is located at the bottom of the sealing plate 26 near the secondary cold head 33. The top of the primary cold head 32 is connected to the sealing plate 26, and the bottom of the primary cold head 32 is connected to the primary cold plate 23.
具体的,密封盘26和一级冷盘23之间的支撑柱27采用高强度且具有低导热率的玻璃纤维材料,真空罩25和密封盘26套在一级冷屏24外侧,真空罩25和密封盘26用于隔绝外部和一级冷屏24,通过真空处理来减少热传递,防止外部热能传递至真空罩25内侧。Specifically, the supporting column 27 between the sealing disk 26 and the primary cold disk 23 is made of a glass fiber material with high strength and low thermal conductivity. The vacuum cover 25 and the sealing disk 26 are sleeved on the outside of the primary cold screen 24. The vacuum cover 25 and the sealing disk 26 are used to isolate the outside and the primary cold screen 24, and reduce heat transfer through vacuum treatment to prevent external heat energy from being transferred to the inside of the vacuum cover 25.
进一步的,还包括预冷制冷机31,所述预冷制冷机31的室温部分位于所述密封盘靠近所述一级冷头一侧,所述预冷制冷机的室温部分与所述密封盘连接。Furthermore, it also includes a pre-cooling refrigerator 31, the room temperature part of the pre-cooling refrigerator 31 is located on the side of the sealing disk close to the primary cold head, and the room temperature part of the pre-cooling refrigerator is connected to the sealing disk.
预冷制冷机31与真空罩25之间设有减震波纹管。A shock-absorbing bellows is provided between the pre-cooling refrigerator 31 and the vacuum cover 25 .
具体的,预冷制冷机31用于进行预冷,采用两级G-M型脉管预冷制冷机31,预冷制冷机31用于提供冷量,减振波纹管可以进行减少预冷制冷机31的振动,预冷制冷机31传输的冷量依次经过一级冷头32、一级冷盘23、二级冷头33、柔性连接件34、二级冷盘22,最后通过第一热开关4进行传输至绝热去磁模块中。Specifically, the pre-cooling refrigerator 31 is used for pre-cooling, and a two-stage G-M type pulse tube pre-cooling refrigerator 31 is adopted. The pre-cooling refrigerator 31 is used to provide cooling capacity. The vibration-damping bellows can reduce the vibration of the pre-cooling refrigerator 31. The cooling capacity transmitted by the pre-cooling refrigerator 31 passes through the first-stage cold head 32, the first-stage cold plate 23, the second-stage cold head 33, the flexible connector 34, and the second-stage cold plate 22 in sequence, and is finally transmitted to the adiabatic demagnetization module through the first thermal switch 4.
进一步的,包括正常制冷模式和无振动制冷模式,其中,正常制冷模式包括以下步骤:Further, it includes a normal cooling mode and a vibration-free cooling mode, wherein the normal cooling mode includes the following steps:
预冷制冷机31启动进行制冷,闭合第一热开关4和第二热开关13,通过预冷模块3对绝热去磁模块1进行预冷;The precooling refrigerator 31 is started to perform cooling, the first thermal switch 4 and the second thermal switch 13 are closed, and the adiabatic demagnetization module 1 is precooled through the precooling module 3;
预冷到热沉14温度之后,绝热去磁模块1进行运作,磁热模块11被磁化的同时被冷却,达到目标磁场后,断开第二热开关13,随后进行绝热去磁,等温去磁制冷,绝热磁化,然后闭合第二热开关13,进行等温磁化,进入周期性制冷。此模式中预冷制冷机31一直保持运行状态,第一热开关4始终处于闭合状态,为正常制冷模式;After precooling to the temperature of the heat sink 14, the adiabatic demagnetization module 1 operates, the magnetocaloric module 11 is magnetized and cooled at the same time, and after reaching the target magnetic field, the second thermal switch 13 is disconnected, followed by adiabatic demagnetization, isothermal demagnetization refrigeration, adiabatic magnetization, and then the second thermal switch 13 is closed, isothermal magnetization is performed, and periodic refrigeration is entered. In this mode, the precooling refrigerator 31 is always kept in operation, and the first thermal switch 4 is always in a closed state, which is a normal refrigeration mode;
无振动制冷模式包括以下步骤:The vibration-free cooling mode includes the following steps:
预冷制冷机31启动进行制冷,闭合第一热开关4和第二热开关13,通过预冷模块3对绝热去磁模块1进行预冷;The precooling refrigerator 31 is started to perform cooling, the first thermal switch 4 and the second thermal switch 13 are closed, and the adiabatic demagnetization module 1 is precooled through the precooling module 3;
预冷到热沉14温度之后,绝热去磁模块1进行运作,磁热模块11被磁化的同时被冷却,达到目标磁场后,断开第二热开关13和第一热开关4,同时预冷制冷机31停止运行,预冷模块3与绝热去磁模块1处于传热断开状态,磁热模块11进行绝热去磁和等温去磁制冷,此模式中预冷制冷机31一直处于停止运行状态,第一热开关4始终处于断开状态,为无振动制冷模式;After precooling to the temperature of the heat sink 14, the adiabatic demagnetization module 1 operates, the magnetocaloric module 11 is magnetized and cooled at the same time, and after reaching the target magnetic field, the second thermal switch 13 and the first thermal switch 4 are disconnected, and the precooling refrigerator 31 stops running at the same time, the precooling module 3 and the adiabatic demagnetization module 1 are in a heat transfer disconnection state, and the magnetocaloric module 11 performs adiabatic demagnetization and isothermal demagnetization refrigeration. In this mode, the precooling refrigerator 31 is always in a stopped state, and the first thermal switch 4 is always in a disconnected state, which is a vibration-free refrigeration mode;
预冷制冷机31重新启动进行制冷,闭合第一热开关4和第二热开关13,绝热去磁模块1进行运作,磁热模块11被磁化的同时被冷却,达到目标磁场后,断开第二热开关13和第一热开关4,同时预冷制冷机31停止运行,开启新一轮无振动制冷模式。The pre-cooling refrigerator 31 restarts to cool, closes the first thermal switch 4 and the second thermal switch 13, and the adiabatic demagnetization module 1 operates. The magnetocaloric module 11 is magnetized and cooled at the same time. After reaching the target magnetic field, the second thermal switch 13 and the first thermal switch 4 are disconnected, and the pre-cooling refrigerator 31 stops running at the same time, starting a new round of vibration-free cooling mode.
具体的,首先对真空罩25内进行抽真空至压力低于0.1Pa,启动预冷制冷机31,并闭合第一热开关4和第二热开关13,预冷模块3对绝热去磁模块1进行预冷,一级冷头32降温至30K附近,二级冷头33降温至4K附近,同时对绝热去磁模块预冷至4K附近;绝热去磁模块1进行运作,磁热模块11被磁化的同时被冷却,达到目标磁场后,进入绝热去磁过程。Specifically, first, the vacuum cover 25 is evacuated to a pressure lower than 0.1Pa, the pre-cooling refrigerator 31 is started, and the first thermal switch 4 and the second thermal switch 13 are closed. The pre-cooling module 3 pre-cools the adiabatic demagnetization module 1, the first-stage cold head 32 is cooled to about 30K, the second-stage cold head 33 is cooled to about 4K, and the adiabatic demagnetization module is pre-cooled to about 4K at the same time; the adiabatic demagnetization module 1 is operated, the magnetocaloric module 11 is magnetized and cooled at the same time, and after reaching the target magnetic field, the adiabatic demagnetization process is entered.
在正常制冷模式中,预冷制冷机31一直保持运行状态,第一热开关4始终处于闭合状态。在绝热去磁过程,当磁热模块11温度降低至制冷温度时,保持第二热开关13断开,进入等温去磁制冷过程,并施加一定负荷12,当等温去磁至磁场为零时,首次制冷结束,保持第二热开关13断开,进入绝热磁化过程,当磁热模块11升温至略高于热沉14温度时,闭合第二热开关13,磁热模块11等温磁化,产生磁化热,并通过第二热开关13释放磁化热给热沉14;当磁热模块11磁化至最大磁场时,进入正常周期性制冷过程;In the normal cooling mode, the precooling refrigerator 31 is always kept in operation, and the first thermal switch 4 is always in a closed state. In the adiabatic demagnetization process, when the temperature of the magnetocaloric module 11 drops to the cooling temperature, the second thermal switch 13 is kept disconnected, and the isothermal demagnetization cooling process is entered, and a certain load 12 is applied. When the isothermal demagnetization reaches zero magnetic field, the first cooling is completed, and the second thermal switch 13 is kept disconnected, and the adiabatic magnetization process is entered. When the magnetocaloric module 11 is heated to a temperature slightly higher than the temperature of the heat sink 14, the second thermal switch 13 is closed, the magnetocaloric module 11 isothermally magnetized, generates magnetization heat, and releases the magnetization heat to the heat sink 14 through the second thermal switch 13; when the magnetocaloric module 11 is magnetized to the maximum magnetic field, it enters the normal periodic cooling process;
在无振动运行模式中,预冷制冷机31一直停止运行,第一热开关4始终处于断开状态。当磁热模块11被冷却同时磁化至目标磁场后,断开第二热开关13和第一热开关4,同时预冷制冷机31停止运行,预冷模块3与绝热去磁模块1处于传热断开状态,磁热模块11进行绝热去磁;当磁热模块11温度降低至制冷温度时,保持第二热开关13断开,进入等温去磁制冷过程,对负荷12实施无振动制冷;当等温去磁至磁场为零时,预冷制冷机31重新启动进行制冷,闭合第一热开关4和第二热开关13,绝热去磁模块1进行运作,磁热模块11被磁化的同时被冷却,达到目标磁场后,断开第二热开关13和第一热开关4,同时预冷制冷机31停止运行,开启新一轮无振动制冷模式。In the vibration-free operation mode, the precooling refrigerator 31 is always stopped, and the first thermal switch 4 is always in the disconnected state. When the magnetocaloric module 11 is cooled and magnetized to the target magnetic field, the second thermal switch 13 and the first thermal switch 4 are disconnected, and the precooling refrigerator 31 stops running at the same time. The precooling module 3 and the adiabatic demagnetization module 1 are in the heat transfer disconnected state, and the magnetocaloric module 11 performs adiabatic demagnetization; when the temperature of the magnetocaloric module 11 drops to the refrigeration temperature, the second thermal switch 13 is kept disconnected, and the isothermal demagnetization refrigeration process is entered, and vibration-free refrigeration is performed on the load 12; when the isothermal demagnetization reaches zero magnetic field, the precooling refrigerator 31 restarts to perform refrigeration, closes the first thermal switch 4 and the second thermal switch 13, and the adiabatic demagnetization module 1 operates, and the magnetocaloric module 11 is magnetized and cooled at the same time. After reaching the target magnetic field, the second thermal switch 13 and the first thermal switch 4 are disconnected, and the precooling refrigerator 31 stops running at the same time, and a new round of vibration-free refrigeration mode is started.
在一个实施例中,预冷制冷机的种类以及预冷制冷机的制冷温度范围可以根据实际情况进行选择,本发明为单级绝热去磁系统,具体也可以根据实际需求进行设置多级绝热去磁,多种制冷温度和多种热沉温度,而绝热去磁模块1的磁热材料也可以根据实际需求进行选择,在单级绝热去磁系统中,可以是钆镓石榴石也可以是氟化钆锂等,在多级绝热去磁系统中,较低温级可以是铬钾明矾或铁铵明矾等,都可以根据实际需求来选择,而本申请中的第一热开关4、第二热开关13也可以根据实际制冷需求进行选择,例如气隙式热开关、超导式热开关、磁阻热开关和机械式热开关等,同理本发明其他的部件材料类型也可以根据实际情况和需求进行选择。In one embodiment, the type of pre-cooling refrigerator and the refrigeration temperature range of the pre-cooling refrigerator can be selected according to actual conditions. The present invention is a single-stage adiabatic demagnetization system, and multi-stage adiabatic demagnetization, multiple refrigeration temperatures and multiple heat sink temperatures can be set according to actual needs. The magnetocaloric material of the adiabatic demagnetization module 1 can also be selected according to actual needs. In the single-stage adiabatic demagnetization system, it can be gadolinium gallium garnet or lithium gadolinium fluoride, etc. In the multi-stage adiabatic demagnetization system, the lower temperature level can be chromium potassium alum or iron ammonium alum, etc., which can be selected according to actual needs. The first thermal switch 4 and the second thermal switch 13 in the present application can also be selected according to actual refrigeration needs, such as air gap thermal switch, superconducting thermal switch, magnetoresistive thermal switch and mechanical thermal switch, etc. Similarly, the material types of other components of the present invention can also be selected according to actual conditions and needs.
当然,本发明还可有其它多种实施方式,基于本实施方式,本领域的普通技术人员在没有做出任何创造性劳动的前提下所获得其他实施方式,都属于本发明所保护的范围。Of course, the present invention may have many other implementations. Based on this implementation, other implementations obtained by ordinary technicians in this field without any creative work are all within the scope of protection of the present invention.
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