CN117815765B - A purification distillation integrated device for vitamin K2 - Google Patents
A purification distillation integrated device for vitamin K2 Download PDFInfo
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- CN117815765B CN117815765B CN202410245263.2A CN202410245263A CN117815765B CN 117815765 B CN117815765 B CN 117815765B CN 202410245263 A CN202410245263 A CN 202410245263A CN 117815765 B CN117815765 B CN 117815765B
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- fixedly connected
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- purification
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- 238000000746 purification Methods 0.000 title claims abstract description 66
- 238000004821 distillation Methods 0.000 title claims abstract description 40
- 235000019143 vitamin K2 Nutrition 0.000 title claims abstract description 25
- 239000011728 vitamin K2 Substances 0.000 title claims abstract description 25
- DKHGMERMDICWDU-GHDNBGIDSA-N menaquinone-4 Chemical compound C1=CC=C2C(=O)C(C/C=C(C)/CC/C=C(C)/CC/C=C(C)/CCC=C(C)C)=C(C)C(=O)C2=C1 DKHGMERMDICWDU-GHDNBGIDSA-N 0.000 title claims abstract description 24
- PFRQBZFETXBLTP-UHFFFAOYSA-N Vitamin K2 Natural products C1=CC=C2C(=O)C(CC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C)=C(C)C(=O)C2=C1 PFRQBZFETXBLTP-UHFFFAOYSA-N 0.000 title claims abstract description 23
- 238000001914 filtration Methods 0.000 claims abstract description 15
- 238000006243 chemical reaction Methods 0.000 claims abstract description 14
- 238000004140 cleaning Methods 0.000 claims abstract description 12
- 239000007787 solid Substances 0.000 claims abstract description 12
- 230000006835 compression Effects 0.000 claims abstract description 8
- 238000007906 compression Methods 0.000 claims abstract description 8
- 230000007246 mechanism Effects 0.000 claims abstract description 8
- 239000002245 particle Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 238000007789 sealing Methods 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- 238000007790 scraping Methods 0.000 claims description 7
- 230000008602 contraction Effects 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 4
- 238000004804 winding Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000013014 purified material Substances 0.000 claims description 2
- 230000000149 penetrating effect Effects 0.000 claims 1
- 239000007788 liquid Substances 0.000 abstract description 10
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 4
- 230000008878 coupling Effects 0.000 description 7
- 238000010168 coupling process Methods 0.000 description 7
- 238000005859 coupling reaction Methods 0.000 description 7
- 238000003756 stirring Methods 0.000 description 6
- 239000013618 particulate matter Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 229940079593 drug Drugs 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 238000010030 laminating Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- KZMGYPLQYOPHEL-UHFFFAOYSA-N Boron trifluoride etherate Chemical compound FB(F)F.CCOCC KZMGYPLQYOPHEL-UHFFFAOYSA-N 0.000 description 2
- 101100298225 Caenorhabditis elegans pot-2 gene Proteins 0.000 description 2
- -1 VK2 Chemical compound 0.000 description 2
- 230000015271 coagulation Effects 0.000 description 2
- 238000005345 coagulation Methods 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 229940041603 vitamin k 3 Drugs 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- HYPYXGZDOYTYDR-HAJWAVTHSA-N 2-methyl-3-[(2e,6e,10e,14e)-3,7,11,15,19-pentamethylicosa-2,6,10,14,18-pentaenyl]naphthalene-1,4-dione Chemical compound C1=CC=C2C(=O)C(C/C=C(C)/CC/C=C(C)/CC/C=C(C)/CC/C=C(C)/CCC=C(C)C)=C(C)C(=O)C2=C1 HYPYXGZDOYTYDR-HAJWAVTHSA-N 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- 208000027089 Parkinsonian disease Diseases 0.000 description 1
- 206010034010 Parkinsonism Diseases 0.000 description 1
- 208000005475 Vascular calcification Diseases 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 238000005904 alkaline hydrolysis reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 230000010405 clearance mechanism Effects 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000011676 menaquinone-4 Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 description 1
- 238000010408 sweeping Methods 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/62—Regenerating the filter material in the filter
- B01D29/64—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element
- B01D29/6469—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers
- B01D29/6476—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers with a rotary movement with respect to the filtering element
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/88—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices
- B01D29/90—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor having feed or discharge devices for feeding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/008—Liquid distribution
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D35/00—Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
- B01D35/16—Cleaning-out devices, e.g. for removing the cake from the filter casing or for evacuating the last remnants of liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/005—Separating solid material from the gas/liquid stream
- B01J8/006—Separating solid material from the gas/liquid stream by filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention relates to a purification and distillation integrated device for vitamin K2, wherein a supporting rod is fixedly connected to the inside of a purification tank, a second fixed barrel is fixedly connected to the inside of the supporting rod, a supporting bucket is fixedly connected to the inside of the purification tank below the second fixed barrel, a diversion bucket is fixedly connected to the bottom of the supporting bucket, a filtering sleeve is fixedly connected to the inside of the diversion bucket, a shielding conveyor is arranged in the inside of the second fixed barrel, an auxiliary cleaning mechanism is arranged in the inside of the diversion bucket, a first fixed barrel is fixedly connected to the top end of the second fixed barrel, and a compression auxiliary piece is arranged in the purification tank. According to the invention, the shielding conveyor is arranged, so that liquid and solid particles after reaction inside the connecting disc enter the guide hopper, and the liquid is discharged into the distillation tank for distillation through the filtration of the filtering sleeve, so that the vitamin K2 raw material can be distilled simultaneously in the step-by-step purification process, the time between the two steps is shortened, and the production efficiency of the vitamin K2 is further improved.
Description
Technical Field
The invention relates to the technical field of vitamin K2 production equipment, in particular to a purification and distillation integrated device for vitamin K2.
Background
Vitamin K2 (Menaquinone, VK2, MK-4) is a menaquinone compound, is an important fat-soluble coagulation vitamin, is used for maintaining normal coagulation function of an organism, and has various important physiological functions of preventing and treating osteoporosis arterial calcification, cardiovascular diseases, tumors, parkinsonism and the like. The synthetic raw materials mainly comprise: toluene, methanol, dioxane, boron trifluoride diethyl etherate, isopropyl ether and n-hexane; (B) acetic acid and sodium hydrosulfite; the crystalline/powdery vitamin K2 bulk drug is synthesized by the processes of alkaline hydrolysis, distillation, neutralization, condensation, hydrolysis, purification, crystallization and the like of the raw materials.
The existing vitamin K2 bulk drug is required to be purified and distilled in the production process, and the purification and distillation steps are separately carried out, and as the purified substances are gradually formed in the vitamin K2 purification process, the purified substances cannot be conveyed into a distillation tank in real time, and the materials are required to be integrally conveyed into the distillation tank for distillation after the purification is completed, the purification and distillation processes need to waste more time, so that the production efficiency of the vitamin K2 bulk drug is reduced, and further improvement is still needed.
Disclosure of Invention
The invention aims to solve the technical problem of overcoming the defects in the prior art and providing a purification and distillation integrated device for vitamin K2.
The invention is realized by the following technical scheme:
The utility model provides a purification distillation integrated device for vitamin K2, includes purification jar, retort and condenser pipe, the inside fixedly connected with branch of purification jar, the inboard fixedly connected with second fixed barrel of branch, the inside of purification jar is located the below fixedly connected with support bucket of second fixed barrel, the bottom fixedly connected with water conservancy diversion fill of support bucket, the inside fixedly connected with filter sleeve of water conservancy diversion fill, the bin outlet department fixedly connected with one-way relief valve of water conservancy diversion fill, the one end of one-way relief valve runs through to the inside of retort, the inside of second fixed barrel is provided with and is used for carrying the inside purified material of purification jar to the inside shielding conveyer of retort in real time; the second discharge valve is arranged in the guide hopper, and an auxiliary cleaning mechanism for discharging solid particles between the guide hopper and the filtering sleeve is arranged in the guide hopper; the top fixedly connected with first fixed bucket of second fixed bucket, the inside of purification jar is provided with runs through to the inside compression auxiliary that is used for compressing of first fixed bucket the inside reaction space of purification jar.
As still further aspects of the invention: the shielding conveyer is including installing the inside electric putter of second fixed bucket, electric putter's output runs through to the external connection of second fixed bucket has the connection pad, the bottom sliding connection of connection pad shelters from the sleeve, shelter from telescopic inboard fixedly connected with second shrink spring, the one end of second shrink spring with connection pad fixed connection, the bottom fixedly connected with dead lever of connection pad, the outer wall fixedly connected with seal piston of dead lever, seal piston sets up in the support bucket bin outlet, seal piston's inboard is provided with first relief valve, the outer wall of connection pad is provided with supplementary clear subassembly.
As still further aspects of the invention: the shielding sleeve is fixedly connected with a limiting block on the inner side of the shielding sleeve, a limiting chute matched with the limiting block is formed in the inner side of the connecting disc, and the shielding sleeve is in sliding connection with the connecting disc through the limiting block fixedly connected on the inner side.
As still further aspects of the invention: the auxiliary cleaning assembly comprises an auxiliary sleeve fixedly connected to the top end of the connecting disc, a base is fixedly connected to one side of the auxiliary sleeve, a connecting shaft is connected to the inner side of the base in a rotating mode, a third driving motor is mounted in the auxiliary sleeve, the output end of the third driving motor is connected with the connecting shaft, a third spur gear is fixedly connected to the outer wall of the connecting shaft, a first connecting rotary disc is fixedly connected to the outer wall of the connecting disc, a first spur gear ring meshed with the third spur gear is fixedly connected to the outer wall of the first connecting rotary disc, a connecting sleeve is fixedly connected to the top of the first connecting rotary disc, a sliding rod is connected to the inner side of the connecting sleeve in a sliding mode, the bottom end of the sliding rod penetrates through the lower portion of the first connecting rotary disc, a material stirring rod is fixedly connected to the bottom end of the sliding rod, a first shrinkage spring is fixedly connected to the connecting sleeve, and one end of the first shrinkage spring is fixedly connected to the connecting sleeve.
As still further aspects of the invention: the auxiliary cleaning mechanism comprises a rotating rod which is connected to the inner side of the diversion bucket in a rotating mode, one end of the rotating rod penetrates through the upper portion of the supporting bucket and is connected with the supporting bucket in a rotating mode, a fourth spur gear is fixedly connected to the bottom of the rotating rod, a second connecting rotating disc is fixedly connected to the inner side of the diversion bucket, a second spur gear ring meshed with the fourth spur gear is fixedly connected to the outer wall of the second connecting rotating disc, an auxiliary rod is fixedly connected to the bottom of the second connecting rotating disc, a scraping plate is fixedly connected to the bottom of the auxiliary rod, the scraping plate is attached to the top of the filtering sleeve, a rectangular linkage rod is fixedly connected to the bottom of the connecting shaft, and one end of the rectangular linkage rod penetrates through the inner portion of the rotating rod and is connected with the rotating rod in a sliding mode.
As still further aspects of the invention: the compression auxiliary piece is including installing the inside second driving motor of first fixed bucket, second driving motor's output is connected with first straight gear, the inside rotation of first fixed bucket is connected with four wind-up rolls, four the equal fixedly connected with of outer wall of wind-up roll with the second straight gear of first straight gear engaged with, the outer wall rolling of wind-up roll has and pulls the rope, the inside sliding connection of purification jar has the sliding tray, pull the one end of rope with sliding tray fixed connection, the inboard threaded connection of sliding tray has sealed lid, the top fixedly connected with coupling shell of branch, the top fixedly connected with coupling spring of coupling shell, the one end of coupling spring with sliding tray fixed connection, the inside rotation of coupling shell is connected with the guide pulley, it is in to pull the rope laminating the inboard of guide pulley.
As still further aspects of the invention: the top of coupling shell is located coupling spring's outside fixedly connected with first protection sleeve, first protection sleeve's inboard sliding connection has the second protection sleeve, second protection sleeve's one end with sliding tray fixed connection, the outer wall fixedly connected with guide block of sliding tray, purification jar inboard seted up with guide block assorted guide slot, purification jar pass through outer wall fixed connection's guide block with purification jar sliding connection.
As still further aspects of the invention: the distillation tank is characterized in that the top end of the distillation tank is provided with a tank cover, the top end of the tank cover is provided with a first driving motor, the output end of the first driving motor penetrates through the inner side of the tank cover and is connected with a rotary disc, one end of the one-way discharge valve is fixedly connected with a hose, the bottom of the rotary disc is fixedly connected with a connecting rod, and the inner side of the connecting rod is fixedly connected with the outer wall of the hose.
The working principle and the beneficial effects of the invention are as follows:
1. Through setting up and shielding the conveyer, intermittently start electric putter, electric putter's output drive connection pad moves down, make the laminating of shielding sleeve behind the top of supporting the fight, liquid and solid particle after shielding sleeve inboard reaction are isolated with the material in the purification jar, then the connection pad continues to push the second shrink spring and slide for shielding the sleeve when moving down, the connection pad moves down and promotes sealed piston through the dead lever and move down, when the connection pad moves down to the biggest, sealed piston shifts out to the inside of water conservancy diversion fill from water conservancy diversion fill feed inlet, thereby open water conservancy diversion fill feed inlet, make liquid and solid particle after the connection pad inboard reaction enter into the water conservancy diversion fill inside, the filtration of liquid through the filter sleeve is discharged to the distillation jar inside and is distilled, thereby make vitamin K2 raw materials distill simultaneously in the in-process of progressively purifying, time between two steps has been shortened, and then vitamin K2's production efficiency has been improved;
2. Through setting up supplementary subassembly that clears away, when the connection pad moves down, start the third driving motor, third driving motor output drive connecting axle drives the third straight-tooth wheel and rotates, thereby drive first straight-tooth wheel ring and drive the stirring rod through first connection capstan and rotate, make shelter from the sleeve and receive the particulate matter when the in-process that supports the bucket top is blocked, can sweep away the particulate matter through stirring rod, thereby make shelter from the sleeve and can completely isolate the product after the inboard reaction with purification jar inside, with this confined effect of shelter from the sleeve has been improved;
3. Through setting up supplementary clearance mechanism, when the third driving motor starts, the second relief valve is opened for the third driving motor output drives the connecting axle and rotates simultaneously and drives the fourth straight-tooth wheel through rectangle gangbar stirring dwang and carry out circumference rotation, thereby drive second straight-tooth wheel ring and drive the scraper blade through the second connection swivel, thereby clean the granule solid that silts up between filter sleeve and water conservancy diversion fill inside the second relief valve, discharge outside through the second relief valve, avoid silting up the particulate matter and pile up at the filter sleeve outer wall, the unobstructed nature when filtering with this has improved the filter sleeve;
4. Through setting up compression auxiliary spare, be provided with seal assembly equally between sliding tray and the purification jar, after electric putter output resets, intermittent type formula starts second driving motor, and second driving motor output drives first straight gear and rotates to drive four second straight gears and drive a wind-up roll respectively and rotate, with this to dragging the rope and rolling, thereby pulling sliding tray downwardly moving compresses the inside reaction space of purification jar, thereby improved the efficiency of multiple material reaction.
Drawings
The invention is described in further detail below with reference to the drawings and the detailed description.
FIG. 1 is a schematic diagram of the structure of the present invention;
FIG. 2 is a cross-sectional view of a purification tank and distillation tank of the present invention;
FIG. 3 is a schematic diagram of the internal structure of the purification tank of the present invention;
FIG. 4 is an enlarged view of the invention at A in FIG. 3;
FIG. 5 is a schematic view of a partial structure of a purification tank according to the present invention;
FIG. 6 is a schematic view of the top structure of the support hopper of the present invention;
FIG. 7 is an enlarged view of the invention at B in FIG. 6;
FIG. 8 is a schematic view of the inside structure of the guide hopper of the present invention;
FIG. 9 is a cross-sectional view of a connection pad of the present invention;
FIG. 10 is an enlarged view of FIG. 9C in accordance with the present invention;
FIG. 11 is a schematic view of an auxiliary cleaning mechanism according to the present invention.
In the figure: 1. a purification tank; 2. a distillation pot; 3. a condensing tube; 4. a can lid; 5. a first driving motor; 6. a support bucket; 7. a diversion bucket; 8. a one-way discharge valve; 9. a first fixed tub; 10. a connection housing; 11. a first protective sleeve; 12. a second protective sleeve; 13. a rotating disc; 14. a hose; 15. a connecting rod; 16. a sliding plate; 17. sealing cover; 18. pulling the rope; 19. a connecting spring; 20. a second fixed barrel; 21. a support rod; 22. a guide wheel; 23. a second driving motor; 24. a first straight gear; 25. a wind-up roll; 26. a second spur gear; 27. a first connection dial; 28. a first spur gear ring; 29. a stirring rod; 30. a slide bar; 31. a connecting sleeve; 32. a sealing piston; 33. a connecting disc; 34. an electric push rod; 35. a shielding sleeve; 36. a rotating lever; 37. a rectangular linkage rod; 38. an auxiliary sleeve; 39. a base; 40. a third driving motor; 41. a third spur gear; 42. a connecting shaft; 43. a fixed rod; 44. a first discharge valve; 45. a second discharge valve; 46. a scraper; 47. a filter sleeve; 48. the second connecting rotating disc; 49. a fourth spur gear; 50. a second spur gear ring; 51. an auxiliary lever; 52. a first retraction spring; 53. and a second retraction spring.
Detailed Description
The present invention will be described in further detail below with reference to the drawings and preferred embodiments, so that those skilled in the art can better understand the technical solutions of the present invention. All other embodiments, based on the embodiments of the invention, which would be apparent to one of ordinary skill in the art without making any inventive effort are intended to be within the scope of the invention.
In the description of the present invention, it should be noted that the directions or positional relationships indicated by the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", etc. are based on the directions or positional relationships shown in the drawings, are merely for convenience of describing the invention and simplifying the description, and do not indicate or imply that the apparatus or elements referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus should not be construed as limiting the invention.
Furthermore, it should be noted that, in the description of the present invention, unless explicitly specified and limited otherwise, the terms "mounted," "configured," and "connected" are to be construed broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected; can be directly connected, can be indirectly connected through an intermediate medium, and can also be communicated with the inside of two elements. The specific meaning of the above terms in the present invention can be understood by those skilled in the art according to the specific circumstances.
Referring to fig. 1 to 11, in the embodiment of the present invention, a purification and distillation integrated device for vitamin K2 includes a purification tank 1, a distillation tank 2 and a condensation pipe 3, wherein a supporting rod 21 is fixedly connected to the inside of the purification tank 1, a second fixed barrel 20 is fixedly connected to the inside of the supporting rod 21, a supporting bucket 6 is fixedly connected to the inside of the purification tank 1 below the second fixed barrel 20, a diversion bucket 7 is fixedly connected to the bottom of the supporting bucket 6, a filtering sleeve 47 is fixedly connected to the inside of the diversion bucket 7, a one-way discharge valve 8 is fixedly connected to a discharge port of the diversion bucket 7, one end of the one-way discharge valve 8 penetrates into the inside of the distillation tank 2, and a shielding conveyer for conveying substances purified in the purification tank 1 to the inside of the distillation tank 2 in real time is arranged in the inside of the second fixed barrel 20; the second discharge valve 45 is arranged in the guide hopper 7, and an auxiliary cleaning mechanism for discharging solid particles between the guide hopper 7 and the filtering sleeve 47 is arranged in the guide hopper 7; the top fixedly connected with first fixed vat 9 of second fixed vat 20, the inside of purification jar 1 is provided with the compression auxiliary that runs through to the inside reaction space of being used for of first fixed vat 9 to purification jar 1, it is provided with supplementary clear subassembly to shield the conveyer including installing the electric putter 34 inside the fixed vat 20 of second, the output of electric putter 34 runs through to the external connection of the fixed vat 20 of second, the bottom sliding connection of connection pad 33 has shielding sleeve 35, shielding sleeve 35's inboard fixedly connected with second shrink spring 53, second shrink spring 53's one end and connection pad 33 fixed connection, connection pad 33's bottom fixedly connected with dead lever 43, dead lever 43's outer wall fixedly connected with seal piston 32, seal piston 32 sets up in the holding hopper 6 bin outlet, seal piston 32's inboard is provided with first relief valve 44, connection pad 33's outer wall is provided with supplementary clear subassembly, shielding sleeve 35's inboard fixedly connected with stopper, spacing spout with stopper assorted is seted up to the inboard of connection pad 33, shielding sleeve 35 passes through inboard fixedly connected stopper and 33 sliding connection.
In this embodiment: the seal piston 32 and support and be provided with seal assembly between fighting 6, seal assembly can be seal rubber etc. seal parts, at first, support the internally mounted of fighting 6 and carry out the heater that heats to purification jar 1 inside material, through support the inside heater of fighting 6 and carry out the heating to the inside multiple material of purification jar 1 and make the material can react, after multiple material reaction gradually forms the liquid accumulation that needs at support and fight 6 top, can intermittently start electric putter 34, when electric putter 34's output drive connection pad 33 moves down, make the laminating of shielding sleeve 35 support the top of fighting 6, liquid and solid particle after will shielding sleeve 35 inboard reaction and purification jar 1 inside material isolation, then connection pad 33 continues to move down and carries out the slip for shielding sleeve 35 when pressing second shrink spring 53, connection pad 33 moves down, promote seal piston 32 through dead lever 43 when moving down, when connection pad 33 moves down to the maximum, thereby open the inside of fighting 7 feed inlet, make the inside of water conservancy diversion jar 7 after the inboard reaction liquid enters into the inside of water conservancy diversion jar 7 and solid particle K, can directly carry out the distillation jar 2 after the distillation jar 2, thereby can carry out the purification jar 2, and the distillation process is carried out in order to improve the time after the inside distillation jar 2, can directly to carry out the purification, thereby the step is discharged into the distillation pot 2, can be finished, and the distillation valve is discharged after the inside can be finished, and the distillation pot 2 is purified.
Referring to fig. 10, the auxiliary cleaning assembly includes an auxiliary sleeve 38 fixedly connected to the top end of the connecting disc 33, a base 39 is fixedly connected to one side of the auxiliary sleeve 38, a connecting shaft 42 is rotatably connected to the inner side of the base 39, a third driving motor 40 is mounted in the auxiliary sleeve 38, an output end of the third driving motor 40 is connected to the connecting shaft 42, a third spur gear 41 is fixedly connected to an outer wall of the connecting shaft 42, a first connecting rotary disc 27 is fixedly connected to an outer wall of the connecting disc 33, a first spur gear ring 28 meshed with the third spur gear 41 is fixedly connected to an outer wall of the first connecting rotary disc 27, a connecting sleeve 31 is fixedly connected to the top of the first connecting rotary disc 27, a sliding rod 30 is slidably connected to the inner side of the connecting sleeve 31, a bottom end of the sliding rod 30 penetrates through to the lower portion of the first connecting rotary disc 27 and is fixedly connected to a stirring rod 29, a first contraction spring 52 is fixedly connected to the top end of the sliding rod 30, and one end of the first contraction spring 52 is fixedly connected to the connecting sleeve 31.
In this embodiment: the bottom of driving lever 29 surpasses the bottom of shielding sleeve 35, when connection pad 33 moves down, start third driving motor 40, third driving motor 40 output drive axle 42 drives third straight-tooth wheel 41 and rotates, thereby drive first straight-tooth wheel ring 28 and drive driving lever 29 through first connection capstan 27 and rotate, make shielding sleeve 35 receive the in-process that supports the top of fighting 6 when the blocking of particulate matter, can sweep the particulate matter through driving lever 29, thereby make shielding sleeve 35 can completely isolate the product after the inboard reaction with purification jar 1 inside, thereby improved shielding sleeve 35 confined effect, when connection pad 33 slides half for shielding sleeve 35, third driving motor 40 stops the operation.
Referring to fig. 10 to 11, the auxiliary cleaning mechanism includes a rotating rod 36 rotatably connected to the inner side of the diversion bucket 7, one end of the rotating rod 36 penetrates through the upper side of the supporting bucket 6 and is rotatably connected with the supporting bucket 6, a fourth spur gear 49 is fixedly connected to the bottom of the rotating rod 36, a second connecting rotating disc 48 is fixedly connected to the inner side of the diversion bucket 7, a second spur gear ring 50 meshed with the fourth spur gear 49 is fixedly connected to the outer wall of the second connecting rotating disc 48, an auxiliary rod 51 is fixedly connected to the bottom of the second connecting rotating disc 48, a scraping plate 46 is fixedly connected to the bottom of the auxiliary rod 51, the scraping plate 46 is attached to the top of the filtering sleeve 47, a rectangular linkage rod 37 is fixedly connected to the bottom of the connecting shaft 42, and one end of the rectangular linkage rod 37 penetrates through the inner side of the rotating rod 36 and is slidably connected with the rotating rod 36.
In this embodiment: the sealing component is also arranged between the rotating rod 36 and the supporting hopper 6, the sealing component can be a part used for sealing such as sealing rubber, and the second discharge valve 45 is opened when the third driving motor 40 is started, so that the output end of the third driving motor 40 drives the connecting shaft 42 to rotate and simultaneously drives the rotating rod 36 to drive the fourth spur gear 49 to rotate circumferentially through the rectangular linkage rod 37, thereby driving the second spur gear ring 50 to drive the scraping plate 46 to rotate through the second connecting rotating disc 48, further sweeping the granular solid deposited between the filtering sleeve 47 and the diversion hopper 7 into the second discharge valve 45, discharging the granular solid to the outside through the second discharge valve 45, and avoiding the deposited granular solid from being deposited on the outer wall of the filtering sleeve 47, thereby improving the smoothness of the filtering sleeve 47 during filtering.
Referring to fig. 2 to 7, the compression auxiliary comprises a second driving motor 23 installed inside a first fixed barrel 9, a first spur gear 24 is connected to the output end of the second driving motor 23, four wind-up rollers 25 are rotatably connected to the inside of the first fixed barrel 9, a second spur gear 26 meshed with the first spur gear 24 is fixedly connected to the outer walls of the four wind-up rollers 25, a pulling rope 18 is wound on the outer wall of the wind-up rollers 25, a sliding disk 16 is slidably connected to the inside of a purification tank 1, one end of the pulling rope 18 is fixedly connected with the sliding disk 16, a sealing cover 17 is in threaded connection with the inner side of the sliding disk 16, a connecting shell 10 is fixedly connected to the top end of the connecting shell 10, a connecting spring 19 is fixedly connected with the sliding disk 16, a guide wheel 22 is rotatably connected to the inside of the connecting shell 10, the pulling rope 18 is attached to the inner side of the guide wheel 22, a first protection sleeve 11 is fixedly connected to the outside of the connecting shell 10, a second protection sleeve 12 is slidably connected to the inner side of the first protection sleeve 11, one end of the second protection sleeve 12 is fixedly connected to the inner side of the guide block 1, and the purification tank 1 is fixedly connected to the outer wall of the guide block 1 through a sliding guide block 16.
In this embodiment: a sealing component is also arranged between the sliding disc 16 and the purification tank 1, after the output end of the electric push rod 34 is reset, the second driving motor 23 is intermittently started, the output end of the second driving motor 23 drives the first straight gear 24 to rotate, and accordingly four second straight gears 26 are driven to respectively drive one winding roller 25 to rotate, so that the pulling rope 18 is wound, the sliding disc 16 is pulled to move downwards to compress the reaction space inside the purification tank 1, and the reaction efficiency of various materials is improved.
Referring to fig. 2, a tank cover 4 is installed at the top end of the distillation tank 2, a first driving motor 5 is installed at the top end of the tank cover 4, an output end of the first driving motor 5 penetrates through the inner side of the tank cover 4 and is connected with a rotary disc 13, one end of the one-way discharge valve 8 is fixedly connected with a hose 14, a connecting rod 15 is fixedly connected with the bottom of the rotary disc 13, and the inner side of the connecting rod 15 is fixedly connected with the outer wall of the hose 14.
In this embodiment: the hose 14 is initially reserved for a certain length, purified liquid enters the distillation tank 2 through the one-way discharge valve 8 and the hose 14 to be distilled, meanwhile, the first driving motor 5 is started, the output end of the first driving motor 5 rotates positively and negatively, the rotary disk 13 is driven by the output end of the first driving motor 5 to drive the hose 14 to rotate for one circle and then rotate reversely, so that purified liquid is uniformly dispersed in the distillation tank 2, and the purified liquid can be distilled in real time.
The foregoing is merely a preferred embodiment of the present invention and it should be noted that modifications and adaptations to those skilled in the art may be made without departing from the principles of the present invention, which are intended to be comprehended within the scope of the present invention.
Claims (6)
1. The utility model provides a purification distillation integrated device for vitamin K2, includes purification jar (1), retort (2) and condenser pipe (3), its characterized in that, the inside fixedly connected with branch (21) of purification jar (1), the inboard fixedly connected with second fixed barrel (20) of branch (21), the inside of purification jar (1) is located the below fixedly connected with support bucket (6) of second fixed barrel (20), the bottom fixedly connected with water conservancy diversion fill (7) of support bucket (6), the inside fixedly connected with filter sleeve (47) of water conservancy diversion fill (7), the bin outlet department fixedly connected with one-way discharge valve (8) of water conservancy diversion fill (7), one end of one-way discharge valve (8) runs through to the inside of retort (2), the inside of second fixed barrel (20) is provided with and is used for carrying the inside purified material of purification jar (1) to the inside shielding conveyer of retort (2) in real time;
A second discharge valve (45) is arranged in the guide hopper (7), and an auxiliary cleaning mechanism for discharging solid particles between the guide hopper (7) and the filtering sleeve (47) is arranged in the guide hopper (7);
The top end of the second fixed barrel (20) is fixedly connected with a first fixed barrel (9), and a compression auxiliary part penetrating into the first fixed barrel (9) and used for compressing the reaction space in the purification tank (1) is arranged in the purification tank (1);
The shielding conveyer comprises an electric push rod (34) arranged in a second fixed barrel (20), an output end of the electric push rod (34) penetrates through to an outer portion of the second fixed barrel (20) and is connected with a connecting disc (33), a shielding sleeve (35) is slidably connected to the bottom of the connecting disc (33), a second contraction spring (53) is fixedly connected to the inner side of the shielding sleeve (35), one end of the second contraction spring (53) is fixedly connected with the connecting disc (33), a fixing rod (43) is fixedly connected to the bottom of the connecting disc (33), a sealing piston (32) is fixedly connected to the outer wall of the fixing rod (43), the sealing piston (32) is arranged in a discharge port of the supporting hopper (6), a first discharge valve (44) is arranged on the inner side of the sealing piston (32), and an auxiliary cleaning assembly is arranged on the outer wall of the connecting disc (33);
The compression auxiliary piece comprises a second driving motor (23) arranged in the first fixed barrel (9), a first straight gear (24) is connected to the output end of the second driving motor (23), four winding rollers (25) are rotatably connected to the inside of the first fixed barrel (9), a second straight gear (26) meshed with the first straight gear (24) is fixedly connected to the outer walls of the four winding rollers (25), a pulling rope (18) is wound on the outer walls of the winding rollers (25), a sliding disc (16) is slidably connected to the inside of the purification tank (1), one end of the pulling rope (18) is fixedly connected with the sliding disc (16), a sealing cover (17) is connected to the inner side of the sliding disc (16) in a threaded mode, a connecting shell (10) is fixedly connected to the top end of each supporting rod (21), a connecting spring (19) is fixedly connected to the sliding disc (16), one end of each connecting spring (19) is fixedly connected to the corresponding inner side of the corresponding guide wheel (22) in a rotating mode;
A heater for heating the materials in the purifying tank (1) is arranged in the supporting hopper (6);
When the output end of the electric push rod (34) drives the connecting disc (33) to move downwards, the shielding sleeve (35) is attached to the top end of the supporting bucket (6).
2. The integrated purification and distillation device for vitamin K2 according to claim 1, wherein a limiting block is fixedly connected to the inner side of the shielding sleeve (35), a limiting chute matched with the limiting block is formed in the inner side of the connecting disc (33), and the shielding sleeve (35) is slidably connected with the connecting disc (33) through the limiting block fixedly connected to the inner side.
3. The integrated purification and distillation device for vitamin K2 according to claim 1, wherein the auxiliary cleaning assembly comprises an auxiliary sleeve (38) fixedly connected to the top end of the connecting disc (33), one side of the auxiliary sleeve (38) is fixedly connected with a base (39), the inner side of the base (39) is rotatably connected with a connecting sleeve (42), a third driving motor (40) is mounted in the auxiliary sleeve (38), the output end of the third driving motor (40) is connected with the connecting sleeve (42), the outer wall of the connecting sleeve (42) is fixedly connected with a third spur gear (41), the outer wall of the connecting disc (33) is fixedly connected with a first connecting rotary disc (27), the outer wall of the first connecting rotary disc (27) is fixedly connected with a first spur gear ring (28) meshed with the third spur gear (41), the top of the first connecting rotary disc (27) is fixedly connected with a connecting sleeve (31), the inner side of the connecting sleeve (31) is slidably connected with a sliding rod (30), the bottom end of the sliding rod (30) is fixedly connected with a first pulling rod (29) fixedly connected with a first pulling rod (30), one end of the first contraction spring (52) is fixedly connected with the connecting sleeve (31).
4. A purification and distillation integrated device for vitamin K2 according to claim 3, wherein the auxiliary cleaning mechanism comprises a rotating rod (36) rotatably connected to the inner side of the guide bucket (7), one end of the rotating rod (36) penetrates to the upper side of the support bucket (6) and is rotatably connected with the support bucket (6), a fourth spur gear (49) is fixedly connected to the bottom of the rotating rod (36), a second connecting rotating disc (48) is fixedly connected to the inner side of the guide bucket (7), a second spur gear ring (50) meshed with the fourth spur gear (49) is fixedly connected to the outer wall of the second connecting rotating disc (48), an auxiliary rod (51) is fixedly connected to the bottom of the second connecting rotating disc (48), a scraping plate (46) is fixedly connected to the bottom of the auxiliary rod (51), the scraping plate (46) is attached to the top of the filter sleeve (47), a rectangular linkage rod (37) is fixedly connected to the bottom of the connecting shaft (42), and the second linkage rod (37) is connected to the inner side of the rotating rod (36) in a sliding manner.
5. The integrated purification and distillation device for vitamin K2 according to claim 1, wherein the top of the connecting shell (10) is positioned outside the connecting spring (19) and fixedly connected with a first protection sleeve (11), the inner side of the first protection sleeve (11) is slidably connected with a second protection sleeve (12), one end of the second protection sleeve (12) is fixedly connected with the sliding disc (16), the outer wall of the sliding disc (16) is fixedly connected with a guide block, the inner side of the purification tank (1) is provided with a guide groove matched with the guide block, and the purification tank (1) is slidably connected with the purification tank (1) through the guide block fixedly connected with the outer wall.
6. The purification and distillation integrated device for vitamin K2 according to claim 1, wherein a tank cover (4) is installed at the top end of the distillation tank (2), a first driving motor (5) is installed at the top end of the tank cover (4), an output end of the first driving motor (5) penetrates through to the inner side of the tank cover (4) and is connected with a rotary disc (13), one end of a one-way discharge valve (8) is fixedly connected with a hose (14), a connecting rod (15) is fixedly connected to the bottom of the rotary disc (13), and the inner side of the connecting rod (15) is fixedly connected to the outer wall of the hose (14).
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| CN202410245263.2A CN117815765B (en) | 2024-03-05 | 2024-03-05 | A purification distillation integrated device for vitamin K2 |
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| CN202410245263.2A CN117815765B (en) | 2024-03-05 | 2024-03-05 | A purification distillation integrated device for vitamin K2 |
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| JPH09125072A (en) * | 1995-11-01 | 1997-05-13 | Shin Meiwa Ind Co Ltd | Purification of pyroligneous acid and apparatus therefor |
| CN105854333A (en) * | 2016-05-19 | 2016-08-17 | 云南悦馨香料科技有限公司 | Simultaneous distillation-extraction device with pistons |
| CN209669103U (en) * | 2019-03-05 | 2019-11-22 | 秦皇岛必爱尔生物科技有限公司 | Equipment for purifying is used in a kind of production of black rice peel anthocyanidin |
| CN218474888U (en) * | 2022-09-07 | 2023-02-14 | 烟台榕兴医疗科技有限公司 | High-efficient purification device is used in nervonic acid production |
| CN117101887A (en) * | 2023-08-23 | 2023-11-24 | 江苏华达环境工程有限公司 | Novel multifunctional centrifugal concentrating machine and application method thereof |
| CN117282147A (en) * | 2023-11-14 | 2023-12-26 | 宜兴市宇翔机械科技有限公司 | Self-cleaning filtering system for sewage treatment and filtering process thereof |
-
2024
- 2024-03-05 CN CN202410245263.2A patent/CN117815765B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09125072A (en) * | 1995-11-01 | 1997-05-13 | Shin Meiwa Ind Co Ltd | Purification of pyroligneous acid and apparatus therefor |
| CN105854333A (en) * | 2016-05-19 | 2016-08-17 | 云南悦馨香料科技有限公司 | Simultaneous distillation-extraction device with pistons |
| CN209669103U (en) * | 2019-03-05 | 2019-11-22 | 秦皇岛必爱尔生物科技有限公司 | Equipment for purifying is used in a kind of production of black rice peel anthocyanidin |
| CN218474888U (en) * | 2022-09-07 | 2023-02-14 | 烟台榕兴医疗科技有限公司 | High-efficient purification device is used in nervonic acid production |
| CN117101887A (en) * | 2023-08-23 | 2023-11-24 | 江苏华达环境工程有限公司 | Novel multifunctional centrifugal concentrating machine and application method thereof |
| CN117282147A (en) * | 2023-11-14 | 2023-12-26 | 宜兴市宇翔机械科技有限公司 | Self-cleaning filtering system for sewage treatment and filtering process thereof |
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| CN117815765A (en) | 2024-04-05 |
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