CN117665029A - Automatic XRF detection device for integrated preparation of glass fuse sample - Google Patents
Automatic XRF detection device for integrated preparation of glass fuse sample Download PDFInfo
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- CN117665029A CN117665029A CN202311683834.2A CN202311683834A CN117665029A CN 117665029 A CN117665029 A CN 117665029A CN 202311683834 A CN202311683834 A CN 202311683834A CN 117665029 A CN117665029 A CN 117665029A
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- xrf detection
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- 238000001514 detection method Methods 0.000 title claims abstract description 92
- 239000011521 glass Substances 0.000 title claims abstract description 69
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000000843 powder Substances 0.000 claims abstract description 35
- 238000002844 melting Methods 0.000 claims abstract description 30
- 230000008018 melting Effects 0.000 claims abstract description 30
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 239000000155 melt Substances 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 238000001816 cooling Methods 0.000 claims description 19
- 239000003795 chemical substances by application Substances 0.000 claims description 18
- 239000000156 glass melt Substances 0.000 claims description 12
- 238000000034 method Methods 0.000 abstract description 13
- 230000004927 fusion Effects 0.000 abstract description 9
- 230000008569 process Effects 0.000 abstract description 7
- 238000004846 x-ray emission Methods 0.000 description 45
- 238000001304 sample melting Methods 0.000 description 8
- 210000001503 joint Anatomy 0.000 description 6
- 230000007246 mechanism Effects 0.000 description 5
- 238000000048 melt cooling Methods 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- 230000006978 adaptation Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000003303 reheating Methods 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 1
- 239000006184 cosolvent Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B25—HAND TOOLS; PORTABLE POWER-DRIVEN TOOLS; MANIPULATORS
- B25J—MANIPULATORS; CHAMBERS PROVIDED WITH MANIPULATION DEVICES
- B25J15/00—Gripping heads and other end effectors
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B25—HAND TOOLS; PORTABLE POWER-DRIVEN TOOLS; MANIPULATORS
- B25J—MANIPULATORS; CHAMBERS PROVIDED WITH MANIPULATION DEVICES
- B25J15/00—Gripping heads and other end effectors
- B25J15/06—Gripping heads and other end effectors with vacuum or magnetic holding means
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B25—HAND TOOLS; PORTABLE POWER-DRIVEN TOOLS; MANIPULATORS
- B25J—MANIPULATORS; CHAMBERS PROVIDED WITH MANIPULATION DEVICES
- B25J15/00—Gripping heads and other end effectors
- B25J15/06—Gripping heads and other end effectors with vacuum or magnetic holding means
- B25J15/0616—Gripping heads and other end effectors with vacuum or magnetic holding means with vacuum
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/2202—Preparing specimens therefor
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/2204—Specimen supports therefor; Sample conveying means therefore
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/223—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material by irradiating the sample with X-rays or gamma-rays and by measuring X-ray fluorescence
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/07—Investigating materials by wave or particle radiation secondary emission
- G01N2223/076—X-ray fluorescence
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/10—Different kinds of radiation or particles
- G01N2223/101—Different kinds of radiation or particles electromagnetic radiation
- G01N2223/1016—X-ray
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/30—Accessories, mechanical or electrical features
- G01N2223/31—Accessories, mechanical or electrical features temperature control
- G01N2223/3106—Accessories, mechanical or electrical features temperature control heating, furnaces
Landscapes
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Health & Medical Sciences (AREA)
- Robotics (AREA)
- Mechanical Engineering (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention discloses an automatic XRF detection device for integrally preparing a glass sheet sample, which comprises the following components: the powder sample placing plate, the fusion machine, the fuse sheet die, the XRF detection equipment and the transfer assembly are arranged on the powder sample placing plate; the melting machine is used for heating and melting the powder sample to form liquid; the fuse die may form the liquid into a glass fuse; the XRF detection device is used for detecting the glass fuse piece. The transfer assembly moves the crucible into a melter that heats and melts the powder sample and pours the liquid into a fuse die to form a glass fuse, and finally the transfer assembly delivers the glass fuse into the XRF detection device. The automatic sample preparation of glass fuse can be realized through the transfer assembly, a user is not contacted with a high-temperature object any more, the risk of scalding is avoided, the sample preparation and detection are integrated, the risk of pollution of a sample in the carrying process can be reduced, the interference of human factors on the sample is reduced, and the accuracy and the reliability of a detection result are improved.
Description
Technical Field
The invention relates to the technical field of XRF detection, in particular to an automatic XRF detection device for integrally preparing a glass sheet sample.
Background
X-ray fluorescence spectroscopy (XRF) is a rapid elemental quantification method, glass melting is a sample pretreatment technique for XRF, by dissolving a sample in a melted solvent to form a glass sheet compound that is readily analyzed by XRF.
The sample of the existing XRF detection device still needs to be prepared manually, the working efficiency of manually preparing the sample is low, and the interference of human factors on the sample can be increased, so that the accuracy and the reliability of the detection result are affected. In addition, manual sample preparation has certain safety risks, such as dust containing heavy metals is inevitably generated in the process of preparing the sample by a tabletting method, the physical health of people is affected, high-temperature objects need to be clamped in a heating furnace in the process of preparing the glass fuse sheet, and the risk of scalding caused by improper clamping exists.
Therefore, how to improve the detection efficiency and the detection accuracy and reliability of the XRF detection device is a technical problem that needs to be solved by those skilled in the art.
Disclosure of Invention
The invention aims to provide an automatic XRF detection device for integrally preparing a glass sheet sample, which can effectively improve the detection efficiency and the detection accuracy and reliability.
In order to achieve the above purpose, the present invention provides the following technical solutions:
an automated XRF detection device for integrated preparation of glass sheet samples, comprising:
the powder sample placing tray is provided with at least one crucible, and the crucible is used for containing powder samples;
the melting machine is used for heating and melting the powder sample in the crucible to form liquid;
the fuse piece die is used for forming glass fuse pieces from liquid obtained after melting the powder sample;
an XRF detection device for detecting the glass melt sheet;
a transfer assembly for moving the crucible into or out of the melter, or transporting the glass melt sheet into the XRF detection apparatus.
Preferably, the transfer assembly comprises a robot for gripping the crucible or the fuse-element mould by the jaws, a jaw and a suction cup assembly, the robot also being adapted to suck the glass fuse-element by the suction cup assembly.
Preferably, the transfer assembly further comprises a suction cup holder, the clamping jaw is connected to the robot, the suction cup assembly is detachably connected to the clamping jaw, and the suction cup holder is used for bearing the detached suction cup assembly.
Preferably, the clamping jaw comprises a connecting piece and a clamping end, one end of the connecting piece is connected with the tail end of the robot, the other end of the connecting piece is connected with the clamping end, a sucker fixing sleeve is arranged on the side portion of the connecting piece, and the sucker assembly is used for being detachably connected with the sucker fixing sleeve.
Preferably, the automated XRF detection device further comprises a release agent placement tray having at least one portion of release agent disposed thereon, the transfer assembly being configured to add the release agent to the crucible.
Preferably, the automated XRF detection device further comprises a die holder for carrying the fuse die and a fuse cooling plate, and the transfer assembly is for transferring the fuse die to the fuse cooling plate for cooling.
Preferably, the automated XRF detection device further comprises a glass fuse placing tray, and the transfer assembly is configured to transfer the glass fuse on the fuse cooling tray to the glass fuse placing tray.
Preferably, the automated XRF detection device further comprises a frame for carrying the powder sample placement tray, the melter, and the transfer assembly.
Preferably, a lofting port is arranged in a region, corresponding to the XRF detection equipment, of the frame.
Preferably, a door capable of opening and closing is arranged above the detection cavity of the XRF detection device.
Compared with the prior art, the technical scheme has the following advantages:
according to the automatic XRF detection device for integrally preparing the glass sheet sample, during detection, a crucible filled with a powder sample is moved into a fusion machine by a transfer assembly, and after the fusion machine heats and melts the powder sample into liquid, the liquid is poured into a fusion sheet die to form a glass fusion sheet; taking out the fuse piece mould with the height Wen Rongpian by the transfer component, and putting the fuse piece mould into a fuse piece cooling disc for cooling; after cooling, the transfer component transfers the glass fuse piece in the fuse piece mould to the fuse piece placing disc; and finally, conveying the glass melting sheet to XRF detection equipment by a transfer assembly for detection. The automatic sample preparation of glass fuse can be realized through the transfer assembly, a user is not contacted with a high-temperature object any more, the risk of scalding is avoided, the sample preparation and detection are integrated, the risk of pollution of a sample in the carrying process can be reduced, the interference of human factors on the sample is reduced, and the accuracy and the reliability of a detection result are improved.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings that are required to be used in the embodiments or the description of the prior art will be briefly described below, and it is obvious that the drawings in the following description are only embodiments of the present invention, and that other drawings can be obtained according to the provided drawings without inventive effort for a person skilled in the art.
FIG. 1 is a schematic diagram of an automated XRF detection device for integrated preparation of glass sheet samples, according to one embodiment of the present invention;
FIG. 2 is a schematic diagram of an XRF detection apparatus;
FIG. 3 is a schematic structural view of a clamping jaw;
FIG. 4 is a schematic view of the structure of the jaw and chuck assembly;
FIG. 5 is a schematic view of the structure of the jaw and chuck assembly when connected together;
figure 6 is a gas circuit diagram of the chuck assembly.
The reference numerals are as follows:
1 is a frame, 2 is a powder sample placing tray, 3 is a crucible, 4 is a fusion machine, 5 is a fuse sheet die, 6 is a die support, 7 is a robot, 8 is a clamping jaw, 81 is a connecting piece, 82 is a clamping end, 83 is a sucker fixing sleeve, 84 is an air port, 85 is a clamping piece, 9 is a sucker component, 91 is a sucker, 92 is a pipe body, 93 is a joint, 10 is a sucker placing rack, 11 is a sample placing port, 12 is a fuse sheet cooling plate, 13 is a glass fuse sheet placing tray, 14 is a release agent placing tray, 15 is a release agent, 16 is a fuse sheet support, 17 is an XRF detection device, 18 is a detection cavity, 19 is a cabin door, 20 is a glass fuse sheet, 21 is a vacuum pump, 22 is a pressure gauge, and 23 is an electromagnetic valve.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Referring to fig. 1, an automated XRF detection device for integrated preparation of glass sheet samples according to an embodiment of the present invention comprises: the powder sample placing tray 2, the fusion machine 4, the fuse sheet die 5, the XRF detection equipment 17 and the transfer assembly, wherein at least one crucible 3 is arranged on the powder sample placing tray 2, and the crucible 3 is used for containing powder samples; the melting machine 4 is used for heating and melting the powder sample in the crucible 3 to form liquid; the fuse die 5 may form the melted liquid of the powder sample into a glass fuse 20; XRF detection device 17 is used to detect glass fuse 20. In the detection process, the crucible 3 filled with the powder sample is moved into the melting machine 4 by the transfer component, the melting machine 4 heats and melts the powder sample into liquid and then poured into the fuse piece mold 5 to form the glass fuse piece 20, and finally the glass fuse piece 20 is conveyed into the XRF detection equipment 17 by the transfer component for detection. The automatic sample preparation of the glass fuse piece 20 can be realized through the transfer assembly, a user does not contact with a high-temperature object any more, the risk of scalding is avoided, the sample preparation and detection are integrated, the risk of pollution of the sample in the carrying process can be reduced, the interference of human factors on the sample is reduced, and the accuracy and the reliability of the detection result are improved.
In some embodiments, as shown in fig. 3-4, the transfer assembly includes a robot 7, a clamping jaw 8 and a suction cup assembly 9, the clamping jaw 8 and the suction cup assembly 9 are located at the end of the robot 7, the robot 7 is used for clamping the crucible 3 or the fuse piece mold 5 through the clamping jaw 8, the clamping stability of the crucible 3 and the fuse piece mold 5 can be improved through the clamping jaw 8, the robot 7 is also used for sucking the glass fuse piece 20 through the suction cup assembly 9, and damage to the glass fuse piece 20 can be reduced through sucking the glass fuse piece 20 through the suction cup assembly 9.
In some embodiments, the transfer assembly further comprises a suction cup holder 10, the clamping jaw 8 is connected to the robot 7, the suction cup assembly 9 is detached or connected to the clamping jaw 8, the suction cup holder 10 can bear the detached suction cup assembly 9, in particular, when the crucible 3 or the fuse piece mold 5 needs to be clamped, the suction cup assembly 9 needs to be placed on the suction cup holder 10 so as to avoid affecting the taking and placing operation of the crucible 3 or the fuse piece mold 5; when it is desired to pick and place the glass fuse piece 20, the suction cup assembly 9 is attached to the clamping jaw 8.
In some embodiments, as shown in fig. 3, the clamping jaw 8 includes a connecting piece 81 and a clamping end 82, one end of the connecting piece 81 is connected with the end of the robot 7, the other end of the connecting piece 81 is connected with the clamping end 82, the clamping end 82 includes two clamping blocks which can be close to or far away from each other, a sucker fixing sleeve 83 is arranged on the side portion of the connecting piece 81, a sucker assembly 9 is used for being detachably connected with the sucker fixing sleeve 83, specifically, an air port 84 for connecting an air pipe is arranged at the upper end of the sucker fixing sleeve 83, the air port 84 is used for connecting an air pressure system, as shown in fig. 6, the air pressure system includes a vacuum pump 21, a pressure gauge 22 and an electromagnetic valve 23, the vacuum pump 21 is used for adsorbing the sucker 91 system, the pressure gauge 22 is used for detecting air path pressure, and the electromagnetic valve 23 is used for controlling on-off of an air path. The lower extreme of the fixed cover 83 of sucking disc is equipped with the interface that is used for supplying sucking disc subassembly 9 upper end to stretch into, and sucking disc subassembly 9 includes sucking disc 91, body 92 and butt joint 93, and butt joint 93 is located the upper end of body 92, and sucking disc 91 is located the lower extreme of body 92, in order to improve the connection compactness of sucking disc subassembly 9 and the fixed cover 83 of sucking disc, can set up seal structure on butt joint 93 to when guaranteeing sucking disc 91 to absorb glass fuse 20, the butt joint department can not influence the suction effect because of the gas leakage. In order to improve the connection stability of the sucker assembly 9 and the sucker fixing sleeve 83, a clamping piece 85 can be arranged on the side portion of the clamping jaw 8, and after the sucker assembly 9 is connected with the sucker fixing sleeve 83, the clamping piece 85 is tightly held on the sucker assembly 9, and the clamping piece 85 comprises two openable and closable arc clamping parts. When the sucker assembly 9 is not used, the sucker assembly 9 is vertically placed on the sucker placing frame 10; when the robot 7 needs to be used, the clamping jaw 8 is moved by the robot 7 so that the sucker fixing sleeve 83 corresponds to the butt joint 93, and then the sucker fixing sleeve moves downwards to connect the sucker fixing sleeve and the butt joint 93 in an inserting way; when the sucker assembly 9 needs to be detached from the clamping jaw 8, the robot 7 moves the sucker assembly 9 onto the sucker rack 10, and then moves the clamping jaw 8 upwards.
In some embodiments, the automated XRF detection device further comprises a release agent placement tray 14, at least one portion of release agent 15 is provided on the release agent placement tray 14, the transfer assembly may add the release agent 15 into the crucible 3, the robot 7 may use a fixture to add the release agent 15 on the release agent placement tray 14 to the crucible 3 after the melter 4 heats and melts the powder sample into a liquid, and after a period of reheating, the liquid is poured into the fuse die 5 to obtain the glass fuse 20. In addition, the release agent 15 for some powder samples can be added during the preparation of the powder samples, in which case the release agent 15 need not be added again to the liquefied sample.
In some embodiments, the automated XRF detection device further comprises a mold support 6 and a melt cooling disk 12, wherein a plurality of melt molds 5 may be placed on the melt cooling disk 12, the mold support 6 is used for carrying the melt molds 5, a transfer assembly may pour liquid melted by the sample melter 4 in the crucible 3 onto the melt molds 5, the transfer assembly may transfer the melt molds 5 to the melt cooling disk 12 for cooling, and the transfer assembly may further place empty melt molds 5 on the mold support 6 for next use. Wherein a camera can be arranged above the fuse piece cooling disc 12, the quality of the glass fuse piece 20 is detected by using machine vision, and the remelting or scrapping treatment is carried out on the inferior glass fuse piece 20.
In some embodiments, the automated XRF detection device further comprises a glass fuse placing tray 13, the transfer assembly may transfer glass fuses 20 on the fuse cooling tray 12 to the glass fuse placing tray 13, and the glass fuse placing tray 13 may place a plurality of glass fuses 20 thereon, specifically, when the glass fuses 20 are cooled to a set temperature, the robot 7 operates the suction cup 91 to suck the glass fuses 20 and place the glass fuses 20 in the glass fuse placing tray 13 for storage, when the glass fuses 20 are not detected in the glass fuse placing tray 13, the robot 7 operates the suction cup 91 to place the glass fuses 20 which are not detected in the XRF detection device 17 for detection, and after detection, the glass fuses 20 are placed back in the glass fuse placing tray 13.
In some embodiments, the automated XRF detection device further comprises a frame 1 for carrying the powder sample placement tray 2, the fusion machine 4 and the transfer assembly, and the powder sample placement tray 2, the fusion machine 4 and the transfer assembly are assembled on the same frame 1, so that the integration level of the detection device can be improved, and the structure of the frame 1 is not limited, and can be a plate-shaped structure or a frame structure. Wherein, the region corresponding to the XRF detection equipment 17 on the frame 1 is provided with a lofting port 11, the number of sampling ports can be a plurality of, the upper part of the detection cavity 18 of the XRF detection equipment 17 is provided with a cabin door 19 which can be opened and closed, and the cabin door 19 is opened when lofting and sampling are needed. In order to increase the working efficiency, the XRF detection apparatus 17 comprises a plurality of independent detection units, each of which is independently operable, and each of which is provided with a detection chamber 18 for placing a glass fuse 20, and a hatch 19 is provided above the detection chamber 18. In addition, the melting machine 4 can be provided with one or a plurality of melting machines, the melting machine 4 can be a high-frequency melting machine, a furnace end electric heating melting machine or gas heating equipment, in order to avoid the high-temperature influence of the melting machine 4, a shell and a melting door which can be opened and closed can be arranged at the periphery of the melting machine 4, and the melting door is opened only when the melting machine 4 is required to be taken and discharged so as to isolate the high temperature of the melting machine and avoid the influence on other structures in the equipment. The sample melting machine 4 is internally provided with a swinging mechanism, the extending end of the swinging mechanism is provided with a sample melting support 16, the crucible 3 can be placed on the sample melting support 16, a sample in the crucible 3 is sufficiently and evenly shaken through the swinging of the swinging mechanism in the sample melting process, after the sample melting is finished, the swinging mechanism swings to the maximum amplitude, so that liquid in the crucible 3 is poured into the fuse piece die 5, and the swinging mechanism returns to the horizontal state after the completion. The robot 7 then removes the fuse-element mold 5 and places it on the fuse-element cooling plate 12, and returns the empty crucible 3 to the fuse-element holder 16. The sample melting operation of the next sample can then be performed.
In order to ensure the safety of detection, a fence and a door can be arranged around the automatic XRF detection device, and in addition, the automatic XRF detection device can be provided with a computer, and the computer stores a plurality of sample melting methods and XRF detection methods so as to facilitate a user to select a proper sample melting method and XRF detection method according to the needs.
In summary, the operation flow of the automated XRF detection device for integrally preparing glass sheet samples provided by the embodiment of the invention is as follows:
1. the powder sample to be detected and the cosolvent are weighed and placed in a crucible 3, the crucible 3 is placed on a powder sample placing plate 2, the powder sample placing plate 2 is placed in a detection device, and the detection device is started.
2. The robot 7 operates the clamping jaw 8 to put the crucible 3 containing the powder sample into the melting sample support of the melting machine 4 according to a preset program, the melting machine 4 starts to work, after the melting machine 4 heats and melts the powder sample into liquid, the robot 7 uses the clamping jaw 8 to add the release agent 15 of the release agent placing disc 14 into the crucible 3, after reheating for a period of time, the liquid is poured into the fuse piece mould 5 of the mould support 6 to obtain the glass fuse piece 20, and the melting is completed.
3. The robot 7 returns the empty crucible 3 to the powder sample placement tray 2, takes out the fuse-element die 5, places the fuse-element die on the fuse-element cooling tray 12 for cooling, and then grabs the empty fuse-element die 5 from the fuse-element cooling tray 12 and places the fuse-element die into the die holder 6. After which the next sample is melted.
4. After the glass melt 20 in the melt cooling plate 12 is cooled to a set temperature, the robot 7 operates the suction cup 91 to suck the glass melt 20 in the mold and put the glass melt into the glass melt placing plate 13, so as to obtain the glass melt 20 which can be used for XRF detection.
5. When an undetected glass fuse 20 exists in the glass fuse placing tray 13, the robot 7 operates the suction cup 91 to place the undetected glass fuse 20 into the XRF detection apparatus 17 for detection, and after detection, the glass fuse 20 is placed back into the glass fuse placing tray 13.
6. The melter 4 and XRF detection device 17 are operated independently until all samples are melted and detected and the device is stopped. The user can obtain the detection results of all the samples. And the glass fuse piece 20 in the glass fuse piece placing tray 13 is taken out for sealing and storing, so that the subsequent detection is convenient.
In the present specification, each embodiment is described in a progressive manner, and each embodiment is mainly described in a different point from other embodiments, and identical and similar parts between the embodiments are all enough to refer to each other.
The invention provides an automated XRF detection device for integrated preparation of glass sheet samples. The principles and embodiments of the present invention have been described herein with reference to specific examples, the description of which is intended only to facilitate an understanding of the method of the present invention and its core ideas. It should be noted that it will be apparent to those skilled in the art that various modifications and adaptations of the invention can be made without departing from the principles of the invention and these modifications and adaptations are intended to be within the scope of the invention as defined in the following claims.
Claims (10)
1. An automated XRF detection device for integrated preparation of glass sheet samples, comprising:
the powder sample placing tray is provided with at least one crucible, and the crucible is used for containing powder samples;
the melting machine is used for heating and melting the powder sample in the crucible to form liquid;
the fuse piece die is used for forming glass fuse pieces from liquid obtained after melting the powder sample;
an XRF detection device for detecting the glass melt sheet;
a transfer assembly for moving the crucible into or out of the melter, or transporting the glass melt sheet into the XRF detection apparatus.
2. The automated XRF detection device of claim 1, wherein the transfer assembly comprises a robot, a jaw, and a suction cup assembly, the robot to grip the crucible or the fuse die with the jaw, the robot further to draw the glass fuse with the suction cup assembly.
3. The automated XRF detection device of claim 2, wherein the transfer assembly further comprises a chuck holder, the chuck assembly being attached to the robot, the chuck assembly being detached or attached to the chuck, the chuck holder for carrying the chuck assembly detached.
4. The automated XRF detection device of claim 3, wherein the jaw comprises a connector and a gripping end, wherein one end of the connector is connected to the end of the robot, the other end of the connector is connected to the gripping end, a suction cup retaining sleeve is provided on a side of the connector, and the suction cup assembly is configured to detachably connect to the suction cup retaining sleeve.
5. The automated XRF detection device of claim 1, further comprising a release agent placement tray having at least one portion of release agent disposed thereon, the transfer assembly configured to add the release agent to the crucible.
6. The automated XRF detection device of claim 1, further comprising a die holder for carrying the fuse die and a fuse cooling plate, the transfer assembly for transferring the fuse die to the fuse cooling plate for cooling.
7. The automated XRF detection device of claim 6, further comprising a glass melt sheet placement tray, the transfer assembly to transfer the glass melt sheet on the melt sheet cooling tray to the glass melt sheet placement tray.
8. The automated XRF detection device of claim 1, further comprising a frame for carrying the powder sample placement tray, the melter, and the transfer assembly.
9. The automated XRF detection device of claim 8, wherein a loft port is provided in an area of the frame corresponding to the XRF detection apparatus.
10. The automated XRF detection device of claim 9, wherein the XRF detection apparatus comprises a door that is openable and closable above the detection chamber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311683834.2A CN117665029A (en) | 2023-12-08 | 2023-12-08 | Automatic XRF detection device for integrated preparation of glass fuse sample |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311683834.2A CN117665029A (en) | 2023-12-08 | 2023-12-08 | Automatic XRF detection device for integrated preparation of glass fuse sample |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN117665029A true CN117665029A (en) | 2024-03-08 |
Family
ID=90073088
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202311683834.2A Pending CN117665029A (en) | 2023-12-08 | 2023-12-08 | Automatic XRF detection device for integrated preparation of glass fuse sample |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN117665029A (en) |
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2023
- 2023-12-08 CN CN202311683834.2A patent/CN117665029A/en active Pending
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