CN117665022A - Switchable monochromator system for neutron diffraction stress texture analysis - Google Patents
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- 238000001683 neutron diffraction Methods 0.000 title claims abstract description 28
- 238000004458 analytical method Methods 0.000 title claims abstract description 19
- 238000006073 displacement reaction Methods 0.000 claims abstract description 83
- 230000033001 locomotion Effects 0.000 claims abstract description 15
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 11
- 229910002804 graphite Inorganic materials 0.000 claims description 11
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- 229910021421 monocrystalline silicon Inorganic materials 0.000 claims description 10
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- 238000002474 experimental method Methods 0.000 claims description 5
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- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
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- 238000001956 neutron scattering Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
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- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/20—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
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Abstract
Description
技术领域Technical field
本发明涉及中子散射技术,具体地,涉及一种用于中子衍射应力织构分析的可切换单色器系统。The present invention relates to neutron scattering technology, and in particular, to a switchable monochromator system for neutron diffraction stress texture analysis.
背景技术Background technique
中子衍射技术是无损分析晶体材料内部的应力和织构的方法之一。不同的材料对中子衍射谱仪的分辨率和样品处中子通量的要求不同。例如,镍基高温合金、锆合金等金属材料要求谱仪具有较高的分辨率,而陶瓷、岩土等材料要求样品处具有较高的中子通量。Neutron diffraction technology is one of the methods to non-destructively analyze the stress and texture inside crystal materials. Different materials have different requirements for the resolution of the neutron diffraction spectrometer and the neutron flux at the sample. For example, metal materials such as nickel-based high-temperature alloys and zirconium alloys require high resolution spectrometers, while materials such as ceramics and geotechnical materials require high neutron flux at the sample.
现有公开号为CN102253405B的中国专利,其公开了一种多轴中子单色器姿态调整装置。该调整装置包括机械台体以及通过电缆与机械台体相连接的控制系统,其中,所述的机械台体包括设置在底盘上的旋转台,旋转台上设有平移调节器,在平移调节器上方设有倾斜调节器,倾斜调节器上设置单色器转位转台,机械台体的各运动机构带动单色器进行多自由度的位置组合调节;所述的控制系统包括设有控制软件的工控计算机以及通过驱动器对步进电机实现控制的电机控制单元。该装置可调节单个中子单色器水平、垂直、倾斜以及旋转的姿态,但不适用于两个及以上的单色器在较小空间内的切换。There is an existing Chinese patent with publication number CN102253405B, which discloses a multi-axis neutron monochromator attitude adjustment device. The adjustment device includes a mechanical platform body and a control system connected to the mechanical platform body through cables. The mechanical platform body includes a rotating platform arranged on the chassis. The rotating platform is provided with a translation regulator. On the translation regulator There is a tilt adjuster above, and a monochromator indexing turntable is set on the tilt adjuster. Each motion mechanism of the mechanical table body drives the monochromator to perform position combination adjustment with multiple degrees of freedom; the control system includes a control software equipped with Industrial control computer and motor control unit that controls the stepper motor through the driver. This device can adjust the horizontal, vertical, tilt and rotation posture of a single neutron monochromator, but is not suitable for switching two or more monochromators in a small space.
大部分基于反应堆中子源的中子衍射谱仪仅配备一个单色器,在一台中子衍射谱仪上配置两个不同类型的单色器,可以满足更多材料的测试需求,降低谱仪研制成本。德国柏林中子散射中心E3谱仪采用旋转换位的方式切换使用三个不同的单色器,慕尼黑中子散射中心STRESS-SPEC谱仪采用上下移动的方式切换单色器,但是这类单色器切换方式需要较大的空间,目前没有公开报道实现相关功能的具体技术细节。Most neutron diffraction spectrometers based on reactor neutron sources are equipped with only one monochromator. Configuring two different types of monochromators on one neutron diffraction spectrometer can meet the testing needs of more materials and reduce the cost of the spectrometer. Development costs. The E3 spectrometer at the Neutron Scattering Center in Berlin, Germany uses a rotational transposition method to switch between three different monochromators. The STRESS-SPEC spectrometer at the Munich Neutron Scattering Center uses an up and down movement method to switch monochromators. However, this type of monochromator The device switching method requires a large space, and there are currently no public reports on the specific technical details of implementing related functions.
因此,发明人认为需要提供一种用于中子衍射应力织构分析的可切换单色器系统,能够解决在较小屏蔽空间内进行单色器切换和高精度运动控制的问题。Therefore, the inventor believes that there is a need to provide a switchable monochromator system for neutron diffraction stress texture analysis, which can solve the problems of monochromator switching and high-precision motion control in a small shielding space.
发明内容Contents of the invention
针对现有技术中的缺陷,本发明的目的是提供一种用于中子衍射应力织构分析的可切换单色器系统。In view of the deficiencies in the prior art, the purpose of the present invention is to provide a switchable monochromator system for neutron diffraction stress texture analysis.
根据本发明提供的一种用于中子衍射应力织构分析的可切换单色器系统,包括:角度旋转台、角度倾斜台、水平位移台、第一单色器以及第二单色器,所述角度旋转台、所述角度倾斜台以及所述水平位移台自下而上依次设置,所述第一单色器和所述第二单色器分别安装在所述水平位移台上;所述第一单色器和所述第二单色器用于产生不同的单色中子束;所述水平位移台用于调节所述第一单色器和所述第二单色器的水平位移,使所述第一单色器或所述第二单色器面对白光中子束;所述角度倾斜台用于调节所述第一单色器或所述第二单色器的倾斜角,使所述单色中子束聚焦于样品测试区域的中心位置;所述角度旋转台用于调节所述第一单色器或所述第二单色器的旋转角度,调节所述第一单色器或所述第二单色器相对于白光中子束的起飞角。According to a switchable monochromator system for neutron diffraction stress texture analysis provided by the present invention, it includes: an angle rotation stage, an angle tilt stage, a horizontal displacement stage, a first monochromator and a second monochromator, The angle rotation stage, the angle tilt stage and the horizontal displacement stage are arranged in sequence from bottom to top, and the first monochromator and the second monochromator are respectively installed on the horizontal displacement stage; The first monochromator and the second monochromator are used to generate different monochromatic neutron beams; the horizontal displacement stage is used to adjust the horizontal displacement of the first monochromator and the second monochromator. , making the first monochromator or the second monochromator face the white light neutron beam; the angle tilting table is used to adjust the tilt angle of the first monochromator or the second monochromator , focusing the monochromatic neutron beam at the center of the sample test area; the angle rotation stage is used to adjust the rotation angle of the first monochromator or the second monochromator, adjusting the first The takeoff angle of the monochromator or said second monochromator relative to the white light neutron beam.
优选地,所述第一单色器为双聚焦完美单晶硅单色器,所述第一单色器的衍射晶面包括311、400,用于产生高分辨率的单色中子束;所述第二单色器为高定向热解石墨单色器,所述第二单色器的衍射晶面包括002、004,用于产生高通量的单色中子束。Preferably, the first monochromator is a double-focused perfect single crystal silicon monochromator, and the diffraction crystal planes of the first monochromator include 311 and 400, which are used to generate a high-resolution monochromatic neutron beam; The second monochromator is a highly directional pyrolytic graphite monochromator. The diffraction crystal planes of the second monochromator include 002 and 004, which are used to generate high-flux monochromatic neutron beams.
优选地,所述第一单色器和所述第二单色器的入射面垂直于水平面,所述第一单色器和所述第二单色器的入射面垂直中线垂直于所述水平位移台的中轴线;所述第一单色器的入射面水平中线平行于所述水平位移台的中轴线;所述第二单色器的入射面水平中线相交于所述水平位移台的中轴线。Preferably, the incident surface of the first monochromator and the second monochromator is perpendicular to the horizontal plane, and the vertical center line of the incident surface of the first monochromator and the second monochromator is perpendicular to the horizontal plane. The central axis of the displacement stage; the horizontal center line of the incident surface of the first monochromator is parallel to the central axis of the horizontal displacement stage; the horizontal center line of the incident surface of the second monochromator intersects with the center line of the horizontal displacement stage axis.
优选地,所述角度旋转台包括角度旋转台固定座和角度旋转台面,所述角度旋转台面安装在所述角度旋转台固定座上,且所述角度旋转台面能够相对于所述角度旋转台固定座做旋转运动;所述角度旋转台的转动范围为+/-180°,角度精度为±0.002°;所述角度旋转台固定座上设置有角度旋转限位开关位置,所述角度旋转限位开关位置为+/-60°。Preferably, the angle rotation table includes an angle rotation table fixed seat and an angle rotation table, the angle rotation table is installed on the angle rotation table fixed seat, and the angle rotation table can be fixed relative to the angle rotation table. The base performs rotational movement; the rotation range of the angle rotation table is +/-180°, and the angle accuracy is ±0.002°; the angle rotation limit switch position is provided on the fixed seat of the angle rotation table, and the angle rotation limit Switch position is +/-60°.
优选地,所述角度旋转台面的回转轴线平行于所述第一单色器和所述第二单色器的入射面垂直中线,所述角度旋转台面的回转轴线通过所述水平位移台的几何中心,所述角度旋转台面的回转轴线与所述水平位移台的中轴线垂直相交。Preferably, the rotation axis of the angle rotation table is parallel to the vertical center line of the incident surface of the first monochromator and the second monochromator, and the rotation axis of the angle rotation table passes through the geometry of the horizontal displacement stage. At the center, the rotation axis of the angle rotation table intersects perpendicularly with the central axis of the horizontal displacement stage.
优选地,所述角度倾斜台包括角度倾斜台固定座和角度倾斜台弧形台面,所述角度倾斜台弧形台面安装在所述角度倾斜台固定座上,所述角度倾斜台弧形台面能够沿所述角度倾斜台固定座上的角度倾斜台弧形轨道做摆动运动;所述角度倾斜台的转动范围为+/-10°,角度精度为±0.005°;所述角度倾斜台固定座上设置有角度倾斜限位开关位置,所述角度倾斜限位开关位置为+/-5°。Preferably, the angle tilt table includes an angle tilt table fixed base and an angle tilt table arc-shaped table. The angle tilt table arc-shaped table is installed on the angle tilt table fixed base, and the angle tilt table arc-shaped table can Swing motion along the arc-shaped track of the angle tilt table on the fixed seat of the angle tilt table; the rotation range of the angle tilt table is +/-10°, and the angle accuracy is ±0.005°; An angle tilt limit switch position is provided, and the angle tilt limit switch position is +/-5°.
优选地,所述角度倾斜台固定座安装在所述角度旋转台面上,所述角度旋转台面的回转轴线通过所述角度倾斜台弧形台面的几何中心。Preferably, the angle tilt table fixed seat is installed on the angle rotation table, and the rotation axis of the angle rotation table passes through the geometric center of the arc-shaped table of the angle tilt table.
优选地,所述水平位移台包括水平位移台固定座、单色器支撑滑块、梯形丝杠,所述梯形丝杠与所述单色器支撑滑块传动连接,所述单色器支撑滑块安装在所述水平位移台固定座上,且能够水平移动;所述水平位移台的位移范围为+/-249.25mm,定位精度为±0.0015mm;所述水平位移台固定座上设置有水平位移限位开关位置,所述水平位移限位开关位置为+/-240mm。Preferably, the horizontal displacement stage includes a horizontal displacement stage fixed seat, a monochromator support slider, and a trapezoidal screw. The trapezoidal screw is drivingly connected to the monochromator support slider. The monochromator support slider is The block is installed on the fixed base of the horizontal displacement stage and can move horizontally; the displacement range of the horizontal displacement stage is +/-249.25mm, and the positioning accuracy is ±0.0015mm; the fixed base of the horizontal displacement stage is provided with a horizontal Displacement limit switch position, the horizontal displacement limit switch position is +/-240mm.
优选地,所述第一单色器和所述第二单色器分别通过支撑件安装在所述单色器支撑滑块上,所述水平位移台固定座安装在所述角度倾斜台弧形台面上。Preferably, the first monochromator and the second monochromator are respectively installed on the monochromator support slider through supports, and the horizontal displacement stage fixed seat is installed on the arc-shaped angle tilt stage. On the countertop.
优选地,当不进行中子衍射实验时,所述第一单色器与所述第二单色器之间的间隙面对白光中子束。Preferably, when no neutron diffraction experiment is performed, the gap between the first monochromator and the second monochromator faces the white light neutron beam.
与现有技术相比,本发明具有如下的有益效果:Compared with the prior art, the present invention has the following beneficial effects:
本发明通过采用角度旋转、角度倾斜以及水平位移等多轴运动集成的结构以及高精度编码器,解决了在较小屏蔽空间内进行单色器切换和高精度运动控制的问题;通过采用水平位移台,即单色器支撑滑块在步进电机驱动下可沿水平位移台固定座101平移的结构,解决了双聚焦完美单晶硅单色器和高定向热解石墨单色器切换的问题;通过不同类型单色器的切换,实现高分辨率/高中子通量测量模式的切换以及空束状态的设置;通过高精度编码器可以确保双聚焦完美单晶硅单色器和高定向热解石墨单色器的垂直轴线与角度旋转台面的回转轴线的重合度在误差范围,保证单色器布拉格角的精度。The present invention solves the problem of monochromator switching and high-precision motion control in a small shielded space by using a multi-axis motion integrated structure such as angular rotation, angular tilt and horizontal displacement, and a high-precision encoder; by using horizontal displacement stage, that is, a structure in which the monochromator support slider can be translated along the horizontal displacement stage fixed seat 101 driven by a stepper motor, which solves the problem of switching between a dual-focus perfect single crystal silicon monochromator and a highly directional pyrolytic graphite monochromator. ; By switching different types of monochromators, the switching of high-resolution/high-medium neutron flux measurement modes and the setting of the empty beam state are achieved; the high-precision encoder can ensure perfect double focusing of single-crystal silicon monochromators and high directional heat The coincidence degree between the vertical axis of the graphite monochromator and the rotation axis of the angle rotation table is within the error range, ensuring the accuracy of the Bragg angle of the monochromator.
附图说明Description of drawings
通过阅读参照以下附图对非限制性实施例所作的详细描述,本发明的其它特征、目的和优点将会变得更明显:Other features, objects and advantages of the present invention will become more apparent by reading the detailed description of the non-limiting embodiments with reference to the following drawings:
图1为本发明主要体现用于中子衍射应力织构分析的可切换单色器系统的结构示意图;Figure 1 is a schematic structural diagram of a switchable monochromator system mainly used for neutron diffraction stress texture analysis according to the present invention;
图2为本发明主要体现角度旋转台的结构示意图;Figure 2 is a schematic structural diagram of the angle rotation table mainly embodying the present invention;
图3为本发明主要体现角度倾斜台的结构示意图;Figure 3 is a schematic structural diagram of an angle tilting table mainly embodying the present invention;
图4为本发明主要体现水平位移台的结构示意图;Figure 4 is a schematic structural diagram of the horizontal displacement stage mainly embodied in the present invention;
图5为本发明主要体现进行中子衍射实验的示意图;Figure 5 is a schematic diagram of the present invention mainly embodying the neutron diffraction experiment;
图6为本发明主要体现空束状态的示意图。Fig. 6 is a schematic diagram mainly showing the empty beam state of the present invention.
图中所示:Shown in the picture:
角度旋转台100 角度旋转台固定座101Angle rotary table 100 Angle rotary table fixed base 101
角度旋转台面102 角度倾斜台200Angle rotating table 102 Angle tilting table 200
角度倾斜台固定座201 角度倾斜台弧形轨道202Angle tilt table fixed base 201 Angle tilt table arc track 202
角度倾斜台弧形台面203 水平位移台300Angle tilt stage curved table 203 Horizontal displacement stage 300
水平位移台固定座301 单色器支撑滑块302Horizontal displacement stage fixed base 301 Monochromator support slider 302
梯形丝杠303 第一单色器400Trapezoidal screw 303 First monochromator 400
第二单色器500Second monochromator 500
具体实施方式Detailed ways
下面结合具体实施例对本发明进行详细说明。以下实施例将有助于本领域的技术人员进一步理解本发明,但不以任何形式限制本发明。应当指出的是,对本领域的普通技术人员来说,在不脱离本发明构思的前提下,还可以做出若干变化和改进。这些都属于本发明的保护范围。The present invention will be described in detail below with reference to specific embodiments. The following examples will help those skilled in the art to further understand the present invention, but do not limit the present invention in any form. It should be noted that, for those of ordinary skill in the art, several changes and improvements can be made without departing from the concept of the present invention. These all belong to the protection scope of the present invention.
如图1所示,根据本发明提供的一种用于中子衍射应力织构分析的可切换单色器系统,包括:角度旋转台100、角度倾斜台200、水平位移台300、第一单色器400以及第二单色器500,角度旋转台100、角度倾斜台200以及水平位移台300自下而上依次设置,第一单色器400和第二单色器500分别安装在水平位移台300上;第一单色器400和第二单色器500用于产生不同的单色中子束;水平位移台300用于调节第一单色器400和第二单色器500的水平位移,使调节第一单色器400或第二单色器500面对白光中子束;角度倾斜台200用于调节第一单色器400或第二单色器500的倾斜角,使单色中子束聚焦于样品测试区域的中心位置;角度旋转台100用于调节第一单色器400或第二单色器500的旋转角度,进而调节相对于白光中子束的起飞角,产生不同波长的单色中子束。As shown in Figure 1, a switchable monochromator system for neutron diffraction stress texture analysis provided according to the present invention includes: an angle rotation stage 100, an angle tilt stage 200, a horizontal displacement stage 300, a first monochromator The color detector 400 and the second monochromator 500, the angle rotation stage 100, the angle tilt stage 200 and the horizontal displacement stage 300 are arranged in sequence from bottom to top. The first monochromator 400 and the second monochromator 500 are respectively installed on the horizontal displacement stage. On the stage 300; the first monochromator 400 and the second monochromator 500 are used to generate different monochromatic neutron beams; the horizontal displacement stage 300 is used to adjust the level of the first monochromator 400 and the second monochromator 500. The displacement is adjusted so that the first monochromator 400 or the second monochromator 500 faces the white light neutron beam; the angle tilting stage 200 is used to adjust the tilt angle of the first monochromator 400 or the second monochromator 500 so that the monochromator 400 or the second monochromator 500 faces the white light neutron beam. The color neutron beam is focused on the center of the sample test area; the angle rotation stage 100 is used to adjust the rotation angle of the first monochromator 400 or the second monochromator 500, and then adjust the take-off angle relative to the white light neutron beam to generate Monochromatic neutron beams of different wavelengths.
单色器在中子衍射应力织构分析中用于产生单色中子束。不同的样品或工程部件对谱仪分辨率或样品处中子通量的要求有所不同,单色中子束对谱仪分辨率或样品处中子通量有关键影响。其设计要点为在有限的屏蔽空间内实现高分辨率或高中子通量测量模式及其切换,并同时保持角度旋转、角度倾斜以及平移的高精度。Monochromators are used to generate monochromatic neutron beams in neutron diffraction stress texture analysis. Different samples or engineering components have different requirements for spectrometer resolution or neutron flux at the sample. The monochromatic neutron beam has a key impact on the resolution of the spectrometer or the neutron flux at the sample. The key point of its design is to achieve high-resolution or high-medium neutron flux measurement modes and switching within a limited shielding space, while maintaining high accuracy in angular rotation, angular tilt, and translation.
由于角度倾斜台200设置于角度旋转台100以及水平位移台300设置于角度倾斜台200,角度旋转台100同时调节角度倾斜台200和水平位移台300的旋转角度,其主要目的是通过调节水平位移台100的旋转角度,进而调节第一单色器400或第二单色器500的旋转角度,即调节相对于白光中子束的起飞角,产生不同波长的单色中子束。Since the angle tilt stage 200 is provided on the angle rotation stage 100 and the horizontal displacement stage 300 is provided on the angle tilt stage 200, the angle rotation stage 100 simultaneously adjusts the rotation angles of the angle tilt stage 200 and the horizontal displacement stage 300, and its main purpose is to adjust the horizontal displacement. The rotation angle of the stage 100 is then adjusted to the rotation angle of the first monochromator 400 or the second monochromator 500, that is, the take-off angle relative to the white light neutron beam is adjusted to generate monochromatic neutron beams of different wavelengths.
第一单色器400为双聚焦完美单晶硅单色器,其所用衍射晶面为(311)和(400),用于产生高分辨率的单色中子束,实现高分辨率测量模式。第二单色器500为高定向热解石墨单色器,其所用衍射晶面为(002)和(004),用于产生高通量的单色中子束,实现高中子通量测量模式。The first monochromator 400 is a double-focused perfect single crystal silicon monochromator, which uses diffraction crystal planes (311) and (400) to generate high-resolution monochromatic neutron beams to achieve high-resolution measurement mode. . The second monochromator 500 is a highly directional pyrolytic graphite monochromator. The diffraction crystal planes used are (002) and (004). It is used to generate a high-flux monochromatic neutron beam to achieve high-medium neutron flux measurement mode. .
第一单色器400和第二单色器500的入射面垂直于水平面,第一单色器400和第二单色器500的入射面垂直中线垂直于水平位移台300的中轴线;第一单色器400的入射面水平中线平行于水平位移台300的中轴线;第二单色器500的入射面水平中线相交于水平位移台300的中轴线。The incident surface of the first monochromator 400 and the second monochromator 500 is perpendicular to the horizontal plane, and the vertical center line of the incident surface of the first monochromator 400 and the second monochromator 500 is perpendicular to the central axis of the horizontal displacement stage 300; first The horizontal center line of the incident surface of the monochromator 400 is parallel to the central axis of the horizontal displacement stage 300 ; the horizontal center line of the incident surface of the second monochromator 500 intersects with the central axis of the horizontal displacement stage 300 .
如图2所示,角度旋转台100设于基座上,角度旋转台100包括角度旋转台固定座101和角度旋转台面102,角度旋转台面102安装在角度旋转台固定座101上,且角度旋转台面102能够相对于角度旋转台固定座101做旋转运动。角度旋转台100的角度旋转台面102通过旋转机构与能够驱动该旋转台面的步进电机相连,步进电机传动轴一端装有编码器作为角度旋转台面102的角度读取器。角度旋转台100的转动范围为+/-180°,角度精度为±0.002°;角度旋转台固定座101上设置有角度旋转限位开关位置,角度旋转限位开关位置为+/-60°。可根据实际使用情况进行调节。As shown in Figure 2, the angle rotation table 100 is installed on the base. The angle rotation table 100 includes an angle rotation table fixed base 101 and an angle rotation table 102. The angle rotation table 102 is installed on the angle rotation table fixed base 101, and the angle rotation table 102 is installed on the angle rotation table fixed base 101. The table 102 can rotate relative to the angle rotation table fixed base 101 . The angle rotation table 102 of the angle rotation table 100 is connected to a stepper motor capable of driving the rotation table through a rotating mechanism. An encoder is installed on one end of the stepper motor transmission shaft as an angle reader of the angle rotation table 102 . The rotation range of the angle rotation table 100 is +/-180°, and the angle accuracy is ±0.002°; the angle rotation limit switch position is set on the fixed base 101 of the angle rotation table, and the angle rotation limit switch position is +/-60°. It can be adjusted according to actual usage.
角度旋转台面102的回转轴线平行于第一单色器400和第二单色器500的入射面垂直中线,角度旋转台面102的回转轴线通过水平位移台300的几何中心,角度旋转台面102的回转轴线与水平位移台300的中轴线垂直相交。The rotation axis of the angle rotation table 102 is parallel to the vertical center line of the incident surface of the first monochromator 400 and the second monochromator 500. The rotation axis of the angle rotation table 102 passes through the geometric center of the horizontal displacement stage 300. The rotation of the angle rotation table 102 The axis intersects perpendicularly with the central axis of the horizontal displacement stage 300 .
如图3所示,角度倾斜台200用于调节单色器400或单色器500的倾斜角,使单色中子束更加精准地聚焦于样品测试区域的中心位置。角度倾斜台200包括角度倾斜台固定座201和角度倾斜台弧形台面203,角度倾斜台弧形台面203安装在角度倾斜台固定座201上,角度倾斜台弧形台面203能够沿角度倾斜台固定座201上的角度倾斜台弧形轨道202做摆动运动。角度倾斜台200的角度倾斜台弧形台面203通过转动机构与能够驱动该弧形台面转动的步进电机相连,步进电机传动轴一端装有编码器作为弧形台面203的位置读取器角度倾斜台200的转动范围为+/-10°,角度精度为±0.005°;角度倾斜台固定座201上设置有角度倾斜限位开关位置,角度倾斜限位开关位置为+/-5°。可根据实际使用情况进行调节。As shown in Figure 3, the angle tilt stage 200 is used to adjust the tilt angle of the monochromator 400 or the monochromator 500 so that the monochromatic neutron beam can be more accurately focused on the center of the sample test area. The angle tilt table 200 includes an angle tilt table fixed base 201 and an angle tilt table arc table 203. The angle tilt table arc table 203 is installed on the angle tilt table fixed base 201. The angle tilt table arc table 203 can be fixed along the angle tilt table. The angle-inclined platform arc track 202 on the base 201 performs a swinging motion. The arc-shaped table 203 of the angle tilt table 200 is connected to a stepper motor that can drive the arc-shaped table to rotate through a rotating mechanism. An encoder is installed on one end of the stepper motor transmission shaft as the position reader angle of the arc-shaped table 203. The rotation range of the tilt table 200 is +/-10°, and the angle accuracy is ±0.005°; the angle tilt limit switch position is provided on the angle tilt table fixed base 201, and the angle tilt limit switch position is +/-5°. It can be adjusted according to actual usage.
角度倾斜台固定座201安装在角度旋转台面102上,角度旋转台面102的回转轴线通过角度倾斜台弧形台面203的几何中心。The angle tilt table fixed base 201 is installed on the angle rotation table 102, and the rotation axis of the angle rotation table 102 passes through the geometric center of the angle tilt table arc table 203.
如图4所示,水平位移台300用于调节单色器400和单色器500的水平位移,使双聚焦完美单晶硅单色器400或高定向热解石墨单色器500面对白光中子束,产生高分辨率或高中子通量的单色中子束,实现高分辨率或高中子通量测量模式及其切换。水平位移台300包括水平位移台固定座301、单色器支撑滑块302、梯形丝杠303,梯形丝杠303与单色器支撑滑块302传动连接,单色器支撑滑块302安装在水平位移台固定座301上,且能够水平移动。单色器支撑滑块302通过丝杆与能够驱动丝杆转动带动支撑滑块302平移的步进电机相连,丝杆一端装有编码器作为支撑滑块302的位置读取器。水平位移台300的位移范围为+/-249.25mm,定位精度为±0.0015mm;水平位移台固定座301上设置有水平位移限位开关位置,水平位移限位开关位置为+/-240mm。可根据实际使用情况进行调节。As shown in Figure 4, the horizontal displacement stage 300 is used to adjust the horizontal displacement of the monochromator 400 and the monochromator 500, so that the double-focused perfect single crystal silicon monochromator 400 or the highly directional pyrolytic graphite monochromator 500 faces white light. Neutron beam, generates a monochromatic neutron beam with high resolution or high neutron flux, and realizes high resolution or high neutron flux measurement mode and its switching. The horizontal displacement stage 300 includes a horizontal displacement stage fixed seat 301, a monochromator support slider 302, and a trapezoidal screw 303. The trapezoidal screw 303 is transmission connected with the monochromator support slider 302. The monochromator support slider 302 is installed horizontally. The displacement stage is fixed on the base 301 and can move horizontally. The monochromator support slider 302 is connected through a screw rod to a stepper motor that can drive the screw rod to rotate and drive the support slider 302 to translate. An encoder is installed at one end of the screw rod as a position reader for the support slider 302. The displacement range of the horizontal displacement stage 300 is +/-249.25mm, and the positioning accuracy is ±0.0015mm; the horizontal displacement limit switch position is provided on the fixed base 301 of the horizontal displacement stage, and the horizontal displacement limit switch position is +/-240mm. It can be adjusted according to actual usage.
第一单色器400和第二单色器500分别通过支撑件安装在单色器支撑滑块302上,水平位移台固定座301安装在角度倾斜台弧形台面203上。The first monochromator 400 and the second monochromator 500 are respectively installed on the monochromator support slider 302 through supports, and the horizontal displacement stage fixed seat 301 is installed on the arc-shaped table 203 of the angle tilt stage.
当不进行中子衍射实验时,第一单色器400与第二单色器500之间的间隙面对白光中子束,不影响白光中子束的传输。When the neutron diffraction experiment is not performed, the gap between the first monochromator 400 and the second monochromator 500 faces the white light neutron beam and does not affect the transmission of the white light neutron beam.
如图5和6所示,利用上述的可切换单色器系统可实现单色器切换,进而实现高分辨率/高中子通量测量模式的切换。将双聚焦完美单晶硅单色器切换至高定向热解石墨单色器或反之,包括如下步骤:As shown in Figures 5 and 6, the above-mentioned switchable monochromator system can be used to realize monochromator switching, thereby achieving switching of high-resolution/high-medium neutron flux measurement modes. Switching a dual-focus perfect monocrystalline silicon monochromator to a highly directional pyrolytic graphite monochromator or vice versa involves the following steps:
步骤1,运行角度旋转台100,调节角度旋转台面102的旋转角度,使水平位移台300垂直于白光中子束;在本实施例中,水平位移台300垂直于白光中子束时对应的角度旋转台面102的旋转角为0°;此步骤主要是因为直接切换会使单色器与其他机械发生碰撞,损坏单色器;Step 1. Run the angle rotation stage 100 and adjust the rotation angle of the angle rotation stage 102 so that the horizontal displacement stage 300 is perpendicular to the white light neutron beam; in this embodiment, the horizontal displacement stage 300 is at the corresponding angle when it is perpendicular to the white light neutron beam. The rotation angle of the rotating table 102 is 0°; this step is mainly because direct switching will cause the monochromator to collide with other machinery and damage the monochromator;
步骤2,运行水平位移台300,调节水平位移台300上的单色器支撑滑块302的位移,使双聚焦完美单晶硅单色器或高定向热解石墨单色器的几何中心与白光中子束的几何中心重合;若未进行中子衍射实验,使第一单色器400和第二单色器500间隙的中心与白光中子束的几何中心重合;此步骤为切换单色器或空束状态;Step 2, run the horizontal displacement stage 300, adjust the displacement of the monochromator support slider 302 on the horizontal displacement stage 300, so that the geometric center of the double-focused perfect single crystal silicon monochromator or the highly directional pyrolytic graphite monochromator is aligned with the white light. The geometric center of the neutron beam coincides; if no neutron diffraction experiment is performed, make the center of the gap between the first monochromator 400 and the second monochromator 500 coincide with the geometric center of the white light neutron beam; this step is to switch the monochromator or empty beam state;
步骤3,运行角度旋转台100,调节角度旋转台面102的旋转角度至设定值;需要注意的是,第一单色器400晶面取向为(400),使用衍射晶面(400)时,布拉格角为角度旋转台面102的旋转角度读数值;使用衍射晶面(311)时,布拉格角为角度旋转台面102的旋转角度加上25.245°;第二单色器500晶面取向为(002),入射面与水平位移台中轴线成夹角30°,使用衍射晶面(002)或(004)时,布拉格角为旋转角度读数值加上30°;根据布拉格定律2dsinθ=λ,可计算单色中子束的波长;Step 3: Run the angle rotation stage 100 and adjust the rotation angle of the angle rotation stage 102 to the set value; it should be noted that the crystal plane orientation of the first monochromator 400 is (400). When using the diffraction crystal plane (400), The Bragg angle is the rotation angle reading value of the angle rotation table 102; when using the diffraction crystal plane (311), the Bragg angle is the rotation angle of the angle rotation table 102 plus 25.245°; the crystal plane orientation of the second monochromator 500 is (002) , the angle between the incident surface and the central axis of the horizontal displacement stage is 30°. When using the diffraction crystal plane (002) or (004), the Bragg angle is the rotation angle reading value plus 30°; according to Bragg's law 2dsinθ=λ, the monochromatic color can be calculated The wavelength of the neutron beam;
步骤4,运行角度倾斜台200,调节角度倾斜台弧形台面203的倾斜角,使单色中子束聚焦于样品或工件的测试区域的中心;此步骤是为了减小实际测量区域与理论测量区域的误差,提高测试精度,同时提高测试区域的中子通量。Step 4, run the angle tilt stage 200, adjust the tilt angle of the arc-shaped table 203 of the angle tilt stage, so that the monochromatic neutron beam is focused on the center of the test area of the sample or workpiece; this step is to reduce the actual measurement area and theoretical measurement regional error, improve test accuracy, and at the same time increase the neutron flux in the test area.
本申请通过第一单色器400和第二单色器500设置于水平位移台300的单色器支撑滑块302上,通过平移位单色器支撑滑块302,可实现双聚焦完美单晶硅单色器400或高定向热解石墨单色器500单色白光中子束,进而实现高分辨率或高中子通量测量模式的切换。In this application, the first monochromator 400 and the second monochromator 500 are arranged on the monochromator support slider 302 of the horizontal displacement stage 300. By translating the monochromator support slider 302, dual-focus perfect single crystals can be achieved. Silicon monochromator 400 or highly directional pyrolytic graphite monochromator 500 monochromatic white light neutron beam, thereby achieving switching between high resolution or high neutron flux measurement modes.
本申请通过采用水平位移台300,即单色器支撑滑块302在步进电机驱动下可沿水平位移台固定座301平移的结构,解决了双聚焦完美单晶硅单色器和高定向热解石墨单色器切换的问题;通过不同类型单色器的切换,实现高分辨率/高中子通量测量模式的切换以及空束状态的设置。This application adopts a horizontal displacement stage 300, that is, a structure in which the monochromator support slider 302 can be translated along the horizontal displacement stage fixed seat 301 under the drive of a stepper motor, to solve the problem of dual-focus perfect single crystal silicon monochromator and highly directional thermal Solve the problem of graphite monochromator switching; by switching different types of monochromators, the switching of high-resolution/high-medium neutron flux measurement modes and the setting of the empty beam state are achieved.
本申请通过采用角度旋转、角度倾斜以及水平位移等多轴运动集成的结构以及高精度编码器,解决了在较小屏蔽空间内进行单色器切换和高精度运动控制的问题;通过高精度编码器可以确保双聚焦完美单晶硅单色器和高定向热解石墨单色器的垂直轴线与角度旋转台面102的回转轴线的重合度在误差范围,保证单色器布拉格角的精度。This application solves the problem of monochromator switching and high-precision motion control in a small shielded space by using a multi-axis motion integrated structure such as angular rotation, angular tilt, and horizontal displacement, as well as a high-precision encoder; through high-precision encoding The device can ensure that the coincidence degree between the vertical axis of the double-focused perfect single crystal silicon monochromator and the highly directional pyrolytic graphite monochromator and the rotation axis of the angle rotating table 102 is within the error range, ensuring the accuracy of the Bragg angle of the monochromator.
在本申请的描述中,需要理解的是,术语“上”、“下”、“前”、“后”、“左”、“右”、“竖直”、“水平”、“顶”、“底”、“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本申请和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本申请的限制。In the description of this application, it should be understood that the terms "upper", "lower", "front", "back", "left", "right", "vertical", "horizontal", "top", The orientations or positional relationships indicated by "bottom", "inner", "outer", etc. are based on the orientations or positional relationships shown in the drawings. They are only for the convenience of describing the present application and simplifying the description, rather than indicating or implying the device referred to. Or elements must have a specific orientation, be constructed and operate in a specific orientation and therefore are not to be construed as limitations on the application.
以上对本发明的具体实施例进行了描述。需要理解的是,本发明并不局限于上述特定实施方式,本领域技术人员可以在权利要求的范围内做出各种变化或修改,这并不影响本发明的实质内容。在不冲突的情况下,本申请的实施例和实施例中的特征可以任意相互组合。Specific embodiments of the present invention have been described above. It should be understood that the present invention is not limited to the specific embodiments described above. Those skilled in the art can make various changes or modifications within the scope of the claims, which does not affect the essence of the present invention. The embodiments of the present application and the features in the embodiments can be combined with each other arbitrarily without conflict.
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