CN117504676A - Emulsifying mixer and system without mechanical stirring - Google Patents

Emulsifying mixer and system without mechanical stirring Download PDF

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Publication number
CN117504676A
CN117504676A CN202311004459.4A CN202311004459A CN117504676A CN 117504676 A CN117504676 A CN 117504676A CN 202311004459 A CN202311004459 A CN 202311004459A CN 117504676 A CN117504676 A CN 117504676A
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CN
China
Prior art keywords
water phase
oil
emulsifying
pipe
fine
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CN202311004459.4A
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Chinese (zh)
Inventor
唐秀永
谭炜琦
陈斌
李明杰
熊晨
张凡华
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Hunan Jinshi Zhizao Technology Co ltd
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Hunan Jinshi Zhizao Technology Co ltd
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Priority to CN202311004459.4A priority Critical patent/CN117504676A/en
Publication of CN117504676A publication Critical patent/CN117504676A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/82Combinations of dissimilar mixers
    • B01F33/821Combinations of dissimilar mixers with consecutive receptacles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • B01F23/41Emulsifying

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)

Abstract

The invention discloses a non-mechanical stirring emulsifying mixer and a system, wherein the non-mechanical stirring emulsifying mixer comprises an oil-water phase primary mixing pipe, an emulsifying device connected with the oil-water phase primary mixing pipe and a sensitizer input pipeline connected with an outlet of the emulsifying device; the emulsifying device comprises an emulsifying container, a rough cutting mechanism and a fine cutting mechanism which are arranged in the emulsifying cavity, wherein the fine cutting mechanism is arranged outside the rough cutting mechanism at intervals, the oil-water phase mixed solution enters the rough cutting mechanism to be sprayed outwards to form rough milk, and the sprayed rough milk from the rough cutting mechanism passes through the fine cutting mechanism to be sheared again to form fine milk. According to the mechanical-stirring-free emulsifying mixer and system, the oil-water phase mixed solution is formed by mixing through the oil-water phase primary mixing pipe, then emulsification is carried out, coarse emulsion is formed through the coarse cutting mechanism, fine emulsion is formed through the fine cutting mechanism, the purpose of uniformly mixing and emulsifying the oil-water phase mixed solution is achieved, and the emulsifying effect is improved.

Description

Emulsifying mixer and system without mechanical stirring
Technical Field
The invention relates to the field of emulsion explosive production and preparation, in particular to a mechanical stirring-free emulsion mixer and a mechanical stirring-free emulsion mixer system.
Background
The emulsion explosive is a water-in-oil emulsion type water-resistant industrial explosive prepared by an emulsifying technology, and is a special water-in-oil emulsion system formed by taking fine droplets of an oxidant aqueous solution as a disperse phase and suspending the fine droplets in a continuous medium consisting of oil-like substances containing dispersed bubbles or hollow glass microspheres. At present, the main emulsification modes of the emulsification process in the production of the emulsion explosive in China are three types of medium-high rotation speed mechanical stirring type single-stage emulsification, medium-low rotation speed mechanical stirring combined emulsification and multi-stage pipeline type mixed emulsification. The emulsifier has the defects of high mechanical stirring speed, high energy consumption, small gap between a stator and a rotor, easy heat accumulation, easy explosion accident caused by metal friction during mechanical failure and incapability of meeting the requirement of safe production; the safety of the medium-low rotation speed mechanical stirring combined type emulsification is greatly improved compared with that of the medium-high rotation speed mechanical stirring single-stage emulsification, but the coarse emulsion is still mechanically stirred, the same as the single-stage emulsification process, has certain safety risk and high energy consumption, and meanwhile, the danger point is further increased by conveying the emulsion matrix between the coarse emulsion stirring process and the fine emulsion through a 0-class equipment screw pump, and the problems are brought into important attention of production enterprises and are expected to be further improved.
Thus, in order to improve the way of dynamic stirring, a mode of emulsification without mechanical stirring occurs. The stirring-free mixed emulsification process utilizes a multi-cavity pipeline mixer to carry out emulsification mixing, the water phase is sprayed into a cavity filled with an oil phase to carry out oil-water mixing and emulsification, the structure is complex, the emulsification parameters are difficult to accurately control, the emulsification degree is poor, the emulsification pressure is too high, and a plurality of defects exist in the process, so that the quality of the produced emulsion explosive product is unstable, and the emulsion explosive product cannot be popularized in a large range all the time.
In view of the above, it is necessary to provide a mechanically stirring-free emulsifying mixer and system for solving the above-mentioned drawbacks.
Disclosure of Invention
The invention mainly aims to provide a mechanical stirring-free emulsifying mixer and a mechanical stirring-free emulsifying system, and aims to solve the problems of low safety, complex structure and poor mixing and emulsifying effects of the traditional mechanical stirring.
The invention provides a mechanical stirring-free emulsifying mixer and a mechanical stirring-free emulsifying system, which comprise an oil-water phase primary mixing pipe for uniformly mixing oil phase and water phase which are pumped, an emulsifying device connected with the oil-water phase primary mixing pipe, and a sensitizer input pipeline connected with an outlet of the emulsifying device.
The emulsifying device comprises an emulsifying container with an emulsifying cavity, a rough cutting mechanism and a fine cutting mechanism, wherein the rough cutting mechanism and the fine cutting mechanism are arranged in the emulsifying cavity, a plurality of shearing holes are formed in the rough cutting mechanism and the fine cutting mechanism at intervals, the fine cutting mechanism is arranged outside the rough cutting mechanism in a surrounding mode, solution enters the rough cutting mechanism to be sprayed outwards to form rough milk, and under the action of spraying pressure, the rough milk sprayed from the rough cutting mechanism passes through the fine cutting mechanism to be sheared again to form fine milk.
Preferably, the rough cutting mechanism comprises a spray pipe and a spray head arranged at the tail end of the spray pipe.
The fine cutting mechanism comprises an upper fine cutting pipe, a lower fine cutting pipe and a cutting increasing barrel.
The emulsifying container includes a cylinder and an introduction section extending in an axial direction from an end of the cylinder.
The cutting barrel is axially arranged in the barrel, the spray pipe axially penetrates from the leading-in section and extends into the cutting barrel, the upper thin cutting pipe is axially sleeved at intervals at one end of the spray pipe positioned at the leading-in section, the lower thin cutting pipe is axially sleeved at intervals at one end of the spray pipe positioned in the cutting barrel, and the shearing holes are respectively formed in the spray pipe, the upper thin cutting pipe, the lower thin cutting pipe and the cutting barrel.
Preferably, the emulsifying device further comprises a fine cutting pipe, the emulsifying container further comprises an output section connected to the leading-in section, the fine cutting pipe is axially arranged in the output section, one end of the fine cutting pipe is connected to the fine cutting mechanism, and emulsion entering the output section is discharged after being sheared by the fine cutting pipe.
Preferably, the apertures of the shearing holes on the upper fine cutting pipe and the lower fine cutting pipe are smaller than the shearing holes on the spray pipe.
Preferably, the apertures of the shearing holes on the upper fine cutting pipe and the lower fine cutting pipe are smaller than the shearing holes on the spray pipe, and the aperture of the shearing hole of the last fine cutting pipe is smaller than the apertures of the shearing holes of the upper fine cutting pipe, the lower fine cutting pipe and the cutting barrel.
Preferably, the spray head is spherical, and a plurality of spray nozzles are annularly arranged on the spherical surface of the spray head.
Preferably, the shearing holes on the cutting drum surround the area close to the spray head.
Preferably, the spray pipe is a straight pipe body; the shearing holes are round holes.
Preferably, a space is formed between the inner side wall and the outer side wall of the emulsifying container at intervals, and the space is filled with heat preservation liquid or heat preservation steam.
A non-mechanical stirring emulsifying mixing system comprises a non-mechanical stirring emulsifying mixer, and further comprises a water phase circulation pipeline, an oil phase circulation pipeline, a water phase check valve and an oil phase check valve.
The water phase circulation pipeline comprises a water phase storage tank, a water phase ball valve I, a water phase coarse filter, a water phase pump, a water phase fine filter, a water phase transmitter, a water phase flowmeter and a water phase ball valve II which are sequentially connected through pipelines, and the water phase circulation pipeline is connected with the oil-water phase primary mixing pipe through a water phase check valve.
The oil phase circulation pipeline comprises an oil phase storage tank, an oil phase ball valve I, an oil phase coarse filter, an oil phase pump, an oil phase fine filter, an oil phase transmitter, an oil phase flowmeter and an oil phase ball valve II which are sequentially connected through pipelines, and the oil phase circulation pipeline is connected with the oil-water phase primary mixing pipe through the oil phase check valve.
Compared with the prior art, the emulsifying mixer and the emulsifying system without mechanical stirring have the following beneficial effects:
according to the mechanical stirring-free emulsifying mixer and system provided by the invention, the oil phase and the water phase are firstly mixed through the arranged oil-water phase primary mixing pipe to form the oil-water phase mixed solution, so that the oil-water phase mixed solution is mixed before entering the emulsifying device, the mixed solution enters the rough cutting mechanism and is sprayed out of the shearing holes on the rough cutting mechanism under the action of high pressure to form rough emulsion, and the rough emulsion continuously passes through the shearing holes of the fine cutting mechanism and is sprayed out of the shearing holes to form refined emulsion under the action of high pressure, so that a water-in-oil emulsion matrix is formed, and the oil-water phase mixed solution is cut by the shearing holes to break dispersed phase droplets into superfine droplets, so that the purpose of uniformly mixing the oil-water mixed solution is realized, and the emulsifying effect is further improved. The whole milk making process does not need a stirring device, and forms an emulsifying mode without mechanical stirring through spraying and shearing, so that the problem of safety accidents caused by stirring in the prior art is avoided, and the problem of poor emulsifying effect caused by the mode without mechanical stirring in the prior art is also avoided.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings that are required in the embodiments or the description of the prior art will be briefly described, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and other drawings may be obtained according to the structures shown in these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a cross-sectional view of an emulsifying mixer without mechanical agitation provided by the present invention;
FIG. 2 is a perspective view of the emulsifying mixer shown in FIG. 1 without mechanical agitation;
FIG. 3 is a schematic view of the emulsifying device shown in FIG. 1;
fig. 4 is an enlarged view of the structure of the portion a shown in fig. 1;
fig. 5 is a schematic structural diagram of the emulsifying and mixing system without mechanical stirring.
The achievement of the objects, functional features and advantages of the present invention will be further described with reference to the accompanying drawings, in conjunction with the embodiments.
Detailed Description
It should be understood that the specific embodiments described herein are for purposes of illustration only and are not intended to limit the scope of the invention.
The following description of the embodiments of the present invention will be made clearly and fully with reference to the accompanying drawings, in which it is evident that the embodiments described are only some, but not all embodiments of the invention. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
It should be noted that all directional indicators (such as up, down, left, right, front, and rear … …) in the embodiments of the present invention are merely used to explain the relative positional relationship, movement, etc. between the components in a particular posture (as shown in the drawings), and if the particular posture is changed, the directional indicator is changed accordingly.
Furthermore, the description of "first," "second," etc. in this disclosure is for descriptive purposes only and is not to be construed as indicating or implying a relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defining "a first" or "a second" may explicitly or implicitly include at least one such feature. In addition, the technical solutions of the embodiments may be combined with each other, but it is necessary to base that the technical solutions can be realized by those skilled in the art, and when the technical solutions are contradictory or cannot be realized, the combination of the technical solutions should be considered to be absent and not within the scope of protection claimed in the present invention.
Referring to fig. 1, the present invention provides a emulsifying mixer without mechanical stirring. The emulsifying mixer without mechanical stirring comprises an oil-water phase primary mixing pipe for uniformly mixing the pumped oil phase and water phase, an emulsifying device 100 connected with the oil-water phase primary mixing pipe, and a sensitizer input pipeline 200 connected with an outlet of the emulsifying device 100. The oil phase and the water phase are firstly conveyed into the oil-water phase primary mixing pipe to form an oil-water phase mixed solution, and then the mixed solution is pumped into the emulsifying device 100 for emulsification treatment. The sensitizer is added into the output pipeline of the emulsifying device 100 through a sensitizer input pipeline, and forms an emulsion explosive after being sensitized with the emulsified matrix which is emulsified successfully and is discharged from an explosive outlet.
Referring to fig. 1-4, the emulsifying device 100 includes an emulsifying container 30 having an emulsifying chamber, a rough cutting mechanism 40 and a fine cutting mechanism 50 mounted in the emulsifying chamber. The rough cutting mechanism 40 and the fine cutting mechanism 50 are provided with a plurality of shearing holes 60, the fine cutting mechanism 50 is surrounded outside the rough cutting mechanism 40 at intervals, the fine cutting mechanism is made to wrap the rough cutting mechanism 40, the mixed solution enters the rough cutting mechanism 40, the solution in the rough cutting mechanism 40 is sprayed outwards through the shearing holes 60, primary solution shearing and mixing are completed, rough milk is formed, and under the action of spraying pressure, the rough milk sprayed from the rough cutting mechanism 40 passes through the fine cutting mechanism 50 and is sheared and mixed again through the shearing holes 60, so that fine milk is formed. The oil phase and the water phase are firstly mixed through the arranged oil-water phase primary mixing pipe to form an oil-water phase mixed solution, the oil-water phase mixed solution is mixed before entering the emulsifying device 100, the mixed solution enters the rough cutting mechanism 40, under the action of high pressure, the mixed solution enters the rough cutting mechanism 40 and is sprayed out of the shearing holes 60 on the rough cutting mechanism to form rough emulsion, and under the action of high pressure, the rough emulsion passes through the shearing holes 60 of the fine cutting mechanism 50 and is sprayed out to form fine emulsion, the solution is sheared for a plurality of times to form a water-in-oil emulsion matrix, and the oil-water phase mixed solution is cut by the shearing holes 60 to break dispersed phase droplets into superfine droplets, so that the purpose of uniformly mixing the oil-water phase mixed solution is realized, and the emulsifying effect is improved. The whole milk making process does not need a stirring device, and a stirring-free emulsification mode is formed through spraying and shearing, so that the problem of safety accidents caused by stirring in the prior art is avoided, and the problem of poor stirring-free emulsification effect in the prior art is also avoided.
In the prior art, the stirring-free mixing is carried out by a multi-cavity mixer, specifically, the water phase is injected into a plurality of cavities filled with the oil phase at high pressure, in the mixing process, the water phase is injected into the mixing cavity by high pressure injection to realize oil-water phase mixing and emulsification, and the water phase is only mixed and introduced into the cavity filled with the oil phase, so that the disadvantage of the method is that the oil phase and the water phase are not fully mixed, the separation condition of the oil phase and the water phase is obvious, the granularity of the formed emulsion is large, and the emulsifying effect is poor.
Specifically, the rough cutting mechanism 40 includes a nozzle 41 and a nozzle 43 mounted at the end of the nozzle 41. The spray pipe 41 is a straight pipe body, and a plurality of shearing holes 60 are formed at the upper end and the lower end of the spray pipe 41, and the oil-water phase mixed solution enters from the spray pipe 41 and is sprayed out from the shearing holes 60 formed in the spray pipe. Of course, in other embodiments, the spout 41 may be configured in a curvilinear fashion, such as an S-shape or a fold line, etc., as desired.
The fine cutting mechanism 50 includes an upper fine cutting pipe 51, a lower fine cutting pipe 53, and a cutting increasing barrel 55. The upper and lower fine cut pipes 51 and 53 are matched with the shape of the nozzle 41, and are also straight pipes. The upper fine cutting pipe 51 and the lower fine cutting pipe 53 are integrally provided with a plurality of shearing holes 60, and the pipe diameters of the upper fine cutting pipe 51 and the lower fine cutting pipe 53 are larger than the pipe diameter of the spray pipe 41 so as to be sleeved outside the spray pipe 41. In order to ensure that the solution ejected from the nozzle 41 is discharged through the upper and lower fine cutting pipes 51 and 53, both ends of the upper and lower fine cutting pipes 51 and 53 are provided in a sealed state so that the solution can be ejected only from the opened shearing holes. Moreover, the fine cutting pipes are arranged up and down, so that the solution can be sheared and mixed through a plurality of positions, and the working efficiency is improved.
Referring to fig. 2, the emulsifying container 30 includes a cylindrical body 31 having a hollow interior, and an introduction section 33 extending from the top of the body 31 along the axial direction thereof, wherein the introduction section 33 is connected to a pipe connecting the oil-water primary mixing pipe through a flange 36, and the oil-water mixed solution fed from the oil-water primary mixing pipe enters the spray pipe 41 from the end of the introduction section 33.
As shown in fig. 1, the cutting barrel 55 is axially mounted in the barrel 31, the nozzle 41 axially penetrates from the introduction section 33 and extends into the cutting barrel 55, the upper fine cutting pipe 51 is axially and alternately sleeved at one end of the nozzle 41 located in the introduction section 33, the lower fine cutting pipe 53 is axially and alternately sleeved at one end of the nozzle 41 located in the cutting barrel 55, and the shearing holes 60 are respectively formed in the nozzle 41, the upper fine cutting pipe 51, the lower fine cutting pipe 53 and the cutting barrel 55. A liquid spraying cavity 52 is formed between the upper fine cutting pipe 51 and the inner side wall of the leading-in section 33, a liquid spraying cavity 54 is also formed between the increasing and cutting barrel 55 and the barrel 31, and the inner side wall of the leading-in section 33 extends to the top of the increasing and cutting barrel 55. As shown in fig. 3, a through hole 331 with a larger aperture is formed at an end of the inner side wall of the introducing section 33 connected to the cutting barrel 55, the inside of the cylinder 31 is communicated with the introducing section 33 through the through hole 331, and under the action of pressure, the emulsion in the inside of the cylinder 31 and the inside of the introducing section 33 are converged to an output pipeline to form a flow passage. It will be appreciated that the oil-water mixture enters the nozzle 41 under high pressure such that the solution entering the nozzle 41 is ejected under pressure towards the shear holes 60 to form coarse emulsion. A part of the coarse emulsion at the upper end is sheared again by the upper fine cutting pipe 51 under the action of pressure to form fine emulsion, another part of the mixed solution entering the spray pipe 41 from the introducing section 33 flows into the lower end of the spray pipe 41, a part of the mixed solution is sheared again by the lower fine cutting pipe 53 and then sprayed into the increasing and cutting barrel 55, and another part of the mixed solution is sprayed into the increasing and cutting barrel 55 by the spray nozzle 43, and all the emulsion in the increasing and cutting barrel 55 is sprayed onto the inner wall of the barrel 31 through the shearing holes 60 on the increasing and cutting barrel 55 under the action of pressure, so that layer percolation is generated along the inner wall. In this way, the emulsion sprayed after being sheared by the spray pipe 41 is sheared and uniformly mixed by the upper fine cutting pipe 51, the lower fine cutting pipe 53 and the cutting increasing barrel 55, and is crushed to form emulsion drops with small particles, so that the emulsion is fully and uniformly mixed, and the water-in-oil emulsion matrix particles are formed.
Wherein, the apertures of the shearing holes 60 on the upper and lower fine cutting pipes 51 and 53 are smaller than the shearing holes 60 on the spray pipe 41, so that the shearing of the spray pipe 41 forms coarse emulsion, and the emulsion particles sprayed from the upper and lower fine cutting pipes 51 and 53 are smaller to form fine emulsion, thereby achieving the purpose of uniform mixing. Specifically, in this embodiment, the shearing hole 60 is a circular hole, and in other embodiments, the shearing hole 60 may be a square hole, a diamond hole, or the like.
As shown in fig. 1, the emulsifying device 100 further comprises a fine cutting tube 70, the emulsifying container 30 further comprises an output section 35 connected to the introducing section 33, the fine cutting tube 70 is axially installed in the output section 35 and one end is connected to an upper fine cutting tube 51 of the fine cutting mechanism 50. The solution entering the output section 35 enters the fine cut pipe 70 to be sheared and discharged from the fine cut pipe 70, and the fine cut pipe 70 is sheared again to improve the mixing effect.
Further, the aperture of the shearing holes 60 of the last fine cutting pipe 70 is smaller than the apertures of the shearing holes 60 of the upper fine cutting pipe 51, the lower fine cutting pipe 53 and the cutting drum 55. The last fine cutting pipe 70 is used as a last fine cutting structure, and the solution finally collected into the output section 35 can be completely discharged from the shearing holes 60 of the last fine cutting pipe 70, so that a step of further fine cutting particles is added to the solution, even if the solution with larger particles exists in the previous step, all the cut and dispersed particles with uniform size can be obtained in the last fine cutting step of the last fine cutting pipe 70, and thus the uniform mixing effect is better.
The spray head 43 is positioned in the cutting barrel 55, the spray head 43 is spherical, and a plurality of spray nozzles 45 are annularly arranged on the spherical surface of the spray head 43. The spray nozzle 43 is connected to the spray pipe 41, and the emulsion is sprayed into the cutting-increasing barrel 55 through the spray nozzle 45, at this time, the emulsion in the cutting-increasing barrel 55 is driven by the spraying force of the spray nozzle 45 to turn the liquid in the barrel up and down, so that the spraying force forms stirring force, and the stirring force is fully collided and mixed with the liquid sprayed from the middle part of the spray pipe 41 to form water-in-oil emulsion matrix particles. Therefore, the spraying force of the nozzle 45 provides stirring force for the solution in the barrel, so that the stirring force is formed, the solution is more uniformly mixed, and the uniform mixing effect is better. No other stirring device is needed, and explosion caused by friction generated by the stirring device is avoided, so that the safety coefficient is greatly improved.
It will be appreciated that, in order to make the solution sprayed from the spray head 43 pass through the shearing holes 60 of the cutting-increasing barrel 55 to be finely cut after being turned up and down, the shearing holes 60 on the cutting-increasing barrel 55 are surrounded by the area close to the spray head 43, and the solution is discharged from the shearing holes 60 on the cutting-increasing barrel 55 during the turning process, so as to further improve the fine cutting efficiency of the cutting-increasing barrel 55.
As shown in fig. 1 and 4, the inner and outer walls of the emulsifying container 30 are spaced apart from each other to form a space, and the space is filled with a heat-insulating liquid or a heat-insulating vapor. Specifically, the heat-preserving liquid may be heat-preserving water, and the heat-preserving water or heat-preserving steam enters the emulsification container 30 to continuously provide temperature for the emulsion therein, so as to ensure the temperature condition required in the process of uniformly mixing the emulsion.
Referring to fig. 5, the invention further provides a system for emulsifying and mixing without mechanical stirring. The non-mechanical stirring emulsifying mixing system comprises the non-mechanical stirring emulsifying mixer, and further comprises a water phase circulation pipeline, an oil phase circulation pipeline, a water phase check valve and an oil phase check valve.
The water phase circulation pipeline comprises a water phase storage tank 1, a water phase ball valve I2, a water phase coarse filter 3, a water phase pump 4, a water phase fine filter 5, a water phase transmitter, a water phase flowmeter 8 and a water phase ball valve II 9 which are sequentially connected through pipelines, and the water phase circulation pipeline is connected with an oil-water phase primary mixing pipe 22 through a water phase check valve 10. The aqueous phase transmitter comprises an aqueous phase pressure transmitter 6 and an aqueous phase temperature transmitter 7.
The working process of the water phase circulation pipeline is that a water phase ball valve I2 is positioned at a water phase passage opening position (high-pressure air and steam are positioned at a closing position), a water phase ball valve II 9 is positioned at a circulation passage opening position (an emulsification passage is positioned at a closing position), a water phase pump 4 is started, a prepared water phase is pumped out of a water phase storage tank 1, and the water phase is returned to the water phase storage tank 1 after passing through the water phase ball valve I2, a water phase coarse filter 3, a water phase fine filter 5, a water phase pressure transmitter 6, a water phase temperature transmitter 7, a water phase flowmeter 8 and the water phase ball valve II 9, and when the water phase circulation flow reaches a set value, the water phase is ready for subsequent emulsification. Specifically, when the temperature of the water phase in the water phase storage tank 1 reaches 80-90 ℃, the water phase ball valve I2 is started to enable the water phase passage to be opened (high-pressure air and steam are in the closed position) and the water phase ball valve II 9 is started to enable the circulation passage to be in the open position (the emulsification passage is in the closed position), meanwhile, the water phase pump 4 is started to pump the prepared water phase out of the water phase storage tank 1, the prepared water phase is returned to the water phase storage tank 1 after passing through the water phase ball valve I2, the water phase coarse filter 3, the water phase fine filter 5, the water phase pressure transmitter 6, the water phase temperature transmitter 7, the water phase flowmeter 8 and the water phase ball valve II 9, and when the circulation flow of the water phase reaches a set value and flows stably and circulates for 1 minute, the water phase is conveyed to the oil-water phase primary mixing pipe, so that no stub bar is generated at the beginning of production, and the waste of materials is reduced.
The oil tank circulation pipeline comprises an oil phase storage tank 11, an oil phase ball valve I12, an oil phase coarse filter 13, an oil phase pump 14, an oil phase fine filter 15, an oil phase transmitter, an oil phase flowmeter 18 and an oil phase ball valve II 19 which are sequentially connected through pipelines, and the oil phase circulation pipeline is connected with an oil-water phase primary mixing pipe 22 through an oil phase check valve 20. The oil phase transmitter comprises an oil phase pressure transmitter and an oil phase temperature transmitter.
The working process of the oil phase circulation system is that the first oil phase ball valve 12 is opened, the second oil phase ball valve 19 is in an opened position (the emulsification passage is in a closed position), the oil phase pump 14 is started, the prepared oil phase is pumped out of the oil phase storage tank 11, and the oil phase is returned to the oil phase storage tank 11 after passing through the first oil phase ball valve 12, the oil phase coarse filter 13, the oil phase fine filter 15, the oil phase pressure transmitter 16, the oil phase temperature transmitter 17, the oil phase flowmeter 18 and the second oil phase ball valve 19, and when the oil phase circulation flow reaches a set value, the oil phase is ready for subsequent emulsification. Specifically, when the temperature of the oil phase in the oil phase storage tank 11 reaches 60-68 ℃, the oil phase ball valve 12 and the oil phase ball valve 19 are started to enable the circulation passage to be in an open position (the emulsification passage is in a closed position), meanwhile, the oil phase pump 14 is started to pump the prepared oil phase out of the oil phase storage tank 11, the oil phase is returned to the oil phase storage tank 11 after passing through the oil phase ball valve I12, the oil phase coarse filter 13, the oil phase fine filter 15, the oil phase pressure transmitter 16, the oil phase temperature transmitter 17, the oil phase flowmeter 18 and the oil phase ball valve II 19, and when the oil phase circulation flow reaches a set value and stably flows and circulates for 1 minute, the oil phase is ready for subsequent emulsification, and the oil phase is conveyed to the oil phase primary mixing pipe, so that a stub bar is not generated at the beginning of production, and the waste of materials is reduced.
The mechanical stirring-free emulsification mixing system works in the process that after oil and water phase circulation flow reach set values, an emulsification channel of a water phase ball valve II 9 is switched to an open position (the circulation channel is in an off position) and an emulsification channel of an oil phase ball valve II 19 is switched to an open position (the circulation channel is in an off position), a water phase and an oil phase are respectively driven by a water phase pump 4 and an oil phase pump 14 to push open a water phase check valve 10 and an oil phase check valve 20, the water phase and the oil phase are initially mixed in an oil-water phase primary mixing pipe 22 and then directly enter an emulsifying device 100 for emulsification, emulsion matrixes are formed after emulsification, an emulsion explosive is formed after the end of an output pipeline of the emulsifying device, to which the sensitizer is injected through an electric ball valve 24, is sensitized, and finally the emulsion explosive is discharged from an explosive outlet. It should be noted that the above process can also be used for on-site mixing without adding sensitizer, and the emulsion matrix can be directly discharged from the outlet, so that the emulsion matrix can be used for on-site mixing emulsion explosive loading vehicle.
The water phase circulation system also has a water phase flushing function, and the working process is that when the production is finished, the circulation passage of the water phase ball valve II 9 is switched to an open position (the emulsification passage is in an off position), the water phase ball valve I2 is in a high-pressure air and steam open position (the water phase passage is in an off position), the water phase pump 4 is continuously opened, and the water phase reserved in the water phase pipeline is blown out by the high-pressure air and steam through the water phase ball valve I2, the water phase coarse filter 3, the water phase pump 4, the water phase fine filter 5, the water phase flowmeter 8 and the water phase ball valve II 9 and then returned to the water phase storage tank 1, so that raw material tails are not produced.
When the production is finished, the water phase circulation pipeline and the oil phase circulation system are operated, the high-pressure air electric ball valve 21 is opened, residual oil and water phase materials in the emulsion sensitization system are blown out through high-pressure air, the oil and water phase materials are discharged after forming emulsion matrixes in the emulsifying device 100 under the condition that the air pump generates high-pressure air blowing, and no raw material tail is produced.
According to the mechanical stirring-free emulsification mixer and system, the oil phase and the water phase are mixed through the oil-water phase primary mixing pipe to form the oil-water phase mixed solution, so that oil-water phase mixing is completed before the mixed solution enters the emulsifying device, the mixed solution enters the rough cutting mechanism and is sprayed out of the shearing holes on the rough cutting mechanism to form rough emulsion under the action of high pressure, the rough emulsion continuously passes through the shearing holes of the fine cutting mechanism and is sprayed out to form refined emulsion under the action of high pressure, a water-in-oil emulsion matrix is formed, the oil-water phase mixed solution is cut by the shearing holes to break dispersed phase liquid drops into superfine liquid drops, a stirring device is not needed in the whole emulsification process, the problem of safety accidents caused by stirring in the prior art is avoided through spraying and shearing, and the problems of uneven mixing and poor emulsification effect are also avoided.
The foregoing description is only of the preferred embodiments of the present invention, and is not intended to limit the scope of the invention, but rather is intended to cover any equivalents of the structures or equivalent processes disclosed herein or in the alternative, which may be employed directly or indirectly in other related arts.

Claims (10)

1. The emulsifying mixer without mechanical stirring is characterized by comprising an oil-water phase primary mixing pipe for uniformly mixing the pumped oil phase and water phase, an emulsifying device connected with the oil-water phase primary mixing pipe, and a sensitizer input pipeline connected with an outlet of the emulsifying device;
the emulsifying device comprises an emulsifying container with an emulsifying cavity, a rough cutting mechanism and a fine cutting mechanism, wherein the rough cutting mechanism and the fine cutting mechanism are arranged in the emulsifying cavity, a plurality of shearing holes are formed in the rough cutting mechanism and the fine cutting mechanism at intervals, the fine cutting mechanism is arranged outside the rough cutting mechanism in a surrounding mode, oil-water phase mixed solution enters the rough cutting mechanism to be sprayed outwards to form rough emulsion, and under the action of spraying pressure, the rough emulsion sprayed from the rough cutting mechanism passes through the fine cutting mechanism to be sheared again to form fine emulsion.
2. The emulsifying mixer without mechanical agitation according to claim 1, wherein,
the rough cutting mechanism comprises a spray pipe and a spray head arranged at the tail end of the spray pipe;
the fine cutting mechanism comprises an upper fine cutting pipe, a lower fine cutting pipe and a cutting barrel;
the emulsifying container comprises a cylinder body and an introducing section extending from the end of the cylinder body along the axial direction;
the cutting barrel is axially arranged in the barrel, the spray pipe axially penetrates from the leading-in section and extends into the cutting barrel, the upper thin cutting pipe is axially sleeved at intervals at one end of the spray pipe positioned at the leading-in section, the lower thin cutting pipe is axially sleeved at intervals at one end of the spray pipe positioned in the cutting barrel, and the shearing holes are respectively formed in the spray pipe, the upper thin cutting pipe, the lower thin cutting pipe and the cutting barrel.
3. The mechanical agitation free emulsification mixer of claim 2 wherein the emulsification device further comprises a last fine cut tube, the emulsification vessel further comprises an output section connected to the introduction section, the last fine cut tube is axially mounted in the output section and one end is connected to the fine cut mechanism, and emulsion entering the output section is discharged after being sheared by the last fine cut tube.
4. The mechanical agitation free emulsification mixer of claim 2 wherein the apertures of the shear holes in the upper and lower fine cut pipes are smaller than the shear holes in the lance.
5. The mechanical agitation less emulsion mixer of claim 3 wherein the apertures of the shear holes in the upper and lower fine cut pipes are smaller than the shear holes in the jet pipe and the apertures of the shear holes in the non-fine cut pipe are smaller than the apertures of the shear holes in the upper fine cut pipe, the lower fine cut pipe and the booster barrel.
6. The emulsifying mixer without mechanical stirring according to claim 2, wherein the spray head is spherical, and a plurality of nozzles are arranged on the spherical surface of the spray head in a surrounding manner.
7. The mechanically stirring-free emulsion mixer of claim 2 wherein the shear holes in the cutting drum surround an area proximate the spray head.
8. The emulsifying mixer without mechanical agitation of claim 2 wherein the spout is a rectilinear tube; the shearing holes are round holes.
9. The emulsifying mixer without mechanical stirring according to claim 1, wherein a space is formed between the inner and outer side walls of the emulsifying container, and the space is filled with a heat-insulating liquid or a heat-insulating vapor.
10. A mechanical-agitation-free emulsion mixing system comprising the mechanical-agitation-free emulsion mixer as recited in any one of claims 1 to 9, further comprising an aqueous phase circulation line, an oil phase circulation line, an aqueous phase check valve, and an oil phase check valve;
the water phase circulation pipeline comprises a water phase storage tank, a water phase ball valve I, a water phase coarse filter, a water phase pump, a water phase fine filter, a water phase transmitter, a water phase flowmeter and a water phase ball valve II which are connected in sequence through pipelines, and is connected with the oil-water phase primary mixing pipe through the water phase check valve;
the oil phase circulation pipeline comprises an oil phase storage tank, an oil phase ball valve I, an oil phase coarse filter, an oil phase pump, an oil phase fine filter, an oil phase transmitter, an oil phase flowmeter and an oil phase ball valve II which are sequentially connected through pipelines, and the oil phase circulation pipeline is connected with the oil-water phase primary mixing pipe through the oil phase check valve.
CN202311004459.4A 2023-08-10 2023-08-10 Emulsifying mixer and system without mechanical stirring Pending CN117504676A (en)

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CN202311004459.4A CN117504676A (en) 2023-08-10 2023-08-10 Emulsifying mixer and system without mechanical stirring

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CN202311004459.4A CN117504676A (en) 2023-08-10 2023-08-10 Emulsifying mixer and system without mechanical stirring

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CN117504676A true CN117504676A (en) 2024-02-06

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118079718A (en) * 2024-04-18 2024-05-28 扬州伊朴斯生物科技有限公司 Emulsion product mixing device and mixing method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN118079718A (en) * 2024-04-18 2024-05-28 扬州伊朴斯生物科技有限公司 Emulsion product mixing device and mixing method thereof
CN118079718B (en) * 2024-04-18 2024-06-25 扬州伊朴斯生物科技有限公司 Emulsion product mixing device and mixing method thereof

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