CN117357439A - Washing and caring composition applied to fixation after dyeing and preparation method thereof - Google Patents
Washing and caring composition applied to fixation after dyeing and preparation method thereof Download PDFInfo
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- CN117357439A CN117357439A CN202311581421.3A CN202311581421A CN117357439A CN 117357439 A CN117357439 A CN 117357439A CN 202311581421 A CN202311581421 A CN 202311581421A CN 117357439 A CN117357439 A CN 117357439A
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- dyeing
- fixation
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- hair
- extract
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- 239000000203 mixture Substances 0.000 title claims abstract description 61
- 238000004043 dyeing Methods 0.000 title claims abstract description 45
- 238000005406 washing Methods 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000000284 extract Substances 0.000 claims abstract description 34
- 239000002383 tung oil Substances 0.000 claims abstract description 26
- 239000001140 aloe barbadensis leaf extract Substances 0.000 claims abstract description 25
- 229940069638 aloe vera leaf extract Drugs 0.000 claims abstract description 25
- 241000512259 Ascophyllum nodosum Species 0.000 claims abstract description 24
- -1 bacteriostat Substances 0.000 claims abstract description 15
- 239000003921 oil Substances 0.000 claims abstract description 14
- 235000019198 oils Nutrition 0.000 claims abstract description 14
- 235000020238 sunflower seed Nutrition 0.000 claims abstract description 14
- 239000003906 humectant Substances 0.000 claims abstract description 13
- 150000007524 organic acids Chemical class 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229920006322 acrylamide copolymer Polymers 0.000 claims abstract description 11
- 239000002280 amphoteric surfactant Substances 0.000 claims abstract description 11
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 11
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 11
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 11
- QYUMESOEHIJKHV-UHFFFAOYSA-M prop-2-enamide;trimethyl(propyl)azanium;chloride Chemical compound [Cl-].NC(=O)C=C.CCC[N+](C)(C)C QYUMESOEHIJKHV-UHFFFAOYSA-M 0.000 claims abstract description 11
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 7
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000002562 thickening agent Substances 0.000 claims abstract description 5
- 239000001069 triethyl citrate Substances 0.000 claims abstract description 5
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 claims abstract description 5
- 235000013769 triethyl citrate Nutrition 0.000 claims abstract description 5
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims abstract description 4
- 102000011782 Keratins Human genes 0.000 claims abstract description 4
- 108010076876 Keratins Proteins 0.000 claims abstract description 4
- 229940101267 panthenol Drugs 0.000 claims abstract description 4
- 235000020957 pantothenol Nutrition 0.000 claims abstract description 4
- 239000011619 pantothenol Substances 0.000 claims abstract description 4
- 239000001243 zingiber officinale rosc. root absolute Substances 0.000 claims abstract description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 34
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 18
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 18
- 239000011976 maleic acid Substances 0.000 claims description 18
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 18
- 235000011187 glycerol Nutrition 0.000 claims description 16
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 claims description 15
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 claims description 15
- 108010020346 Polyglutamic Acid Proteins 0.000 claims description 13
- 229920002643 polyglutamic acid Polymers 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 4
- 230000008569 process Effects 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 2
- 210000004209 hair Anatomy 0.000 abstract description 82
- 230000000694 effects Effects 0.000 abstract description 20
- 238000004140 cleaning Methods 0.000 abstract description 4
- 239000000126 substance Substances 0.000 description 22
- 210000004761 scalp Anatomy 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 14
- 239000002245 particle Substances 0.000 description 11
- 210000000434 stratum corneum Anatomy 0.000 description 10
- 235000015097 nutrients Nutrition 0.000 description 9
- 239000011241 protective layer Substances 0.000 description 6
- 239000010410 layer Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 244000144927 Aloe barbadensis Species 0.000 description 4
- 235000002961 Aloe barbadensis Nutrition 0.000 description 4
- 241001466453 Laminaria Species 0.000 description 4
- 235000011399 aloe vera Nutrition 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000008399 tap water Substances 0.000 description 3
- 235000020679 tap water Nutrition 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 239000004909 Moisturizer Substances 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical group [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 150000001450 anions Chemical class 0.000 description 2
- 239000003242 anti bacterial agent Substances 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 239000004359 castor oil Substances 0.000 description 2
- 235000019438 castor oil Nutrition 0.000 description 2
- 125000002091 cationic group Chemical group 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical group CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 description 2
- 229940073507 cocamidopropyl betaine Drugs 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 230000037308 hair color Effects 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 230000001333 moisturizer Effects 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical group OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 1
- VFKZECOCJCGZQK-UHFFFAOYSA-M 3-hydroxypropyl(trimethyl)azanium;chloride Chemical compound [Cl-].C[N+](C)(C)CCCO VFKZECOCJCGZQK-UHFFFAOYSA-M 0.000 description 1
- XPFCZYUVICHKDS-UHFFFAOYSA-N 3-methylbutane-1,3-diol Chemical compound CC(C)(O)CCO XPFCZYUVICHKDS-UHFFFAOYSA-N 0.000 description 1
- 244000303965 Cyamopsis psoralioides Species 0.000 description 1
- JDRSMPFHFNXQRB-CMTNHCDUSA-N Decyl beta-D-threo-hexopyranoside Chemical group CCCCCCCCCCO[C@@H]1O[C@H](CO)C(O)[C@H](O)C1O JDRSMPFHFNXQRB-CMTNHCDUSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 241000015177 Saccharina japonica Species 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000002981 blocking agent Substances 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 229940073499 decyl glucoside Drugs 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000000118 hair dye Substances 0.000 description 1
- 210000004919 hair shaft Anatomy 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical class OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920006254 polymer film Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229940057950 sodium laureth sulfate Drugs 0.000 description 1
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical group [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/004—Preparations used to protect coloured hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The application relates to the field of washing and caring products, in particular to a washing and caring composition for fixation after dyeing and a preparation method thereof. A cleaning and care composition for post-dyeing fixation comprising: anionic surfactant, amphoteric surfactant, nonionic surfactant, humectant, bacteriostat, essence, pH regulator, panthenol, ammonia-end polydimethylsiloxane, thickener, conditioner, hydrolyzed keratin, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, kelp extract, ginger root extract, aloe vera leaf extract, triethyl citrate, tung oil, unsaturated organic acid, sunflower seed oil and water. The color fixing method has the advantage of improving the color fixing effect on dyed hair.
Description
Technical Field
The application relates to the field of washing and caring products, in particular to a washing and caring composition for fixation after dyeing and a preparation method thereof.
Background
With the improvement of living standard, people pursue beauty more and more, and hair dyeing becomes a common hairdressing project. Hair dyes in the current market are mainly divided into three main categories according to dyeing mechanism and coloring durability: temporary, semi-permanent, and permanent. The temporary hair conditioner does not enter into the cortex layer and the cuticle of the hair, and can be washed out by shampoo and clean water. And both the semi-permanent type and the permanent type require that the hair scale is opened so that the dye and the color particles act on the cortex layer and the cuticle. Semi-permanent and permanent types may remain longer than temporary types.
However, the semi-permanent type and permanent type may excessively open the hair scales, resulting in that the color particles are very easily detached from the hair during hair washing, resulting in a non-lasting hair dyeing effect. It is therefore desirable to provide a color-fixing cleaning product.
Disclosure of Invention
In order to improve the fixation effect on dyed hair, the application provides a washing and protecting composition applied to fixation after dyeing and a preparation method thereof.
In a first aspect, the present application provides a cleaning and care composition for fixing color after dyeing, which adopts the following technical scheme:
the washing and caring composition for fixation after dyeing comprises the following components in percentage by mass: 10-20% of anionic surfactant, 1-5% of amphoteric surfactant, 1-5% of nonionic surfactant, 1-5% of humectant, 0-1% of bacteriostat, 0-1% of essence, 0-1% of pH regulator, 0-0.5% of panthenol, 0-1% of amino end polydimethylsiloxane, 0-1% of thickener, 0-1% of conditioner, 0-0.5% of hydrolyzed keratin, 0.1-2% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 0.05-2% of kelp extract, 0.05-2% of ginger root extract, 0.01-1% of aloe vera leaf extract, 0.1-5% of triethyl citrate, 0.1-3% of tung oil, 0.1-5% of unsaturated organic acid, 0.1-5% of sunflower seed oil and the balance of water is added to 100%.
The tung oil and the sunflower seed oil are unsaturated grease with the unsaturation degree not less than 2, and can be polymerized in situ under the action of heat and oxygen in the air with unsaturated organic acid to form a compact film, so that the aim of color protection is fulfilled. Compared with the traditional polymer film forming agent, the small-molecule unsaturated grease and the organic acid have strong permeability, can be absorbed by damaged hair after dyeing more quickly, and are filled into the hair and the surface to form a film, so that the hair is not easy to fall off.
The triethyl citrate can replace traditional carcinogenic phthalate esters in cosmetics, can be used as a plasticizer and a blocking agent, and can promote the film formation of the substances.
Further, by adopting the technical scheme, under the common cooperation of the kelp extract, the aloe vera leaf extract, the tung oil and the sunflower seed oil, the kelp extract is wrapped by the wadding glue during washing, so that nutrients such as hydrolyzed protein and the like are effectively deposited on the scalp and hair, and the scalp and hair are nourished. In addition, under the common combination of the wedge-based kelp extract, the aloe vera leaf extract and the tung oil, gel-like substances are generated, and the gel-like substances are also matched with the wadding glue and wrapped on the hair, so that the nutrient substances are favorably absorbed by the hair and the hair scales are smoothed. The gel-like substances also increase the viscosity of the composition, are easier to hang on the hair, enable the nutrient substances to nourish the hair for a longer time, and are beneficial to making the hair after dyeing more flexible.
Dyeing is achieved by opening the stratum corneum with an alkaline substance in the dye, and hydrogen peroxide in the oxidizing agent enters the hair shaft through the stratum corneum space. The alkaline substances sometimes excessively open the stratum corneum, which not only causes great damage to the scalp, but also causes the color particles to fail to stay firmly on the hair.
Under the co-cooperation of the kelp extract, the aloe vera leaf extract and the tung oil, the composition can be promoted to rapidly spread on the surface of the scalp, and the gel-like substance can be flexibly filled and spread into the opened stratum corneum, so that more nutrient substances can be promoted to nourish the scalp; meanwhile, the filling also plays a role in squeezing and fixing the color particles in the stratum corneum, so that the color particles are not easy to separate from the stratum corneum, and a good color fixing effect is achieved. After the composition is spread on the surfaces of scalp and hair wires, carboxyl groups on the surfaces of the kelp extract and the aloe vera leaf extract are bonded with hydrogen on the surfaces of hair, and a uniform, comprehensive and firm protective layer can be formed on the surfaces of the hair, so that color particles are further prevented from separating from horny layers, and the color fixation effect is enhanced.
Preferably, the mass percentage of the wedge-based kelp extract in the composition is 0.1-1%, the mass percentage of the aloe vera leaf extract in the composition is 0.05-0.3%, and the mass percentage of the tung oil in the composition is 1-2%.
By adopting the technical scheme, the blending amount of the wedge-based kelp extract, the aloe vera leaf extract and the tung oil is further limited, so that gel substances can be generated more quickly, and the gel substances uniformly spread and cover all the positions on the surfaces of the scalp and the hair wires, thereby playing better roles of protecting colors, fixing colors, nourishing the scalp and softening and beautifying hair.
Preferably, the mass percentage of the sunflower seed oil in the composition is 1-3%.
By adopting the technical scheme, the specific dosage of the sunflower seed oil, the wedge-based kelp extract, the aloe vera leaf extract and the tung oil is further limited, so that the effective precipitation of nutrient substances and gel-like substances on the scalp is promoted, and the hair is further fully cared.
Preferably, the mass ratio of the ammonia-terminal polydimethylsiloxane to the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer is 1: (0.8-1.2).
Along with the combined action of anions on the surface of the hair in the composition, electrostatic action can be generated between the anions and the composition, negative charges of the anionic surfactant can shield negative charges on the surface of the hair, so that the electrostatic repulsion effect is weakened, the composition is adsorbed on the hair, and the hair is cleaned more fully.
The cationic substances such as the amino-terminal polydimethylsiloxane and the acrylamide-propyl trimethyl ammonium chloride/acrylamide copolymer have a certain attraction effect with the anionic surfactant at the beginning and can be attached to the hair along with the reaction. Along with the dilution of the anionic surfactant in the hair washing process, the specially selected cationic substances can be deposited and formed on the surface of hair, so that the stability of a protective layer formed by the kelp extract, the aloe vera leaf extract and the tung oil can be further enhanced, and color particles are prevented from separating from the stratum corneum.
Furthermore, especially after hair is washed, the hair is dried by using an air duct or a clamping plate at 50-180 ℃, so that the speed of polymerization film forming can be increased, and the color protection effect is quickly achieved.
Preferably, the unsaturated organic acid at least comprises one of maleic acid and itaconic acid.
Preferably, the unsaturated organic acid is maleic acid or itaconic acid, and the mass ratio of the maleic acid to the itaconic acid is 1: (2-3) based on the mass of maleic acid.
By adopting the technical scheme, specific maleic acid and itaconic acid are selected, and the mixing proportion of the maleic acid and the itaconic acid is further limited. The maleic acid and the itaconic acid both contain carboxyl, and after being mixed with the kelp extract with wedge groups, the aloe vera leaf extract and the tung oil, the bonding effect between the composition and the hair can be effectively enhanced, the connection strength between the protective layer and the hair can be enhanced, the coverage is more comprehensive and lasting, and the color fixation and nourishing effects can be further improved.
Preferably, the humectant comprises at least one of glycerin and polyglutamic acid.
Preferably, the humectant is glycerin and polyglutamic acid, and the mass ratio of glycerin to polyglutamic acid is 1: (0.1-0.3) based on the mass of glycerin.
By adopting the technical scheme, the specific glycerin and polyglutamic acid are selected as the humectant, the mass ratio between the glycerin and the polyglutamic acid is further limited, the composition is endowed with good water solubility, and the hair is helped to absorb and retain moisture, so that the softness and glossiness of the hair are improved.
In a second aspect, the present application provides a method for preparing a color fixing washing and protecting composition applied to hair dyeing, which adopts the following technical scheme:
a method for preparing a color fixing washing and protecting composition applied to hair dyeing, comprising the following steps:
mixing anionic surfactant, 45-55% amphoteric surfactant and water, heating to 75-85deg.C, and stirring to uniformity;
cooling to 60-65deg.C, adding the rest amphoteric surfactant, nonionic surfactant, 60-90% humectant, pH regulator, and conditioner, and stirring to uniformity;
cooling to 40-45deg.C, adding the rest materials, and stirring to uniformity to obtain the final product.
In summary, the present application has the following beneficial effects:
1. under the common coordination of the kelp extract, the aloe vera leaf extract, the tung oil and the sunflower seed oil, nutrients such as hydrolyzed protein and the like can be promoted to be effectively deposited on scalp and hair, and the scalp and hair can be nourished. And gel-like substances are generated and further wrapped on the hair wires, so that the nutrient substances are promoted to be absorbed by the hair, the nutrient substances can nourish the hair for a longer time, and the dyed hair is more flexible.
2. Under the common cooperation of the kelp extract, the aloe vera leaf extract and the tung oil, the composition can be promoted to rapidly spread on the surface of the scalp, gel substances can be filled into the opened stratum corneum, and nutrient substances can be promoted to nourish the scalp; meanwhile, the color particles in the stratum corneum are extruded, so that the color particles are not easy to separate from the stratum corneum, and a good color fixing effect is achieved.
3. After the composition provided by the application is spread on the surfaces of scalp and hair wires, carboxyl groups on the surfaces of the kelp extract and the aloe vera leaf extract are bonded with hydrogen bonds on the surfaces of hair, and a uniform, comprehensive and firm protective layer can be formed on the surfaces of the hair, so that color particles are further prevented from separating from horny layers, and the color fixation effect is enhanced.
Detailed Description
The present application is described in further detail below with reference to examples.
The raw materials used in the following examples and comparative examples are all commercially available products.
Examples
Example 1
A washing and caring composition for fixation after hair dyeing comprises anionic surfactant, amphoteric surfactant, nonionic surfactant, humectant, antibacterial agent, essence, pH regulator, panthenol, ammonia-terminated polydimethylsiloxane, thickener, conditioner, hydrolyzed keratin, isoprene glycol, acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, herba Zosterae Marinae extract, rhizoma Zingiberis recens extract, aloe vera leaf extract, triethyl citrate, oleum Vera, unsaturated organic acid, sunflower seed oil, and water.
The specific amounts of the various raw materials are shown in Table 1.
The anionic surfactant is sodium laureth sulfate.
The amphoteric surfactant is cocamidopropyl betaine and sodium lauroyl amphoacetate.
The nonionic surfactant is decyl glucoside.
The humectant is glycerin and polyglutamic acid.
The antibacterial agent is phenoxyethanol and sodium benzoate.
The pH regulator is citric acid.
The thickener is sodium chloride.
The conditioner is guar hydroxypropyl trimethyl ammonium chloride and polyquaternium-10.
The unsaturated organic acid is maleic acid or itaconic acid.
The embodiment of the application also provides a preparation method of the washing and caring composition for fixation after dyeing, which comprises the following steps:
step 1): adding the anionic surfactant, cocamidopropyl betaine in the amphoteric surfactant and water into a reaction kettle, mixing, heating to 80 ℃, and starting to homogenize for 8min. Then stirring was started again until complete dissolution.
Step 2): cooling to 60 ℃, adding the rest amphoteric surfactant, nonionic surfactant, glycerin in humectant, pH regulator and conditioner into the material in the step 1), and stirring until uniform.
Step 3): cooling to 40 ℃, continuously adding the rest raw materials into the materials in the step 2), and stirring uniformly to obtain a finished product.
Example 2
A washing and caring composition for fixation after dyeing is different from example 1 in that,
the mass ratio of the ammonia-end polydimethylsiloxane to the acrylamide propyl trimethyl ammonium chloride to the acrylamide copolymer is 1:0.8.
The mass ratio of the maleic acid to the itaconic acid is 1:2.
The mass ratio of glycerin to polyglutamic acid is 1:0.1.
the specific amounts of the materials are shown in Table 1.
A process for the preparation of a care composition for fixation after dyeing of hair, which differs from example 1 in that: step 1) heating to 75 ℃.
Example 3
A washing and caring composition for fixation after dyeing is different from example 1 in that,
the mass ratio of the ammonia-end polydimethylsiloxane to the acrylamide propyl trimethyl ammonium chloride to the acrylamide copolymer is 1:1.2.
The mass ratio of the maleic acid to the itaconic acid is 1:3.
The mass ratio of glycerin to polyglutamic acid is 1:0.3.
the specific amounts of the materials are shown in Table 1.
A process for the preparation of a care composition for fixation after dyeing of hair, which differs from example 1 in that: step 1) is heated to 85 ℃, step 2) is cooled to 65 ℃, and step 3) is cooled to 45 ℃.
Example 4
A washing and caring composition for fixation after dyeing is different from example 1 in that the amount of the kelp extract with wedge group is 0.1kg, the amount of the aloe vera leaf extract with aloe vera is 0.01kg, the amount of tung oil is 0.1kg, and the amount of sunflower seed oil is 1kg.
Example 5
A washing and caring composition for fixation after dyeing is different from example 1 in that the kelp extract is 1kg, aloe vera leaf extract is 1kg, tung oil is 3kg, and sunflower seed oil is 3kg.
Example 6
A washing and caring composition for fixation after dyeing is different from example 1 in that the extract of Laminaria japonica is 0.05kg, the extract of aloe vera leaf is 0.01kg, tung oil is 1.99kg, and sunflower seed oil is 5kg.
Example 7
A washing and caring composition applied to fixation after dyeing is different from example 1 in that the mass ratio of the ammonia end polydimethylsiloxane to the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer is 1:10.
Example 8
The washing and caring composition applied to fixation after dyeing is different from example 1 in that the unsaturated organic acid is maleic acid, i.e., maleic acid is 3kg, itaconic acid is 0kg.
Example 9
A washing and caring composition applied to fixation after dyeing is different from example 1 in that the mass ratio of maleic acid to itaconic acid is 1:0.1, namely 2.7kg of maleic acid and 0.3kg of itaconic acid.
Example 10
The washing and caring composition applied to fixation after dyeing is different from the example 1 in that the mass ratio of glycerin to polyglutamic acid is 1:1, i.e. 1.25kg of glycerol and 1.25kg of polyglutamic acid.
Comparative example
Comparative example 1
A washing and caring composition for fixation after hair dyeing is different from example 1 in that the extract of Laminaria cuneata is replaced with extract of Aloe barbadensis leaf, i.e. 0, 0.55kg.
Comparative example 2
A washing and caring composition for fixation after hair dyeing is different from that of example 1 in that aloe vera leaf extract is replaced with Laminaria cuneata extract, i.e. 0.55kg of Laminaria cuneata extract and 0.
Comparative example 3
A washing and caring composition applied to fixation after dyeing is different from example 1 in that tung oil is replaced by castor oil, namely, the tung oil is 0, and the castor oil is 1.5kg.
Comparative example 4
A washing and caring composition for fixation after dyeing is different from example 1 in that the extract of Laminaria cuneata is 0.02kg, the extract of Aloe barbadensis leaf is 2kg, and tung oil is 0.03kg.
Performance test
1. Color fixation effect:
1) Detecting a sample: the compositions of examples 1 to 10 and comparative examples 1 to 4 were mixed with clear water to prepare a 5% (w/v) solution.
2) The detection method comprises the following steps: 42 identical flat wig bundles (15 cm 1.5cm 2.5g, bleaching treatment bundles) were randomly selected and randomly divided into 14 groups, each group corresponding to 3 bundles.
Each group of hair strands was stained with an equal amount of stain to reddish brown. After the dyeing treatment, the mixture was allowed to stand in an atmosphere of constant temperature and humidity (21 ℃ C., 55% RH) for 24 hours. After removal, each set of hair strands was tested using a colorimeter CL 400 and L was recorded 0 、a 0 、b 0 。
Each group of hair strands was then soaked in 50mL of the corresponding solution and washed in a water bath thermostatted shaker for 2min. Taking out, washing hair bundles with tap water, and drying the hair bundles.
The hair bundles were repeatedly washed 30 times, and then each group of hair bundles was tested using a colorimeter CL 400, recording L 1 、a 1 、b 1 。
The color difference deltae for each hair strand is calculated using the following disclosure.
The average of deltae for the hair tresses in the same group is shown as the result for this group and is reported in table 2.
2. Comb rationality:
1) Detecting a sample: the compositions of examples 1 to 10 and comparative examples 1 to 4 were mixed with clear water to prepare a 5% (w/v) solution.
2) The detection method comprises the following steps: 42 identical flat wig bundles (15 cm 1.5cm 2.5g, bleaching treatment bundles) were randomly selected and randomly divided into 14 groups, each group corresponding to 3 bundles.
Each group of hair strands was stained with an equal amount of stain to reddish brown. After the dyeing treatment, the mixture was allowed to stand in an atmosphere of constant temperature and humidity (21 ℃ C., 55% RH) for 24 hours.
Each group of hair strands was then soaked in 50mL of the corresponding solution and washed in a water bath thermostatted shaker for 2min. Taking out, washing hair bundles with tap water, and drying the hair bundles.
The hair tresses were repeatedly washed 10 times, and after the hair tresses were washed with tap water for the last time, combed once with a comb to remove excess moisture.
The tresses were then tested for wet combing using a tensile tester at a stretch rate of 300mm/min and the average wet combing work for each group of tresses was calculated as set forth in Table 2.
Then the hair is dried in air, after the drying, the wet combing property of the hair bundles is detected by using a tension tester, the stretching speed is 300mm/min, and the average dry combing power of each group of hair bundles is calculated as shown in Table 2.
TABLE 2
As can be seen from comparison of the test data of example 1 and comparative examples 1-3 in Table 2, the color difference of the obtained composition in the test of the fixation effect was 8-10, which is much higher than that of example 1, after the special compounding of the kelp wedge-based extract, aloe vera leaf extract, tung oil was destroyed. The composition of example 1 demonstrated good fixation to dyed hair and maintained good dyeing after repeated cleaning. Moreover, example 1 was also tested for dry combing and wet combing properties significantly better than comparative examples 1-3, and the product of example 1 was used to clean hair and exhibited better softness. The hair color fixing agent has the advantages that under the special combination of the wedge-based kelp extract, the aloe vera leaf extract and the tung oil, a layer of protective film can be formed on the hair, the hair scales are filled, the color particles are fixed, and the scalp is nourished, so that the hair color fixing agent has good color fixing and hair nourishing effects.
As can be seen from comparison of the test data of comparative example 4 in Table 2, the color difference of comparative example 4 is smaller than that of comparative examples 1 to 3, and the comb property is better than that of comparative examples 1 to 3; but is clearly less effective than example 1. The method has the advantages that the mixing of the wedge-based kelp extract, the aloe vera leaf extract and the tung oil is limited, and the dosage of the wedge-based kelp extract, the aloe vera leaf extract and the tung oil in a system is limited, so that the special mixing effect of all the substances can be fully exerted.
As can be seen from comparison of the test results of examples 1, 4 and 5 with that of example 6 in Table 2, the color fixing effect and the comb property of example 6 are slightly inferior to those of examples 1, 4 and 5. The color fixation and nourishing effects of the composition can be further improved by further limiting the special dosage of the wedge-based kelp extract, the aloe vera leaf extract, the tung oil and the sunflower seed oil.
From comparison of the test data of example 1 and example 7 in table 2, it is known that further limiting the mass ratio between the ammonia-terminal polydimethylsiloxane and the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer can further improve the stability of the protective layer, thereby exhibiting better fixation effect.
As can be seen from comparison of the test data of examples 1 and 8-9 in Table 2, the types and proportions of the unsaturated organic acids are limited to a specific range, which is beneficial to enhancing the connection strength between the protective layer and the hair, thereby showing good fixation and nourishing effects.
From comparison of the test data of example 1 and example 10 in table 2, it is understood that the use of specific moisturizers and the limitation of the mass ratio of the compounding between the specific moisturizers can further improve the combing property of hair.
The present embodiment is merely illustrative of the present application and is not intended to be limiting, and those skilled in the art, after having read the present specification, may make modifications to the present embodiment without creative contribution as required, but is protected by patent laws within the scope of the claims of the present application.
Claims (9)
1. The washing and caring composition for fixation after dyeing is characterized by comprising the following components in percentage by mass: 10-20% of anionic surfactant, 1-5% of amphoteric surfactant, 1-5% of nonionic surfactant, 1-5% of humectant, 0-1% of bacteriostat, 0-1% of essence, 0-1% of pH regulator, 0-0.5% of panthenol, 0-1% of amino end polydimethylsiloxane, 0-1% of thickener, 0-1% of conditioner, 0-0.5% of hydrolyzed keratin, 0.1-2% of acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer, 0.05-2% of kelp extract, 0.05-2% of ginger root extract, 0.01-1% of aloe vera leaf extract, 0.1-5% of triethyl citrate, 0.1-3% of tung oil, 0.1-5% of unsaturated organic acid, 0.1-5% of sunflower seed oil and the balance of water is added to 100%.
2. A care composition for post-dyeing fixation as claimed in claim 1, wherein: the mass percentage of the wedge-based kelp extract in the composition is 0.1-1%, the mass percentage of the aloe vera leaf extract in the composition is 0.05-0.3%, and the mass percentage of the tung oil in the composition is 1-2%.
3. A care composition for post-dyeing fixation as claimed in claim 1, wherein: the mass percentage of the sunflower seed oil in the composition is 1-3%.
4. A care composition for post-dyeing fixation as claimed in claim 1, wherein: the mass ratio of the ammonia-terminal polydimethylsiloxane to the acrylamide propyl trimethyl ammonium chloride/acrylamide copolymer is 1: (0.8-1.2).
5. A care composition for post-dyeing fixation as claimed in claim 1, wherein: the unsaturated organic acid at least comprises one of maleic acid and itaconic acid.
6. The composition for color fixation after dyeing according to claim 5, wherein: the unsaturated organic acid is maleic acid and itaconic acid, and the mass ratio of the maleic acid to the itaconic acid is 1: (2-3) based on the mass of maleic acid.
7. A care composition for post-dyeing fixation as claimed in claim 1, wherein: the humectant at least comprises one of glycerol and polyglutamic acid.
8. The care composition for post-dyeing fixation as claimed in claim 7, wherein: the humectant is glycerin and polyglutamic acid, and the mass ratio of the glycerin to the polyglutamic acid is 1: (0.1-0.3) based on the mass of glycerin.
9. A process for the preparation of a care composition for post-dyeing fixation based on any one of claims 1 to 8, comprising the steps of:
mixing anionic surfactant, 45-55% amphoteric surfactant and water, heating to 75-85deg.C, and stirring to uniformity;
cooling to 60-65deg.C, adding the rest amphoteric surfactant, nonionic surfactant, 60-90% humectant, pH regulator, and conditioner, and stirring to uniformity;
cooling to 40-45deg.C, adding the rest materials, and stirring to uniformity to obtain the final product.
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|---|---|---|---|---|
| CN104398441A (en) * | 2014-12-08 | 2015-03-11 | 上海海洋大学 | Seaweed pigment hair dye and application method thereof |
| CN113520947A (en) * | 2021-08-04 | 2021-10-22 | 广州葆妍生物科技有限公司 | Color-fixing hair-care composition and preparation and application thereof |
| CN115341399A (en) * | 2022-08-10 | 2022-11-15 | 绍兴市上虞丰达染整有限公司 | Printing and dyeing fixation auxiliary agent for low-temperature dyeing |
| CN116035984A (en) * | 2023-03-06 | 2023-05-02 | 苏州猫尔科技有限公司 | Composition with color locking and hair care functions and application thereof |
| CN116807910A (en) * | 2023-06-20 | 2023-09-29 | 章华化妆品科技有限公司 | Protein hair dyeing cream and preparation method thereof |
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- 2023-11-24 CN CN202311581421.3A patent/CN117357439B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104398441A (en) * | 2014-12-08 | 2015-03-11 | 上海海洋大学 | Seaweed pigment hair dye and application method thereof |
| CN113520947A (en) * | 2021-08-04 | 2021-10-22 | 广州葆妍生物科技有限公司 | Color-fixing hair-care composition and preparation and application thereof |
| CN115341399A (en) * | 2022-08-10 | 2022-11-15 | 绍兴市上虞丰达染整有限公司 | Printing and dyeing fixation auxiliary agent for low-temperature dyeing |
| CN116035984A (en) * | 2023-03-06 | 2023-05-02 | 苏州猫尔科技有限公司 | Composition with color locking and hair care functions and application thereof |
| CN116807910A (en) * | 2023-06-20 | 2023-09-29 | 章华化妆品科技有限公司 | Protein hair dyeing cream and preparation method thereof |
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