CN117074231B - Rapid detection method for solid content of wastewater slurry in green building construction - Google Patents
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- 239000002002 slurry Substances 0.000 title claims abstract description 172
- 239000002351 wastewater Substances 0.000 title claims abstract description 139
- 239000007787 solid Substances 0.000 title claims abstract description 82
- 238000001514 detection method Methods 0.000 title claims abstract description 34
- 238000009435 building construction Methods 0.000 title claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 58
- 238000000034 method Methods 0.000 claims abstract description 23
- 238000001035 drying Methods 0.000 claims description 23
- 239000000843 powder Substances 0.000 claims description 23
- 239000002994 raw material Substances 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 9
- 238000005303 weighing Methods 0.000 claims description 9
- 239000012153 distilled water Substances 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 4
- 241001081179 Litsea Species 0.000 claims description 3
- 235000012854 Litsea cubeba Nutrition 0.000 claims description 3
- 239000003350 kerosene Substances 0.000 claims description 3
- 238000004364 calculation method Methods 0.000 abstract description 12
- 238000004064 recycling Methods 0.000 abstract description 9
- 238000010276 construction Methods 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 238000010790 dilution Methods 0.000 abstract description 3
- 239000012895 dilution Substances 0.000 abstract description 3
- 238000013178 mathematical model Methods 0.000 abstract description 3
- 238000009825 accumulation Methods 0.000 abstract description 2
- 239000002699 waste material Substances 0.000 description 17
- 238000012360 testing method Methods 0.000 description 16
- 239000004568 cement Substances 0.000 description 7
- 238000001704 evaporation Methods 0.000 description 7
- 230000008020 evaporation Effects 0.000 description 7
- 239000000203 mixture Substances 0.000 description 6
- 239000004575 stone Substances 0.000 description 5
- 239000004576 sand Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 239000010802 sludge Substances 0.000 description 2
- 238000007619 statistical method Methods 0.000 description 2
- 230000001133 acceleration Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000003908 quality control method Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N5/00—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
- G01N5/02—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content
- G01N5/025—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content for determining moisture content
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/18—Water
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/24—Earth materials
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N9/00—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
- G01N9/02—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity by measuring weight of a known volume
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N9/00—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
- G01N9/36—Analysing materials by measuring the density or specific gravity, e.g. determining quantity of moisture
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N9/00—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity
- G01N9/02—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity by measuring weight of a known volume
- G01N2009/022—Investigating density or specific gravity of materials; Analysing materials by determining density or specific gravity by measuring weight of a known volume of solids
Abstract
The invention relates to the technical field of engineering construction, in particular to a rapid detection method for the solid content of wastewater slurry in green building construction. According to the invention, the solid content of the wastewater slurry is obtained by rapidly measuring the density and the air content of the wastewater slurry and combining the measured density and the measured internal water concentration of solid matters in the wastewater slurry through calculation of a mathematical model, and the solid content of the wastewater slurry can be rapidly monitored in real time, so that the doping amount and the dilution measure of the wastewater slurry during the recycling of the wastewater slurry are guided, the recycling efficiency of the wastewater slurry is improved, and the production efficiency and the quality of concrete are ensured. In addition, the invention greatly improves the accuracy of the solid content detection of the wastewater slurry by adding two influencing factors of the solid content internal water accumulation rate and the gas content of the wastewater slurry in the solid content detection process of the wastewater slurry.
Description
Technical Field
The invention relates to the technical field of engineering construction, in particular to a rapid detection method for the solid content of wastewater slurry in green building construction.
Background
In recent years, with the vigorous development of the building industry in China, more and more wastewater and slurry are generated in construction, such as scrapped cement slurry caused by pumping construction pipe-wetting mortar and blocking pump interruption in construction engineering, and considerable amount of unset concrete mixture waste is inevitably generated by ready-mixed concrete production enterprises every day due to test, production and other reasons. The common practice is to separate sand, stones and wastewater slurry from concrete mixture waste through a sand-stone separator, the separated sand and stones can be directly used for producing concrete, and the separated wastewater slurry is not recycled well.
At present, many enterprises do not have large-scale waste slurry recycling facility equipment, only use waste water for producing concrete through the sedimentation tank, but the waste slurry of sediment can not be recycled, once the storage capacity of the sedimentation tank is exceeded, the waste slurry can only be cleaned and excavated, and the waste slurry is transported away through a transport vehicle, even some bad illegal transport vehicles steal and discharge the waste slurry, and the environment is seriously polluted. The method can be used for recycling the wastewater slurry and producing concrete, but the solid content is an important control index, and has certain influence on the strength and the mixing performance of the concrete. Therefore, how to quickly determine the solid content of the waste cement slurry is significant for the recycling efficiency and the design and adjustment of the mixing ratio.
Through investigation, the solid content detection of the wastewater slurry is usually a drying method, which is time-consuming and is not beneficial to real-time rapid monitoring; in addition, solid matter particles in the wastewater slurry have cohesive property due to a certain micropore structure, and in addition, the traditional detection method only estimates the solid content of the wastewater slurry by measuring the density of the wastewater slurry, and the influence of the cohesive water content of the solid matter in the wastewater slurry and the gas content of the wastewater slurry on the density of the wastewater slurry is not considered, so that larger test deviation is easy to occur, and the control of the quality of concrete is not facilitated.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a rapid detection method for the solid content of wastewater slurry in green building construction. Compared with the existing detection method, the detection method provided by the invention can realize real-time and rapid detection of the solid content of the wastewater slurry; and the accuracy of the solid content detection of the wastewater slurry is improved by adding two influencing factors of the water content of solid substances in the wastewater slurry and the gas content of the wastewater slurry. In order to achieve the above purpose, the present invention provides the following technical solutions:
a rapid determination method for the solid content of wastewater slurry in green building construction comprises the following steps:
(1) From the waste water slurry to be measuredTaking a wastewater slurry sample from the raw materials, filtering and drying to constant weight to obtain wastewater slurry solid powder, and determining the density rho of the wastewater slurry solid powder Fixing device 。
(2) Taking a wastewater slurry sample from the wastewater slurry raw material to be tested used in the step (1), filtering, drying to constant weight to obtain wastewater slurry sample solid powder, and uniformly stirring and mixing the wastewater slurry sample solid powder and distilled water to obtain slurry; taking part of the slurry as a slurry sample for subsequent detection, and weighing the mass of the slurry sample to be m 0 The method comprises the steps of carrying out a first treatment on the surface of the Drying the slurry sample, weighing according to time steps, and respectively calculating time t i Water dispersion m of (2) wi Drying to constant weight, and weighing the solid powder mass m in the slurry sample Fixing device The method comprises the steps of carrying out a first treatment on the surface of the The water content of the slurry sample is calculated according to the mass ratio of the solid powder of the wastewater slurry sample and distilled water when the solid powder is stirred and mixed w The method comprises the steps of carrying out a first treatment on the surface of the Calculating water loss m by using a quadratic differential quotient wi For time t i The second derivative of (a) is delta 2 m wi /Δ 2 t i ,Δ 2 m wi /Δ 2 t i The water loss at this time point corresponding to zero is m w0 Namely, the critical point of surface moisture loss; find delta 2 m wi /Δ 2 t i Two adjacent time points when positive and negative changes occur, and delta is calculated by interpolation 2 m wi /Δ 2 t i Water loss m at time point corresponding to zero w0 The method comprises the steps of carrying out a first treatment on the surface of the The solid matter of the wastewater slurry contains cohesive water rate gamma Fixing device The calculation is carried out according to the following formula:
the influence factor of the solid matter water content rate is introduced in the calculation of the solid content of the wastewater slurry, so that the actual free water is corrected, and the accuracy of the solid content detection of the wastewater slurry is improved.
(3) From the wastewater slurry raw material to be tested used in the step (1)Taking a wastewater slurry sample, uniformly stirring, and measuring the gas content lambda of the wastewater slurry sample Air flow ;
When the composition of the wastewater slurry is unchanged, the larger the gas content of the wastewater slurry is, the smaller the density of the wastewater slurry is, and the influence factor of the gas content of the wastewater slurry is introduced in the calculation of the solid content of the wastewater slurry, so that the accuracy of the solid content detection of the wastewater slurry is improved.
(4) Taking a wastewater slurry sample from the wastewater slurry raw material to be detected used in the step (1), uniformly stirring, and measuring the density rho of the wastewater slurry sample Pulp 。
(5) The solid content omega of the waste water slurry raw material to be detected used in the step (1) Fixing device The results were accurate to 0.01% as calculated by the following formula.
Further, in step (1), the ρ is Fixing device The method is characterized by comprising the step of measuring solid powder of a wastewater slurry sample in a constant-temperature water bath by adopting anhydrous kerosene and a Litsea bottle.
Further, in step (3), the lambda Air flow The method is obtained by measuring the air content of the concrete by a concrete air content measuring instrument.
Further, in step (4), the ρ is Pulp Is measured by densitometer.
When the composition of the wastewater slurry is unchanged, the larger the gas content of the wastewater slurry is, the smaller the corresponding density of the wastewater slurry is, and the influence factor of the gas content of the wastewater slurry is introduced into the calculation formula of the solid content of the wastewater slurry, so that the accuracy of the solid content detection of the wastewater slurry is improved.
The invention calculates the water dispersion m by a quadratic differential quotient method according to the characteristic that the free water in the wastewater slurry and the water polymerized in the solid matters are different in evaporation rate along with time in a drying state because of the existence of a certain microporous structure in the solid matters particles in the wastewater slurry wi For time t i Is a second derivative of (a) 2 m wi /Δ 2 ti,Δ 2 m wi /Δ 2 t i When the water evaporation rate is zero, the acceleration of the water evaporation rate is zero, the water evaporation rate can be characterized as the water evaporation quantity m of the wastewater slurry at the corresponding time point when the wastewater slurry is converted into solid matters from free water evaporation to cohesive water evaporation w0 Can be approximated to the free water content in the wastewater slurry, thereby realizing the water cohesion rate gamma of the solid matters of the wastewater slurry Fixing device The accurate measurement is carried out; introducing the water content gamma of solid matters in the wastewater slurry into a calculation formula of the solid content of the wastewater slurry Fixing device The influence factor corrects the actual free water, and is helpful for improving the accuracy of the solid content detection of the wastewater slurry.
According to the invention, the density and the air content of the waste cement slurry to be detected are detected in real time, the density and the internal water accumulation rate of solid matters in the waste cement slurry are combined, the solid content of the waste cement slurry is calculated through a mathematical model, and the doping amount and the dilution measure of the waste cement slurry during recycling of the waste cement slurry are guided.
The beneficial effects of the invention are as follows:
1. according to the invention, the density and the air content of the wastewater slurry sample are rapidly measured, the solid content of the wastewater slurry is obtained by calculating through a mathematical model in combination with the density and the water content of solid substances in the wastewater slurry measured previously, the solid content of the wastewater slurry can be rapidly monitored in real time, the doping amount and the dilution measure of the wastewater slurry during the recycling of the wastewater slurry are guided, the recycling efficiency of the wastewater slurry is improved, and the production efficiency and the quality of concrete are ensured.
2. According to the invention, two influencing factors of the air content of the wastewater slurry and the water cohesion rate of solid substances are introduced into a calculation formula of the solid content of the wastewater slurry, so that the accuracy of the solid content detection of the wastewater slurry is greatly improved.
Drawings
FIG. 1 is a graph showing the change of the water loss amount with time in the drying process of a wastewater slurry sample
Detailed Description
The present invention will be further illustrated by the following examples, which should be construed as merely illustrative and not limiting the scope of the invention.
Certain XX constructional engineering generates certain concrete mixture waste in the concrete production and construction process, sand, stones and wastewater slurry are separated from the concrete mixture waste through a sand-stone separator, and the wastewater slurry is mixed into concrete according to a certain mixing amount for production, so that recycling of construction waste is realized, and the rapid real-time monitoring of the solid content of the wastewater slurry is an important quality control means.
Example 1
1. Extracting 30 wastewater slurry samples from wastewater slurry raw materials, filtering, drying to constant weight to obtain wastewater slurry sample solid powder, and measuring the density rho of the wastewater slurry sample solid powder in a constant-temperature water bath by adopting anhydrous kerosene and a Litsea bottle according to related standards Fixing device The detection results are shown in Table 1.
TABLE 1 summary of solid powder Density detection results for wastewater sludge samples
The percentage of the sample deviation to the average value is 2.0 percent and is not more than 3.0 percent, and the density rho of the solid powder of the wastewater slurry sample is not more than 3.0 percent Fixing device The average value was taken as a representative value, i.e., 2.95g/mL.
2. Taking a wastewater slurry sample from the wastewater slurry raw material used in the step (1), filtering, and drying to constant weight to obtain solid powder of the wastewater slurry sample; uniformly stirring and mixing the solid powder of the wastewater slurry sample and distilled water according to a mass ratio of 3:7 to obtain slurry; taking part of the slurry as a slurry sample to carry out subsequent experiments, wherein the mass m of the weighed slurry sample 0 300.23g; preparing a slurry sample into a cake-shaped test piece with the diameter of about 100mm in a metal disc, placing the slurry sample test piece into a drying box, drying at 80 ℃, taking out and weighing according to a time step of 5min, and calculating the time t i Water dispersion m of (2) wi The change curve of the water loss amount with time in the drying process of the slurry sample is shown in figure 1; drying to constant weight, weighing solid mass of slurry sample to be m Fixing device Root of Chinese characterAccording to the mass ratio of the solid powder of the wastewater slurry sample to distilled water of 3:7, calculating to obtain the water content m of the slurry sample w The test results are shown in Table 2.
As can be seen from table 2: test number 33, time t i 160min, and the water loss m of the drying wi 205.52g, delta 2 m wi /Δ 2 t i 0.0014; test number 34, time t i 165min, and the water loss m of the drying wi 207.97g, delta 2 m wi /Δ 2 t i Is-0.0048; interpolation is used to calculate delta 2 m wi /Δ 2 t i Water loss m at time point corresponding to zero w0 The calculation is as follows:
m w0 =206.08g
the solid matter of the wastewater slurry contains cohesive water rate gamma Fixing device Calculated according to equation 1 to an accuracy of 0.1%.
Equation 1:
the water loss m is calculated by the calculation w0 = 206.08g, and m is known Fixing device 90.08g, water consumption m w = 210.15g; substituting the water content into formula 1, and calculating to obtain the water content gamma of the solid matters in the wastewater slurry Fixing device =4.5%。
Table 2 summary of results of drying test of wastewater sludge samples
3. Taking a wastewater slurry sample from the wastewater slurry raw material used in the step (1), uniformly stirring, and measuring the gas content lambda of the wastewater slurry sample by adopting a concrete gas content measuring instrument Air flow Lambda was measured Air flow 0.8%.
4. Taking another wastewater slurry sample from the wastewater slurry raw material used in the step (1), uniformly stirring, standing for about 1-2min, and measuring the density rho of the wastewater slurry sample by adopting a densimeter Pulp Measuring ρ Pulp 1.055g/mL.
5. Solid content omega of waste water slurry Fixing device Calculated according to formula 2, to an accuracy of 0.01%.
Equation 2:
calculated omega Fixing device 8.46%.
6. And (3) taking another wastewater slurry sample from the wastewater slurry raw material used in the step (1), putting the wastewater slurry sample into a drying box, drying the wastewater slurry sample to constant weight at 80 ℃, and weighing and calculating to obtain the wastewater slurry sample with the solid content of 8.35%.
7. The test error of the invention is I (8.46% -8.35%)/8.35%) |=1.29%, the test error of the invention is not more than 2%, and the detection accuracy is good.
8. Irrespective of the air content lambda Air flow And a water content gamma Fixing device According to the calculation formula of the solid content of the wastewater slurry recorded in the standard DB 51/T2681-2020:
the test error is | (7.98% -8.35%)/8.35%) |=5.55%, the test error is greater than 2%, and the detection accuracy is poor.
Example 2
The waste slurry raw material of example 1 was taken at different time intervals, and the detection and calculation were performed according to steps 1 to 8 of example 1, and the detection results are shown in table 3.
TABLE 3 solids content omega of wastewater slurries Fixing device Statistical table of detection results
As can be seen from table 3:
1) The solid content omega of the wastewater slurry detected in this example Fixing device The test errors of the method are all within +/-2%, the average value of the absolute value of the test errors is 1.02% through statistical analysis and calculation, the average value of the absolute value of the standard deviation is 0.48%, and the detection accuracy is good.
2) If the air content lambda is not taken into consideration Air flow And a water content gamma Fixing device The influence factors of the test error absolute value is calculated by statistical analysis, the average value of the test error absolute value is 12.39 percent, and the average value of the standard deviation absolute value is 5.51 percent, so that the detection accuracy is poor.
Therefore, the detection method provided by the invention detects the solid content of the wastewater slurry, and considers the air content lambda Air flow And a water content gamma Fixing device The detection errors of the two influencing factors are not more than 2%, and the detection accuracy is good; by detecting the density of the wastewater slurry in real time, the method provided by the invention is used for detecting the solid content of the wastewater slurry, and has the advantages of short detection time and high detection efficiency compared with a drying method.
Claims (4)
1. The method for rapidly determining the solid content of the wastewater slurry in the green building construction is characterized by comprising the following steps of:
(1) Taking a wastewater slurry sample from a wastewater slurry raw material to be detected, filtering, drying to constant weight to obtain wastewater slurry solid powder, and measuring the density rho of the wastewater slurry solid powder Fixing device ;
(2) Taking another wastewater slurry sample from the wastewater slurry raw material to be tested used in the step (1), filtering and drying the wastewater slurry sample untilConstant weight, obtaining solid powder of the wastewater slurry sample; uniformly stirring and mixing the solid powder of the wastewater slurry sample with distilled water to obtain slurry; taking part of the slurry as a slurry sample for subsequent detection, and weighing the mass of the slurry sample to be m 0 The method comprises the steps of carrying out a first treatment on the surface of the Drying the slurry sample, weighing according to time steps, and respectively calculating time t i Water dispersion m of (2) wi Drying to constant weight, weighing the solid powder mass of the slurry sample to be m Fixing device The method comprises the steps of carrying out a first treatment on the surface of the The water content of the slurry sample is calculated according to the mass ratio of the solid powder of the wastewater slurry sample and distilled water when the solid powder is stirred and mixed w The method comprises the steps of carrying out a first treatment on the surface of the Calculating water loss m by using a quadratic differential quotient wi For time t i The second derivative of (a) is delta 2 m wi /Δ 2 t i ,Δ 2 m wi /Δ 2 t i The water loss at this time point corresponding to zero is m w0 Finding delta 2 m wi /Δ 2 t i Two adjacent time points when positive and negative changes occur, and delta is calculated by interpolation 2 m wi /Δ 2 t i Water loss m at time point corresponding to zero w0 The method comprises the steps of carrying out a first treatment on the surface of the The solid matter of the wastewater slurry contains cohesive water rate gamma Fixing device Calculating according to the following formula;
(3) Taking a wastewater slurry sample from the wastewater slurry raw material to be detected used in the step (1), uniformly stirring, and measuring the air content lambda of the wastewater slurry sample Air flow ;
(4) Taking a wastewater slurry sample from the wastewater slurry raw material to be detected used in the step (1), uniformly stirring, standing, and measuring the density rho of the wastewater slurry sample Pulp ;
(5) The solid content omega of the waste water slurry raw material to be detected used in the step (1) Fixing device Calculating according to the following formula;
2. the method according to claim 1, wherein in step (1), the ρ is Fixing device The method is characterized by comprising the step of measuring solid powder of a wastewater slurry sample in a constant-temperature water bath by adopting anhydrous kerosene and a Litsea bottle.
3. The method according to claim 1, wherein in the step (3), the lambda is Air flow The method is obtained by measuring the air content of the concrete by a concrete air content measuring instrument.
4. The method according to claim 1, wherein in the step (4), the ρ is Pulp Is measured by densitometer.
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