CN116965412A - Foliar fertilizer for flower and fruit protecting plants - Google Patents
Foliar fertilizer for flower and fruit protecting plants Download PDFInfo
- Publication number
- CN116965412A CN116965412A CN202310968646.8A CN202310968646A CN116965412A CN 116965412 A CN116965412 A CN 116965412A CN 202310968646 A CN202310968646 A CN 202310968646A CN 116965412 A CN116965412 A CN 116965412A
- Authority
- CN
- China
- Prior art keywords
- fertilizer
- paclitaxel
- active component
- foliar fertilizer
- plant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 41
- 235000013399 edible fruits Nutrition 0.000 title abstract description 10
- RCINICONZNJXQF-MZXODVADSA-N taxol Chemical compound O([C@@H]1[C@@]2(C[C@@H](C(C)=C(C2(C)C)[C@H](C([C@]2(C)[C@@H](O)C[C@H]3OC[C@]3([C@H]21)OC(C)=O)=O)OC(=O)C)OC(=O)[C@H](O)[C@@H](NC(=O)C=1C=CC=CC=1)C=1C=CC=CC=1)O)C(=O)C1=CC=CC=C1 RCINICONZNJXQF-MZXODVADSA-N 0.000 claims abstract description 49
- 229930012538 Paclitaxel Natural products 0.000 claims abstract description 48
- 229960001592 paclitaxel Drugs 0.000 claims abstract description 48
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 31
- 229930182764 Polyoxin Natural products 0.000 claims abstract description 20
- YEBIHIICWDDQOL-YBHNRIQQSA-N polyoxin Polymers O[C@@H]1[C@H](O)[C@@H](C(C=O)N)O[C@H]1N1C(=O)NC(=O)C(C(O)=O)=C1 YEBIHIICWDDQOL-YBHNRIQQSA-N 0.000 claims abstract description 20
- 239000005758 Cyprodinil Substances 0.000 claims abstract description 14
- HAORKNGNJCEJBX-UHFFFAOYSA-N cyprodinil Chemical compound N=1C(C)=CC(C2CC2)=NC=1NC1=CC=CC=C1 HAORKNGNJCEJBX-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000005783 Fluopyram Substances 0.000 claims abstract description 9
- 239000004480 active ingredient Substances 0.000 claims abstract description 9
- 201000010099 disease Diseases 0.000 claims abstract description 9
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 claims abstract description 9
- KVDJTXBXMWJJEF-UHFFFAOYSA-N fluopyram Chemical compound ClC1=CC(C(F)(F)F)=CN=C1CCNC(=O)C1=CC=CC=C1C(F)(F)F KVDJTXBXMWJJEF-UHFFFAOYSA-N 0.000 claims abstract description 9
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 10
- 239000004033 plastic Substances 0.000 claims description 8
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims description 8
- 239000002270 dispersing agent Substances 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 7
- 239000000080 wetting agent Substances 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 235000019270 ammonium chloride Nutrition 0.000 claims description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- 229960000892 attapulgite Drugs 0.000 claims description 4
- RYAGRZNBULDMBW-UHFFFAOYSA-L calcium;3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Ca+2].COC1=CC=CC(CC(CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O RYAGRZNBULDMBW-UHFFFAOYSA-L 0.000 claims description 4
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims description 4
- 235000019796 monopotassium phosphate Nutrition 0.000 claims description 4
- 229910052625 palygorskite Inorganic materials 0.000 claims description 4
- 235000010333 potassium nitrate Nutrition 0.000 claims description 4
- 239000004323 potassium nitrate Substances 0.000 claims description 4
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims description 4
- 229960001763 zinc sulfate Drugs 0.000 claims description 4
- 229910000368 zinc sulfate Inorganic materials 0.000 claims description 4
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 3
- 239000000440 bentonite Substances 0.000 claims description 3
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 3
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 3
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims description 3
- 229910052939 potassium sulfate Inorganic materials 0.000 claims description 3
- 235000011151 potassium sulphates Nutrition 0.000 claims description 3
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 3
- KZOJQMWTKJDSQJ-UHFFFAOYSA-M sodium;2,3-dibutylnaphthalene-1-sulfonate Chemical compound [Na+].C1=CC=C2C(S([O-])(=O)=O)=C(CCCC)C(CCCC)=CC2=C1 KZOJQMWTKJDSQJ-UHFFFAOYSA-M 0.000 claims description 3
- LEZAYTDLNNEFJT-UHFFFAOYSA-N tetracosasodium octaborate tetrahydrate Chemical compound O.O.O.O.[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[O-]B([O-])[O-].[O-]B([O-])[O-].[O-]B([O-])[O-].[O-]B([O-])[O-].[O-]B([O-])[O-].[O-]B([O-])[O-].[O-]B([O-])[O-].[O-]B([O-])[O-] LEZAYTDLNNEFJT-UHFFFAOYSA-N 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- 229910000281 calcium bentonite Inorganic materials 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- 229920005551 calcium lignosulfonate Polymers 0.000 claims description 2
- 239000006229 carbon black Substances 0.000 claims description 2
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 2
- 229920005552 sodium lignosulfonate Polymers 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 8
- 230000009286 beneficial effect Effects 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 5
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 230000001954 sterilising effect Effects 0.000 abstract description 2
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 2
- 241000196324 Embryophyta Species 0.000 description 18
- 235000002566 Capsicum Nutrition 0.000 description 10
- 239000005782 Fluopicolide Substances 0.000 description 9
- 244000052616 bacterial pathogen Species 0.000 description 8
- GBOYJIHYACSLGN-UHFFFAOYSA-N fluopicolide Chemical compound ClC1=CC(C(F)(F)F)=CN=C1CNC(=O)C1=C(Cl)C=CC=C1Cl GBOYJIHYACSLGN-UHFFFAOYSA-N 0.000 description 8
- 241000722363 Piper Species 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 6
- 239000003814 drug Substances 0.000 description 6
- 230000002195 synergetic effect Effects 0.000 description 6
- 241000208293 Capsicum Species 0.000 description 5
- 206010059866 Drug resistance Diseases 0.000 description 5
- 239000001390 capsicum minimum Substances 0.000 description 5
- 239000013043 chemical agent Substances 0.000 description 5
- 239000006002 Pepper Substances 0.000 description 4
- 235000016761 Piper aduncum Nutrition 0.000 description 4
- 235000017804 Piper guineense Nutrition 0.000 description 4
- 235000008184 Piper nigrum Nutrition 0.000 description 4
- 230000004071 biological effect Effects 0.000 description 4
- 238000011161 development Methods 0.000 description 4
- 239000000447 pesticide residue Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 241000193738 Bacillus anthracis Species 0.000 description 3
- 241000233654 Oomycetes Species 0.000 description 3
- 229940065181 bacillus anthracis Drugs 0.000 description 3
- 239000003899 bactericide agent Substances 0.000 description 3
- 238000003912 environmental pollution Methods 0.000 description 3
- 230000002401 inhibitory effect Effects 0.000 description 3
- 244000052769 pathogen Species 0.000 description 3
- 230000002265 prevention Effects 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000011282 treatment Methods 0.000 description 3
- 241000222199 Colletotrichum Species 0.000 description 2
- 241000222201 Colletotrichum capsici Species 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- 230000001580 bacterial effect Effects 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000001934 delay Effects 0.000 description 2
- 230000012010 growth Effects 0.000 description 2
- 239000001963 growth medium Substances 0.000 description 2
- 230000001717 pathogenic effect Effects 0.000 description 2
- 239000000575 pesticide Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 150000004579 taxol derivatives Chemical class 0.000 description 2
- 230000001018 virulence Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 206010006187 Breast cancer Diseases 0.000 description 1
- 208000026310 Breast neoplasm Diseases 0.000 description 1
- 241000218631 Coniferophyta Species 0.000 description 1
- 206010058467 Lung neoplasm malignant Diseases 0.000 description 1
- 206010033128 Ovarian cancer Diseases 0.000 description 1
- 206010061535 Ovarian neoplasm Diseases 0.000 description 1
- 241000233614 Phytophthora Species 0.000 description 1
- 241000233616 Phytophthora capsici Species 0.000 description 1
- 241000233647 Phytophthora nicotianae var. parasitica Species 0.000 description 1
- 241000948155 Phytophthora sojae Species 0.000 description 1
- 241000758706 Piperaceae Species 0.000 description 1
- 241001149649 Taxus wallichiana var. chinensis Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000008485 antagonism Effects 0.000 description 1
- 239000002246 antineoplastic agent Substances 0.000 description 1
- 229940041181 antineoplastic drug Drugs 0.000 description 1
- 229910000278 bentonite Inorganic materials 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000007405 data analysis Methods 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 description 1
- 230000009036 growth inhibition Effects 0.000 description 1
- 201000010536 head and neck cancer Diseases 0.000 description 1
- 208000014829 head and neck neoplasm Diseases 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 201000005202 lung cancer Diseases 0.000 description 1
- 208000020816 lung neoplasm Diseases 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000010413 mother solution Substances 0.000 description 1
- 230000003032 phytopathogenic effect Effects 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- GNSKLFRGEWLPPA-UHFFFAOYSA-M potassium dihydrogen phosphate Chemical compound [K+].OP(O)([O-])=O GNSKLFRGEWLPPA-UHFFFAOYSA-M 0.000 description 1
- LWIHDJKSTIGBAC-UHFFFAOYSA-K potassium phosphate Substances [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229930000044 secondary metabolite Natural products 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- 239000008223 sterile water Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/20—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom three- or four-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G13/00—Protecting plants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/12—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P3/00—Fungicides
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C3/00—Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/50—Surfactants; Emulsifiers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/70—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting wettability, e.g. drying agents
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Plant Pathology (AREA)
- Environmental Sciences (AREA)
- Wood Science & Technology (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Dentistry (AREA)
- Mycology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Toxicology (AREA)
- Microbiology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention belongs to the technical field of medical fertilizers, and particularly relates to a flower and fruit protecting plant foliar fertilizer. The bactericidal active component is prepared from paclitaxel and fluopyram, polyoxin or cyprodinil according to the proportion of 1-200:200-1 by weight ratio. The plant foliar fertilizer is essentially a medical fertilizer, and when the plant foliar fertilizer is used, the sterilization active ingredient can effectively prevent and control diseases, and the fertilizer active ingredient can provide nutrient substances, thereby being beneficial to improving the yield and quality of crops and having good application prospect. When plant diseases occur, flower and fruit dropping of plants are easy to occur, and the bactericidal active component can achieve the effect of protecting flowers and fruits by preventing and controlling the plant diseases.
Description
Technical Field
The invention belongs to the technical field of medical fertilizers, and particularly relates to a flower and fruit protecting plant foliar fertilizer.
Background
Paclitaxel, CAS:33069-62-4, molecular formula: c (C) 47 H 51 NO 14 The structural formula is as follows:
paclitaxel (Paclitaxel) is a natural secondary metabolite isolated and purified from the bark of the gymnosperm species taxus chinensis, which is also a natural anticancer drug, and has been widely used clinically for the treatment of breast cancer, ovarian cancer and part of head and neck cancer and lung cancer. Paclitaxel has a novel and complex chemical structure, a wide and remarkable biological activity and a totally new and unique action mechanism, and is greatly favored by botanicals, chemists, pharmacologists, molecular biologists and the like. It is found from the related research that paclitaxel has the potential to be developed into a crop bactericide. For example, patent application number CN201610167401.5 discloses an agricultural oomycete agent containing paclitaxel or a paclitaxel derivative and application thereof, and the patent discloses that the agricultural oomycete agent containing paclitaxel or a paclitaxel derivative has an inhibiting effect on phytopathogenic oomycetes such as phytophthora sojae, phytophthora capsici, phytophthora nicotianae, phytophthora meloidogypti and the like.
In the agricultural pest control process, spraying chemical agents is the most common and convenient and effective control means. The chemical agent has the advantages of quick effect and the like, but if the chemical agent with single component is applied for a long time, the prevention target is easy to generate drug resistance, so that the prevention effect of the chemical agent is reduced. In order to improve the control effect, the application dosage of the chemical agent is blindly increased, the development of drug resistance is aggravated, and the problems of environmental pollution, exceeding pesticide residues and the like are also caused.
Different chemical bactericides are reasonably compounded, so that the pesticide residue can be reduced and the generation and development of the drug resistance of pathogenic bacteria can be delayed while the control effect is improved. The inventor combines taxol with the existing bactericidal active ingredients, and discovers that when taxol is reasonably combined with fluopyram, polyoxin or cyprodinil, the taxol has good synergistic effect on pathogenic bacteria of pepper anthracnose caused by pepper colletotrichum (Colletotrichum capsici); meanwhile, the fertilizer active component is added into the compound, so that the pepper disease can be prevented and treated when the compound is used, and nutrient substances can be provided for plant growth, thereby being beneficial to improving the yield and quality of the peppers.
Disclosure of Invention
The invention aims to provide a flower and fruit protecting plant foliar fertilizer.
In order to achieve the above purpose, the present invention provides the following technical solutions:
the bactericidal active component is prepared from paclitaxel and fluopyram, polyoxin or cyprodinil according to the proportion of 1-200:200-1 by weight ratio.
More specifically, the mass ratio of the taxol to the fluopyram is 1-10:8-1.
More specifically, the mass ratio of the taxol to the polyoxin is 1-15:15-1.
More specifically, the mass ratio of the taxol to the cyprodinil is 1:7-1.
The invention also provides application of the bactericidal active component in prevention and control of plant diseases.
The invention also provides a plant foliar fertilizer which comprises the bactericidal active component.
More specifically, the plant foliar fertilizer comprises the following components in percentage by weight: 1-15% of bactericidal active component, 30-60% of fertilizer active component, 1-5% of wetting agent, 2-8% of dispersing agent and 100% of carrier.
More specifically, the fertilizer active component is selected from one or more of potassium dihydrogen phosphate, ammonium chloride, potassium nitrate, zinc sulfate, potassium sulfate and sodium octaborate tetrahydrate;
the wetting agent is selected from one or more of sodium dodecyl sulfate, sodium dodecyl benzene sulfonate and sodium dibutyl naphthalene sulfonate;
the dispersing agent is one or more selected from calcium lignosulfonate and sodium lignosulfonate; the carrier is one or more selected from white carbon black, attapulgite, light calcium carbonate, bentonite and talcum powder.
The invention also provides a preparation method of the plant foliar fertilizer, which comprises the following steps:
(1) Weighing the raw materials according to the weight percentage;
(2) Uniformly mixing the bactericidal active components, the wetting agent, the dispersing agent and the carrier, crushing by a jet mill, uniformly mixing, bagging the mixed materials, and carrying out plastic package;
(3) And packaging the fertilizer active components in a plastic package mode, wherein when the number of the fertilizer active components is more than 2, each fertilizer active component is independently packaged in a plastic package mode.
Compared with the prior art, the invention has the following beneficial effects:
(1) The bactericidal active component has good synergistic effect on inhibiting target pathogenic bacteria, can improve the control effect on the pathogenic bacteria, is beneficial to reducing the pesticide application amount and reducing the environmental pollution and pesticide residues. Meanwhile, the bactericidal active component of the invention also delays the development of drug resistance of pathogenic bacteria.
(2) When plant diseases occur, the flower and fruit dropping of plants are easy to occur. For example, pepper anthracnose is easy to cause flower and fruit dropping of pepper plants. The bactericidal active component can achieve the effects of protecting flowers and fruits by preventing and controlling plant diseases, and is beneficial to high and stable yield of crops.
(3) The plant foliar fertilizer is essentially a medical fertilizer, and when the plant foliar fertilizer is used, the sterilization active ingredient can effectively prevent and control diseases, and the fertilizer active ingredient can provide nutrient substances, thereby being beneficial to improving the yield and quality of crops and having good application prospect.
Detailed Description
The technical scheme of the invention patent is clearly and completely described below.
Example 1
The plant foliar fertilizer comprises the following components in percentage by weight: 2.5% of bactericidal active components, 10% of zinc sulfate, 15% of ammonium chloride, 18% of potassium nitrate, 5% of sodium dodecyl benzene sulfonate, 4% of calcium lignin sulfonate and 100% of attapulgite; wherein the bactericidal active component is prepared from paclitaxel and fluopicolide according to a proportion of 5:1 by weight ratio binary compounding.
The preparation method of the plant foliar fertilizer comprises the following steps:
(1) Weighing the raw materials according to the weight percentage;
(2) Uniformly mixing the bactericidal active components, the wetting agent, the dispersing agent and the carrier, crushing by a jet mill, uniformly mixing, bagging the mixed materials, and carrying out plastic package;
(3) And (3) independently bagging each fertilizer active component, and plastic packaging.
Example 2
The plant foliar fertilizer comprises the following components in percentage by weight: 8% of bactericidal active components, 2% of sodium octaborate tetrahydrate, 12% of potassium dihydrogen phosphate, 10% of zinc sulfate, 20% of ammonium chloride, 3% of sodium dodecyl sulfate, 7% of sodium lignin sulfonate and 100% of bentonite; wherein, the bactericidal active component is prepared from paclitaxel and polyoxin according to the weight ratio of 15:1 by weight ratio binary compounding.
The preparation method of the plant foliar fertilizer is the same as that of example 1.
Example 3
The plant foliar fertilizer comprises the following components in percentage by weight: 15% of bactericidal active components, 26% of monopotassium phosphate, 8% of ammonium chloride, 15% of potassium nitrate, 10% of potassium sulfate, 2.5% of sodium dibutyl naphthalene sulfonate, 8% of calcium lignin sulfonate and 100% of attapulgite; wherein the bactericidal active components are prepared from paclitaxel and cyprodinil according to the proportion of 1:7, and is compounded in a binary mode according to the mass ratio.
The preparation method of the plant foliar fertilizer is the same as that of example 1.
Example 4
1. Test strain
And c, colletotrichum glomeratum (Colletotrichum capsici) is obtained from infected pepper plants through a tissue separation method and is stored on a PDA culture medium.
2. Test agent
99% of taxol raw material (Wuhan Dong Kangyuan technology Co., ltd.), 96% of fluopyram raw material (Bayer stock Co.), 99% of polyoxin raw material (Wuhan Xinxin Jiali biological technology Co., ltd.), 98% of cyprodinil raw material (Jiangsu Feng crop protection stock Co., ltd.)
Dissolving the test agent with dimethyl sulfoxide, diluting with 0.1% Tween-80 water solution, preparing into single-agent mother solution, setting multiple groups of ratios, and setting 5 mass concentration gradients according to equal ratio method.
3. Test method
The hypha growth rate method is adopted. Adding melted 45mL of PDA culture medium into a sterile conical flask, cooling to 50-55 ℃, adding 5mL of liquid medicine, shaking uniformly, pouring into 3 culture dishes with the diameter of 9cm, preparing medicine-containing plates with corresponding concentrations, setting 4 repetitions for each concentration, and setting treatment of sterile water as a blank. Cutting bacterial cakes with the diameter of 5mm from the colony edge of the strain to be tested by using a puncher, inoculating the bacterial cakes to the center of a flat plate, covering a dish cover, placing the flat plate in a constant temperature oven at 25 ℃ for culturing for 72 hours, measuring the colony diameter by using a crisscross method, and calculating the inhibition rate of different treatments on hypha growth.
4. Data analysis: performing data statistical analysis by DPS software, and collecting corresponding mycelium with a bactericide concentration logarithmic value of xLinear regression is carried out with the growth inhibition rate value of y to obtain a virulence regression equation and virulence EC of the medicament on target bacteria 50 Values and co-toxicity coefficients (CTCs) were calculated according to the grand cloud Pei method.
5. Measurement results
The synergy of the agents was evaluated based on the calculated co-toxicity coefficient (CTC), CTC.ltoreq.80 being antagonism, CTC.ltoreq.120 being additive, CTC.ltoreq.120 being synergy, the results being shown in tables 1-3.
TABLE 1 indoor biological Activity of paclitaxel and fluopyram combinations against Capsicum anthracnose pathogens
| Medicament name and ratio | EC50(mg/L) | ATI | TTI | CTC |
| Paclitaxel (Taxol) | 41.2670 | 100.0000 | -- | -- |
| Fluopicolide | 2.0981 | 1966.8748 | -- | -- |
| Paclitaxel 1: fluopicolide 8 | 1.3204 | 3125.3408 | 1759.4443 | 177.6323 |
| Paclitaxel 1: fluopicolide 5 | 2.0683 | 1995.2135 | 1655.7290 | 120.5036 |
| Paclitaxel 1: fluopicolide 3 | 1.8618 | 2216.5109 | 1500.1561 | 147.7520 |
| Paclitaxel 1: fluopicolide 1 | 3.2551 | 1267.7644 | 1033.4374 | 122.6745 |
| Paclitaxel 3: fluopicolide 1 | 4.8414 | 852.3774 | 566.7187 | 150.4057 |
| Paclitaxel 5: fluopicolide 1 | 5.5582 | 742.4526 | 411.1458 | 180.5813 |
| Paclitaxel 10: fluopicolide 1 | 9.2146 | 447.8436 | 269.7159 | 166.0427 |
As shown in Table 1, after the paclitaxel and fluopyram are compounded, the mass ratio is 1-10: the co-toxicity coefficient of the bacillus anthracis to the capsicum within the range of 8-1 is more than 120, and the synergistic effect is shown.
TABLE 2 indoor biological Activity of paclitaxel and polyoxin complex against Capsicum anthracnose pathogen
| Medicament name and ratio | EC50(mg/L) | ATI | TTI | CTC |
| Paclitaxel (Taxol) | 41.2670 | 100.0000 | -- | -- |
| Polyoxin | 11.1756 | 369.2598 | -- | -- |
| Paclitaxel 1: polyoxin 15 | 6.7816 | 608.5142 | 352.4311 | 172.6619 |
| Paclitaxel 1: polyoxin 10 | 8.1555 | 506.0021 | 344.7817 | 146.7602 |
| Paclitaxel 1: polyoxin 5 | 10.3096 | 400.2774 | 324.3832 | 123.3965 |
| Paclitaxel 1: polyoxin 3 | 7.4302 | 555.3955 | 301.9449 | 183.9394 |
| Paclitaxel 1: polyoxin 1 | 12.5728 | 328.2244 | 234.6299 | 139.8903 |
| Paclitaxel 3: polyoxin 1 | 14.6430 | 281.8207 | 167.3150 | 168.4372 |
| Paclitaxel 5: polyoxin 1 | 17.8097 | 231.7108 | 144.8766 | 159.9366 |
| Paclitaxel 10: polyoxin 1 | 19.4632 | 212.0258 | 124.4782 | 170.3317 |
| Paclitaxel 15: polyoxin 1 | 13.1793 | 313.1198 | 116.8287 | 268.0161 |
As can be seen from Table 2, after the paclitaxel and polyoxin are compounded, the mass ratio is 1-15: the co-toxicity coefficient of the bacillus anthracis to the capsicum within the range of 15-1 is more than 120, and the synergistic effect is shown.
TABLE 3 indoor biological Activity of paclitaxel and cyprodinil combination against Capsici fructus anthracnose pathogen
| Medicament name and ratio | EC50(mg/L) | ATI | TTI | CTC |
| Paclitaxel (Taxol) | 41.2670 | 100.0000 | -- | -- |
| Cyprodinil | 6.5249 | 632.4541 | -- | -- |
| Paclitaxel 1: cyprodinil 7 | 4.5306 | 910.8507 | 565.8974 | 160.9569 |
| Paclitaxel 1: cyprodinil 3 | 6.2153 | 663.9583 | 499.3406 | 132.9670 |
| Paclitaxel 1: cyprodinil 1 | 7.9528 | 518.8990 | 366.2271 | 141.6878 |
As can be seen from table 3, after the paclitaxel and cyprodinil are compounded, the mass ratio is 1: the co-toxicity coefficient of the bacillus anthracis to the capsicum within the range of 7-1 is more than 120, and the synergistic effect is shown.
The bactericidal active component has good synergistic effect on inhibiting target pathogenic bacteria, can improve the control effect on the pathogenic bacteria, is beneficial to reducing the pesticide application amount and reducing the environmental pollution and pesticide residues. Meanwhile, the bactericidal active component of the invention also delays the development of drug resistance of pathogenic bacteria.
Claims (9)
1. The bactericidal active component is characterized by comprising paclitaxel, fluopyram, polyoxin or cyprodinil according to the proportion of 1-200:200-1 by weight ratio.
2. The bactericidal active ingredient according to claim 1, wherein the mass ratio of paclitaxel to fluopyram is 1-10:8-1.
3. The bactericidal active ingredient according to claim 1, wherein the mass ratio of paclitaxel to polyoxin is 1-15:15-1.
4. The bactericidal active ingredient according to claim 1, wherein the mass ratio of paclitaxel to cyprodinil is 1:7-1.
5. Use of the bactericidal active ingredient as set forth in any one of claims 1 to 4 for controlling plant diseases.
6. A plant foliar fertilizer comprising the bactericidal active component of any one of claims 1 to 4.
7. The plant foliar fertilizer of claim 6 wherein the plant foliar fertilizer comprises the following components in weight percent: 1-15% of bactericidal active component, 30-60% of fertilizer active component, 1-5% of wetting agent, 2-8% of dispersing agent and 100% of carrier.
8. The plant foliar fertilizer of claim 6 wherein the fertilizer active component is selected from one or more of potassium dihydrogen phosphate, ammonium chloride, potassium nitrate, zinc sulfate, potassium sulfate, and sodium octaborate tetrahydrate;
the wetting agent is selected from one or more of sodium dodecyl sulfate, sodium dodecyl benzene sulfonate and sodium dibutyl naphthalene sulfonate;
the dispersing agent is one or more selected from calcium lignosulfonate and sodium lignosulfonate;
the carrier is one or more selected from white carbon black, attapulgite, light calcium carbonate, bentonite and talcum powder.
9. A method for preparing the plant foliar fertilizer according to any one of claims 6 to 8, which comprises the following steps:
(1) Weighing the raw materials according to the weight percentage;
(2) Uniformly mixing the bactericidal active components, the wetting agent, the dispersing agent and the carrier, crushing by a jet mill, uniformly mixing, bagging the mixed materials, and carrying out plastic package;
(3) And packaging the fertilizer active components in a plastic package mode, wherein when the number of the fertilizer active components is more than 2, each fertilizer active component is independently packaged in a plastic package mode.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202310968646.8A CN116965412A (en) | 2023-08-03 | 2023-08-03 | Foliar fertilizer for flower and fruit protecting plants |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310968646.8A CN116965412A (en) | 2023-08-03 | 2023-08-03 | Foliar fertilizer for flower and fruit protecting plants |
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| Country | Link |
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