CN1169461C - Production process of extracting food fiber from muriculate eucheuma frond - Google Patents

Production process of extracting food fiber from muriculate eucheuma frond Download PDF

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Publication number
CN1169461C
CN1169461C CNB021148996A CN02114899A CN1169461C CN 1169461 C CN1169461 C CN 1169461C CN B021148996 A CNB021148996 A CN B021148996A CN 02114899 A CN02114899 A CN 02114899A CN 1169461 C CN1169461 C CN 1169461C
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China
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eucheuma
dietary fiber
alkali treatment
present
washed
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Expired - Fee Related
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CN1370445A (en
Inventor
李来好
杨贤庆
陈培基
吴燕燕
刁石强
徐泽智
李刘冬
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South China Sea Fisheries Research Institute Chinese Academy Fishery Sciences
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South China Sea Fisheries Research Institute Chinese Academy Fishery Sciences
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Abstract

The present invention discloses a production technology for extracting dietary fibers from eucheuma, which comprises: A. cleaned eucheuma which is removed of residues is put in alkaline liquor for alkali treatment and soaked at a normal temperature for 20 to 24 hours; B. after the alkali treatment, the eucheuma is taken out from the alkaline liquor to be sufficiently washed to neutral and then bleached by a bleaching solution for 20 to 40 minutes; C. the bleached eucheuma is sufficiently washed to neutral and then treated by centrifugal dewatering, vacuum drying and grinding into powder, and the powdery dietary fibers are obtained. The present invention extracts dietary fibers from eucheuma for the first time, and thus, the utilization value of the eucheuma is increased; low-value non-edible algae are deep-processed into products with high added value so as to be sufficiently developed and utilized, and thus, the economic benefits are high.

Description

A kind of production method of from Eucheuma, extracting dietary fiber
Affiliated technical field
The present invention relates to a kind of production method of extracting dietary fiber, especially relate to a kind of production method of from Eucheuma, extracting dietary fiber.
Background technology
Dietary fiber is the polysaccharide of the non-starch of a class, and by dissolubility, dietary fiber can be divided into water-insoluble and water-soluble two kinds.Water insoluble dietary fiber is the part of cell membrane, comprises cellulose, hemicellulose, lignin and shitosan etc.; Water-soluble dietary fiber is meant storage material and the secretion in the plant cell wall, also comprises part microbial polysaccharide and synthetic class polysaccharide in addition, as pectin, melon glue, algin, CMC and fungi polysaccharide etc.
Dietary fiber is called " the 7th nutrient " by medical science and nutritionist, the experiment proved that has a lot of important physical functions to health: (1) makes the ight soil deliquescing and increases the ight soil discharge rate, can prevent constipation, colon cancer, intestinal diverticulum, hemorrhoid and varix of lower limb; (2) reduce serum cholesterol, the heart disease that prevention is caused by hat artery sclerosis; (3) improve the sensitivity of nerve ending tissue, the blood sugar level that can regulate the diabetes patient to insulin; (4) be a kind of noenergy inserts, can prevent and treat obesity; (5) shortage of dietary fiber or not enough also very big relation is arranged with the incidence of disease and the occurring degree of diseases such as appendicitis, intermittent hernia, gall stone, kidney stone, vesical calculus, duodenal ulcer, ulcerative colitis and breast cancer.
Eucheuma mainly originate in islands and reefs such as Hainan and Nansha and country in Southeast Asia coastal, contain abundant algin, cellulose, hemicellulose, vitamin and mineral matter etc., at present, Eucheuma is mainly used in the production carragheen, but drug on the market for the carragheen product, stockpiling of unsold product, price descends, and manufacturing enterprise is of poor benefits; Caused the waste of Eucheuma resource.
Summary of the invention
The object of the present invention is to provide a kind of production method of from Eucheuma, extracting dietary fiber, the unedible Eucheuma deep processing of this low value is become high value added product.
For achieving the above object, production method of the present invention may further comprise the steps successively: a, will clean up the Eucheuma of removing impurity and put into alkali lye and carry out alkali treatment, normal temperature soaked 20~24 hours down; B, the Eucheuma of pulling alkali treatment from alkali lye out fully are washed to neutrality, handle 20~40 minutes with the bleaching liquid bleaching again; C, the Eucheuma that will bleach again fully are washed to neutrality, and then with its centrifugal dehydration, vacuum drying is crushed to the powdery agent; Promptly obtain powdery agent dietary fiber.
Production method of the present invention is further comprising the steps of: add embedding medium in the pulvis after pulverizing, stir; This embedding medium is mixed by 1%~3% calcium lactate and 0.5%~2% vitamin C.
Alkali lye described in the step a of production method of the present invention is 5%~15% sodium hydroxide solution, and its consumption is 12~15 times of the Eucheuma weight of putting into.
Bleaching liquid described in the step b of production method of the present invention is 0.1%~0.3% clorox, and its pH is 4.0-4.5, and consumption is 8~12 times of Eucheuma weight of required bleaching.
The present invention compared with prior art has following advantage: 1. it is coastal that Eucheuma mainly originates in countries such as Hainan Province of China and Southeast Asia, and resource is quite abundant, and breeding way is mainly half-natural and total man worker cultures; The present invention extracts dietary fiber first from Eucheuma, improved the value of Eucheuma, and the non-edible algae deep processing of low value is become high value added product, and it is developed fully, has produced very high economic benefit.2, the present invention has obtained extraction simultaneously to soluble dietary fiber in the Eucheuma and insoluble diedairy fiber, makes in the Eucheuma processing and does not produce residue, and the dietary fiber that extracts is the dietary fiber of high activity with higher physiological function.Clinical comparison is carried out in effect to the 100 routine constipation patients of taking dietary fiber of high activity that the present invention extracts and wheat bran dietary fiber respectively, and experiment statistics is as shown in the table, proves that the effect of the dietary fiber of high activity that the present invention extracts is more obvious.
After testing before the patient tests
Sample
3 days/time 7 days/time 1 day/time 2 days/time 3 days/time
Eucheuma meals fibre
75% 25% 87.5% 10.0% 2.5%
Dimension
The wheat bran meals
75% 25% 37.5% 30.0% 32.5%
Fiber 3, since hydroxyl in the dietary fiber chemical constitution or side-chain radical such as carboxyl can combine with some mineral element, thereby influence the metabolic balance of the interior mineral matter of human body intestinal canal; Add embedding medium in the dietary fiber of the present invention side-chain radicals such as hydroxyl or carboxyl are closed, avoid influencing the metabolic balance of human body mineral matter, further improve its physiological function.4, the dietary fiber of high activity constant product quality that extracts of the present invention, its major function index retention ability 1450%, expansive force 24.5ml/g.5, the alkali lye in the production method of the present invention recycles, not only environmental protection but also economy.
The specific embodiment
The present invention is further illustrated below in conjunction with specific embodiment.
Embodiment 1
Eucheuma is carried out preliminary treatment, remove impurity, clean up, the sodium hydroxide solution with 10%, general consumption is 13 times of Eucheuma weight, soaks Eucheuma, stirs, and at room temperature handles 22 hours; Pull Eucheuma out, alkali lye can be used for the alkali treatment of next group raw material, if the concentration of alkali is not enough, then adds alkali.The Eucheuma of pulling out is fully washed near neutral, bleach with 0.2% the clorox Eucheuma frond after to alkali treatment again, the pH of clorox is 4.2, the bleaching liquid consumption is above-mentioned 10 times of pulling Eucheuma weight out, bleached 30 minutes, the venting bleaching liquid, once more the Eucheuma frond fully is washed to neutrality, be placed on and carry out centrifugal dehydration in the centrifuge, under 50 ℃ condition, carry out vacuum drying, be crushed to 70 purpose powderies through micronizer again, add the embedding medium that mixes by 2% calcium lactate and 1% vitamin C then with vacuum drier, packed products after stirring is the Eucheuma dietary fiber of high activity.
Embodiment 2
Eucheuma is carried out preliminary treatment, remove impurity, clean up, the sodium hydroxide solution with 5%, general consumption is 15 times of Eucheuma weight, soaks Eucheuma, stirs, and at room temperature handles 24 hours; Pulling Eucheuma out fully washes near neutral, bleach with 0.1% the clorox Eucheuma frond after to alkali treatment again, the pH of clorox is 4.5, the bleaching liquid consumption is above-mentioned 12 times of pulling Eucheuma weight out, bleached 40 minutes, the venting bleaching liquid, once more the Eucheuma frond fully is washed to neutrality, be placed on and carry out centrifugal dehydration in the centrifuge, under 50 ℃ condition, carry out vacuum drying, be crushed to 60 purpose powderies through micronizer again, add the embedding medium that mixes by 3% calcium lactate and 0.5% vitamin C then with vacuum drier, packed products after stirring is the Eucheuma dietary fiber of high activity.
Embodiment 3
Eucheuma is carried out preliminary treatment, remove impurity, clean up, the sodium hydroxide solution with 15%, general consumption is 12 times of Eucheuma weight, soaks Eucheuma, stirs, and at room temperature handles 20 hours; Pull Eucheuma out, alkali lye can be used for the alkali treatment of next group raw material, if the concentration of alkali is not enough, then adds alkali.The Eucheuma of pulling out is fully washed near neutral, bleach with 0.3% the clorox Eucheuma frond after to alkali treatment again, the pH of clorox is 4, the bleaching liquid consumption is above-mentioned 8 times of pulling Eucheuma weight out, bleached 20 minutes, the venting bleaching liquid, once more the Eucheuma frond fully is washed to neutrality, be placed on and carry out centrifugal dehydration in the centrifuge, under 50 ℃ condition, carry out vacuum drying, be crushed to 80 purpose powderies through micronizer again, add the embedding medium that mixes by 1% calcium lactate and 2% vitamin C then with vacuum drier, packed products after stirring is the Eucheuma dietary fiber of high activity.

Claims (1)

1, a kind of production method of from Eucheuma, extracting dietary fiber, it is characterized in that may further comprise the steps successively: a, will clean up the Eucheuma of removing impurity and put into 5%~15% sodium hydroxide solution and carry out alkali treatment, normal temperature soaked 20~24 hours down, and wherein the consumption of sodium hydroxide solution is 12~15 times of the Eucheuma weight of putting into; B, the Eucheuma of pulling alkali treatment from alkali lye out fully are washed to neutrality, handle 20~40 minutes with 0.1%~0.3% sodium hypochlorite bleaching again; Wherein the pH of clorox is 4.0-4.5, and consumption is 8~12 times of Eucheuma weight of required bleaching; C, the Eucheuma that will bleach again fully are washed to neutrality, and then with its centrifugal dehydration, vacuum drying is crushed to the powdery agent; Add the embedding medium that mixes by 1%~3% calcium lactate and 0.5%~2% vitamin C in d, the pulvis after pulverizing, stir.
CNB021148996A 2002-02-26 2002-02-26 Production process of extracting food fiber from muriculate eucheuma frond Expired - Fee Related CN1169461C (en)

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Publication number Priority date Publication date Assignee Title
CN100333666C (en) * 2006-01-20 2007-08-29 张广军 Preparation method of edible cellulose of sweet potato powder dross
JP6050572B2 (en) * 2011-08-10 2016-12-21 ロート製薬株式会社 Elastic fiber formation promoter
CN103815415A (en) * 2014-03-21 2014-05-28 许自霖 High-quality functional alga dietary fiber

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