CN116922601A - Mixing method for producing carbon fiber heat insulation material - Google Patents
Mixing method for producing carbon fiber heat insulation material Download PDFInfo
- Publication number
- CN116922601A CN116922601A CN202311002527.3A CN202311002527A CN116922601A CN 116922601 A CN116922601 A CN 116922601A CN 202311002527 A CN202311002527 A CN 202311002527A CN 116922601 A CN116922601 A CN 116922601A
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- Prior art keywords
- kneader
- carbon fiber
- mixing
- filler
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002156 mixing Methods 0.000 title claims abstract description 58
- 229920000049 Carbon (fiber) Polymers 0.000 title claims abstract description 52
- 239000004917 carbon fiber Substances 0.000 title claims abstract description 52
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 title claims abstract description 50
- 239000012774 insulation material Substances 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title abstract description 7
- 239000000945 filler Substances 0.000 claims abstract description 52
- 239000011810 insulating material Substances 0.000 claims abstract description 14
- 239000012856 weighed raw material Substances 0.000 claims abstract description 10
- 238000007599 discharging Methods 0.000 claims abstract description 7
- 230000001105 regulatory effect Effects 0.000 claims abstract description 6
- 238000004898 kneading Methods 0.000 claims description 23
- 229920002379 silicone rubber Polymers 0.000 claims description 23
- 239000011521 glass Substances 0.000 claims description 19
- 239000011324 bead Substances 0.000 claims description 16
- 239000002994 raw material Substances 0.000 claims description 11
- 239000004945 silicone rubber Substances 0.000 claims description 9
- 238000005303 weighing Methods 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- 239000004005 microsphere Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 abstract description 14
- 238000009413 insulation Methods 0.000 abstract description 7
- 239000011159 matrix material Substances 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 12
- 230000008569 process Effects 0.000 description 8
- 238000010074 rubber mixing Methods 0.000 description 7
- 238000003756 stirring Methods 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 3
- 238000010923 batch production Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000011256 inorganic filler Substances 0.000 description 2
- 229910003475 inorganic filler Inorganic materials 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229920000620 organic polymer Polymers 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 description 1
- 239000006087 Silane Coupling Agent Substances 0.000 description 1
- 238000002679 ablation Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- HIHIPCDUFKZOSL-UHFFFAOYSA-N ethenyl(methyl)silicon Chemical compound C[Si]C=C HIHIPCDUFKZOSL-UHFFFAOYSA-N 0.000 description 1
- 239000011152 fibreglass Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/002—Methods
- B29B7/005—Methods for mixing in batches
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/80—Component parts, details or accessories; Auxiliary operations
- B29B7/82—Heating or cooling
- B29B7/823—Temperature control
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/80—Component parts, details or accessories; Auxiliary operations
- B29B7/86—Component parts, details or accessories; Auxiliary operations for working at sub- or superatmospheric pressure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/80—Component parts, details or accessories; Auxiliary operations
- B29B7/88—Adding charges, i.e. additives
- B29B7/90—Fillers or reinforcements, e.g. fibres
- B29B7/905—Fillers or reinforcements, e.g. fibres with means for pretreatment of the charges or fibres
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
Abstract
The application relates to the technical field of preparation of carbon fiber heat insulation materials, in particular to a mixing method for producing carbon fiber heat insulation materials. And putting the weighed raw materials into a kneader and starting the kneader to carry out mixing. And stopping the kneader after the mixing is completed, discharging and storing. Although the single mixing time of the kneader is longer than that of the open mill, the mixing efficiency of the kneader is higher than that of the open mill for a carbon fiber heat insulating material with a large demand because the mixing amount of the kneader is far greater than that of the open mill, so that the mixing efficiency is improved by using the kneader for mixing. When the filler is completely added and mixed, the kneader is firstly regulated to be heated to 150 ℃ and kept at a constant temperature, and then the interior of the kneader is vacuumized. The compatibility and the dispersibility of the carbon fiber in the matrix can be improved, the moisture and other low molecules in the material can be removed more fully, and the heat insulation performance of the material is better.
Description
Technical Field
The application relates to the technical field of preparation of carbon fiber heat insulation materials, in particular to a mixing method for producing a carbon fiber heat insulation material.
Background
The carbon fiber heat insulating material is a heat insulating material used for high-tech equipment. The glass fiber reinforced plastic is prepared by taking 110 silicon rubber as a substrate, adding carbon fiber, hollow glass beads and other fillers, and mixing.
At present, an open mill is used for mixing, and after a proper amount of 110 silicon rubber, carbon fiber, hollow glass beads and other fillers are weighed, the mixture is put into the open mill for mixing. And as the size space of the open mill is smaller, the maximum rubber mixing amount is lower, and the mixing efficiency is lower for carbon fiber heat insulation materials with large demand.
Disclosure of Invention
In order to overcome the problems in the related art at least to a certain extent, the application aims to provide a mixing method for producing a carbon fiber heat insulation material, which can solve the problem that the mixing efficiency is low when an open mill is used for producing the carbon fiber heat insulation material at present. The preferred technical solutions of the technical solutions provided by the present application can produce a plurality of technical effects described below.
The application provides a mixing method for producing a carbon fiber heat insulation material, which comprises the following steps:
weighing raw materials for producing the carbon fiber heat insulation material, and placing the raw materials beside a kneader for standby;
putting the weighed raw materials into a kneader and starting the kneader to carry out mixing;
stopping the kneader after the mixing is completed;
and (5) discharging and storing.
Optionally, the raw materials for producing the carbon fiber heat insulation material are weighed and placed beside a kneader for standby, comprising:
weighing 250-300kg of 110 silicone rubber and placing the silicone rubber beside a kneader for standby;
250-300kg of filler is weighed and placed beside a kneader for standby, wherein the filler comprises carbon fiber filler and hollow glass microsphere filler.
Optionally, the weighed raw materials are put into a kneader and the kneader is started to carry out mixing, including:
the kneader is powered on;
putting the weighed 110 silicon rubber into a kneader;
starting the kneader;
putting the weighed filler;
and regulating the kneader until the mixing working condition starts mixing.
Optionally, the weighed carbon fiber filler and the hollow glass microsphere filler are added for 3-5 times, and the mixture is mixed for 5-10 minutes after each time of adding.
Optionally, a filler surface treating agent for modifying the filler is added when the weighed filler is put in.
Optionally, adjusting the kneader to a mixing regime to begin mixing, comprising:
regulating the kneader to heat to 150 ℃ and keeping constant temperature;
the interior of the kneader was evacuated.
Optionally, the vacuum degree is greater than-0.1 MPa when the interior of the kneader is vacuumized.
Optionally, stopping the kneader after the completion of the kneading, comprising:
stopping heating and vacuumizing after mixing for 2 hours;
cooling to below 50deg.C.
The technical scheme provided by the application can comprise the following beneficial effects:
during mixing, raw materials for producing the carbon fiber heat insulation material are weighed, and the weighed raw materials are placed beside a kneader for standby. And putting the weighed raw materials into a kneader and starting the kneader to carry out mixing. And stopping the kneader after the mixing is completed, discharging and storing. Although the single mixing time of the kneader is longer than that of the open mill, the mixing efficiency of the kneader is higher than that of the open mill for a carbon fiber heat insulating material with a large demand because the mixing amount of the kneader is far greater than that of the open mill, so that the mixing efficiency is improved by using the kneader for mixing.
It is to be understood that both the foregoing general description and the following detailed description are exemplary and explanatory only and are not restrictive of the application as claimed.
Drawings
The accompanying drawings, which are incorporated in and constitute a part of this specification, illustrate embodiments consistent with the application and together with the description, serve to explain the principles of the application.
In order to more clearly illustrate the embodiments of the application or the technical solutions in the prior art, the drawings that are required in the embodiments or the description of the prior art will be briefly described, it being obvious that the drawings in the following description are only some embodiments of the application, and that other drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a schematic flow diagram of a compounding process for producing carbon fiber insulation;
FIG. 2 is a schematic flow chart of a process for weighing raw materials used for producing carbon fiber insulation;
FIG. 3 is a schematic view showing a flow of putting the weighed raw materials into a kneader and starting the kneader to knead;
FIG. 4 is a schematic flow chart of the kneading machine adjusted to the kneading condition to start kneading;
FIG. 5 is a schematic view showing a flow of stopping the kneader after completion of kneading.
Detailed Description
In order to make the objects, technical solutions and advantages of the present application more apparent, the technical solutions of the present application will be described in detail below. It will be apparent that the described embodiments are only some, but not all, embodiments of the application. All other embodiments, based on the examples herein, which are within the scope of the application as defined by the claims, will be within the scope of the application as defined by the claims.
Hereinafter, embodiments will be described with reference to the drawings. Furthermore, the embodiments shown below do not limit the summary of the application described in the claims. The whole contents of the constitution shown in the following examples are not limited to the solution of the application described in the claims.
Referring to fig. 1 to 5, the present embodiment provides a kneading method for producing a carbon fiber heat insulating material using a kneader. The kneader is an ideal apparatus for kneading, vulcanizing and polymerizing high-viscosity, elastoplastic materials. The kneader is a special mixing stirring device, and most commonly adopts two sigma paddles, adopts side by side tangent differential arrangement, namely, the speed of one stirring paddle is high, the speed of the other stirring paddle is low so as to generate shearing force, and the different paddle speeds enable the mixed materials to be sheared rapidly, so that the materials can be mixed uniformly. The kneader may be heated up and evacuated. Wherein the kneader may be a NHZ-1000 kneader.
Firstly, raw materials for producing the carbon fiber heat insulation material are weighed, and the weighed raw materials are placed beside a kneader for standby. And putting the weighed raw materials into a kneader and starting the kneader to carry out mixing. And stopping the kneader after the mixing is completed, discharging and storing.
The mixing amount of the kneader is far larger than that of an open mill, such as a NHZ-1000 kneader with respect to the dimensional space of a 14-inch open mill, the maximum mixing amount of the 14-inch open mill is 7kg, and the maximum mixing amount of the NHZ-1000 kneader is 600kg. Although the single mixing time of the NHZ-1000 kneader is longer than that of the open mill, the mixing efficiency of the kneader is higher than that of the open mill for a large demand of 600kg because the mixing amount of the kneader is much larger than that of the open mill. Therefore, the kneading by the kneader improves the kneading efficiency.
Specifically, according to the formula, the raw materials 110 are silicon rubber, carbon fiber, hollow glass beads and other filler density and expansibility, and the maximum rubber mixing amount of each batch of NHZ-1000 is 600kg by combining the operating volume of a NHZ-1000 kneader, according to the required heat insulation performance, mechanical strength, spraying technology and the like. Firstly weighing 250-300kg of 110 silicone rubber, placing 110 silicone rubber beside a kneader for standby, weighing 250-300kg of filler, and placing the filler beside the kneader for standby. Weighing for 0.5-1 hr. Wherein the 110 silicone rubber is 110 methyl vinyl silicone rubber, and the filler comprises carbon fiber filler, hollow glass bead filler and the like.
When mixing, firstly, the kneader is powered on, then the weighed 110 silicon rubber is sequentially put into the kneader, after the putting is finished, the kneader is started to rotate, and the proper rotation speed is adjusted to stir the put 110 silicon rubber uniformly. And then adding fillers such as carbon fibers, hollow glass beads and the like. After the filler is added, a kneader is started to carry out mixing for two hours, and the whole is 4-5 hours.
Firstly, 110 silicon rubber is added and stirred, and then fillers such as carbon fiber and hollow glass beads are added, so that the 110 silicon rubber is more uniformly mixed with the fillers such as carbon fiber and hollow glass beads.
In some embodiments, the filler such as carbon fiber, hollow glass beads, etc. is added 3-5 times. And after the fillers such as carbon fiber and hollow glass beads are added each time, firstly mixing for 5-10 minutes, and then adding the fillers such as carbon fiber and hollow glass beads for the next time. By the arrangement, the 110 silicon rubber is more uniformly mixed with the carbon fiber, the hollow glass bead and other fillers.
In other embodiments, after the filler is added, a filler surface treating agent, such as KH550, i.e. a silane coupling agent, also known as gamma-aminopropyl triethoxysilane, is a colorless transparent liquid, and can be used for coupling an organic polymer and an inorganic filler, enhancing the cohesiveness of the organic polymer and the inorganic filler, and improving the mechanical, water-resistant, anti-aging performance of the product. The filler surface treating agent is added for modifying the filler, so that the surface polarity of the filler such as carbon fiber, hollow glass beads and the like is weakened, the oil absorption value is lower, and the compatibility with nonpolar 110 silicon rubber is better, thereby relatively improving the addition amount of the filler and improving the mechanical property, high temperature resistance and heat insulation property of the material.
When the filler is completely added and mixed, the kneader is firstly regulated to be heated to 150 ℃ and kept at a constant temperature, and then the interior of the kneader is vacuumized. And then mixing, thus providing high temperature treatment and negative pressure environment, being capable of better removing moisture, micromolecule and other volatile substances in the 110 silicon rubber and the filler, providing higher surface energy of the sizing material, leading the compatibility to be better, leading the product to be more stable and being beneficial to the high temperature resistance and ablation resistance of the rear end product. Wherein, when the interior of the kneader is vacuumized, the vacuum degree is more than-0.1 MPa.
The heating and vacuumizing functions of the kneader can be utilized to effectively treat the surface of the carbon fiber material, so that the compatibility and the dispersibility of the carbon fiber in a matrix can be improved, and meanwhile, moisture and other low molecules in the material can be more fully removed at high temperature and in a vacuum state, which is beneficial to the heat insulation performance of the material.
It is worth noting that the whole 4-5 hours is calculated after the time of adding the filler excessively, adding the filler surface treating agent, heating up and evacuating.
After the rubber mixing is finished, stopping heating and vacuumizing, starting cooling and cooling to below 50 ℃ to discharge, and storing 600kg of mixed materials in a 200L stainless steel barrel for the next working procedure for 1.5-2 hours.
In general, 600kg of mixed materials can be produced in each batch of the kneader batch production process, the time is about 6-8H, the required labor is 2-3 people, the operation process is continuous operation under the condition of heating and reducing pressure, and the rubber mixing process is finished mechanically except for the manual operation in the feeding and discharging packaging stages, so that the labor intensity is low; the production process can continuously produce 1 batch per working day according to 8H working hours per working day, the daily productivity is 600kg, and the monthly productivity is 15600kg according to 26 working days per month.
For an open mill, according to the formula raw materials 110 silicon rubber, carbon fiber, hollow glass beads and other fillers density and expansibility, the maximum rubber mixing amount is 7kg in combination with the size space of the 14-inch open mill, according to the required heat insulation performance, mechanical strength, spraying technology and the like, 3-4kg110 silicon rubber is weighed and temporarily stored in a 5LPP white barrel, 2-3kg carbon fiber, hollow glass beads and other fillers are weighed and temporarily stored in the 5LPP white barrel, and the open mill is placed beside the open mill for standby, and the time is 0.5H.
When in rubber mixing, the open mill is powered on, the roll gap is adjusted, 110 silicone rubber is put between the two rolls at one time, the rolls start to be started, fillers such as carbon fibers, hollow glass beads and the like are added gradually in sections, the addition is generally divided into 5-6 times, the mixing is carried out for 10 minutes after each filler addition, the mixing is carried out for 0.5 hour after the filler addition, and the working period is 1.5 hours.
After the rubber mixing is completed, each batch of mixed materials is temporarily stored in a 20kg PP barrel for the next working procedure to be used, and the time is 0.5 hour.
In general, 7kg of mixed materials can be produced in each batch by the batch production process of the open mill, the time is about 2.5 hours, the required labor is 2-3 people, the operation process is continuous operation at normal temperature and normal pressure, and the whole process of batching, mixing, discharging and packaging is manually operated, so that the labor time of operators is long, and the labor intensity is high; three batches can be produced in batches per working day according to the working hour of 8 hours per working day, namely, the daily productivity is 21kg, and the monthly productivity is 546kg calculated according to 26 working days per month.
Compared with the mixing method using an open mill, the mixing method using the kneader has the advantages that the mixing efficiency is greatly improved, and the labor intensity is reduced.
It should be noted that, the terms "center", "longitudinal", "transverse", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", etc. are used herein for convenience of description and simplicity of description only, and do not indicate or imply that the apparatus or elements referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus should not be construed as limiting the application. Furthermore, the terms "first," "second," "third," and the like are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description herein, it should also be noted that the terms "mounted," "connected," "coupled," and "connected," are to be construed broadly, and may be either fixedly connected, detachably connected, or integrally connected, for example, unless otherwise specifically indicated and defined; can be mechanically or electrically connected; can be directly connected or indirectly connected through an intermediate medium. The specific meaning of the above terms in the present application can be understood as appropriate by those of ordinary skill in the art.
While embodiments of the present application have been shown and described above, it will be understood that the above embodiments are illustrative and not to be construed as limiting the application, and that variations, modifications, alternatives, and variations may be made to the above embodiments by one of ordinary skill in the art within the scope of the application. It is to be understood that the same or similar parts in the above embodiments may be referred to each other, and that in some embodiments, the same or similar parts in other embodiments may be referred to. The schemes provided by the application comprise the basic schemes of the schemes, are independent of each other and are not mutually restricted, but can be combined with each other under the condition of no conflict, so that a plurality of effects are realized together.
Claims (8)
1. A kneading method for producing a carbon fiber heat insulating material, comprising:
weighing raw materials for producing the carbon fiber heat insulation material, and placing the raw materials beside a kneader for standby;
putting the weighed raw materials into a kneader and starting the kneader to carry out mixing;
stopping the kneader after the mixing is completed;
and (5) discharging and storing.
2. The kneading method for producing a carbon fiber heat insulating material according to claim 1, wherein raw materials for producing a carbon fiber heat insulating material are weighed and placed aside a kneader for use, comprising:
weighing 250-300kg of 110 silicone rubber and placing the silicone rubber beside a kneader for standby;
250-300kg of filler is weighed and placed beside a kneader for standby, wherein the filler comprises carbon fiber filler and hollow glass microsphere filler.
3. The kneading method for producing a carbon fiber heat insulating material according to claim 2, wherein the weighed raw materials are put into a kneader and the kneader is started to conduct kneading, comprising:
the kneader is powered on;
putting the weighed 110 silicon rubber into a kneader;
starting the kneader;
putting the weighed filler;
and regulating the kneader until the mixing working condition starts mixing.
4. The kneading method for producing a carbon fiber heat insulating material according to claim 3, wherein the weighed carbon fiber filler and hollow glass bead filler are fed in 3 to 5 times, and kneading is performed for 5 to 10 minutes after each feeding.
5. The kneading method for producing a carbon fiber heat insulating material according to claim 3, wherein a filler surface treating agent for modifying the filler is added when the weighed filler is put in.
6. A kneading method for producing a carbon fiber heat insulating material according to claim 3, wherein the kneading machine is adjusted to a kneading condition to start kneading, comprising:
regulating the kneader to heat to 150 ℃ and keeping constant temperature;
the interior of the kneader was evacuated.
7. The kneading method for producing a carbon fiber heat insulating material according to claim 6, wherein the vacuum degree is more than-0.1 MPa when the inside of the kneader is evacuated.
8. The kneading method for producing a carbon fiber heat insulating material according to claim 6, wherein the kneader is stopped after the completion of kneading, comprising:
stopping heating and vacuumizing after mixing for 2 hours;
cooling to below 50deg.C.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202311002527.3A CN116922601A (en) | 2023-08-09 | 2023-08-09 | Mixing method for producing carbon fiber heat insulation material |
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Application Number | Priority Date | Filing Date | Title |
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CN202311002527.3A CN116922601A (en) | 2023-08-09 | 2023-08-09 | Mixing method for producing carbon fiber heat insulation material |
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CN116922601A true CN116922601A (en) | 2023-10-24 |
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CN202311002527.3A Pending CN116922601A (en) | 2023-08-09 | 2023-08-09 | Mixing method for producing carbon fiber heat insulation material |
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