CN116832748A - Reaction kettle for fumaric acid synthesis - Google Patents
Reaction kettle for fumaric acid synthesis Download PDFInfo
- Publication number
- CN116832748A CN116832748A CN202310636828.5A CN202310636828A CN116832748A CN 116832748 A CN116832748 A CN 116832748A CN 202310636828 A CN202310636828 A CN 202310636828A CN 116832748 A CN116832748 A CN 116832748A
- Authority
- CN
- China
- Prior art keywords
- reaction kettle
- kettle body
- fumaric acid
- spacing
- belt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 68
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 title claims abstract description 49
- 239000001530 fumaric acid Substances 0.000 title claims abstract description 24
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 title claims abstract description 24
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 8
- 230000015572 biosynthetic process Effects 0.000 title claims description 7
- 238000003756 stirring Methods 0.000 claims abstract description 23
- 238000007599 discharging Methods 0.000 claims abstract description 8
- 230000002194 synthesizing effect Effects 0.000 claims description 11
- 238000007790 scraping Methods 0.000 claims description 10
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims description 3
- 235000017491 Bambusa tulda Nutrition 0.000 claims description 3
- 241001330002 Bambuseae Species 0.000 claims description 3
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims description 3
- 230000006978 adaptation Effects 0.000 claims description 3
- 239000011425 bamboo Substances 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 239000003381 stabilizer Substances 0.000 claims 3
- 239000000463 material Substances 0.000 abstract description 43
- 239000003054 catalyst Substances 0.000 abstract description 20
- 238000002360 preparation method Methods 0.000 abstract description 6
- 230000000149 penetrating effect Effects 0.000 abstract description 3
- 238000004140 cleaning Methods 0.000 description 19
- 235000011087 fumaric acid Nutrition 0.000 description 14
- 230000000087 stabilizing effect Effects 0.000 description 10
- 239000007788 liquid Substances 0.000 description 9
- 238000002156 mixing Methods 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000000034 method Methods 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical compound CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 description 1
- 241000218176 Corydalis Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- IAQRGUVFOMOMEM-UHFFFAOYSA-N butene Natural products CC=CC IAQRGUVFOMOMEM-UHFFFAOYSA-N 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000002075 main ingredient Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
- B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The application relates to a fumaric acid synthesis reaction kettle, which comprises a reaction kettle body, wherein a support frame is arranged on the outer surface of the reaction kettle body, a control panel is arranged on one side of the surface of the reaction kettle body, a discharging pipe is arranged at the bottom end of the reaction kettle body, an electromagnetic valve is arranged on the outer surface of the discharging pipe, a limiting cylinder and a motor body are sequentially arranged at the top end of the reaction kettle body from left to right, a rotating shaft is connected with the output end of the motor body penetrating through the top surface of the reaction kettle body, and a first gear is arranged at the bottom end of the rotating shaft. According to the application, the materials are added through the first conveying pipe and the second conveying pipe, and can be thrown out to the middle end part of the reaction kettle body, so that the problems of adding the catalyst and directly throwing the materials in the past are solved, the dispersibility of the materials is ensured through throwing at different positions, the preparation efficiency is enhanced, and meanwhile, the materials can be directly stirred after entering the reaction kettle body, so that the stirring can be fully performed.
Description
Technical Field
The application relates to the technical field of reaction kettles, in particular to a reaction kettle for fumaric acid synthesis.
Background
Fumaric acid, also known as fumaric acid, corydalic acid or lichenic acid, is a colorless, flammable crystal, carboxylic acid derived from butene. The taste of fumaric acid is fruit-like, and it is found in corydalis, bolete, lichen and iceberg that fumaric acid has a strong buffering property to maintain the pH of an aqueous solution at about 3.0 (pH of an aqueous solution is 2.25-2.7), which is of particular importance for preservatives and the like which suitably act at about pH 3.0, and is therefore often used as one of the main ingredients of a compounded preservative and the like. In addition, it has weak antioxidant capacity and has stabilizing effect on water-in-oil emulsifier.
For this, chinese application number: CN106669572B discloses a reaction kettle, which comprises a reaction kettle body, wherein a heating cavity is formed in the side wall of the reaction kettle body, a water filling port is formed in one side of the heating cavity, a liquid suction pipe is wound outside the reaction kettle body, a funnel-shaped liquid inlet is formed in one end of the liquid suction pipe, a first one-way valve is arranged at the liquid inlet, a liquid outlet is formed in the other end of the liquid suction pipe, the liquid inlet and the liquid outlet are both positioned in the reaction kettle body, and the vertical distance between the liquid outlet and the bottom of the reaction kettle body is 1-3 cm; but reation kettle body upper portion threaded connection has the kettle cover, and it has the through-hole to open on the kettle cover, and the through-hole fit has the (mixing) shaft, and the (mixing) shaft top is equipped with drive arrangement, and the (mixing) shaft bottom is eccentric to be provided with the (mixing) wheel, and the (mixing) wheel corresponds the setting with the inlet, and extrudees the inlet when the (mixing) wheel rotates to radius biggest department. Compared with the prior art, the material in the reaction kettle can be fully stirred and uniformly heated.
In the preparation process of fumaric acid, materials and catalysts need to be mixed and stirred in a heated state, but when the catalysts or the materials are added, the materials are directly put into a reaction kettle, the materials still need to be mixed with the solution in the reaction kettle, the amount of the catalysts in the reaction kettle cannot be controlled, and the putting position cannot be controlled, so that the preparation efficiency is affected, and therefore, the design of the reaction kettle for synthesizing fumaric acid is needed to solve the problems.
Disclosure of Invention
In order to overcome the technical problems described above, the present application aims to provide a reaction kettle for synthesizing fumaric acid, which solves the problems that stirring is performed in a heated state while the reaction kettle is being proposed in the prior art, but when a catalyst or a material is being added, the catalyst or the material is directly put into the reaction kettle, the material is still required to be mixed with the solution in the reaction kettle in time, the amount of the catalyst in the reaction kettle cannot be controlled, and the putting position cannot be controlled, so that the efficiency in preparation is affected.
The application adopts the following technical scheme for realizing the purposes: the utility model provides a fumaric acid is reation kettle for synthesis, includes the reation kettle body, the surface of reation kettle body is provided with the support frame, surface one side of reation kettle body is provided with control panel, the bottom of reation kettle body is provided with the discharging pipe, the surface of discharging pipe is provided with the solenoid valve, the top of reation kettle body has set gradually spacing section of thick bamboo and motor body from a left side to the right side, the output of motor body runs through the top surface of reation kettle body and is connected with the axis of rotation, the bottom of axis of rotation is provided with first gear, the surface meshing of first gear is connected with the second gear, the inside wall fixedly connected with feed cylinder of second gear, the surface fixedly connected with of feed cylinder throws the dish.
Preferably, the inner side wall of the throwing disc is provided with through grooves, the through grooves are provided with four groups, the through grooves are uniformly arranged on the inner wall of the throwing disc, the inside of the through grooves is provided with a through pipe, and the through pipe is provided with four groups and is mutually matched with the four groups of the through grooves.
Preferably, the surface fixedly connected with swivel becket of feed cylinder, the surface fixedly connected with stirring board of swivel becket, the right-hand member of stirring board is provided with scrapes the cushion, it contradicts each other with the inner wall of reation kettle body to strike off the cushion.
Preferably, the rotating ring is provided with three groups, the throwing disc is provided with three groups, and the rotating ring and the throwing disc are uniformly arranged on the surface of the feeding barrel.
Preferably, the surface fixedly connected with first spacing of axis of rotation, the surface of first spacing is provided with first belt, the inside wall of first belt is provided with the second spacing, the bottom fixedly connected with rotation post of second spacing.
Preferably, the surface of the rotating column is provided with a stabilizing plate, the surface of the rotating column penetrating through the stabilizing plate is provided with a reciprocating screw rod, the outer surface of the reciprocating screw rod is provided with a movable ring, the inside of the movable ring is provided with a positioning rod, and the bottom end of the movable ring is provided with a sealing ring.
Preferably, the first conveying pipe and the second conveying pipe are sequentially arranged in the stabilizing plate from left to right, and the first conveying pipe and the second conveying pipe are arranged in the limiting cylinder.
Preferably, the bottom fixedly connected with spliced pole of first gear, the mounting groove has been seted up to the inside wall of reation kettle body, the surface of spliced pole has set gradually fourth spacing and third spacing from last to down, the surface of third spacing is provided with the second belt, the inside wall of second belt is provided with first clearance post, the surface of first clearance post is provided with first clearance brush, the mutual adaptation between mounting groove and the first clearance post.
Preferably, the outer surface of fourth spacing is provided with the third belt, the inside wall of third belt is provided with the second clearance post, the surface of second clearance post is provided with the second clearance brush.
Compared with the prior art, the application has the beneficial effects that:
the reaction kettle for synthesizing fumaric acid comprises a rotating shaft, a first gear, a second gear, a feeding cylinder, a throwing disc, a through groove, a through pipe, a rotating ring, a stirring plate, a scraping cushion, a first limiting frame, a first belt, a second limiting frame, a rotating column, a stabilizing plate and a reciprocating screw rod, wherein when the reaction kettle is used, firstly, the movable ring can convey materials and catalysts to the surface of the movable ring at the bottom end part of the stabilizing plate, then the first conveying pipe and the second conveying pipe are used for conveying materials and catalysts to the surface of the movable ring, then a motor body is started, the rotating shaft can be driven to rotate through the motor body, then the rotating shaft drives the first gear and the first limiting frame to rotate, the first gear and the second gear are meshed, so that the second gear can drive the feeding cylinder to rotate, then the first limiting frame and the first belt can drive the second limiting frame to rotate, and the second limiting frame can drive the rotating column to rotate, when the rotating column rotates, the movable ring is driven to move upwards, meanwhile, the material can be arranged at the top end of the movable ring, when the movable ring ascends, the solution can be thrown out through the through pipe in the through groove when passing through the throwing disc, so that the material can be thrown in the bottom end part of the reaction kettle body, meanwhile, the throwing disc and the rotating ring are in a rotating state, the throwing disc and the rotating ring can stir the thrown material, then the movable ring continuously moves upwards, the material is added through the first conveying pipe and the second conveying pipe in the moving process, when the movable ring ascends to the upper group of throwing disc, the material can be thrown out to the middle end part of the reaction kettle body, the problem of adding catalyst and directly throwing the material in the past is solved, the dispersibility of the material is ensured through throwing in different positions, the preparation efficiency is enhanced, simultaneously, the materials can be directly stirred after entering the reaction kettle body, so that the stirring can be fully performed, and the designed functionality is embodied.
This reation kettle for fumaric acid synthesis, through the spliced pole that sets up, the fourth spacing, the third spacing, the second belt, first clearance post, first clearance brush, the third belt, the second clearance post, second clearance brush and mounting groove, when using, when the inside of reation kettle body is thrown the dish and is rotated the stirring with the rotation ring, the rotation ring drives four sets of stirring boards and is scraped the cushion and stir in the inside of reation kettle body, and strike off the cushion and can scrape some adnexed catalyst on the reation kettle body inner wall, drive the spliced pole through first gear and rotate, can drive fourth spacing and third spacing through the spliced pole and rotate, drive the second belt through the second belt and rotate, first clearance post and the mounting groove are mutually adapted, first clearance post rotates, can drive first clearance brush and rotate this moment, can strike off the catalyst that the cushion surface was attached in rotation, thereby continue to carry out the reaction in the inside of reation kettle body, with the fourth spacing and the third clearance post can all rotate through the second belt, the second clearance post is designed, the inside of this reaction kettle can be guaranteed to the material fully.
Drawings
FIG. 1 is a schematic view of a three-dimensional structure of the present application;
FIG. 2 is a schematic cross-sectional view of the structure of the reactor body of the present application;
FIG. 3 is a schematic perspective view of a first gear and feed cylinder configuration of the present application;
FIG. 4 is a schematic cross-sectional view of the feed cylinder structure of the present application;
FIG. 5 is a schematic perspective view of a connecting column and a first cleaning column structure of the present application;
FIG. 6 is a schematic perspective view of a tray structure of the present application;
FIG. 7 is a schematic diagram showing the motor body and the rotating shaft structure of the present application;
fig. 8 is an enlarged schematic view of the structure of fig. 2 a according to the present application.
In the figure: 1. a reaction kettle body; 2. a support frame; 3. a control panel; 4. a discharge pipe; 5. an electromagnetic valve; 6. a motor body; 7. a limiting cylinder; 8. a rotating shaft; 9. a first gear; 10. a second gear; 11. a feed cylinder; 12. a throwing disc; 13. a through groove; 14. a through pipe; 15. a rotating ring; 16. a stirring plate; 17. scraping off the soft cushion; 18. a first limiting frame; 19. a first belt; 20. the second limiting frame; 21. rotating the column; 22. a stabilizing plate; 23. a reciprocating screw rod; 24. a movable ring; 25. a positioning rod; 26. a seal ring; 27. a first feed delivery tube; 28. a second feed delivery tube; 29. a connecting column; 32. a third limiting frame; 33. a fourth limiting frame; 34. a second belt; 35. a first cleaning column; 36. a first cleaning brush; 37. a third belt; 38. a second cleaning column; 39. a second cleaning brush; 40. and a mounting groove.
Detailed Description
The following description of the embodiments of the present application will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present application, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the application without making any inventive effort, are intended to be within the scope of the application.
Referring to fig. 1-8, an embodiment of the present application is provided: the application relates to a reaction kettle for fumaric acid synthesis, which is characterized in that a reaction kettle body 1, a control panel 3, an electromagnetic valve 5 and a motor body 6 which are used in the application are directly purchased in the market, the principle and the connection mode are all the prior art well known to the person skilled in the art, the reaction kettle comprises a reaction kettle body 1, a support frame 2 is arranged on the outer surface of the reaction kettle body 1, the control panel 3 is arranged on one side of the surface of the reaction kettle body 1, a discharging pipe 4 is arranged at the bottom end of the reaction kettle body 1, the electromagnetic valve 5 is arranged on the outer surface of the discharging pipe 4, a limiting cylinder 7 and the motor body 6 are sequentially arranged at the top end of the reaction kettle body 1 from left to right, a rotating shaft 8 is connected at the output end of the motor body 6 penetrating through the top surface of the reaction kettle body 1, a first limiting frame 18 is fixedly connected on the outer surface of the rotating shaft 8, a first belt 19 is arranged on the surface of the first limiting frame 18, the inner side wall of the first belt 19 is provided with a second limiting frame 20, the bottom end of the second limiting frame 20 is fixedly connected with a rotating column 21, the outer surface of the rotating column 21 is provided with a stabilizing plate 22, the inside of the stabilizing plate 22 is provided with a first conveying pipe 27 and a second conveying pipe 28 in sequence from left to right, the first conveying pipe 27 and the second conveying pipe 28 are all arranged in the limiting cylinder 7, the rotating column 21 penetrates through the surface of the stabilizing plate 22 and is provided with a reciprocating screw rod 23, the outer surface of the reciprocating screw rod 23 is provided with a movable ring 24, the inside of the movable ring 24 is provided with a positioning rod 25, the bottom end of the movable ring 24 is provided with a sealing ring 26, the bottom end of the rotating shaft 8 is provided with a first gear 9, the bottom end of the first gear 9 is fixedly connected with a connecting column 29, the inner side wall of the reaction kettle body 1 is provided with a mounting groove 40, the outer surface of the connecting column 29 is provided with a fourth limiting frame 33 and a third limiting frame 32 in sequence from top to bottom, the outer surface of the fourth limiting frame 33 is provided with a third belt 37, the inner side wall of the third belt 37 is provided with a second cleaning post 38, the outer surface of the second cleaning post 38 is provided with a second cleaning brush 39, the outer surface of the third limiting frame 32 is provided with a second belt 34, the inner side wall of the second belt 34 is provided with a first cleaning post 35, the outer surface of the first cleaning post 35 is provided with a first cleaning brush 36, a mounting groove 40 and the first cleaning post 35 are mutually matched, the outer surface of the first gear 9 is in meshed connection with a second gear 10, the inner side wall of the second gear 10 is fixedly connected with a feeding cylinder 11, the outer surface of the feeding cylinder 11 is fixedly connected with a rotating ring 15, the rotating ring 15 is provided with three groups, a casting disc 12 is provided with three groups, the rotating ring 15 and the casting disc 12 are uniformly arranged on the surface of the feeding cylinder 11, the outer surface of the rotating ring 15 is fixedly connected with a stirring plate 16, the right end of the stirring plate 16 is provided with a scraping cushion 17, the scraping cushion 17 is mutually abutted against the inner wall of the reaction kettle body 1, the outer surface of the feeding cylinder 11 is fixedly connected with a throwing disc 12, the inner side wall of the throwing disc 12 is provided with a through groove 13, the through groove 13 is provided with four groups of through grooves which are uniformly arranged on the inner wall of the throwing disc 12, the inside of the through groove 13 is provided with a through pipe 14, the through pipe 14 is provided with four groups of through grooves 13 which are mutually matched, firstly, a movable ring 24 can convey materials and catalysts to the surface of the movable ring 24 through a first conveying pipe 27 and a second conveying pipe 28, then the motor body 6 is started, the rotating shaft 8 can be driven to rotate through the motor body 6, then the rotating shaft 8 drives a first gear 9 and a first limiting frame 18 to rotate, the first gear 9 is meshed with a second gear 10, therefore the second gear 10 can drive the feeding cylinder 11 to rotate, then the first limiting frame 18 and the first belt 19 drive the second limiting frame 20 to rotate, so that the second limiting frame 20 drives the rotating column 21 to rotate, the movable ring 24 is driven to move upwards when the rotating column 21 rotates, meanwhile, the material is arranged at the top end of the movable ring 24, when the movable ring 24 ascends, the solution passes through the throwing disc 12, and is thrown out through the through pipe 14 in the through groove 13, so that the material can be thrown in the bottom end part of the reaction kettle body 1, and meanwhile, the throwing disc 12 and the rotating ring 15 are in a rotating state, so that the throwing disc 12 and the rotating ring 15 stir the thrown material, then the movable ring 24 continues to move upwards, the material is added through the first conveying pipe 27 and the second conveying pipe 28 in the moving process, and the material is thrown out to the middle end part of the reaction kettle body 1 when the movable ring 24 ascends to the upper group of throwing disc 12, the problems of adding catalyst and directly throwing materials in the past are solved, the dispersibility of the materials is ensured through throwing at different positions, the preparation efficiency is enhanced, when the inner throwing disc 12 and the rotating ring 15 of the reaction kettle body 1 start rotating and stirring, the rotating ring 15 drives four groups of stirring plates 16 and scraping cushions 17 to stir the inner part of the reaction kettle body 1, the scraping cushions 17 scrape off some adhered catalyst on the inner wall of the reaction kettle body 1, the connecting column 29 is driven to rotate through the first gear 9, the fourth limiting frame 33 and the third limiting frame 32 can be driven to rotate through the connecting column 29, the second belt 34 is driven to rotate through the third limiting frame 32, the first cleaning column 35 is driven to rotate through the second belt 34, the first cleaning column 35 is mutually matched with the mounting groove 40, and when the first cleaning column 35 rotates, at this time, the first cleaning brush 36 is driven to rotate, and the catalyst attached to the surface of the scraping cushion 17 in rotation is scraped when the first cleaning brush 36 rotates, so that the reaction is continuously performed in the reaction kettle body 1, and the operation can be performed similarly through the design of the fourth limiting frame 33, the third belt 37, the second cleaning column 38 and the second cleaning brush 39, so that the materials in the reaction kettle body 1 can be fully reacted.
Working principle: in use, firstly the movable ring 24 will convey the material and the catalyst to the surface of the movable ring 24 through the first conveying pipe 27 and the second conveying pipe 28, then the motor body 6 is started, the motor body 6 can drive the rotating shaft 8 to rotate, then the rotating shaft 8 drives the first gear 9 and the first limiting frame 18 to rotate, the first gear 9 is meshed with the second gear 10, so the second gear 10 can drive the feeding cylinder 11 to rotate, then the first limiting frame 18 and the first belt 19 can drive the second limiting frame 20 to rotate, so the second limiting frame 20 can drive the rotating column 21 to rotate, the movable ring 24 is driven to move upwards when the rotating column 21 rotates, meanwhile, the material can be arranged at the top end of the movable ring 24, when the movable ring 24 ascends, the solution passes through the throwing disc 12, the solution can be arranged in the through groove 13, the material can be thrown out through the through pipe 14, so that the material can be thrown in the bottom end part of the reaction kettle body 1, meanwhile, the throwing disc 12 and the rotating ring 15 are in a rotating state, so that the throwing disc 12 and the rotating ring 15 stir the thrown material, then the movable ring 24 continues to move upwards, the material is added through the first conveying pipe 27 and the second conveying pipe 28 in the moving process, when the material rises to the upper group of throwing disc 12, the material is thrown out to the middle end part of the reaction kettle body 1, the problems of adding catalyst and directly throwing the material in the past are solved, the dispersibility of the material is ensured through throwing in different positions, when the throwing disc 12 and the rotating ring 15 in the reaction kettle body 1 start to rotate and stir, the rotating ring 15 drives the four groups of stirring plates 16 and the scraping cushion 17 to stir in the reaction kettle body 1, and strike off the cushion 17 and can scrape some catalyst that adhere to on the inner wall of reation kettle body 1, drive spliced pole 29 through first gear 9 and rotate, can drive fourth spacing 33 and third spacing 32 through spliced pole 29 and rotate, drive second belt 34 through third spacing 32 and rotate, drive first clearance post 35 through second belt 34 and rotate, the mutual adaptation between first clearance post 35 and the mounting groove 40, when first clearance post 35 rotates, drive first clearance brush 36 and rotate this moment, first clearance brush 36 rotates the catalyst that will scrape off cushion 17 surface adhesion in rotation, thereby continue to react in reation kettle body 1's inside, and similarly can carry out this operation through the design of fourth spacing 33, third belt 37, second clearance post 38 and second clearance brush 39, ensure that the material in reation kettle body 1 inside can all fully react, above is the whole theory of operation of the application.
It will be evident to those skilled in the art that the application is not limited to the details of the foregoing illustrative embodiments, and that the present application may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the application being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (9)
1. The utility model provides a reation kettle for fumaric acid synthesis, includes reation kettle body (1), the surface of reation kettle body (1) is provided with support frame (2), the surface one side of reation kettle body (1) is provided with control panel (3), its characterized in that: the bottom of reation kettle body (1) is provided with discharging pipe (4), the surface of discharging pipe (4) is provided with solenoid valve (5), the top of reation kettle body (1) has set gradually spacing section of thick bamboo (7) and motor body (6) from a left side to the right side, the output of motor body (6) runs through the top surface of reation kettle body (1) and is connected with axis of rotation (8), the bottom of axis of rotation (8) is provided with first gear (9), the surface meshing of first gear (9) is connected with second gear (10), the inside wall fixedly connected with feed cylinder (11) of second gear (10), the surface fixedly connected with of feed cylinder (11) puts in dish (12).
2. The reaction kettle for synthesizing fumaric acid according to claim 1, wherein: through grooves (13) are formed in the inner side wall of the throwing disc (12), four groups of through grooves (13) are formed and uniformly arranged on the inner wall of the throwing disc (12), a through pipe (14) is arranged in the through grooves (13), and the through pipe (14) is provided with four groups and is mutually matched with the four groups of through grooves (13).
3. The reaction kettle for synthesizing fumaric acid according to claim 1, wherein: the feeding cylinder is characterized in that a rotating ring (15) is fixedly connected to the outer surface of the feeding cylinder (11), a stirring plate (16) is fixedly connected to the outer surface of the rotating ring (15), a scraping cushion (17) is arranged at the right end of the stirring plate (16), and the scraping cushion (17) is mutually abutted to the inner wall of the reaction kettle body (1).
4. The reaction kettle for synthesizing fumaric acid according to claim 3, wherein: the rotary ring (15) is provided with three groups, the throwing disc (12) is provided with three groups, and the rotary ring (15) and the throwing disc (12) are uniformly arranged on the surface of the feeding barrel (11).
5. The reaction kettle for synthesizing fumaric acid according to claim 1, wherein: the outer surface fixedly connected with first spacing (18) of axis of rotation (8), the surface of first spacing (18) is provided with first belt (19), the inside wall of first belt (19) is provided with second spacing (20), the bottom fixedly connected with rotation post (21) of second spacing (20).
6. The reaction kettle for synthesizing fumaric acid according to claim 5, wherein: the outer surface of rotation post (21) is provided with stabilizer plate (22), the surface that rotation post (21) runs through stabilizer plate (22) is provided with reciprocating screw (23), the surface of reciprocating screw (23) is provided with expansion ring (24), the inside of expansion ring (24) is provided with locating lever (25), the bottom of expansion ring (24) is provided with sealing washer (26).
7. The reaction kettle for synthesizing fumaric acid according to claim 6, wherein: the inside of stabilizer board (22) has set gradually first conveying pipeline (27) and second conveying pipeline (28) from left to right, first conveying pipeline (27) and second conveying pipeline (28) are all installed in the inside of spacing section of thick bamboo (7).
8. The reaction kettle for synthesizing fumaric acid according to claim 1, wherein: the bottom fixedly connected with spliced pole (29) of first gear (9), mounting groove (40) have been seted up to the inside wall of reation kettle body (1), the surface of spliced pole (29) has set gradually fourth spacing (33) and third spacing (32) from last to down, the surface of third spacing (32) is provided with second belt (34), the inside wall of second belt (34) is provided with first clearance post (35), the surface of first clearance post (35) is provided with first clearance brush (36), the mutual adaptation between mounting groove (40) and first clearance post (35).
9. The reaction kettle for synthesizing fumaric acid according to claim 8, wherein: the outer surface of fourth spacing (33) is provided with third belt (37), the inside wall of third belt (37) is provided with second clearance post (38), the surface of second clearance post (38) is provided with second clearance brush (39).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310636828.5A CN116832748A (en) | 2023-05-31 | 2023-05-31 | Reaction kettle for fumaric acid synthesis |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310636828.5A CN116832748A (en) | 2023-05-31 | 2023-05-31 | Reaction kettle for fumaric acid synthesis |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN116832748A true CN116832748A (en) | 2023-10-03 |
Family
ID=88166080
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202310636828.5A Pending CN116832748A (en) | 2023-05-31 | 2023-05-31 | Reaction kettle for fumaric acid synthesis |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN116832748A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117696564A (en) * | 2024-02-06 | 2024-03-15 | 威海市正威机械设备股份有限公司 | Reaction kettle inner wall cleaning device with expansion assembly |
| CN117735660A (en) * | 2024-02-06 | 2024-03-22 | 爱德士制鞋(枣庄)有限责任公司 | Rinsing wastewater treatment equipment for clothing production |
-
2023
- 2023-05-31 CN CN202310636828.5A patent/CN116832748A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117696564A (en) * | 2024-02-06 | 2024-03-15 | 威海市正威机械设备股份有限公司 | Reaction kettle inner wall cleaning device with expansion assembly |
| CN117735660A (en) * | 2024-02-06 | 2024-03-22 | 爱德士制鞋(枣庄)有限责任公司 | Rinsing wastewater treatment equipment for clothing production |
| CN117735660B (en) * | 2024-02-06 | 2024-05-24 | 爱德士制鞋(枣庄)有限责任公司 | Rinsing wastewater treatment equipment for clothing production |
| CN117696564B (en) * | 2024-02-06 | 2024-06-07 | 威海市正威机械设备股份有限公司 | Reaction kettle inner wall cleaning device with expansion assembly |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN116832748A (en) | Reaction kettle for fumaric acid synthesis | |
| CN207734887U (en) | A kind of calciferol light reaction liquid proportioner | |
| CN210545151U (en) | Reaction kettle for preparing emulsified milk essence by enzymolysis technology | |
| CN208553917U (en) | A kind of high-molecular water paint Efficient Agitator | |
| CN114098046A (en) | Salted egg yolk salad dressing, preparation method thereof and emulsifying device for preparation | |
| CN208340663U (en) | Wet mixed granulating machine | |
| CN216093471U (en) | High-efficient mixing apparatus is used in chemical product processing of multidirectional stirring | |
| CN220759264U (en) | Reaction kettle | |
| CN217939913U (en) | Ginseng cream modulation is with mixing preparation jar | |
| CN220443644U (en) | Stirring device for calcium stearate emulsion | |
| CN215540819U (en) | High-efficient reation kettle is used in production of weak base oil-displacing agent | |
| CN219942450U (en) | Mixing stirring device for pet food | |
| CN211363047U (en) | Rubber stirrer | |
| CN220088182U (en) | Irrigation equipment that food processing was used | |
| CN221117447U (en) | Pharmaceutical equipment with PH value adjusting function | |
| CN220071329U (en) | Traditional Chinese medicine liquid preparation tank for producing and processing oral solution | |
| CN219836376U (en) | Automatic glue mixer convenient to clean | |
| CN221156219U (en) | Aquatic product processing raw material mixing device | |
| CN220589765U (en) | Premixing equipment for shell powder coating | |
| CN220311232U (en) | Cleaning structure of horizontal mixing barrel | |
| CN220328373U (en) | Mixing arrangement is used in fungus chaff fermentation | |
| CN218339585U (en) | High-speed compounding device of even natural seasoning of compounding | |
| CN215429061U (en) | Novel chemical industry reaction stirring device | |
| CN220779942U (en) | Mixing equipment for steamed stuffed bun stuffing production | |
| CN219314956U (en) | Enzymolysis device with controllable auxiliary material feeding |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |