CN116762943A - Sucrose auxiliary material and preparation method thereof - Google Patents
Sucrose auxiliary material and preparation method thereof Download PDFInfo
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- CN116762943A CN116762943A CN202310659446.4A CN202310659446A CN116762943A CN 116762943 A CN116762943 A CN 116762943A CN 202310659446 A CN202310659446 A CN 202310659446A CN 116762943 A CN116762943 A CN 116762943A
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- sucrose
- sweetener
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- finishing
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- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 title claims abstract description 71
- 229930006000 Sucrose Natural products 0.000 title claims abstract description 60
- 239000005720 sucrose Substances 0.000 title claims abstract description 60
- 239000000463 material Substances 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000002245 particle Substances 0.000 claims abstract description 25
- 235000003599 food sweetener Nutrition 0.000 claims abstract description 19
- 239000003765 sweetening agent Substances 0.000 claims abstract description 19
- 238000000034 method Methods 0.000 claims abstract description 17
- 238000003825 pressing Methods 0.000 claims abstract description 9
- 238000012216 screening Methods 0.000 claims abstract description 8
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 18
- 239000008103 glucose Substances 0.000 claims description 18
- 239000004378 Glycyrrhizin Substances 0.000 claims description 15
- LPLVUJXQOOQHMX-UHFFFAOYSA-N glycyrrhetinic acid glycoside Natural products C1CC(C2C(C3(CCC4(C)CCC(C)(CC4C3=CC2=O)C(O)=O)C)(C)CC2)(C)C2C(C)(C)C1OC1OC(C(O)=O)C(O)C(O)C1OC1OC(C(O)=O)C(O)C(O)C1O LPLVUJXQOOQHMX-UHFFFAOYSA-N 0.000 claims description 15
- 229960004949 glycyrrhizic acid Drugs 0.000 claims description 15
- UYRUBYNTXSDKQT-UHFFFAOYSA-N glycyrrhizic acid Natural products CC1(C)C(CCC2(C)C1CCC3(C)C2C(=O)C=C4C5CC(C)(CCC5(C)CCC34C)C(=O)O)OC6OC(C(O)C(O)C6OC7OC(O)C(O)C(O)C7C(=O)O)C(=O)O UYRUBYNTXSDKQT-UHFFFAOYSA-N 0.000 claims description 15
- 235000019410 glycyrrhizin Nutrition 0.000 claims description 15
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 claims description 15
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 11
- 239000008187 granular material Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 239000010419 fine particle Substances 0.000 claims description 7
- 238000004513 sizing Methods 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 5
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 4
- 229920002472 Starch Polymers 0.000 claims description 4
- 239000008101 lactose Substances 0.000 claims description 4
- 239000008107 starch Substances 0.000 claims description 4
- 235000019698 starch Nutrition 0.000 claims description 4
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 3
- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 claims description 3
- 108010011485 Aspartame Proteins 0.000 claims description 3
- UDIPTWFVPPPURJ-UHFFFAOYSA-M Cyclamate Chemical compound [Na+].[O-]S(=O)(=O)NC1CCCCC1 UDIPTWFVPPPURJ-UHFFFAOYSA-M 0.000 claims description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 3
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims description 3
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 3
- 239000004386 Erythritol Substances 0.000 claims description 3
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 claims description 3
- 229930091371 Fructose Natural products 0.000 claims description 3
- 239000005715 Fructose Substances 0.000 claims description 3
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 3
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 3
- 229930195725 Mannitol Natural products 0.000 claims description 3
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims description 3
- 239000004376 Sucralose Substances 0.000 claims description 3
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 3
- 235000010358 acesulfame potassium Nutrition 0.000 claims description 3
- 229960004998 acesulfame potassium Drugs 0.000 claims description 3
- 239000000619 acesulfame-K Substances 0.000 claims description 3
- 239000000605 aspartame Substances 0.000 claims description 3
- 235000010357 aspartame Nutrition 0.000 claims description 3
- IAOZJIPTCAWIRG-QWRGUYRKSA-N aspartame Chemical compound OC(=O)C[C@H](N)C(=O)N[C@H](C(=O)OC)CC1=CC=CC=C1 IAOZJIPTCAWIRG-QWRGUYRKSA-N 0.000 claims description 3
- 229960003438 aspartame Drugs 0.000 claims description 3
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 claims description 3
- 235000019414 erythritol Nutrition 0.000 claims description 3
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 claims description 3
- 229940009714 erythritol Drugs 0.000 claims description 3
- 239000000845 maltitol Substances 0.000 claims description 3
- 235000010449 maltitol Nutrition 0.000 claims description 3
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 claims description 3
- 229940035436 maltitol Drugs 0.000 claims description 3
- 239000000594 mannitol Substances 0.000 claims description 3
- 235000010355 mannitol Nutrition 0.000 claims description 3
- 229960001855 mannitol Drugs 0.000 claims description 3
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 3
- 239000000600 sorbitol Substances 0.000 claims description 3
- 235000010356 sorbitol Nutrition 0.000 claims description 3
- 229960002920 sorbitol Drugs 0.000 claims description 3
- 229940013618 stevioside Drugs 0.000 claims description 3
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims description 3
- 235000019202 steviosides Nutrition 0.000 claims description 3
- 235000019408 sucralose Nutrition 0.000 claims description 3
- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims description 3
- 239000000811 xylitol Substances 0.000 claims description 3
- 235000010447 xylitol Nutrition 0.000 claims description 3
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims description 3
- 229960002675 xylitol Drugs 0.000 claims description 3
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 2
- 239000000625 cyclamic acid and its Na and Ca salt Substances 0.000 claims description 2
- 229960001375 lactose Drugs 0.000 claims description 2
- 229960001462 sodium cyclamate Drugs 0.000 claims description 2
- 239000002671 adjuvant Substances 0.000 claims 3
- WINXNKPZLFISPD-UHFFFAOYSA-M Saccharin sodium Chemical compound [Na+].C1=CC=C2C(=O)[N-]S(=O)(=O)C2=C1 WINXNKPZLFISPD-UHFFFAOYSA-M 0.000 claims 1
- 239000011148 porous material Substances 0.000 claims 1
- 229940079593 drug Drugs 0.000 abstract description 4
- 239000003814 drug Substances 0.000 abstract description 4
- 235000013305 food Nutrition 0.000 abstract description 4
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 description 11
- 238000002425 crystallisation Methods 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- 230000006872 improvement Effects 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 238000007873 sieving Methods 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 238000005054 agglomeration Methods 0.000 description 4
- 230000002776 aggregation Effects 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 230000007547 defect Effects 0.000 description 4
- 150000003445 sucroses Chemical class 0.000 description 4
- 238000001291 vacuum drying Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 3
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 235000015110 jellies Nutrition 0.000 description 2
- 239000008274 jelly Substances 0.000 description 2
- 229940085605 saccharin sodium Drugs 0.000 description 2
- 229920002774 Maltodextrin Polymers 0.000 description 1
- 239000005913 Maltodextrin Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000008122 artificial sweetener Substances 0.000 description 1
- 235000021311 artificial sweeteners Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 229940109275 cyclamate Drugs 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229960004903 invert sugar Drugs 0.000 description 1
- 229940035034 maltodextrin Drugs 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000021096 natural sweeteners Nutrition 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Abstract
The invention provides a sucrose auxiliary material and a preparation method thereof, which belong to the technical field of medicines and foods and comprise the following steps: crushing sucrose and sweetener, adding into a dry granulator, pressing into large tablets, finishing the large tablets by a finishing cutter, screening the finished products, and screening sucrose auxiliary materials with the particle size of 425-850 mu m. Compared with the prior art, the preparation method provided by the invention has the advantages of simplifying the process steps, reducing the material types, along with low cost, low energy consumption and no pollution, and has a wide application prospect.
Description
Technical Field
The invention relates to the technical field of medicines and foods, in particular to a sucrose auxiliary material and a preparation method thereof.
Background
Sucrose is used as an important sweetener and an energy source, and is widely applied in the production fields of foods, health products, medicines and the like. Currently, the following compressible sugar products exist abroad, and the brands and the production processes thereof are as follows: (1) di-pac is produced by concentrating sucrose solution containing physiologically acceptable additives, comprising the technical processes of mechanically stirring supersaturated sucrose solution, solidifying operation and the like, and the principle is that crystals in the solution are mutually agglomerated into paste and solidified, and the production is carried out by utilizing the agglomeration principle of the crystals; (2) Nutab is produced by compacting sucrose powder, invert sugar and starch; (3) Alveosure is obtained by granulating with wet sucrose powder and maltodextrin.
In addition, there are many patent documents on compressible sucrose particles, such as:
CN1520463C discloses a method of drying sucrose solutions, the products thus obtained and their use. The method involves a process for preparing a compressible sugar solution comprising a drying step of atomizing an initial sucrose solution with the addition of at least one anti-crystallization agent, wherein the initial sucrose solution has a sucrose content below saturation and preferably has a dry matter content of about 60wt% based on the total weight of the composition. However, the method needs multi-stage spray drying equipment, and has the defects of large equipment investment, low concentration of sucrose solution, large energy consumption and the like.
CN1884584a discloses a method for producing granular compressible sugar, which comprises the steps of mixing super-heated supersaturated sucrose solution containing an anti-crystallization agent with powdery compressible sugar varieties, stirring, vacuum drying, crushing and sieving to obtain granular compressible sugar products. However, the method is a crystallization method, and has the defects of low yield, high hardness of the material after vacuum drying, difficult pulverization and the like.
CN103820583B discloses a preparation method of granular compressible sucrose, the method is that the super-heated supersaturated sucrose solution of the anti-crystallization agent and the powdery compressible sugar seed crystal are stirred and mixed, and then are granulated by a high-speed mixer granulator after vacuum drying, and then are dried by blowing and screened to obtain the granular compressible sugar product. However, the method has the defects of complex process, low yield and the like, and simultaneously improves the compressibility, and simultaneously greatly influences the fluidity and agglomeration performance of the particles.
CN1884584a discloses a method for producing compressible sugar. The method adopts a crystallization method to stir and mix the overheated supersaturated sucrose solution containing the anti-crystallization agent and powdery compressible sugar seed crystal, and the mixture is crushed and sieved after vacuum drying to obtain a granular compressible sugar product. However, the method has the defects that the hardness of the material is high after the material is dried in vacuum completely and then crushed, the crushing operation is difficult, and the yield of compressible sugar with ideal granularity is low.
In a word, the existing method for producing the compressible sucrose particles has the problems of large equipment investment, high energy consumption and long operation time, and the product contains insoluble auxiliary materials. The compressible sucrose particles with easy obtaining of production equipment, low investment, simple operation, no addition of insoluble auxiliary materials and higher sucrose purity and the production process thereof are needed to be found in industry.
Disclosure of Invention
The invention aims to provide a sucrose auxiliary material and a preparation method thereof, and the sucrose auxiliary material prepared by the method has the advantages of compressibility and good fluidity.
The technical scheme of the invention is realized as follows:
the invention provides a sucrose auxiliary material which is in a fine particle shape, has the particle size of 425-850 mu m, the moisture content of less than 0.5%, the bulk density of 0.55-0.78g/ml and the repose angle of less than 30 degrees.
As a further improvement of the invention, the sucrose auxiliary material contains a sweetener, wherein the mass proportion of the sucrose is 80% -100%, and the mass proportion of the sweetener is 0% -20%.
As a further improvement of the present invention, the sweetener is selected from one or more of glucose, fructose, maltose, starch sugar, lactose, xylitol, sorbitol, maltitol, mannitol, erythritol, saccharin sodium, cyclamate, acesulfame potassium, aspartame, sucralose, stevioside, or glycyrrhizin.
As a further improvement of the invention, the sweetener is selected from natural sugar substances such as glucose, fructose, maltose, starch sugar, lactose and the like, or natural or artificial sweeteners such as xylitol, sorbitol, maltitol, mannitol, erythritol, saccharin sodium, sodium cyclamate, acesulfame potassium, aspartame, sucralose, stevioside, glycyrrhizin and the like.
As a further improvement of the invention, the sweetener is a mixture of glucose and glycyrrhizin, and the mass ratio is 6-8:3. When the sweetener is a mixture of glucose and glycyrrhizin, a small amount of glycyrrhizin is decomposed by adding water under the action of acid, is insoluble in water and diluted ethanol, is soluble in hot water, is in viscous jelly after being cooled, is insoluble in grease, and is soluble in propylene glycol. The addition of the sweetener has good improvement on the particle size, bulk density and repose angle of the sucrose auxiliary material.
The invention further provides a preparation method of the sucrose auxiliary material, which comprises the following steps:
s1, crushing sucrose and a sweetener until the particle size is smaller than 180 mu m, adding the crushed sucrose and the sweetener into a dry granulator, adjusting the pressure of the dry granulator to 80-100 bar, enabling the pressure clearance to be 0.6-1.2mm, enabling the rotating speed of a pressing wheel to be 8-15rpm, and operating the machine to press large tablets;
s2, installing a granule finishing screen with the aperture of 0.7-1.0mm, and finishing the prepared large sheets by a granule finishing cutter with the rotating speed of 100-200 rpm;
s3, screening the granulated product, screening out the product with the particle size of 425-850 mu m, and returning the rest particles or powder to a dry granulating machine for granulating.
The invention has the following beneficial effects:
the sucrose particles are controlled to have the particle size of 425-850 microns, the moisture content of less than 0.5%, the bulk density of 0.55-0.78g/ml and the repose angle of less than 30 ℃ by adopting a specific preparation process, and the sucrose particles have good compressibility, flowability, no agglomeration and no caking and have high purity (the sucrose is not required to be dissolved and an anti-crystallization agent is not required to be introduced). The innovative auxiliary sucrose material has the characteristics of wide purity range, capability of being set according to actual requirements, small moisture, easiness in storage and transportation, no pollution to the environment in the production process, capability of completely dissolving all components in water, convenience in production and use of foods, health-care products and medicines, and capability of retaining the natural flavor of sucrose and improving chewing feeling.
Description of the embodiments
The following description of the technical solutions in the embodiments of the present invention will be clear and complete, and it is obvious that the described embodiments are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Examples
1. Crushing 1000g of sucrose, sieving with an 80-mesh sieve, and adding into a dry granulator;
2. the dry granulator is set to a pressure of 80bar, the radial gap is 0.6mm, and the rotation speed of the pressing wheel is 8rpm. Running a machine, and pressing into large sheets with the thickness of about 0.8mm;
3. installing a sizing screen with the aperture of 0.7mm, and sizing the prepared large sheets at the rotating speed of a sizing cutter of 200 rpm;
4. sieving sucrose particles with the particle size of 425-850 μm required by customers to obtain the compressible sucrose fine particles;
examples
1. Crushing 900g of sucrose, sieving with a 80-mesh sieve together with 100g of lactose, uniformly mixing, and adding into a dry granulator;
2, regulating the pressure spoke working pressure of the dry granulator to 90bar, setting a pressure mixing gap to 0.9mm, setting the pressure spread rotating speed to 12rpm, operating the machine, and pressing to obtain large sheets with the thickness of about 1.1mm;
3. installing a sizing screen with the aperture of 0.7mm, and sizing the prepared large sheets at the rotating speed of a sizing cutter of 150 rpm;
4. sucrose particles with a customer's desired particle size of 425 μm to 850 μm were sieved out to give the compressible sucrose fine particles of the invention.
Examples
1. Crushing 800g of sucrose, sieving with a 80-mesh sieve together with 200g of glucose, uniformly mixing, and adding into a dry granulator;
2. the working pressure of the dry granulator is adjusted to 100bar, the spoke clearance is 1.2mm, and the spoke rotating speed is 15rpm. Running a machine, and pressing into large sheets with the thickness of about 1.3mm;
3. installing a finishing screen with the aperture of 1.0mm, and finishing the prepared large sheets at the speed of 100rpm of a finishing cutter;
4. sucrose particles with a customer's desired particle size of 425 μm to 850 μm were sieved out to give the compressible sucrose fine particles of the invention.
Examples
1. Crushing 950g of sucrose, sieving with a 80-mesh sieve together with 50g of glucose, uniformly mixing, and adding into a dry granulator;
2. the rolling working pressure of the dry-method granulator is adjusted to 90bar, the gap of the pressing wheel is 1.0mm, the rotation speed of the pressing spoke is 10rpm, the machine is operated, and large sheets are pressed, wherein the thickness of the large sheets is about 1.2mm;
3. installing a finishing screen with the aperture of 1.0mm, and finishing the prepared large sheets at the speed of 100rpm of a finishing cutter;
4. sucrose particles with a customer's desired particle size of 425 μm to 850 μm were sieved out to give the compressible sucrose fine particles of the invention.
Examples
Compared with example 3, the difference is that glucose is replaced by a mixture of glucose and glycyrrhizin, and the mass ratio is 7:3.
Examples
Compared with example 3, the difference is that glucose is replaced by a mixture of glucose and glycyrrhizin, and the mass ratio is 1:3.
Examples
Compared with example 3, the difference is that glucose is replaced by a mixture of glucose and glycyrrhizin, and the mass ratio is 15:3.
Examples
The difference compared to example 3 is that glucose is replaced with glycyrrhizin.
The sucrose fine particles of examples 1 to 4 were measured for their respective performance indexes such as repose angle, compressibility karl coefficient, moisture, agglomeration, etc., and left to stand at room temperature and 45% relative humidity for 1 month to see whether they are liable to absorb moisture and agglomerate, and the results are shown in table 1 below:
TABLE 1
When the sweetener is a mixture of glucose and glycyrrhizin, a small amount of glycyrrhizin is decomposed by adding water under the action of acid, is insoluble in water and diluted ethanol, is soluble in hot water, is in viscous jelly after being cooled, is insoluble in grease, and is soluble in propylene glycol. The mixing of glucose and glycyrrhizin in proper proportion can well improve the particle size, bulk density and repose angle of the sucrose auxiliary material. The sucrose auxiliary material with better performance cannot be obtained when the ratio of glucose to glycyrrhizin is too high or too low.
The foregoing description of the preferred embodiments of the invention is not intended to be limiting, but rather is intended to cover all modifications, equivalents, alternatives, and improvements that fall within the spirit and scope of the invention.
Claims (9)
1. The sucrose auxiliary material is characterized in that the sucrose auxiliary material is in a fine particle shape, the particle size is 425-850 mu m, the moisture is less than 0.5%, the bulk density is 0.55-0.78g/ml, and the repose angle is less than 30 degrees.
2. Sucrose adjuvant according to claim 1, characterized in that it contains a sweetener, wherein the mass proportion of sucrose is 80-100% and the mass proportion of sweetener is 0-20%.
3. The sucrose adjuvant according to claim 2, wherein the sweetener is selected from one or more of glucose, fructose, maltose, starch sugar, lactose, xylitol, sorbitol, maltitol, mannitol, erythritol, sodium saccharin, sodium cyclamate, acesulfame potassium, aspartame, sucralose, stevioside or glycyrrhizin.
4. A sweetener selection according to claim 3 wherein the sweetener is a mixture of glucose and glycyrrhizin in a mass ratio of 6-8:3.
5. A method for preparing the sucrose adjuvant according to claim 1, comprising the steps of:
s1, crushing sucrose to a particle size smaller than 180 mu m, adding the crushed sucrose into a dry granulator, and running the machine to press large tablets;
s2, installing a granule finishing screen, and finishing granules by using a granule finishing cutter;
s3, screening the granulated product, screening the product, and returning the rest granules or powder to the dry granulating machine for granulating.
6. A process for the preparation of a sucrose adjunct as claimed in any one of claims 2 to 4, comprising the steps of:
s1, crushing sucrose and a sweetener until the particle size is smaller than 180 mu m, adding the crushed sucrose and the sweetener into a dry granulating machine, running the machine, and pressing into large tablets;
s2, installing a granule finishing screen, and finishing granules by using a granule finishing cutter;
s3, screening the granulated product, screening the product, and returning the rest granules or powder to the dry granulating machine for granulating.
7. The preparation method according to claim 5 or 6, wherein the press working pressure of the dry granulator is adjusted to 80-100 bar, the press gap is 0.6-1.2mm, and the press wheel rotation speed is 8-15rpm.
8. The method according to claim 5 or 6, wherein the mesh has a pore size of 0.7 to 1.0mm.
9. The method according to claim 5 or 6, wherein the rotational speed of the sizing cutter is 100-200rpm.
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| CN202310659446.4A CN116762943A (en) | 2023-06-06 | 2023-06-06 | Sucrose auxiliary material and preparation method thereof |
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