CN116651367A - Constant temperature reaction device for preparing high-temperature-resistant nonionic active agent - Google Patents

Constant temperature reaction device for preparing high-temperature-resistant nonionic active agent Download PDF

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Publication number
CN116651367A
CN116651367A CN202310647521.5A CN202310647521A CN116651367A CN 116651367 A CN116651367 A CN 116651367A CN 202310647521 A CN202310647521 A CN 202310647521A CN 116651367 A CN116651367 A CN 116651367A
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China
Prior art keywords
wall
plate
box
control valve
rod
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CN202310647521.5A
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Chinese (zh)
Inventor
吴月
吴余冬
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Nantong Hongshen Chemical Co ltd
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Nantong Hongshen Chemical Co ltd
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Priority to CN202310647521.5A priority Critical patent/CN116651367A/en
Publication of CN116651367A publication Critical patent/CN116651367A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00092Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention discloses a constant temperature reaction device for preparing a high-temperature-resistant nonionic active agent, which comprises a box body, a fixed plate, a controller and a warning indicator, wherein the fixed plate is arranged on the inner wall of the box body, a cooling box is arranged at the bottom of the fixed plate, a vertical plate is arranged at the top of a transverse plate, two groups of first electric telescopic rods are arranged on the outer wall of the vertical plate, and an extrusion rod is arranged at one end of each first electric telescopic rod. According to the invention, an automatic adjusting function can be realized by installing the temperature sensor, the temperature sensor controls the first electric telescopic rod to extend, the first electric telescopic rod extends to drive the extrusion rod to move, the extrusion rod moves to extrude the lifting plate, the bottom of the lifting plate descends to drive the first spring to shrink, the trigger rod at the bottom of the lifting plate descends to be in contact with the trigger switch, and the trigger switch controls the first control valve and the second control valve to control the flow in the pipeline, so that the temperature is controlled, and an automatic control function is realized.

Description

Constant temperature reaction device for preparing high-temperature-resistant nonionic active agent
Technical Field
The invention relates to the technical field of active agent reaction devices, in particular to a constant temperature reaction device for preparing a high-temperature-resistant nonionic active agent.
Background
The surfactant is a substance capable of significantly reducing the surface tension of the target solution. Has immobilized hydrophilic and lipophilic groups, and can be oriented on the surface of the solution. The molecular structure of the surfactant has amphoteric properties: one end is hydrophilic group, and the other end is hydrophobic group; the hydrophilic group is usually a polar group such as carboxylic acid, sulfonic acid, sulfuric acid, amino or amine group and salts thereof, and hydroxyl group, amide group, ether bond and the like can also be used as the polar hydrophilic group; while hydrophobic groups are often nonpolar hydrocarbon chains, such as hydrocarbon chains of more than 8 carbon atoms. Surfactants are classified into ionic surfactants (including cationic surfactants and anionic surfactants), nonionic surfactants, amphoteric surfactants, built surfactants, other surfactants, and the like.
The existing reaction device has the following defects:
1. patent document CN115318227a discloses a constant temperature reaction device for surfactant production, and the protection rights "comprises an outer tank, wherein the top of the outer tank is provided with symmetrically arranged jacks in a penetrating way, and inserted bars are embedded in the two groups of jacks; the sealing cover is installed at the top of two sets of inserted bars, the retort is installed to the diapire of outer jar, keep off the stopper is installed at the top of sealed lid, keep off the surface and the internal surface of stopper respectively with the internal surface of outer jar and the surface laminating mutually of retort, the surface of outer jar and sealed lid is all run through and is provided with the notch, the surface that keeps off the stopper runs through and is provided with the spout the surface mounting of retort has the intake pipe. According to the invention, the outer tank, the jack, the inserted link, the blocking plug and the reaction tank are arranged, and the blocking plug is inserted into a space formed by the outer tank and the reaction tank through the insertion of the inserted link and the jack, so that convenience can be provided for the disassembly and assembly of the reaction device to a certain extent, and further a certain convenience can be provided for the cleaning of the subsequent reaction tank;
2. patent document CN115193385a discloses an organic modified potassium silicate constant temperature reaction device, and the claim of protection "belongs to the technical field of chemical product processing, and comprises a bottom plate and a supporting plate frame fixedly connected to the top of the bottom plate, wherein a heating assembly is arranged on the outer side of the supporting plate frame, a circulating assembly and an operating assembly are arranged on the top of the supporting plate frame, and the circulating assembly comprises a rotary table rotatably connected to the top of the supporting plate frame and a frame fixedly connected to the top of the rotary table. According to the invention, the heating assembly, the circulating assembly and the operating assembly are arranged, wherein the heating assembly and the circulating assembly are matched to heat the charging barrels in different areas, so that the discharging of the device is kept at a certain frequency to be in butt joint with the production nodes, the stable yield is ensured, meanwhile, the heating assembly covers the outer side of the circulating assembly to keep the constant temperature in the material stirring process, meanwhile, due to the matching of the circulating assembly and the operating assembly, the material at the material exchanging port can be prevented from interfering with the adjacent charging barrels when the material is released and added, and the heat loss caused when the material is exchanged is avoided, and the existing device is not accurate enough when the material is fed, so that the reaction material is insufficient or too much;
3. patent document CN112250038A discloses a solid hydrogen constant temperature reaction hydrogen generating device, and the protection claim "the device comprises a hydrogen generating device, wherein solid metal hydride is stored in the hydrogen generating device, and the hydrogen generating device conveys the generated hydrogen into an external hydrogen storage device; the water adding device is used for adding water into the hydrogen generating device; the temperature adjusting device comprises a heater and a heat radiating device, wherein the heater can heat reaction water or aqueous solution when being started, the heat radiating device comprises a radiator and a semiconductor refrigerating sheet, the radiator can radiate the reaction water or the aqueous solution, and the semiconductor refrigerating sheet is used for radiating the hydrogen generating device; the invention realizes the fixed-point control of hydrogen quantity control, hydrogen pressure and reaction temperature through the monitoring unit at normal temperature and normal pressure so as to ensure that the device has higher safety and solid hydrogen utilization rate, and most of the existing devices are not uniformly mixed, so that the reaction effect is poor;
4. patent document CN107748583a discloses a sequencing batch sealed constant temperature reaction device, and the protection rights "comprise a sealed device box, a plurality of conical bottle reactors fixed in the device box, a plurality of stirrers correspondingly arranged in the device box and positioned at the bottom of the conical bottle reactors, and a temperature regulating module arranged on left and right side panels of the box, wherein the front surface of the device box is provided with a main switch, a stirrer switch, a temperature display and control panel, a plurality of timers and a display panel; the device comprises a box body, and is characterized in that a top cover through hole is formed in the top cover of the box body, each top cover through hole is sealed by a threaded screw cover, a sampling tube and a vent tube are connected to the bottle mouth of the conical bottle reactor in a sealing manner, the sampling tube is connected with the corresponding top cover through hole, and the sampling tube penetrates through the front side panel and the rear side panel of the box body to be connected with the corresponding sampling injector. The invention does not need to open the device box body in the whole reaction process, minimizes the interference of sampling to the reaction condition, adopts the conduit for sampling and sampling, simplifies experimental operation ", and most of the existing devices can not warn when the temperature is abnormal, thus being inconvenient.
Disclosure of Invention
The invention aims to provide a constant temperature reaction device for preparing a high-temperature-resistant nonionic active agent, which aims to solve the problems in the background technology.
In order to achieve the above purpose, the present invention provides the following technical solutions: the utility model provides a high temperature resistant nonionic activator prepares uses constant temperature reaction unit, includes box, fixed plate, controller and attention device, the fixed plate is installed to the inner wall of box, the cooling tank is installed to the bottom of fixed plate, the diaphragm is installed to the outer wall of cooling tank, a plurality of first springs are installed at the top of diaphragm, the lifter plate is installed at the top of first spring, the trigger lever is installed to the bottom of lifter plate, trigger switch is installed at the top of diaphragm, the riser is installed at the top of diaphragm, two sets of first electric telescopic handle are installed to the outer wall of riser, the extrusion pole is installed to one end of first electric telescopic handle;
the top of the box body is provided with a controller, and the outer wall of the box body is provided with an alarm.
Preferably, the front face of the box body is provided with a display screen, the front face of the box body is provided with a plurality of control buttons, the bottom of the box body is provided with pulleys, and the outer wall of the box body is provided with a plurality of radiating holes.
Preferably, the dead lever is installed to the inner wall of box, and the reactor is installed to the outer wall of dead lever, and agitator motor is installed to the bottom of reactor, and the puddler is installed to agitator motor's output, and stirring leaf is installed to the outer wall of puddler, and temperature sensor is installed to the inside diapire of reactor.
Preferably, the outer wall of the reactor is provided with a first fixed shell, the inner wall of the first fixed shell is provided with a first coil pipe, the outer wall of the reactor is provided with a second fixed shell, and the inner wall of the second fixed shell is provided with a second coil pipe.
Preferably, the trigger switch is located at the bottom of the lifting plate, the control button is located below the display screen, the output end of the stirring motor extends into the reactor, and one end of the first coil pipe extends into the bottom of the fixing plate.
Preferably, the cooling tank is installed to the bottom of fixed plate, first water pump is installed to the bottom of fixed plate, the inlet tube is installed to the input of first water pump, and the one end of inlet tube extends into the inside of cooling tank, radiator fan is installed to the inner wall of box, the outer wall of cooling tank runs through and installs the heat dissipation post, the outer wall of heat dissipation post encircles and installs heat dissipation coil pipe, waterproof housing is installed to the inside diapire of cooling tank, the second water pump is installed to the inside diapire of waterproof housing, the top of waterproof housing is extended to the input of second water pump, the output and the one end of heat dissipation coil pipe are connected, the other end of heat dissipation coil pipe extends into the inside of cooling tank, first control valve is installed at the top of fixed plate, the top of first control valve runs through and installs the connecting pipe, the one end and the one end of connecting pipe are connected, the other end and the output of first water pump of connecting pipe are connected, the seal groove is installed to the inner wall of connecting pipe, the second electric telescopic link is installed to the inner wall of first control valve, the one end of second electric telescopic link installs the closing plate, the outer wall of closing plate encircles and installs the second spring.
Preferably, the heater is installed to the inside diapire of box, and the output of heater installs the heating pipe, and the one end of heating pipe is connected with the one end of second coil pipe, and the second control valve is installed to the outer wall of heating pipe, and the sealing block is installed to the inner wall of second control valve, and the third spring is installed to the outer wall of sealing block, and the movable plate is installed to the one end of third spring, and the shutoff piece is installed to the outer wall of movable plate, and the motor is installed at the top of second control valve, and the rotation axis is installed to the output of motor, and the cam is installed to the outer wall of rotation axis.
Preferably, the controller, the inner wall of controller is installed and is No. one board, and a plurality of No. two boards are installed at the top of No. one board, and the inlet pipe is installed in running through in the bottom of No. one board, and the automatically controlled valve is installed to the outer wall of inlet pipe.
Preferably, a plurality of warning lamps are installed to the outer wall of attention device, and a plurality of current-conducting plates are installed to the inside diapire of attention device, and the motor is installed to the inner wall of attention device, and the lead screw is installed to the output of motor, and the movable block is installed to the outer wall of lead screw, and the conducting rod is installed to the bottom of movable block, and the spacing groove is installed to the inner wall of attention device, and the one end of movable block extends into the inside of spacing groove.
Preferably, the working steps of the constant temperature reaction device are as follows:
s1, when the temperature inside the device is regulated, a temperature sensor detects the temperature change inside the reactor, when the temperature is abnormal, the temperature sensor controls the first electric telescopic rod to stretch, the first electric telescopic rod stretches to drive the extrusion rod to move, the extrusion rod moves to extrude the lifting plate, the bottom of the lifting plate descends to drive the first spring to shrink, the triggering rod at the bottom of the lifting plate descends to contact with the triggering switch, and the triggering switch controls the first control valve and the second control valve to control the flow inside the pipeline, so that the temperature is controlled, and an automatic control function is realized;
s2, when the discharging is controlled, a plurality of materials are respectively poured into the controller, the first plate can be divided into a plurality of chambers by the second plates, the electric control valve is opened to enable the materials to flow out of the feeding pipe, and the discharging amount can be controlled by the electric control valve, so that a control function is realized;
s3, pouring a plurality of materials into the reactor, driving a stirring rod to rotate by a stirring motor, and driving a stirring blade to rotate by the stirring rod, so that the materials are fully mixed, and a mixing function is realized;
s4, when the temperature is abnormal, the warning indicator starts to work, the motor drives the screw rod to rotate, the screw rod drives the moving block to move, and the moving block drives the conducting rod to contact with the conducting plate, so that the warning lamp is lighted, the moving block moves in the limiting groove, and the warning lamp is lighted to warn the staff.
The step S1 also comprises the following steps;
s11, the first water pump works to pump out cooling liquid in the cooling box, then the heat dissipation fan works to drive air to flow, then the first control valve is opened, the second electric telescopic rod contracts to drive the sealing plate to move, the sealing plate is separated from the sealing groove, the cooling liquid enters the first coil through the connecting pipe, the cooling liquid in the first coil absorbs heat in the reactor and then flows back to the cooling box, the second water pump works to pump out the cooling liquid and convey the cooling liquid to the cooling coil, and the heat dissipation fan drives air to flow, so that the heated cooling liquid is cooled rapidly;
s12, the second control valve works, the motor rotates to drive the rotating shaft to rotate, the rotating shaft rotates to drive the cam to rotate, the cam does not squeeze the movable plate any more, the movable plate moves under the action of the third spring, the movable plate drives the sealing block to move, the sealing block does not seal a channel formed by the sealing block any more, hot air enters the heating pipe, and the heater conveys the hot air into the heating pipe and the second coil pipe to heat the reactor.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the invention, an automatic adjusting function can be realized by installing the temperature sensor, when the temperature inside the device is adjusted, the temperature sensor detects the temperature change inside the reactor, when the temperature is abnormal, the temperature sensor controls the first electric telescopic rod to extend, the first electric telescopic rod extends to drive the extrusion rod to move, the extrusion rod moves to extrude the lifting plate, the bottom of the lifting plate descends to drive the first spring to contract, the triggering rod at the bottom of the lifting plate descends to be in contact with the triggering switch, so that the triggering switch controls the flow inside the first control valve and the second control valve control pipeline, and the temperature is controlled, and an automatic control function is realized;
2. according to the invention, a control function can be realized by installing the controller, when the discharging is controlled, various materials are respectively poured into the controller, the first plate can be divided into a plurality of chambers by the plurality of second plates, the electric control valve is opened to enable the materials to flow out of the feeding pipe, and the discharging quantity can be controlled by the electric control valve, so that the control function is realized;
3. according to the invention, a stirring function can be realized by installing the stirring motor, a plurality of materials are poured into the reactor, the stirring motor drives the stirring rod to rotate, and the stirring rod drives the stirring blade to rotate, so that the materials are fully mixed, and a mixing function is realized;
4. according to the invention, the warning function is realized by installing the warning device, when the temperature is abnormal, the warning device starts to work, the motor drives the screw rod to rotate, the screw rod drives the moving block to move, and the moving block drives the conducting rod to contact with the conducting plate, so that the warning lamp is lighted, the moving block moves in the limiting groove, and the warning lamp is lighted to warn the staff.
Drawings
FIG. 1 is a schematic diagram of the overall structure of the present invention;
FIG. 2 is a schematic elevational view of the present invention;
FIG. 3 is a schematic diagram of a second control valve according to the present invention;
FIG. 4 is a schematic diagram of a first control valve according to the present invention;
FIG. 5 is a schematic view of a cross plate portion of the present invention;
FIG. 6 is a schematic diagram of a controller portion of the present invention;
fig. 7 is a schematic view of a part of the structure of the alarm according to the present invention.
In the figure: 1. a case; 2. a display screen; 3. a control knob; 4. a pulley; 5. a heat radiation hole; 6. a fixed rod; 7. a reactor; 8. a stirring motor; 9. a stirring rod; 10. stirring the leaves; 11. a temperature sensor; 12. a first fixed housing; 13. a first coil; 14. a second fixed housing; 15. a second coil; 16. a fixing plate; 17. a cooling box; 18. a first water pump; 19. a heat radiation fan; 20. a heat radiation column; 21. a heat dissipation coil; 22. a waterproof case; 23. a second water pump; 24. a first control valve; 25. a connecting pipe; 26. sealing grooves; 27. a second electric telescopic rod; 28. a sealing plate; 29. a second spring; 30. a heater; 31. heating the pipe; 32. a second control valve; 33. a sealing block; 34. a third spring; 35. a moving plate; 36. a block; 37. a motor; 38. a rotation shaft; 39. a cam; 40. a cross plate; 41. a first spring; 42. a lifting plate; 43. a trigger lever; 44. triggering a switch; 45. a riser; 46. a first electric telescopic rod; 47. an extrusion rod; 48. a controller; 49. a first plate; 50. a second plate; 51. a feed pipe; 52. an electric control valve; 53. an alarm; 54. a warning light; 55. a conductive plate; 56. a motor; 57. a screw rod; 58. a moving block; 59. and a limit groove.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
In the description of the present invention, it should be noted that the directions or positional relationships indicated by the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", etc. are based on the directions or positional relationships shown in the drawings, are merely for convenience of describing the present invention and simplifying the description, and do not indicate or imply that the devices or elements referred to must have a specific direction, be configured and operated in the specific direction, and thus should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and the like, are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it should be noted that, unless explicitly specified and limited otherwise, the terms "mounted," "provided," "connected," and the like are to be construed broadly, and may be either fixedly connected, detachably connected, or integrally connected, for example; can be mechanically or electrically connected; can be directly connected or indirectly connected through an intermediate medium, and can be communication between two elements. The specific meaning of the above terms in the present invention will be understood in specific cases by those of ordinary skill in the art.
Referring to fig. 1-7, an embodiment of the present invention is provided: the utility model provides a high temperature resistant nonionic activator preparation is with constant temperature reaction unit, includes box 1, fixed plate 16, controller 48 and attention device 53, fixed plate 16 is installed to the inner wall of box 1, cooling tank 17 is installed to the bottom of fixed plate 16, diaphragm 40 is installed to the outer wall of cooling tank 17, a plurality of first springs 41 are installed at the top of diaphragm 40, lifter 42 is installed at the top of first spring 41, trigger lever 43 is installed to the bottom of lifter 42, trigger switch 44 is installed at the top of diaphragm 40, riser 45 is installed at the top of diaphragm 40, two sets of first electric telescopic handle 46 are installed to the outer wall of riser 45, extrusion rod 47 is installed to the one end of first electric telescopic handle 46, controller 48 is installed at the top of box 1, attention device 53 is installed to the outer wall of box 1, display screen 2 is installed in the front of box 1, a plurality of control buttons 3 are installed at the top of box 1, the bottom of box 1 installs the inner wall 7 of motor 7 is installed to the bottom of box 4, the inner wall 7 is installed to the inner wall 7 of box 6 is installed to the inner wall 7, and the inner wall 7 is installed to the inner wall 7 of box 7 is installed to the inner wall 7, and the inner wall 7 is installed to the inner wall 7 is equipped with 7, and the inner wall 7 is installed to the inner wall 7 of heater 7, and the inner wall 7 is installed 7.
The first fixed shell 12 is installed to the outer wall of reactor 7, and first coil pipe 13 is installed to the inner wall of first fixed shell 12, and second fixed shell 14 is installed to the outer wall of reactor 7, and second coil pipe 15 is installed to the inner wall of second fixed shell 14, trigger switch 44 is located the bottom of lifter plate 42, control button 3 is located the below of display screen 2, agitator motor 8's output extends into the inside of reactor 7, the one end of first coil pipe 13 extends into the bottom of fixed plate 16.
The cooling box 17 is arranged at the bottom of the fixed plate 16, the first water pump 18 is arranged at the bottom of the fixed plate 16, the water inlet pipe is arranged at the input end of the first water pump 18, one end of the water inlet pipe extends into the cooling box 17, the heat radiation fan 19 is arranged on the inner wall of the box body 1, the heat radiation column 20 is arranged on the outer wall of the cooling box 17 in a penetrating way, the heat radiation coil 21 is arranged on the outer wall of the heat radiation column 20 in a surrounding way, the waterproof shell 22 is arranged on the inner bottom wall of the cooling box 17, the second water pump 23 is arranged on the inner bottom wall of the waterproof shell 22, the input end of the second water pump 23 extends out of the top of the waterproof shell 22, the output end of the second water pump 23 is connected with one end of the heat radiation coil 21, the other end of the heat radiation coil 21 extends into the cooling box 17, the first control valve 24 is arranged on the top of the fixed plate 16, the connecting pipe 25 is arranged on the top of the first control valve 24 in a penetrating way, one end of the connecting pipe 25 is connected with one end of the first coil pipe 13, the other end of the connecting pipe 25 is connected with the output end of the first water pump 18, a sealing groove 26 is arranged on the inner wall of the connecting pipe 25, a second electric telescopic rod 27 is arranged on the inner wall of the first control valve 24, a sealing plate 28 is arranged on one end of the second electric telescopic rod 27, a second spring 29 is arranged on the outer wall of the sealing plate 28 in a surrounding manner, a heater 30 is arranged on the inner bottom wall of the box body 1, a heating pipe 31 is arranged at the output end of the heater 30, one end of the heating pipe 31 is connected with one end of the second coil pipe 15, a second control valve 32 is arranged on the outer wall of the heating pipe 31, a sealing block 33 is arranged on the inner wall of the second control valve 32, a third spring 34 is arranged on the outer wall of the sealing block 33, a moving plate 35 is arranged on one end of the third spring 34, a sealing block 36 is arranged on the outer wall of the moving plate 35, a motor 37 is arranged on the top of the second control valve 32, a rotary shaft 38 is mounted at the output end of the motor 37, and a cam 39 is mounted on the outer wall of the rotary shaft 38.
The controller 48, the inner wall of controller 48 installs No. one board 49, and a plurality of No. two boards 50 are installed at No. one board 49's top, and feed pipe 51 is installed in running through in No. one board 49's bottom, and automatically controlled valve 52 is installed to the outer wall of feed pipe 51.
The outer wall of the warning indicator 53 is provided with a plurality of warning lamps 54, the inner bottom wall of the warning indicator 53 is provided with a plurality of conducting plates 55, the inner wall of the warning indicator 53 is provided with a motor 56, the output end of the motor 56 is provided with a lead screw 57, the outer wall of the lead screw 57 is provided with a moving block 58, the bottom of the moving block 58 is provided with a conducting rod, the inner wall of the warning indicator 53 is provided with a limiting groove 59, and one end of the moving block 58 extends into the limiting groove 59.
The working steps of the constant temperature reaction device are as follows:
s1, when the temperature inside the device is regulated, the temperature sensor 11 detects the temperature change inside the reactor 7, when the temperature is abnormal, the temperature sensor 11 controls the first electric telescopic rod 46 to extend, the first electric telescopic rod 46 extends to drive the extrusion rod 47 to move, the extrusion rod 47 moves to extrude the lifting plate 42, the bottom of the lifting plate 42 descends to drive the first spring 41 to shrink, the trigger rod 43 at the bottom of the lifting plate 42 descends to be in contact with the trigger switch 44, so that the trigger switch 44 controls the first control valve 24 and the second control valve 32 to control the flow inside a pipeline, and the temperature is controlled, and an automatic control function is realized;
s2, when the discharging is controlled, a plurality of materials are respectively poured into the controller 48, the first plate 49 can be divided into a plurality of chambers by the second plates 50, the electric control valve 52 is opened to enable the materials to flow out of the feeding pipe 51, and the amount of the discharging material 51 can be controlled by the electric control valve 52, so that a control function is realized;
s3, pouring a plurality of materials into the reactor 7, driving the stirring rod 9 to rotate by the stirring motor 8, and driving the stirring blade 10 to rotate by the stirring rod 9 to fully mix the materials so as to realize a mixing function;
s4, when the temperature is abnormal, the warning indicator 53 starts to work, the motor 56 drives the screw rod 57 to rotate, the screw rod 57 drives the moving block 58 to move, the moving block 58 drives the conducting rod to contact with the conducting plate 55, the warning lamp 54 is enabled to be on, the moving block 58 moves in the limiting groove 59, and the warning lamp 54 is enabled to be on to warn workers.
The step S1 also comprises the following steps;
s11, a first water pump 18 works to pump out cooling liquid in the cooling box 17, then a cooling fan 19 works to drive air to flow, then a first control valve 24 is opened, a second electric telescopic rod 27 contracts to drive a sealing plate 28 to move, the sealing plate 28 is separated from a sealing groove 26, the cooling liquid enters the first coil 13 through a connecting pipe 25, heat in the cooling liquid absorption reactor 7 in the first coil 13 then flows back to the cooling box 17, the second water pump 23 works to pump out the cooling liquid to the cooling coil 21, and the cooling fan 19 drives air to flow, so that the heated cooling liquid is cooled rapidly;
s12, the second control valve 32 works, so that the motor 37 rotates to drive the rotating shaft 38 to rotate, the rotating shaft 38 rotates to drive the cam 39 to rotate, the cam 39 does not squeeze the moving plate 35 any more, the moving plate 35 moves under the action of the third spring 34, the moving plate 35 drives the plugging block 36 to move, the plugging block 36 does not plug a channel formed by the sealing block 33 any more, hot air enters the heating tube 31, and the heater 30 conveys the hot air into the heating tube 31 and the second coil 15 to heat the reactor 7.
The working principle is that when the temperature inside the device is firstly regulated, the temperature sensor 11 detects the temperature change inside the reactor 7, when the temperature is abnormal, the temperature sensor 11 controls the first electric telescopic rod 46 to stretch, the first electric telescopic rod 46 stretches to drive the extrusion rod 47 to move, the extrusion rod 47 moves to extrude the lifting plate 42, the bottom of the lifting plate 42 descends to drive the first spring 41 to shrink, the trigger rod 43 at the bottom of the lifting plate 42 descends to be contacted with the trigger switch 44, so that the trigger switch 44 controls the first control valve 24 and the second control valve 32 to control the flow of the inside of a pipeline, thereby controlling the temperature, realizing the automatic control function, the first water pump 18 works to pump the cooling liquid inside the cooling box 17, then the heat dissipation fan 19 works to drive the air to flow, then the first control valve 24 is opened, the second electric telescopic rod 27 contracts to drive the sealing plate 28 to move, the sealing plate 28 is separated from the sealing groove 26, the cooling liquid enters the first coil 13 through the connecting pipe 25, the cooling liquid in the first coil 13 absorbs heat in the reactor 7 and then flows back to the cooling box 17, the second water pump 23 works to pump the cooling liquid out and convey the cooling liquid to the cooling coil 21, the cooling fan 19 drives air to flow, the heated cooling liquid is cooled quickly, the second control valve 32 works, the motor 37 rotates to drive the rotating shaft 38 to rotate, the rotating shaft 38 rotates to drive the cam 39 to rotate, the cam 39 no longer presses the moving plate 35, the moving plate 35 moves under the action of the third spring 34, the moving plate 35 drives the blocking block 36 to move, the blocking block 36 no longer blocks a channel formed by the sealing block 33, hot air enters the inside of the heating pipe 31, the heating pipe 30 conveys the hot air to the inside of the heating pipe 31 and the second coil 15, heating the reactor 7;
when the discharging is controlled, various materials are respectively poured into the controller 48, the first plate 49 can be divided into a plurality of chambers by the plurality of second plates 50, the electric control valve 52 is opened to enable the materials to flow out of the feeding pipe 51, and the amount of the discharging material 51 can be controlled by the electric control valve 52, so that a control function is realized;
pouring a plurality of materials into the reactor 7, driving a stirring rod 9 to rotate by a stirring motor 8, and driving a stirring blade 10 to rotate by the stirring rod 9, so as to fully mix the materials and realize a mixing function;
when the temperature is abnormal, the warning indicator 53 starts to work, the motor 56 drives the screw rod 57 to rotate, the screw rod 57 drives the moving block 58 to move, the moving block 58 drives the conducting rod to be in contact with the conducting plate 55, the warning lamp 54 is turned on, the moving block 58 moves in the limiting groove 59, and the warning lamp 54 is turned on to warn the staff.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.

Claims (11)

1. The utility model provides a high temperature resistant nonionic activator preparation is with constant temperature reaction unit, includes box (1), fixed plate (16), controller (48) and warning ware (53), its characterized in that: the inner wall of the box body (1) is provided with a fixed plate (16), the bottom of the fixed plate (16) is provided with a cooling box (17), the outer wall of the cooling box (17) is provided with a transverse plate (40), the top of the transverse plate (40) is provided with a plurality of first springs (41), the top of the first springs (41) is provided with a lifting plate (42), the trigger switch (44) is arranged at the top of the transverse plate (40), the vertical plate (45) is arranged at the top of the transverse plate (40), two groups of first electric telescopic rods (46) are arranged on the outer wall of the vertical plate (45), and the extrusion rod (47) is arranged at one end of each first electric telescopic rod (46);
the top of the box body (1) is provided with a controller (48), and the outer wall of the box body (1) is provided with a warning indicator (53).
2. The thermostatic reaction device for preparing high-temperature resistant nonionic active agents according to claim 1, wherein: the front of box (1) is installed display screen (2), and a plurality of control button (3) are installed in the front of box (1), and pulley (4) are installed to the bottom of box (1), and a plurality of louvres (5) are installed to the outer wall of box (1).
3. The thermostatic reaction device for preparing high-temperature resistant nonionic active agents according to claim 1, wherein: the utility model discloses a reactor, including box (1), reactor, temperature sensor, stirring rod (9), stirring blade (10) are installed to the inner wall of box (1), reactor (7) are installed to the outer wall of dead lever (6), agitator motor (8) are installed to the bottom of reactor (7), stirring rod (9) are installed to the output of agitator motor (8), stirring blade (10) are installed to the outer wall of stirring rod (9), temperature sensor (11) are installed to the inside diapire of reactor (7).
4. A thermostatic reaction device for preparing a high temperature resistant nonionic surfactant according to claim 3, wherein: the outer wall of the reactor (7) is provided with a first fixed shell (12), the inner wall of the first fixed shell (12) is provided with a first coil pipe (13), the outer wall of the reactor (7) is provided with a second fixed shell (14), and the inner wall of the second fixed shell (14) is provided with a second coil pipe (15).
5. The thermostatic reaction device for preparing high-temperature resistant nonionic active agent according to any one of claims 1 to 4, wherein: the trigger switch (44) is located the bottom of lifter plate (42), control button (3) are located the below of display screen (2), the output of agitator motor (8) extends into inside of reactor (7), the bottom of fixed plate (16) is extended into to one end of first coil (13).
6. The thermostatic reaction device for preparing high-temperature resistant nonionic active agents according to claim 1, wherein: the cooling box (17) is installed at the bottom of the fixed plate (16), the first water pump (18) is installed at the bottom of the fixed plate (16), the water inlet pipe is installed at the input end of the first water pump (18), one end of the water inlet pipe extends into the cooling box (17), the cooling fan (19) is installed on the inner wall of the box (1), the heat radiation column (20) is installed in a penetrating manner on the outer wall of the cooling box (17), the heat radiation coil (21) is installed in a surrounding manner on the outer wall of the heat radiation column (20), the waterproof shell (22) is installed on the inner bottom wall of the cooling box (17), the second water pump (23) is installed on the inner bottom wall of the waterproof shell (22), the input end of the second water pump (23) extends out of the top of the waterproof shell (22), the output end of the second water pump (23) is connected with one end of the heat radiation coil (21), the other end of the heat radiation coil (21) extends into the inside of the cooling box (17), the first control valve (24) is installed on the top of the first control valve (24), the connecting pipe (25) is installed in a penetrating manner on the top of the first control valve (25), one end of the connecting pipe (25) is installed on the inner wall of the first connecting pipe (13), one end of the connecting pipe (25) is connected with the other end of the first connecting pipe (18), a second electric telescopic rod (27) is arranged on the inner wall of the first control valve (24), a sealing plate (28) is arranged at one end of the second electric telescopic rod (27), and a second spring (29) is arranged on the outer wall of the sealing plate (28) in a surrounding mode.
7. The thermostatic reaction device for preparing high-temperature resistant nonionic active agents according to claim 1, wherein: the inside diapire of box (1) is installed and is made hot ware (30), make the output of hot ware (30) and install heating tube (31), and the one end of heating tube (31) is connected with the one end of second coil pipe (15), second control valve (32) are installed to the outer wall of heating tube (31), sealing block (33) are installed to the inner wall of second control valve (32), third spring (34) are installed to the outer wall of sealing block (33), movable plate (35) are installed to the one end of third spring (34), shutoff piece (36) are installed to the outer wall of movable plate (35), motor (37) are installed at the top of second control valve (32), rotation axis (38) are installed to the output of motor (37), cam (39) are installed to the outer wall of rotation axis (38).
8. The thermostatic reaction device for preparing high-temperature resistant nonionic active agents according to claim 1, wherein: the device comprises a controller (48), wherein a first plate (49) is arranged on the inner wall of the controller (48), a plurality of second plates (50) are arranged on the top of the first plate (49), a feeding pipe (51) is arranged at the bottom of the first plate (49) in a penetrating mode, and an electric control valve (52) is arranged on the outer wall of the feeding pipe (51).
9. The thermostatic reaction device for preparing high-temperature resistant nonionic active agents according to claim 1, wherein: the outer wall of alarm (53) is installed a plurality of warning lights (54), a plurality of conducting plates (55) are installed to the inside diapire of alarm (53), motor (56) are installed to the inner wall of alarm (53), lead screw (57) are installed to the output of motor (56), movable block (58) are installed to the outer wall of lead screw (57), the conducting rod is installed to the bottom of movable block (58), spacing groove (59) are installed to the inner wall of alarm (53), and the inside of spacing groove (59) is extended into to the one end of movable block (58).
10. The method of using a thermostatic reaction device for preparing a high temperature resistant nonionic active agent according to any one of claims 1 to 9, characterized in that the thermostatic reaction device comprises the following working steps:
s1, when the internal temperature of the device is regulated, a temperature sensor (11) detects the temperature change in the reactor (7), when the temperature is abnormal, the temperature sensor (11) controls a first electric telescopic rod (46) to stretch, the first electric telescopic rod (46) stretches to drive a squeezing rod (47) to move, the squeezing rod (47) moves to squeeze a lifting plate (42), the bottom of the lifting plate (42) descends to drive a first spring (41) to shrink, a triggering rod (43) at the bottom of the lifting plate (42) descends to contact with a triggering switch (44), and the triggering switch (44) controls the flow in a pipeline, so that the temperature is controlled, and an automatic control function is realized;
s2, when the discharging is controlled, a plurality of materials are respectively poured into the controller (48), the first plate (49) can be divided into a plurality of chambers by the plurality of second plates (50), the electric control valve (52) is opened to enable the materials to flow out of the feeding pipe (51), and the quantity of the discharged materials (51) can be controlled through the electric control valve (52), so that a control function is realized;
s3, pouring a plurality of materials into the reactor (7), driving a stirring rod (9) to rotate by a stirring motor (8), and driving a stirring blade (10) to rotate by the stirring rod (9), so as to fully mix the materials and realize a mixing function;
s4, when the temperature is abnormal, the warning indicator (53) starts to work, the motor (56) drives the screw rod (57) to rotate, the screw rod (57) drives the moving block (58) to move, the moving block (58) drives the conducting rod to contact with the conducting plate (55) so that the warning lamp (54) is lightened, the moving block (58) moves in the limiting groove (59), and the warning lamp (54) is lightened to warn staff.
11. The method of using a thermostatic reaction device for preparing a high temperature resistant nonionic surfactant according to claim 10, wherein said step S1 further comprises the steps of;
s11, a first water pump (18) works to pump out cooling liquid in the cooling box (17), then a cooling fan (19) works to drive air to flow, then a first control valve (24) is opened, a second electric telescopic rod (27) contracts to drive a sealing plate (28) to move, the sealing plate (28) is separated from a sealing groove (26), the cooling liquid enters the first coil (13) through a connecting pipe (25), the cooling liquid in the first coil (13) absorbs heat in the reactor (7) and then flows back to the cooling box (17), a second water pump (23) works to pump out the cooling liquid to the cooling coil (21), and the cooling fan (19) drives air to flow, so that the heated cooling liquid is cooled rapidly;
s12, second control valve (32) work, make motor (37) rotate and drive rotation axis (38) to rotate, rotation axis (38) rotate and drive cam (39) to rotate, cam (39) no longer extrudes movable plate (35), movable plate (35) is moved under the effect of third spring (34), make movable plate (35) drive shutoff piece (36) remove, shutoff piece (36) no longer to the passageway shutoff that sealing piece (33) formed, make hot air enter into the inside of heating pipe (31), inside heating pipe (31) and second coil pipe (15) are carried with hot air to heater (30), heat reactor (7).
CN202310647521.5A 2023-06-02 2023-06-02 Constant temperature reaction device for preparing high-temperature-resistant nonionic active agent Pending CN116651367A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202310647521.5A CN116651367A (en) 2023-06-02 2023-06-02 Constant temperature reaction device for preparing high-temperature-resistant nonionic active agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202310647521.5A CN116651367A (en) 2023-06-02 2023-06-02 Constant temperature reaction device for preparing high-temperature-resistant nonionic active agent

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Publication Number Publication Date
CN116651367A true CN116651367A (en) 2023-08-29

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