CN116422255A - Ammonia water preparation all-in-one - Google Patents
Ammonia water preparation all-in-one Download PDFInfo
- Publication number
- CN116422255A CN116422255A CN202310331943.1A CN202310331943A CN116422255A CN 116422255 A CN116422255 A CN 116422255A CN 202310331943 A CN202310331943 A CN 202310331943A CN 116422255 A CN116422255 A CN 116422255A
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- Prior art keywords
- pipe
- ammonia
- cooling
- water
- collecting bottle
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- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 235000011114 ammonium hydroxide Nutrition 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 101
- 238000001816 cooling Methods 0.000 claims abstract description 86
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 62
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 42
- 238000001514 detection method Methods 0.000 claims abstract description 32
- 239000008233 hard water Substances 0.000 claims abstract description 24
- 238000012546 transfer Methods 0.000 claims abstract description 20
- 238000010438 heat treatment Methods 0.000 claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 claims abstract description 10
- 239000012153 distilled water Substances 0.000 claims abstract description 9
- 239000000376 reactant Substances 0.000 claims abstract description 9
- 238000009413 insulation Methods 0.000 claims description 19
- 238000012360 testing method Methods 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 17
- 239000000498 cooling water Substances 0.000 claims description 8
- 238000005192 partition Methods 0.000 claims description 7
- 239000002699 waste material Substances 0.000 claims description 3
- 238000009736 wetting Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 8
- 230000000694 effects Effects 0.000 abstract description 3
- 238000002474 experimental method Methods 0.000 abstract description 3
- 239000002918 waste heat Substances 0.000 abstract description 3
- 230000005540 biological transmission Effects 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 7
- 239000003513 alkali Substances 0.000 description 5
- 150000003863 ammonium salts Chemical class 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000010893 paper waste Substances 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/022—Preparation of aqueous ammonia solutions, i.e. ammonia water
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
The invention discloses an ammonia water preparation integrated machine, which comprises a bottom plate and also comprises an outer layer pipe, wherein the outer layer pipe is arranged on the bottom plate, and an inner layer pipe is arranged inside the outer layer pipe and is used for generating ammonia gas through reaction; the transmission assembly is arranged between the outer layer pipe and the inner layer pipe, and is used for fixing the pipe, and the fixed pipe is arranged on the bottom plate; cooling component, aqueous ammonia preparation all-in-one are different from prior art for the staff when preparing aqueous ammonia, realized the sequential preparation of distilled water and ammonia, reduced the occupation space when preparing the experiment, utilize transfer assembly can utilize the heat when heating the hard water, realizes the preheating work to the respectively waste heat of reactant and the later hard water of adding, utilizes cooling component can cool off vapor and ammonia, has improved the cooling effect, utilizes detection component can detect the interface position on the collecting bottle, avoids ammonia to appear leaking the condition, the timely discovery of operating personnel of being convenient for.
Description
Technical Field
The invention relates to the technical field of ammonia water preparation, in particular to an ammonia water preparation integrated machine.
Background
Ammonia water is an aqueous solution of ammonia gas, is colorless and transparent, has pungent smell, is easy to dissolve in water and ethanol, is easy to volatilize, has the universality of partial alkali, is prepared by introducing ammonia gas into water, is toxic, has irritation and corrosiveness to eyes, nose and skin, and can suffocate people, and the preparation method of the ammonia water in a laboratory comprises the following steps: 1. heating hard water, cooling water vapor to prepare distilled water, and then preparing ammonia gas, wherein ammonium salt and alkali are adopted for mixing and heating during the preparation; 2. collecting and cooling the gas, and then introducing the gas into water to form ammonia water; 3. treating the tail gas and detecting whether the connecting position leaks air or not; 4. the prepared ammonia water is bottled by a brown bottle, and when the prepared ammonia water is in actual use, various equipment needs to be assembled in the existing ammonia water preparation process, the steps are complicated, the ammonia water preparation efficiency is low, the equipment intervals are relatively separated, the occupied space is relatively large, and therefore, a laboratory or small-batch ammonia water preparation all-in-one machine is provided.
Disclosure of Invention
The invention aims to provide an ammonia water preparation integrated machine so as to solve the problems in the background technology.
In order to achieve the above purpose, the present invention provides the following technical solutions: the ammonia water preparation all-in-one machine comprises a bottom plate and also comprises an outer layer pipe, wherein the outer layer pipe is arranged on the bottom plate and is used for storing hard water; the inner layer pipe is arranged inside the outer layer pipe and is used for generating ammonia through reaction; the transmission assembly is arranged between the outer layer pipe and the inner layer pipe, and is used for fixing the pipe, and the fixed pipe is arranged on the bottom plate; the cooling assembly is arranged in the fixed pipe, and the collecting bottle is arranged on the bottom plate; the detection component is arranged at the top of the collecting bottle, is different from the prior art, ensures that staff can prepare distilled water and ammonia sequentially when preparing ammonia water, reduces the occupied space during preparation experiments, utilizes the transfer component to utilize heat generated during heating of hard water, realizes the preheating work of the reactant by waste heat and the subsequently added hard water respectively, utilizes the cooling component to cool water vapor and ammonia, improves the cooling effect, and utilizes the detection component to detect the interface position on the collecting bottle, so that the leakage condition of ammonia gas is avoided, and the timely discovery of operators is facilitated.
Preferably, the transfer assembly comprises a first electric furnace arranged on a bottom plate and used for heating an outer layer pipe, a middle layer pipe is arranged in the outer layer pipe, a heat insulation layer is arranged in the middle layer pipe, a filling layer is arranged between the middle layer pipe and the heat insulation layer, heat generated when hard water is heated can be utilized by utilizing the filling layer, the inner layer pipe is arranged in the heat insulation layer, and a second electric furnace used for heating the inner layer pipe is arranged in the heat insulation layer;
the heat insulation layer is provided with a preheating piece, and reactants can be respectively preheated by the preheating piece.
Preferably, the preheating piece comprises two transfer pipes which are arranged in the filling layer and used for feeding, the transfer pipes all penetrate through the heat insulation layer and extend into the inner layer pipe, control valves are arranged on the transfer pipes, and storage pipes are arranged at the tops of the transfer pipes.
Preferably, the cooling assembly comprises a liquid inlet pipe arranged at the front end of the fixed pipe and a liquid outlet pipe arranged at the rear end of the fixed pipe, a partition plate is arranged in the fixed pipe, the fixed pipe is divided into a water vapor cooling area and an ammonia cooling area by using the partition plate, a fixed plate is arranged at the end part of the liquid inlet pipe, a first cooling piece is arranged in the water vapor cooling area, and the water vapor can be cooled in the water vapor cooling area by using the first cooling piece;
the ammonia cooling zone is provided with a second cooling piece, and the ammonia is cooled by the second cooling piece.
Preferably, the first cooling piece comprises a steam pipe which is arranged in the steam cooling area and communicated with the outer layer pipe, a first discharge port is arranged at the end part of the steam pipe, and the first discharge port is communicated with the collecting bottle;
the fixing plate is provided with a first through hole, one side, close to the fixing plate, of the steam cooling area of the fixing pipe is communicated with the first through hole, and cooling water flow for the steam pipe is formed through the first through hole and the liquid outlet pipe.
Preferably, the second cooling piece comprises an ammonia pipe arranged between the fixed pipe and the inner pipe, two ends of the ammonia pipe are respectively communicated with the fixed pipe and the inner pipe, a second exhaust port is arranged at the end part of the ammonia cooling area of the fixed pipe, and the second exhaust port is communicated with the collecting bottle;
a plurality of second through holes are uniformly formed in the fixing plate, a plurality of cooling pipes are uniformly arranged in the ammonia cooling area of the fixing pipe, the cooling pipes are respectively communicated with the adjacent second through holes, one end, away from the second through holes, of each cooling pipe is communicated with the water vapor cooling area, and cooling water flows for ammonia are formed through the second through holes, the cooling pipes and the liquid outlet pipe.
Preferably, the detection assembly comprises an auxiliary pipe arranged on the collecting bottle, an air bag for temporarily storing air in the collecting bottle and ammonia which is not dissolved in distilled water is arranged at the end part of the auxiliary pipe, a fixed cavity is arranged on the collecting bottle, a detection piece is arranged in the fixed cavity, and the position of an interface on the collecting bottle is detected by the detection piece;
the collecting bottle is provided with a guide frame, the guide frame is provided with a driving piece, the driving piece is matched with the detecting piece for use, and after air intake of each air bag, the detecting piece can be driven to automatically start working by the driving piece.
Preferably, the detecting piece comprises a main shaft rotatably arranged in the fixed cavity, a rotating frame body is arranged on the main shaft, a plurality of detecting test papers are arranged in the rotating frame body, a water storage tank is arranged on the collecting bottle, and the middle part of the rotating frame body is of a hollow structure, so that the detecting test papers are wetted by contact with water before detection;
the collecting bottle is provided with a waste test paper box, and the collecting bottle is provided with a cutter.
Preferably, the driving piece comprises a shifting seat which is arranged in the guide frame in a sliding manner, one side of the shifting seat, which is close to the air bag, is higher than the other side of the shifting seat, a rotating shaft is rotatably arranged in the shifting seat, a deflector rod is arranged on the rotating shaft, a torsion spring is arranged on the rotating shaft, two ends of the torsion spring are respectively connected with the deflector rod and the shifting seat, and the end part of the deflector rod is in a protruding structure;
the rotary plate is arranged on one side of the rotary shaft extending to the outside of the fixed cavity, a plurality of first magnets are arranged on the rotary plate, a second magnet for absorbing the first magnets is arranged at the top of the collecting bottle, and a reset spring is arranged on the guide frame.
Preferably, protruding blocks are arranged at the middle positions of the rotating frame body.
The invention has at least the following beneficial effects:
compared with the prior art, when preparing aqueous ammonia for the staff has realized the successive preparation of distilled water and ammonia, has reduced the occupation space when preparing the experiment, utilizes transfer unit can utilize the heat when heating the hard water, realizes the preheating work to the respectively waste heat and the follow-up hard water of adding of reactant, utilizes cooling unit can cool off vapor and ammonia, has improved the cooling effect, utilizes detection unit can detect the interface position on the collecting bottle, avoids ammonia to appear leaking the condition, the timely discovery of operating personnel of being convenient for.
Drawings
FIG. 1 is a schematic diagram of the overall structure of the present invention;
FIG. 2 is a schematic view of the structure of FIG. 1 in another orientation in accordance with the present invention;
FIG. 3 is a schematic view of the partial cross-section of FIG. 1 in accordance with the present invention;
FIG. 4 is an enlarged schematic view of the structure of the area A of the present invention;
FIG. 5 is an enlarged schematic view of the structure of the area B of the present invention;
FIG. 6 is a schematic plan view of a portion of the structure of FIG. 1 according to the present invention.
FIG. 7 is a schematic view of the structure of the fixing tube and the ammonia tube of the present invention;
FIG. 8 is a schematic view of the structure of the collection bottle of the present invention;
FIG. 9 is an enlarged schematic view of the structure of the C area of the present invention;
FIG. 10 is a schematic view of a stationary chamber structure according to the present invention;
FIG. 11 is an exploded view of a portion of the structure of FIG. 10 in accordance with the present invention.
FIG. 12 is a schematic view of a turret body structure according to the present invention;
fig. 13 is a schematic view of the driving member structure of the present invention.
In the figure: 1. a bottom plate; 2. a transfer assembly; 21. an electric furnace I; 22. a middle layer tube; 23. a thermal insulation layer; 24. a filling layer; 25. an electric furnace II; 3. a preheating piece; 31. a transfer tube; 32. a control valve; 33. a storage tube; 4. a cooling assembly; 41. a liquid inlet pipe; 42. a liquid outlet pipe; 43. a partition plate; 44. a water vapor cooling zone; 45. an ammonia cooling zone; 46. a fixing plate; 5. a first cooling member; 51. a steam pipe; 52. a first discharge port; 53. a first through hole; 6. a second cooling member; 61. an ammonia gas pipe; 62. a second discharge port; 63. a second through hole; 64. a cooling tube; 7. a detection assembly; 71. an auxiliary tube; 72. an air bag; 73. a fixed cavity; 74. a guide frame; 8. a detecting member; 81. a main shaft; 82. a rotating frame body; 83. detecting test paper; 84. a water storage tank; 85. waste paper boxes; 86. a cutter; 9. a driving member; 91. a shift seat; 92. a rotation shaft; 93. a deflector rod; 94. a torsion spring; 95. a rotating disc; 96. a first magnet; 97. a second magnet; 98. a return spring; 10. an outer layer tube; 11. an inner layer tube; 12. a fixed tube; 13. a collection bottle; 14. protruding blocks.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Referring to fig. 1-13, the present invention provides a technical solution:
an ammonia water preparation all-in-one machine comprises a bottom plate 1 and also comprises
The outer layer pipe 10 is arranged on the bottom plate 1 and used for storing hard water, the outer layer pipe 10 is provided with a water inlet pipe and used for filling the hard water into the inner part, a valve is arranged on the outer layer pipe 10 and used for preventing water vapor from being discharged from the valve, a drain pipe is arranged at the bottom and used for discharging the reacted hard water, and zeolite is arranged in the outer layer pipe 10 and used for preventing bumping;
an inner layer pipe 11, wherein the inner layer pipe 11 is arranged inside the outer layer pipe 10 and is used for generating ammonia gas through reaction, and a discharge pipe is arranged at the bottom of the inner layer pipe 11 and is used for discharging residual substances after the reaction;
the transfer component 2 is arranged between the outer layer pipe 10 and the inner layer pipe 11, the transfer component 2 can be used for utilizing heat generated when the hard water is heated, the reaction sequence is that the hard water is heated firstly, the filling layer 24 is gradually heated but slower than the hard water, reactants are preheated by the heat of the filling layer 24, then ammonia gas is produced by mixing and heating ammonium salt and alkali, wherein the alkali is powder and is added into the inner layer pipe 11 at one time, the ammonium salt adopts a solution mixed by water, in the process, the opening size is regulated by controlling the valve 32, the flow speed is controlled, reactants are continuously preheated by the filling layer 24 in the process, substances of the outer layer pipe 10 and the inner layer pipe 11 are discharged after the reaction is completed, then the hard water is added again, and the residual heat of the filling layer 24 can be transferred to the hard water at the moment;
the transfer assembly 2 comprises an electric furnace I21 arranged on the bottom plate 1 and used for heating the outer layer pipe 10, a middle layer pipe 22 is arranged in the outer layer pipe 10, a heat insulation layer 23 is arranged in the middle layer pipe 22, a filling layer 24 is arranged between the middle layer pipe 22 and the heat insulation layer 23, heat generated when hard water is heated can be utilized by the filling layer 24, the inner layer pipe 11 is arranged in the heat insulation layer 23, an electric furnace II 25 used for heating the inner layer pipe 11 is arranged in the heat insulation layer 23, the filling layer 24 adopts water, but is not limited to, and the heat insulation layer 23 adopts polyurethane foaming materials;
the heat insulating layer 23 is provided with a preheating piece 3, and reactants can be respectively preheated by the preheating piece 3;
the preheating piece 3 comprises two transfer pipes 31 which are arranged in the filling layer 24 and used for feeding, the transfer pipes 31 penetrate through the heat insulation layer 23 and extend into the inner layer pipe 11, control valves 32 are arranged on the transfer pipes 31, and storage pipes 33 are arranged at the tops of the transfer pipes 31;
a fixing tube 12, the fixing tube 12 being provided on the base plate 1;
the cooling component 4 is arranged in the fixed pipe 12, and the cooling component 4 can be used for cooling the water vapor and the ammonia gas;
the cooling assembly 4 comprises a liquid inlet pipe 41 arranged at the front end of the fixed pipe 12 and a liquid outlet pipe 42 arranged at the rear end of the fixed pipe 12, a partition plate 43 is arranged in the fixed pipe 12, the fixed pipe 12 is divided into a water vapor cooling zone 44 and an ammonia cooling zone 45 by the partition plate 43, a fixed plate 46 is arranged at the end part of the liquid inlet pipe 41, a first cooling piece 5 is arranged in the water vapor cooling zone 44, and the water vapor can be cooled in the water vapor cooling zone 44 by the first cooling piece 5;
the first cooling element 5 comprises a steam pipe 51 which is arranged in the steam cooling zone 44 and is communicated with the outer layer pipe 10, a first discharge outlet 52 is arranged at the end part of the steam pipe 51, and the first discharge outlet 52 is communicated with the collecting bottle 13;
the fixing plate 46 is provided with a first through hole 53, the water vapor cooling area 44 of the fixing pipe 12 is communicated with the first through hole 53 at one side close to the fixing plate 46, and cooling water flow for the water vapor pipe 51 is formed through the first through hole 53 and the liquid outlet pipe 42;
the ammonia cooling region 45 is provided with a second cooling member 6, and the ammonia is cooled by the second cooling member 6;
the second cooling element 6 comprises an ammonia pipe 61 arranged between the fixed pipe 12 and the inner pipe 11, two ends of the ammonia pipe 61 are respectively communicated with the fixed pipe 12 and the inner pipe 11, a second exhaust port 62 is arranged at the end part of an ammonia cooling region 45 of the fixed pipe 12, and the second exhaust port 62 is communicated with the collecting bottle 13;
the fixing plate 46 is uniformly provided with a plurality of second through holes 63, the ammonia cooling area 45 of the fixing pipe 12 is uniformly provided with a plurality of cooling pipes 64, the plurality of cooling pipes 64 are respectively communicated with the adjacent second through holes 63, one end of each cooling pipe 64 far away from each second through hole 63 is communicated with the water vapor cooling area 44, and cooling water flow for ammonia is formed through the plurality of second through holes 63, the cooling pipes 64 and the liquid outlet pipe 42;
a collection bottle 13, the collection bottle 13 being arranged on the base plate 1;
the detection assembly 7 is arranged at the top of the collecting bottle 13, and the detection assembly 7 can be used for detecting the interface position on the collecting bottle 13 so as to avoid the leakage of ammonia gas;
the detection assembly 7 comprises an auxiliary pipe 71 arranged on the collecting bottle 13, an air bag 72 for temporarily storing air and ammonia which is not dissolved in distilled water in the collecting bottle 13 is arranged at the end part of the auxiliary pipe 71, a fixed cavity 73 is arranged on the collecting bottle 13, a detection piece 8 is arranged in the fixed cavity 73, and the interface position on the collecting bottle 13 is detected by the detection piece 8;
the detecting piece 8 comprises a main shaft 81 rotatably arranged in a fixed cavity 73, a rotating frame 82 is arranged on the main shaft 81, a plurality of detecting test papers 83 are arranged in the rotating frame 82, a water storage tank 84 is arranged on the collecting bottle 13, and the middle part of the rotating frame 82 is of a hollow structure, so that the detecting test papers 83 are wetted by contact with water before detection, and in the scheme, the detecting test papers 83 are automatically arranged according to use, preferably 6 detecting test papers 83 are prevented from being exposed outside for a long time, and the detecting accuracy is prevented from being influenced;
the collecting bottle 13 is provided with a waste test paper box 85, and the collecting bottle 13 is provided with a cutter 86;
the protruding blocks 14 are arranged in the middle of the rotating frame 82, the protruding blocks 14 are utilized to facilitate the contact wetting of the detection test paper 83 with water, meanwhile, the separation of the test paper is realized by matching with the cutter 86, the wetted detection test paper 83 is slightly heavy, the protruding blocks and the rotating frame 82 cannot be attached, and the test paper is easy to scratch, so that the accuracy of the subsequent detection test paper 83 cannot be affected;
the collecting bottle 13 is provided with a guide frame 74, the guide frame 74 is provided with a driving piece 9, the driving piece 9 is matched with the detecting piece 8 for use, and after the air bag 72 is in air every time, the detecting piece 8 can be driven to automatically start working by the driving piece 9;
the driving piece 9 comprises a shifting seat 91 which is arranged in the guide frame 74 in a sliding manner, one side of the shifting seat 91, which is close to the air bag 72, is higher than the other side, a rotating shaft 92 is rotationally arranged in the shifting seat 91, a deflector rod 93 is arranged on the rotating shaft 92, a torsion spring 94 is arranged on the rotating shaft 92, two ends of the torsion spring 94 are respectively connected with the deflector rod 93 and the shifting seat 91, and the end part of the deflector rod 93 is in a protruding structure;
a rotary disk 95 is provided on one side of the rotary shaft 92 extending to the outside of the fixed cavity 73, a plurality of first magnets 96 are provided on the rotary disk 95, a second magnet 97 for attracting the first magnets 96 is provided on the top of the collecting bottle 13, and a return spring 98 is provided on the guide frame 74.
When the device is used, the reaction sequence is that hard water is firstly heated, water vapor enters the water vapor pipe 51, after being cooled by water, the water vapor is discharged into the collecting bottle 13 from the first discharge port 52, at the moment, the filling layer 24 is gradually heated, but slower than the heating of the hard water, reactants are preheated by the heat of the filling layer 24, then ammonia gas is produced by the mixed heating reaction of ammonium salt and alkali, in the process, the ammonia gas enters the fixed pipe 12 through the ammonia pipe 61, after the cooling of the water in the cooling pipe 64, distilled water is introduced into the distilled water through the second discharge port 62 to form ammonia water, at the moment, air in the collecting bottle 13 and unreacted ammonia gas are discharged into the air bag 72 through the auxiliary pipe 71, the air bag is driven to be inflated, the shifting seat 91 is pushed to be shifted previously, the shifting seat 91 is pushed to shift the magnet 96 under the limit of the shifting seat 93, at the moment, the rotating disc 95 and the rotating shaft 92 rotate, then the internal detection test paper 83 is wetted and conveyed to the connecting position on the collecting bottle 13 for detection, after the one-stage reaction is finished, the air bag 72 is gradually reduced, gas in the hard 72 is better extruded under the cooperation of the reset spring 98, the condition, the air in the hard 72 is enabled to be filled with the hard water layer, the water is discharged into the air bag 72 through the auxiliary pipe 71, the air bag is enabled to be filled with the water, the water layer is filled with the water layer, the water is filled into the outer layer 11, the outer layer is filled with the water layer, and the water layer is filled with the water layer is 11, and the outer layer is filled with the water layer, and the water layer is 11, and the water is filled.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (10)
1. The utility model provides an aqueous ammonia preparation all-in-one, includes bottom plate (1), its characterized in that: and also comprises
An outer layer pipe (10), the outer layer pipe (10) being arranged on the bottom plate (1) for storing hard water;
an inner layer pipe (11), wherein the inner layer pipe (11) is arranged inside the outer layer pipe (10) and is used for generating ammonia through reaction;
the transfer assembly (2) is arranged between the outer layer pipe (10) and the inner layer pipe (11), and the heat generated when the hard water is heated can be utilized by utilizing the transfer assembly (2);
a fixed pipe (12), wherein the fixed pipe (12) is arranged on the bottom plate (1);
a cooling assembly (4), wherein the cooling assembly (4) is arranged in the fixed pipe (12), and the cooling assembly (4) can be used for cooling water vapor and ammonia;
a collection bottle (13), wherein the collection bottle (13) is arranged on the bottom plate (1);
the detection assembly (7), detection assembly (7) set up at collecting bottle (13) top, utilize detection assembly (7) can detect the interface position on collecting bottle (13), avoid ammonia to appear leaking the condition.
2. The ammonia water production all-in-one machine according to claim 1, wherein: the transfer assembly (2) comprises an electric furnace I (21) which is arranged on the bottom plate (1) and used for heating the outer layer pipe (10), a middle layer pipe (22) is arranged in the outer layer pipe (10), a heat insulation layer (23) is arranged in the middle layer pipe (22), a filling layer (24) is arranged between the middle layer pipe (22) and the heat insulation layer (23), heat generated when hard water is heated can be utilized by utilizing the filling layer (24), the inner layer pipe (11) is arranged in the heat insulation layer (23), and an electric furnace II (25) which is used for heating the inner layer pipe (11) is arranged in the heat insulation layer (23);
the heat insulation layer (23) is provided with a preheating piece (3), and reactants can be respectively preheated by the preheating piece (3).
3. The ammonia water production all-in-one machine according to claim 2, wherein: the preheating piece (3) comprises two conveying pipes (31) which are arranged in the filling layer (24) and used for feeding, the conveying pipes (31) all penetrate through the heat insulation layer (23) and extend into the inner-layer pipe (11), control valves (32) are arranged on the conveying pipes (31), and storage pipes (33) are arranged at the tops of the conveying pipes (31).
4. An ammonia water preparation all-in-one machine according to claim 3, wherein: the cooling assembly (4) comprises a liquid inlet pipe (41) arranged at the front end of the fixed pipe (12) and a liquid outlet pipe (42) arranged at the rear end of the fixed pipe (12), a partition plate (43) is arranged in the fixed pipe (12), the fixed pipe (12) is divided into a water vapor cooling zone (44) and an ammonia cooling zone (45) by the partition plate (43), a fixed plate (46) is arranged at the end part of the liquid inlet pipe (41), a first cooling piece (5) is arranged in the water vapor cooling zone (44), and water vapor can be cooled in the water vapor cooling zone (44) by the first cooling piece (5);
the ammonia cooling zone (45) is provided with a second cooling member (6), and the ammonia is cooled by the second cooling member (6).
5. The ammonia water production all-in-one machine according to claim 4, wherein: the first cooling piece (5) comprises a steam pipe (51) which is arranged in the steam cooling area (44) and is communicated with the outer layer pipe (10), a first discharge outlet (52) is arranged at the end part of the steam pipe (51), and the first discharge outlet (52) is communicated with the collecting bottle (13);
the fixing plate (46) is provided with a first through hole (53), one side, close to the fixing plate (46), of the steam cooling area (44) of the fixing pipe (12) is communicated with the first through hole (53), and cooling water flow for the steam pipe (51) is formed through the first through hole (53) and the liquid outlet pipe (42).
6. The ammonia water production all-in-one machine according to claim 5, wherein: the second cooling piece (6) comprises an ammonia pipe (61) arranged between the fixed pipe (12) and the inner pipe (11), two ends of the ammonia pipe (61) are respectively communicated with the fixed pipe (12) and the inner pipe (11), a second exhaust port (62) is arranged at the end part of an ammonia cooling area (45) of the fixed pipe (12), and the second exhaust port (62) is communicated with the collecting bottle (13);
a plurality of second through holes (63) are uniformly formed in the fixing plate (46), a plurality of cooling pipes (64) are uniformly arranged in an ammonia cooling area (45) of the fixing pipe (12), the cooling pipes (64) are respectively communicated with adjacent second through holes (63), one ends, far away from the second through holes (63), of the cooling pipes (64) are communicated with the water vapor cooling area (44), and cooling water flows for ammonia are formed through the second through holes (63), the cooling pipes (64) and the liquid outlet pipe (42).
7. The ammonia water production all-in-one machine according to claim 6, wherein: the detection assembly (7) comprises an auxiliary pipe (71) arranged on the collecting bottle (13), an air bag (72) for temporarily storing air and ammonia which is not dissolved in distilled water in the collecting bottle (13) is arranged at the end part of the auxiliary pipe (71), a fixed cavity (73) is arranged on the collecting bottle (13), a detection piece (8) is arranged in the fixed cavity (73), and the interface position on the collecting bottle (13) is detected by the detection piece (8);
be provided with leading truck (74) on collecting bottle (13), be provided with driving piece (9) on leading truck (74), driving piece (9) and detection piece (8) cooperate the use, after gasbag (72) are admitted air at every turn, utilize driving piece (9) can order about detection piece (8) automatic start work.
8. The ammonia water production all-in-one machine according to claim 7, wherein: the detection part (8) comprises a main shaft (81) which is rotatably arranged in a fixed cavity (73), a rotating frame body (82) is arranged on the main shaft (81), a plurality of detection test papers (83) are arranged in the rotating frame body (82), a water storage tank (84) is arranged on the collecting bottle (13), and the middle parts of the rotating frame body (82) are hollow structures, so that the detection test papers (83) are in contact with water for wetting before detection;
the waste test paper box (85) is arranged on the collecting bottle (13), and a cutter (86) is arranged on the collecting bottle (13).
9. The ammonia water production all-in-one machine according to claim 8, wherein: the driving piece (9) comprises a shifting seat (91) which is arranged in the guide frame (74) in a sliding manner, one side of the shifting seat (91) close to the air bag (72) is higher than the other side, a rotating shaft (92) is rotationally arranged on the shifting seat (91), a deflector rod (93) is arranged on the rotating shaft (92), a torsion spring (94) is arranged on the rotating shaft (92), two ends of the torsion spring (94) are respectively connected with the deflector rod (93) and the shifting seat (91), and the end part of the deflector rod (93) is of a protruding structure;
the rotary shaft (92) extends to one side outside the fixed cavity (73) and is provided with a rotary disk (95), be provided with a plurality of first magnets (96) on rotary disk (95), collecting bottle (13) top is provided with carries out absorptive magnet two (97) to first magnet (96), be provided with reset spring (98) on leading truck (74).
10. The ammonia water production all-in-one machine according to claim 9, wherein: protruding blocks (14) are arranged in the middle of the rotating frame body (82).
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| CN202310331943.1A CN116422255B (en) | 2023-03-28 | 2023-03-28 | Ammonia water preparation all-in-one |
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Denomination of invention: An ammonia water preparation all-in-one machine Granted publication date: 20230912 Pledgee: Shandong Tengzhou rural commercial bank Limited by Share Ltd. SME branch Pledgor: Tengzhou Xiangrun Chemical Co.,Ltd. Registration number: Y2024980008231 |