CN116406778A - Method for quickly preparing pickled Chinese cabbage with assistance of mixed gas - Google Patents

Method for quickly preparing pickled Chinese cabbage with assistance of mixed gas Download PDF

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Publication number
CN116406778A
CN116406778A CN202310307290.3A CN202310307290A CN116406778A CN 116406778 A CN116406778 A CN 116406778A CN 202310307290 A CN202310307290 A CN 202310307290A CN 116406778 A CN116406778 A CN 116406778A
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fermentation
gas
fermentation device
vegetables
chinese cabbage
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王刚
徐海涛
李佳智
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Zhijin Technology Dalian Co ltd
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Zhijin Technology Dalian Co ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L19/00Products from fruits or vegetables; Preparation or treatment thereof
    • A23L19/20Products from fruits or vegetables; Preparation or treatment thereof by pickling, e.g. sauerkraut or pickles
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/90Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation

Abstract

The invention discloses a method for quickly preparing pickled Chinese cabbage by using mixed gas, and belongs to the technical field of pickled Chinese cabbage preparation. The method mainly comprises the following steps: cleaning fresh vegetables, adding seasonings, uniformly mixing, loading into a fermentation device, sealing the fermentation device, introducing carbon dioxide gas into the fermentation device through a gas replacement valve to replace air in the fermentation device and the vegetables to be fermented, enabling the volume content of oxygen in a fermentation tank to be less than 0.1% through repeated exhaust-inflation operation, then further isolating air by filling inert gas, closing the gas replacement valve, fermenting the fermentation device at the environment temperature of 20-35 ℃, and performing exhaust treatment through an automatic air pressure regulating valve on the fermentation device when the pressure is too high in the fermentation process, and completing fermentation after 24-72 hours. The method can obviously reduce nitrite production, shorten fermentation time, and effectively avoid the problems of vegetable decay and the like.

Description

Method for quickly preparing pickled Chinese cabbage with assistance of mixed gas
Technical Field
The invention belongs to the technical field of pickled Chinese cabbage preparation, and particularly relates to a method for quickly preparing pickled Chinese cabbage by using mixed gas.
Background
The pickled Chinese cabbage is a common pickled vegetable which is very popular in daily life, common vegetable raw materials comprise Chinese cabbage, cucumber, cabbage, onion, celery, radish, turnip, beet, spring lettuce, tender ginger, green hyacinth bean, sword bean, green tomato and the like, the conventional preparation method is that the vegetable raw materials are placed in a container, and after salt is sprayed, the vegetables are pressed into salt water for long-term soaking and pickling, bacterial growth is effectively inhibited through pickling treatment, the quality guarantee period of food materials is prolonged, and the pickled Chinese cabbage is good in taste.
The fermentation process of the natural vegetable strain comprises two stages: (1) starting fermentation: in this stage, aerobic microorganisms such as spoilage bacteria, acid-resistant escherichia coli, yeast and the like are active due to the existence of oxygen; the neutral environment (ph=7) provides suitable conditions for nitrate in vegetables to nitrite by nitrate reductase; the putrefying bacteria and nitrate reductase act together to hydrolyze and convert proteins into nitrite; during the process, abnormal lactic acid fermentation is carried out simultaneously to generate fermentation products such as organic acid, ethanol, carbon dioxide and the like, and along with the consumption of oxygen and the continuous accumulation of the organic acid, anaerobic and acidic environments suitable for the activity of lactic acid bacteria are gradually formed, anaerobic and acid-resistant lactic acid bacteria take the dominant role, and the fermentation enters a second stage; (2) lactic acid fermentation: in an anaerobic and low pH fermentation environment formed by initial fermentation, dominant lactobacillus performs positive lactic acid fermentation, and a large amount of acid is produced to further reduce the pH value of fermentation liquor, so that nitrate reductase is deactivated; at H + The nitrite formed in the first stage is further degraded and reduced, and when the pH value is reduced to below 3.8, the fermentation enters the maturation stage, and the activities of aerobic and non-acid-resistant microorganisms are inhibited or even killed.
Aiming at the problems of nitrite production, long fermentation time, improper operation, easy decay and the like in the traditional pickled Chinese cabbage preparation process, a plurality of improvement methods have been developed, and the common method is that measures for inhibiting putrefying bacteria and reducing pH value, such as sodium benzoate (fresh pickled Chinese cabbage), acetic acid, citric acid, ascorbic acid and the like, are added, so that the measures are effective for preventing food from being decayed, but the influence of residues on health and taste is to be examined.
Disclosure of Invention
In view of the above, the invention aims to provide a method for rapidly preparing pickled Chinese cabbage by using mixed gas, which can remarkably reduce nitrite production, shorten fermentation time and effectively avoid the problems of vegetable decay and the like.
The invention aims at realizing the following steps:
the invention provides a method for quickly preparing pickled Chinese cabbage by using mixed gas, which mainly comprises the following steps:
(1) Cleaning fresh vegetables, adding flavoring, mixing, loading into fermentation device, and sealing the fermentation device;
(2) Firstly, introducing carbon dioxide gas into a fermentation device through a gas replacement valve to replace air in the fermentation device and vegetables to be fermented, enabling the volume content of oxygen in a fermentation tank to be less than 0.1% through repeated exhaust-inflation operation, then, filling inert gas to further isolate the air, and closing the gas replacement valve;
(3) Fermenting the fermentation device at the ambient temperature of 20-35 ℃, and when the pressure is too high in the fermentation process, performing exhaust treatment through an automatic air pressure regulating valve on the fermentation device, and completing the fermentation after lasting 24-72 hours.
Based on the above technical scheme, further, the vegetables in step (1) include cabbage, cucumber, cabbage, onion, celery, radish, turnip, beet, spring lettuce, tender ginger, tender lentil, sword bean and green tomato.
Based on the technical scheme, the flavoring in the step (1) comprises salt, and the adding amount of the flavoring is 0.1-0.5% of the weight of the vegetables.
Based on the technical scheme, further, the fermentation device in the step (1) comprises a fermentation tank and a fermentation bag.
Based on the technical scheme, further, the material of fermentation cylinder is stainless steel material, and the material of fermentation bag is polyethylene or polyvinyl chloride material.
Based on the above technical scheme, further, the inert gas in the step (2) is one or more than two of nitrogen, argon and helium.
Based on the technical scheme, in the step (2), after the gas replacement valve is closed, the volume percentage of carbon dioxide in the mixed gas in the fermentation device is 10-80%.
Based on the technical scheme, further, the fermentation temperature in the step (3) is 25-30 ℃.
Based on the technical scheme, further, the gas exhausted by the fermentation device in the step (3) through the automatic air pressure regulating valve is connected with the gas collecting and purifying device through a pipeline, and is discharged to the atmosphere after being purified.
Compared with the prior art, the invention has the following beneficial effects:
1. the invention optimizes the traditional natural fermentation process conditions by adopting natural strains, and the optimization principle is that firstly, carbon dioxide is adopted to expel oxygen in a fermentation container and food materials to be fermented, and the property that carbon dioxide is dissolved to form carbonic acid is utilized to reduce the pH value of liquid, and meanwhile, anaerobic and acidic environments which are beneficial to the life activities of lactic acid bacteria are produced; under this environment, the activity of aerobic bacteria such as spoilage bacteria is suppressed; the activity of nitrate reductase is reduced; the nitrite is quickly reduced and degraded in the form of nitric oxide, the anaerobic and acidic fermentation environment produced by carbon dioxide solves the problems of nitrite production, food decay and the like in the traditional process of starting the fermentation stage, then inert gas is introduced to completely isolate oxygen, further inhibit the activity of aerobic bacteria such as putrefying bacteria and the like, plays a better role in protection, and finally, the fermentation time is greatly shortened by providing proper temperature for lactic acid fermentation.
2. The invention detects the fermented product, the pH is as low as 3.0-3.1, the nitrite content is less than 1.0mg/Kg, the content of the fermented active microorganism is far less than the national standard, and the content of the fermented active microorganism can reach 1.8X10 6 The CFU/mL can obviously shorten the fermentation time, improve the quality of pickled Chinese cabbage, shorten the fermentation time of 30-40 days in the traditional process to 1-3 days, and is very suitable for large-scale industrial production.
Detailed Description
The following detailed description of the invention is provided in connection with examples, but the implementation of the invention is not limited thereto, and it is obvious that the examples described below are only some examples of the invention, and that it is within the scope of protection of the invention to those skilled in the art to obtain other similar examples without inventive faculty.
Example 1
The embodiment provides a method for quickly preparing pickled Chinese cabbage by using mixed gas, which comprises the following steps:
(1) Cleaning fresh cabbage, adding salt with weight of 0.2% of vegetable, mixing, placing into fermentation tank, and sealing fermentation tank;
(2) Firstly, introducing carbon dioxide gas into a fermentation tank through a gas replacement valve to replace air in the fermentation tank and vegetables to be fermented, enabling the volume content of oxygen in the fermentation tank to be less than 0.1% through repeated exhaust-inflation operation, then, charging nitrogen to further isolate air, and closing the gas replacement valve;
(3) Fermenting the fermentation tank at 25 ℃ and when the pressure is too high in the fermentation process, exhausting the fermentation tank through an automatic air pressure regulating valve on the fermentation tank for 60 hours to finish the fermentation.
Example 2
The embodiment provides a method for quickly preparing pickled Chinese cabbage by using mixed gas, which comprises the following steps:
(1) Cleaning fresh cabbage, adding salt with weight of 0.5% of vegetable, mixing, placing into fermentation tank, and sealing fermentation tank;
(2) Firstly, introducing carbon dioxide gas into a fermentation tank through a gas replacement valve to replace air in the fermentation tank and vegetables to be fermented, enabling the volume content of oxygen in the fermentation tank to be less than 0.1% through repeated exhaust-inflation operation, then, charging helium gas to further isolate air, and closing the gas replacement valve;
(3) Fermenting the fermentation tank at the ambient temperature of 30 ℃, and when the pressure is too high in the fermentation process, performing exhaust treatment through an automatic air pressure regulating valve on the fermentation tank, and completing the fermentation after 48 hours.
Example 3
The embodiment provides a method for quickly preparing pickled Chinese cabbage by using mixed gas, which comprises the following steps:
(1) Cleaning fresh Chinese cabbage with water, shredding, adding salt with weight of 0.5% of vegetable, mixing, packaging into fermentation bag with gas replacement valve, and sealing;
(2) Firstly, introducing carbon dioxide gas into a fermentation bag through a gas replacement valve to replace air in the fermentation bag and vegetables to be fermented, enabling the volume content of oxygen in the fermentation bag to be less than 0.1% through repeated exhausting-inflating operation, then, charging helium gas to further isolate air, and closing the gas replacement valve;
(3) Fermenting the fermentation bag at 35 ℃ and when the pressure is too high in the fermentation process, exhausting through an automatic air pressure regulating valve on the fermentation bag for 72 hours to finish the fermentation.
Comparative example 1
The comparative example provides a method for preparing pickled Chinese cabbage with the assistance of carbon dioxide, comprising the following steps:
(1) Cleaning fresh cabbage, adding salt with weight of 0.2% of vegetable, mixing, placing into fermentation tank, and sealing fermentation tank;
(2) Firstly, introducing carbon dioxide gas into a fermentation tank through a gas replacement valve to replace air in the fermentation tank and vegetables to be fermented, enabling the volume content of oxygen in the fermentation tank to be less than 0.1% through repeated exhaust-inflation operation, and closing the gas replacement valve;
(3) Fermenting the fermentation tank at 25 ℃ and when the pressure is too high in the fermentation process, exhausting the fermentation tank through an automatic air pressure regulating valve on the fermentation tank for 84 hours to finish the fermentation.
Comparative example 2
The comparative example provides a method for preparing pickled Chinese cabbage with the assistance of carbon dioxide, comprising the following steps:
(1) Cleaning fresh cabbage, adding salt with weight of 0.5% of vegetable, mixing, placing into fermentation tank, and sealing fermentation tank;
(2) Firstly, introducing carbon dioxide gas into a fermentation tank through a gas replacement valve to replace air in the fermentation tank and vegetables to be fermented, enabling the volume content of oxygen in the fermentation tank to be less than 0.1% through repeated exhaust-inflation operation, and closing the gas replacement valve;
(3) Fermenting the fermentation tank at the ambient temperature of 30 ℃, and when the pressure is too high in the fermentation process, performing exhaust treatment through an automatic air pressure regulating valve on the fermentation tank, and completing the fermentation after 72 hours.
Comparative example 3
The comparative example provides a method for preparing pickled Chinese cabbage with the assistance of carbon dioxide, comprising the following steps:
(1) Cleaning fresh Chinese cabbage with water, shredding, adding salt with weight of 0.5% of vegetable, mixing, packaging into fermentation bag with gas replacement valve, and sealing;
(2) Firstly, introducing carbon dioxide gas into a fermentation bag through a gas replacement valve to replace air in the fermentation bag and vegetables to be fermented, enabling the volume content of oxygen in the fermentation bag to be less than 0.1% through repeated exhausting-inflating operation, and closing the gas replacement valve;
(3) Fermenting the fermentation bag at 35 ℃ and when the pressure is too high in the fermentation process, exhausting the fermentation bag through an automatic air pressure regulating valve on the fermentation bag for 100 hours to finish the fermentation.
Example 4
This example shows the pH, nitrite content, active microbial biomass and sensory properties of the pickled Chinese cabbage prepared in examples 1 to 3 and comparative examples 1 to 3, and the specific results are shown in Table 1.
TABLE 1 evaluation results of the pickled Chinese cabbage prepared in examples 1-3 and comparative examples 1-3
Figure BDA0004147266020000051
The content of nitrite in pickled vegetable is smaller than 20mg/Kg specified in GB15198-1994, and the content of nitrite in pickled vegetable prepared by the method is smaller than 1.0mg/Kg, which is far smaller than national standardPrescribing; the active microorganism content after fermentation by the method can reach 1.8X10 6 CFU/mL can obviously shorten the fermentation time and improve the quality of pickled Chinese cabbage. Therefore, the fermentation method has obvious advantages compared with the traditional fermentation process of pickled Chinese cabbage.
Finally, it should be noted that: the above embodiments are only for illustrating the technical solution of the present invention, and not for limiting the same; although the invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical scheme described in the foregoing embodiments can be modified or some or all of the technical features thereof can be replaced by equivalents; such modifications and substitutions do not depart from the spirit of the invention.

Claims (9)

1. The method for quickly preparing pickled Chinese cabbage by using mixed gas is characterized by mainly comprising the following steps of:
(1) Cleaning fresh vegetables, adding flavoring, mixing, loading into fermentation device, and sealing the fermentation device;
(2) Firstly, introducing carbon dioxide gas into a fermentation device through a gas replacement valve to replace air in the fermentation device and vegetables to be fermented, enabling the volume content of oxygen in a fermentation tank to be less than 0.1% through repeated exhaust-inflation operation, then, filling inert gas to further isolate the air, and closing the gas replacement valve;
(3) Fermenting the fermentation device at the ambient temperature of 20-35 ℃, and when the pressure is too high in the fermentation process, performing exhaust treatment through an automatic air pressure regulating valve on the fermentation device, and completing the fermentation after lasting 24-72 hours.
2. The method of claim 1, wherein the vegetables in step (1) comprise cabbage, cucumber, cabbage, onion, celery, radish, turnip, beet, spring lettuce, tender ginger, green hyacinth bean, sword bean, and green tomato.
3. The method of claim 1, wherein the flavoring in step (1) comprises salt and the flavoring is added in an amount of 0.1-0.5% by weight of the vegetables.
4. The method of claim 1, wherein the fermentation device of step (1) comprises a fermenter and a fermentation bag.
5. The method of claim 4, wherein the fermenter is made of stainless steel and the fermenter is made of polyethylene or polyvinyl chloride.
6. The method according to claim 1, wherein the inert gas in the step (2) is one or a mixture of two or more of nitrogen, argon and helium.
7. The method according to claim 1, wherein in the step (2), after the gas replacement valve is closed, the volume percentage of carbon dioxide in the mixed gas in the fermentation device is 10-80%.
8. The process according to claim 1, wherein the fermentation temperature in step (3) is 25-30 ℃.
9. The method according to claim 1, wherein the gas discharged from the fermentation apparatus in the step (3) through the automatic gas pressure regulating valve is connected to a gas collecting and purifying apparatus through a pipeline, and is discharged to the atmosphere after being purified.
CN202310307290.3A 2023-03-27 2023-03-27 Method for quickly preparing pickled Chinese cabbage with assistance of mixed gas Pending CN116406778A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116649550A (en) * 2023-07-31 2023-08-29 吉林天泽二氧化碳科技有限公司 Full-ecological pickled Chinese cabbage, pickled vegetable and efficient pickling method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116649550A (en) * 2023-07-31 2023-08-29 吉林天泽二氧化碳科技有限公司 Full-ecological pickled Chinese cabbage, pickled vegetable and efficient pickling method thereof

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