CN116392849A - Reaction kettle for sodium sulfate processing - Google Patents
Reaction kettle for sodium sulfate processing Download PDFInfo
- Publication number
- CN116392849A CN116392849A CN202310668231.9A CN202310668231A CN116392849A CN 116392849 A CN116392849 A CN 116392849A CN 202310668231 A CN202310668231 A CN 202310668231A CN 116392849 A CN116392849 A CN 116392849A
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- China
- Prior art keywords
- groove
- main body
- sodium sulfate
- tray
- reaction kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 title claims abstract description 60
- 229910052938 sodium sulfate Inorganic materials 0.000 title claims abstract description 60
- 235000011152 sodium sulphate Nutrition 0.000 title claims abstract description 60
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 31
- 230000007246 mechanism Effects 0.000 claims abstract description 25
- 238000003756 stirring Methods 0.000 claims description 47
- 238000000926 separation method Methods 0.000 claims description 33
- 238000009434 installation Methods 0.000 claims description 9
- 239000013078 crystal Substances 0.000 abstract description 38
- 239000007788 liquid Substances 0.000 abstract description 5
- 238000000034 method Methods 0.000 abstract description 5
- 230000008569 process Effects 0.000 abstract description 5
- 230000000903 blocking effect Effects 0.000 abstract description 2
- 238000012824 chemical production Methods 0.000 abstract description 2
- 238000000605 extraction Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000007790 scraping Methods 0.000 description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 6
- 238000002425 crystallisation Methods 0.000 description 6
- 230000008025 crystallization Effects 0.000 description 6
- 229910052708 sodium Inorganic materials 0.000 description 6
- 239000011734 sodium Substances 0.000 description 6
- 239000006185 dispersion Substances 0.000 description 4
- 238000001816 cooling Methods 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- 230000009471 action Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/02—Crystallisation from solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/0804—Cleaning containers having tubular shape, e.g. casks, barrels, drums
- B08B9/0808—Cleaning containers having tubular shape, e.g. casks, barrels, drums by methods involving the use of tools, e.g. by brushes, scrapers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D2009/0086—Processes or apparatus therefor
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention provides a reaction kettle for sodium sulfate processing, which relates to the technical field of chemical production equipment and comprises a mounting mechanism and a rotary flashboard, wherein the flashboard is used for blocking a through hole in a separating plate, sodium sulfate liquid mixed in sodium sulfate crystals enters a drain groove in a tray through a drain hole, the tray is downwards moved to the bottom of an inner groove, the drain groove is communicated with a containing piece, so that separated sodium sulfate liquid is collected in the containing piece, and the rest sodium sulfate crystals are left on the tray, so that uninterrupted extraction can be carried out on the sodium sulfate crystals under the conditions of not damaging the internal preparation environment and interrupting the processing process, and the processing efficiency can be effectively improved. The processing structure of the existing sodium sulfate processing reaction kettle is imperfect, and crystals can be taken out of the reaction kettle only after sodium sulfate solution in the reaction kettle is completely crystallized in the processing process, and then the next batch can be crystallized, so that the processing efficiency is low, and the problem that crystals cannot be extracted at any time is solved.
Description
Technical Field
The invention relates to the technical field of chemical production equipment, in particular to a reaction kettle for sodium sulfate processing.
Background
The reaction kettle is widely understood to be a container with physical or chemical reaction, and the structural design and parameter configuration of the container are adopted to realize the heating, evaporating, cooling and low-speed mixing functions of technological requirements, so that the crystallization reaction kettle is required to be used for carrying out crystallization processing in the sodium sulfate production process.
For example, the application number is CN201911039147.0, which relates to a crystallization reaction kettle with high dispersion stirring property, comprising a kettle body and a kettle sleeve, wherein a cooling cavity is formed between the outer wall of the kettle body and the inner wall of the kettle sleeve, a high dispersion stirring mechanism is arranged in the kettle body and comprises a hollow shaft rod and a plurality of dispersion stirring units, the upper end and the lower end of the hollow shaft rod extend out of the kettle body and are communicated with the cooling cavity, the dispersion stirring units are uniformly distributed on the hollow shaft rod from top to bottom, and the lower end of the kettle body is provided with a first outlet and a second outlet.
For the existing sodium sulfate processing reaction kettle, the processing structure is imperfect, in the process of crystallization processing, crystals can be taken out from the reaction kettle only after sodium sulfate solution in the reaction kettle is completely crystallized, then the next batch of crystals can be processed, the processing mode is low in efficiency, crystallized sodium sulfate cannot be extracted at any time, the existing sodium sulfate processing reaction kettle is inconvenient to extract, sodium sulfate after crystallization can be attached to the inner wall of the reaction kettle during use, and when sodium sulfate is extracted, a user is required to manually scrape and coat the sodium sulfate crystals to extract.
Disclosure of Invention
In view of the above, the present invention provides a reaction vessel for sodium sulfate processing, which has a separation plate and a tray with a solid-liquid separation function, and can extract sodium sulfate which has already been crystallized at any time during the approaching process of sodium sulfate, without taking time or the like to completely crystallize sodium sulfate and then extract.
The invention provides a reaction kettle for sodium sulfate processing, which specifically comprises: a mounting mechanism; the mounting mechanism comprises a main body and an adjusting groove, wherein a circular groove is formed in the main body, four groups of support rods are arranged on the bottom side of the main body, and the upper end of the main body is of a cylindrical structure; the two groups of the regulating grooves are arranged in total, the regulating grooves are formed in two sides of the inside of the main body, and the regulating grooves penetrate through two ends of the main body; the installation mechanism is provided with a filter assembly, a separation plate of the filter assembly is arranged on the inner side of the main body, a movable groove in the separation plate is communicated with adjusting grooves on two sides of the main body, and an operating rod on the outer side of the separation plate is positioned in the adjusting grooves; the mounting mechanism is provided with a containing assembly, the containing assembly comprises a tray, a drain groove and a bottom groove, the upper end of the tray is provided with micro drain holes at equal intervals, the tray is positioned at the bottom end of the inner side of the main body, and the tray is attached to the bottom of the separating plate; the leakage groove is formed in the middle side of the inside of the tray, the upper end of the leakage groove is communicated with the leakage hole at the top of the tray, and two sides of the leakage groove penetrate through the tray through three groups of circular through holes respectively; the bottom groove is formed in the bottom side of the tray and is clamped with the push plate in the main body, and the bottom groove penetrates through the rear end of the tray; the installation mechanism is provided with a movable assembly, a fixed ring of the movable assembly is arranged at the top of the main body, the outer edge of a scraper blade at the bottom side of the fixed ring is contacted with the inner wall of the main body, and the lower end of the scraper blade is adjacent to the separation plate; the movable assembly is provided with a top assembly, a top cover of the top assembly is arranged at the top of the fixed ring, the stirring rod at the bottom side of the top cover is positioned at the inner side of the main body, and the clamping block at the outer side of the stirring rod is clamped with the connecting groove on the rotating piece at the outer end of the separating plate.
Further, the mounting mechanism further includes: side slots and receiving members; the side grooves are arranged in two groups, the side grooves are symmetrically arranged at the inner ends of two sides of the main body, and the side grooves penetrate through two ends of the main body; the holding piece is inserted into the inner end of the side groove, two sides of the holding piece penetrate through the side groove, pull rings are arranged at two ends of the holding piece, the holding piece is of a hollow structure, and three groups of circular through holes are formed in the outer side of the holding piece.
Further, the mounting mechanism includes: an inner groove and a push plate; the inner groove is formed in the bottom end of the inner side of the main body, the inner groove penetrates through the front side of the main body, two ends of the inner groove are respectively communicated with the side grooves through three groups of circular through holes, and the inner groove is communicated with the inside of the containing piece through three groups of circular through holes; the push plate is arranged in the inner groove, and the bottom of the push plate is rotatably provided with a screw rod which is in threaded connection with the main body.
Further, the filter assembly includes: a separating plate and a movable groove; round holes are formed in the separating plate at equal intervals, the round holes penetrate through two sides of the separating plate, and a cylindrical protruding structure is arranged at the top of the separating plate; the movable groove is formed in the inner side of the separating plate and is communicated with the round hole in the separating plate, and two ends of the movable groove penetrate through the separating plate through the rectangular through grooves.
Further, the filter assembly includes: a rotating member and a connecting groove; the rotating piece is arranged at the top of the separating plate, the rotating piece is rotationally connected with the cylindrical protruding structure at the upper end of the separating plate, and blades at two sides of the rotating piece are attached to the top of the separating plate; the connecting groove is formed in the middle of the top of the rotating piece.
Further, the filter assembly includes: a flashboard and a control rod; the flashboard is rotatably arranged in the movable groove in the separating plate, circular through holes are formed in the flashboard at equal intervals, the flashboard is communicated with the circular through holes in the separating plate, and rectangular protruding blocks at two ends of the flashboard are positioned at two sides of the movable groove; the control rods are provided with two groups in total, and the control rods are inserted into rectangular protruding blocks at two ends of the flashboard.
Further, the movable assembly includes: a fixing ring and a connecting ring; the fixed ring is internally provided with an annular guide rail; the connecting ring is arranged on the inner side of the fixed ring and is in sliding connection with the guide rail in the fixed ring, and two groups of rectangular grooves are symmetrically arranged in the connecting ring.
Further, the movable assembly includes: a mounting member and a squeegee; the mounting pieces are provided with two groups in total, the mounting pieces are positioned at two sides of the bottom of the connecting ring, the top of each mounting piece is in sliding connection with the rectangular groove in the connecting ring through the elastic piece, and the bottom end of each mounting piece is provided with a T-shaped groove; the scraping plates are provided with two groups, the scraping plates are positioned on the outer sides of the mounting pieces, and the T-shaped blocks at the outer ends of the scraping plates are clamped with the T-shaped grooves in the mounting pieces.
Further, the top assembly includes: a top cover and a fixing frame; the upper end of the top cover is provided with a charging window; the fixed frame is arranged at the middle position of the top cover, the bottom of the fixed frame penetrates through the middle side of the top cover, and the motor is arranged in the fixed frame.
Further, the top assembly includes: stirring rod and clamping block; the stirring rod is rotatably arranged at the lower end of the fixing frame, the stirring rod is positioned at the bottom side of the top cover, the stirring rod is connected with the bottom of the motor, and stirring blades are arranged at the lower end of the stirring rod; the clamping block is arranged at the bottom side of the stirring rod.
The beneficial effects are that: 1. in the invention, a filter component and a movable component are arranged, a separating plate is arranged in a main body, a rotating piece is rotatably arranged at the upper end of the separating plate, the top of the rotating piece is connected with a stirring rod, a through hole flashboard is rotatably arranged in a movable groove in the separating plate, a control rod is arranged at two sides of the flashboard, a tray is arranged at the inner bottom side of the main body, the bottom groove at the lower end of the tray is clamped with a push plate in the main body, a drain groove is arranged in the tray, the drain groove is communicated with a miniature drain hole at the top of the tray, two ends of the drain groove respectively penetrate through the tray through circular through holes, circular side grooves are arranged at two ends of the main body, the containing piece with the circular through holes is spliced into the side grooves, and is communicated with the inner groove through the circular through holes, when sodium sulfate in the main body is stirred and crystallized, the stirring rod drives the rotating piece to rotate, sodium sulfate crystals deposited at the upper end of the separating plate are pushed into the inner drain hole, sodium sulfate crystals are piled up to the upper end of the tray, the drain groove is rotated, the drain groove is formed in the manner, the drain groove is communicated with the sodium sulfate crystals in the separating plate through holes, sodium sulfate crystals are left in the separating plate, sodium sulfate crystals are left in the drain groove and sodium sulfate crystals are continuously in the drain groove, sodium sulfate crystal is continuously in the tray, sodium sulfate crystal is continuously discharged from the drain groove, sodium crystal is continuously discharged from the crystal is continuously, and the sodium crystal is continuously filtered, and is continuously processed in the drain groove, and can be processed in the drain groove through the tray, and is continuously, and can be processed through the drain sodium crystal is continuously, and is continuously in the drain crystal through the sodium crystal, and is continuously in the sodium crystal, and is continuously in the sodium crystal through the crystal through crystal, and is continuously in the crystal through bottom through crystal through, thus, the processing efficiency can be effectively improved.
2. According to the invention, the movable assembly is arranged, the fixed ring is arranged between the main body and the top cover, the connecting ring is rotatably arranged on the inner side of the fixed ring, the inner side of the connecting ring is provided with two groups of rectangular grooves, the L-shaped mounting piece is slidably arranged in the rectangular grooves through the elastic piece, the outer end of the mounting piece is inserted with the scraping plate, the elastic piece pushes the mounting piece, the outer end of the scraping plate is attached to the inner wall of the main body, in the crystallization process, the rotating piece pushes the scraping plate to move along the inner wall of the main body through rotation, and then sodium sulfate crystals attached to the inner wall of the main body are scraped off.
Drawings
In order to more clearly illustrate the technical solution of the embodiments of the present invention, the drawings of the embodiments will be briefly described below. The drawings described below are only for illustration of some embodiments of the invention and are not intended to limit the invention.
In the drawings:
fig. 1 shows a schematic perspective view of an embodiment according to the present invention;
FIG. 2 shows a schematic bottom view of an embodiment of the present invention;
FIG. 3 shows an exploded schematic view of an embodiment according to the present invention;
FIG. 4 shows a schematic view of the internal structure of a mounting mechanism according to an embodiment of the present invention;
FIG. 5 shows a schematic view of a partial connection structure according to an embodiment of the invention;
FIG. 6 shows a schematic cross-sectional structural view of a mounting mechanism according to an embodiment of the present invention;
FIG. 7 shows a partial cross-sectional schematic of an embodiment in accordance with the invention;
FIG. 8 illustrates a schematic cross-sectional view of a movable assembly in accordance with an embodiment of the invention;
fig. 9 shows an exploded view of a filter assembly according to an embodiment of the present invention.
List of reference numerals
1. A mounting mechanism;
101. a main body; 1011. an adjustment tank;
102. a side groove; 1021. a holding member;
103. an inner tank; 1031. a push plate;
2. a filter assembly;
201. a separation plate; 2011. a movable groove;
202. a rotating member; 2021. a connecting groove;
203. a flashboard; 2031. a control lever;
3. a receiving assembly;
301. a tray; 302. a drain groove; 303. a bottom groove;
4. a movable assembly;
401. a fixing ring; 4011. a connecting ring;
402. a mounting member; 403. a scraper;
5. a top assembly;
501. a top cover; 5011. a fixing frame;
502. a stirring rod; 5021. and (5) clamping blocks.
Detailed Description
In order to make the objects, aspects and advantages of the technical solution of the present invention more clear, the technical solution of the embodiment of the present invention will be clearly and completely described below with reference to the accompanying drawings of the specific embodiment of the present invention.
Examples: please refer to fig. 1 to 9:
the invention provides a reaction kettle for sodium sulfate processing, which comprises: a mounting mechanism 1; the mounting mechanism 1 comprises a main body 101 and an adjusting groove 1011, wherein a circular groove is formed in the main body 101, four groups of supporting rods are arranged on the bottom side of the main body 101, and the upper end of the main body 101 is of a cylindrical structure; the two groups of the adjusting grooves 1011 are arranged in total, the adjusting grooves 1011 are arranged on two sides of the inside of the main body 101, and the adjusting grooves 1011 penetrate through two ends of the main body 101; the installation mechanism 1 is provided with a filter assembly 2, a separation plate 201 of the filter assembly 2 is arranged on the inner side of the main body 101, a movable groove 2011 in the separation plate 201 is communicated with adjusting grooves 1011 on two sides of the main body 101, and a control rod 2031 on the outer side of the separation plate 201 is positioned in the adjusting grooves 1011; the mounting mechanism 1 is provided with a containing and connecting assembly 3, the containing and connecting assembly 3 comprises a tray 301, a drain groove 302 and a bottom groove 303, micro drain holes are formed in the upper end of the tray 301 at equal intervals, the tray 301 is positioned at the bottom end of the inner side of the main body 101, and the tray 301 is attached to the bottom of the separation plate 201; the drain groove 302 is formed in the middle side of the inside of the tray 301, the upper end of the drain groove 302 is communicated with a drain hole in the top of the tray 301, and two sides of the drain groove 302 penetrate through the tray 301 through three groups of circular through holes respectively; the bottom groove 303 is formed on the bottom side of the tray 301, the bottom groove 303 is engaged with the push plate 1031 in the main body 101, and the bottom groove 303 penetrates through the rear end of the tray 301; the installation mechanism 1 is provided with a movable component 4, a fixed ring 401 of the movable component 4 is arranged at the top of the main body 101, the outer edge of a scraping plate 403 at the bottom side of the fixed ring 401 is contacted with the inner wall of the main body 101, and the lower end of the scraping plate 403 is adjacent to the separation plate 201; the movable component 4 is provided with a top component 5, a top cover 501 of the top component 5 is arranged at the top of the fixed ring 401, a stirring rod 502 at the bottom side of the top cover 501 is positioned at the inner side of the main body 101, and a clamping block 5021 at the outer side of the stirring rod 502 is clamped with a connecting groove 2021 on the rotating piece 202 at the outer end of the separating plate 201.
As shown in fig. 6, the mounting mechanism 1 further includes: side slots 102, receiving members 1021, inner slots 103, and push plates 1031; the side grooves 102 are provided with two groups in total, the side grooves 102 are symmetrically arranged at the inner ends of the two sides of the main body 101, and the side grooves 102 penetrate through the two ends of the main body 101; the containing piece 1021 is inserted into the inner end of the side groove 102, two sides of the containing piece 1021 penetrate through the side groove 102, two ends of the containing piece 1021 are provided with pull rings, the containing piece 1021 is of a hollow structure, and three groups of circular through holes are formed in the outer side of the containing piece 1021; circular side grooves 102 are provided, the containing pieces 1021 can be mounted on both sides of the main body 101 through the side grooves 102, and cylindrical containing pieces 1021 are provided, so that sodium sulfate solution flowing out of the tray 301 can be collected; the inner groove 103 is formed at the bottom end of the inner side of the main body 101, the inner groove 103 penetrates through the front side of the main body 101, two ends of the inner groove 103 are respectively communicated with the side groove 102 through three groups of circular through holes, and the inner groove 103 is communicated with the inside of the containing member 1021 through three groups of circular through holes; the push plate 1031 is disposed in the inner groove 103, a screw is rotatably mounted at the bottom of the push plate 1031, the screw is in threaded connection with the main body 101, the rectangular inner groove 103 is provided, the tray 301 can be taken out of the main body 101 through the inner groove 103, the circular push plate 1031 is provided, the push plate 1031 is engaged with the bottom groove 303 at the lower end of the tray 301, and when the screw is rotated, the push plate 1031 can push up the tray 301, and the tray 301 is tightly attached to the bottom of the separation plate 201.
As shown in fig. 4 to 5, the filter assembly 2 includes: a separation plate 201, a movable groove 2011, a rotary member 202, a connecting groove 2021, a shutter 203, and a lever 2031; round holes are formed in the separating plate 201 at equal intervals, the round holes penetrate through two sides of the separating plate 201, and a cylindrical protruding structure is arranged at the top of the separating plate 201; the movable groove 2011 is formed in the inner side of the separation plate 201, the movable groove 2011 is communicated with a round hole in the separation plate 201, and two ends of the movable groove 2011 penetrate through the separation plate 201 through rectangular through grooves; a circular separating plate 201 is arranged, a circular through hole is formed in the separating plate 201, crystals can be separated from sodium sulfate solution and then fall into a circular hole in the separating plate 201 for storage, a circular movable groove 2011 is arranged, and the control rod 2031 is positioned in the movable groove 2011, so that the functions of guiding and limiting can be achieved when the flashboard 203 rotates in the movable groove 2011; the rotating piece 202 is arranged at the top of the separating plate 201, the rotating piece 202 is rotationally connected with a cylindrical protruding structure at the upper end of the separating plate 201, and blades at two sides of the rotating piece 202 are attached to the top of the separating plate 201; the connecting groove 2021 is formed in the middle position of the top of the rotating member 202; the rotating member 202 is arranged to push the crystal on the separating plate 201 into the circular hole when the rotating member 202 rotates, and drive the scraping plate 403 to rotate along the guide rail on the fixed ring 401 when the rotating member 202 rotates; the flashboard 203 is rotatably arranged in a movable groove 2011 in the separating plate 201, circular through holes are formed in the flashboard 203 at equal intervals, the flashboard 203 is communicated with the circular through holes in the separating plate 201, and rectangular protruding blocks at two ends of the flashboard 203 are positioned at two sides of the movable groove 2011; the control rods 2031 are provided with two groups in total, the control rods 2031 are inserted on rectangular protruding blocks at two ends of the flashboard 203, the circular flashboard 203 is arranged, the communication state of two sides of the separation plate 201 can be controlled by rotating the flashboard 203, the C-shaped control rods 2031 are arranged, and the flashboard 203 can be controlled to rotate inside the separation plate 201 by pulling the control rods 2031.
As shown in fig. 8, the movable assembly 4 includes: a fixing ring 401, a connecting ring 4011, a mount 402, and a scraper 403; the fixed ring 401 is internally provided with an annular guide rail; the connecting ring 4011 is arranged on the inner side of the fixed ring 401, the connecting ring 4011 is in sliding connection with the guide rail in the fixed ring 401, and two groups of rectangular grooves are symmetrically arranged in the connecting ring 4011; a circular fixing ring 401 is arranged, the connecting ring 4011 can be movably mounted on the upper end of the main body 101 through the fixing ring 401, the circular connecting ring 4011 is arranged, and two groups of mounting pieces 402 can be movably mounted in the connecting ring 4011; the two groups of mounting pieces 402 are arranged in total, the mounting pieces 402 are positioned on two sides of the bottom of the connecting ring 4011, the top of each mounting piece 402 is in sliding connection with a rectangular groove in the connecting ring 4011 through an elastic piece, and a T-shaped groove is formed in the bottom end of each mounting piece 402; the scraper 403 is provided with two groups, the scraper 403 is positioned at the outer side of the mounting piece 402, the T-shaped block at the outer end of the scraper 403 is clamped with the T-shaped groove in the mounting piece 402, the L-shaped mounting piece 402 is arranged, the scraper 403 can be mounted on the connecting ring 4011 through the mounting piece 402, the long scraper 403 is arranged, the scraper 403 is attached to the inner side of the main body 101, and when the scraper 403 rotates along the inner wall of the main body 101, sodium sulfate crystals attached to the inner wall of the main body 101 can be scraped.
As another embodiment of the invention, when in use, a T-shaped groove is formed in the mounting piece 402, a strip-shaped brush with a T-shaped protruding block is arranged, the brush is fixed on the mounting piece 402 through the T-shaped block, and then the brush replaces the original position of the scraping plate 403, and by the arrangement, when the interior of the reaction kettle is cleaned in the later stage, the rotating piece 202 pushes the brush to rotate, so that the brush can synchronously clean the inner wall of the reaction kettle.
As shown in fig. 5, the top assembly 5 includes: the stirring rod 502 comprises a top cover 501, a fixing frame 5011, a stirring rod 502 and a clamping block 5021; the upper end of the top cover 501 is provided with a charging window; the fixing frame 5011 is arranged at the middle position of the top cover 501, the bottom of the fixing frame 5011 penetrates through the middle side of the top cover 501, and a motor is arranged in the fixing frame 5011; a circular top cover 501 is provided, the inside of the main body 101 can be sealed by mounting the top cover 501 to the upper end of the fixing ring 401, a cylindrical fixing bracket 5011 is provided, and a stirring rod 502 connected with a motor can be mounted on the top cover 501 through the fixing bracket 5011; the stirring rod 502 is rotatably arranged at the lower end of the fixing frame 5011, the stirring rod 502 is positioned at the bottom side of the top cover 501, the stirring rod 502 is connected with the bottom of the motor, and stirring blades are arranged at the lower end of the stirring rod 502; the fixture block 5021 is arranged at the bottom side of the stirring rod 502, the stirring rod 502 is arranged, the sodium sulfate solution is stirred by using the stirring rod 502, the sodium sulfate solution can be crystallized, the rectangular fixture block 5021 is arranged, when the top cover 501 with the stirring rod 502 is buckled on the main body 101, the fixture block 5021 at the bottom of the stirring rod 502 is spliced into the connecting groove 2021 of the rotating piece 202, and the stirring rod 502 can drive the rotating piece 202 to rotate during stirring.
Specific use and action of the embodiment:
in the present invention, as shown in fig. 1 to 9, a fixing ring 401 is fixedly installed to the top of a main body 101, a connection ring 4011 is rotatably installed to the inside of the fixing ring 401, two sets of installation members 402 are slidably installed to rectangular grooves in the connection ring 4011 by means of elastic members, then a scraper 403 is inserted to the outer ends of the installation members 402, and the outer ends of the scraper 403 are fitted to the inner wall of the main body 101, a separation plate 201 is installed to the inside of the main body 101, then a rotation member 202 is rotatably installed to the upper end of the separation plate 201, a top cover 501 with a stirring rod 502 is fastened to the top of the main body 101, and a clip 5021 at the bottom of the stirring rod 502 is inserted into a connection groove 2021 at the top of the rotation member 202, a shutter 203 with a through hole is rotatably installed in a movable groove 2011 in the separation plate 201, a tray 301 is installed to the bottom side of the separation plate 201, so that the tray 301 plugs a leak hole at the bottom of the separation plate 201, the bottom groove 303 at the lower end of the tray 301 is engaged with the push plate 1031 in the main body 101, the two ends of the main body 101 are provided with circular side grooves 102, the holding member 1021 is inserted into the side grooves 102, sodium sulfate solution is poured into the inner side of the main body 101, then a motor is started, the stirring rod 502 is used for stirring the sodium sulfate solution, the stirring rod 502 rotates and drives the rotating member 202 to rotate, the rotating member 202 pushes sodium sulfate crystals deposited at the upper end of the separating plate 201 into the leak holes, sodium sulfate crystals are accumulated at the upper end of the tray 301, the scraper 403 rotates along with the rotation of the rotating member 202, the inner wall of the main body 101 is coated, the shutter 203 is rotated, the shutter 203 is used for blocking the through holes in the separating plate 201, at this time, the sodium sulfate crystals are positioned in the through holes between the tray 301 and the separating plate 201, the sodium sulfate liquid mixed in the sodium sulfate crystals can enter the leak grooves 302 in the tray 301 through the leak holes, the screw rod is rotated to enable the push plate 1031 to drive the tray 301 to move downwards, the tray 301 is moved to the bottom of the inner groove 103, the drain groove 302 is communicated with the containing piece 1021, sodium sulfate liquid separated in the drain groove 302 can be collected into the containing piece 1021, crystallized sodium sulfate crystals are remained on the tray 301, the tray 301 is pulled out from the front side of the inner groove 103, at the moment, the sodium sulfate crystals on the tray 301 can be taken down, and after taking out, the tray 301 is moved to the original position and is convenient for next extraction.
Claims (10)
1. The reaction kettle for processing sodium sulfate is characterized by comprising an installation mechanism (1); the mounting mechanism (1) comprises a main body (101) and an adjusting groove (1011), wherein a circular groove is formed in the main body (101), four groups of supporting rods are arranged on the bottom side of the main body (101), and the upper end of the main body (101) is of a cylindrical structure; the two groups of the adjusting grooves (1011) are arranged in total, the adjusting grooves (1011) are arranged on two sides of the inside of the main body (101), and the adjusting grooves (1011) penetrate through two ends of the main body (101); the installation mechanism (1) is provided with a filter assembly (2), a separation plate (201) of the filter assembly (2) is arranged on the inner side of the main body (101), a movable groove (2011) in the separation plate (201) is communicated with adjusting grooves (1011) on two sides of the main body (101), and a control rod (2031) on the outer side of the separation plate (201) is positioned in the adjusting grooves (1011); the mounting mechanism (1) is provided with a containing component (3), the containing component (3) comprises a tray (301), a leakage groove (302) and a bottom groove (303), micro leakage holes are formed in the upper end of the tray (301) at equal intervals, the tray (301) is arranged at the bottom end of the inner side of the main body (101), and the tray (301) is attached to the bottom of the separation plate (201); the leakage groove (302) is formed in the middle side of the inside of the tray (301), the upper end of the leakage groove (302) is communicated with a leakage hole at the top of the tray (301), and two sides of the leakage groove (302) penetrate through the tray (301) through three groups of circular through holes respectively; the bottom groove (303) is formed in the bottom side of the tray (301), the bottom groove (303) is clamped with the push plate (1031) in the main body (101), and the bottom groove (303) penetrates through the rear end of the tray (301); the installation mechanism (1) is provided with a movable assembly (4), a fixed ring (401) of the movable assembly (4) is arranged at the top of the main body (101), the outer edge of a scraper (403) at the bottom side of the fixed ring (401) is contacted with the inner wall of the main body (101), and the lower end of the scraper (403) is adjacent to the separation plate (201); the movable assembly (4) is provided with a top assembly (5), a top cover (501) of the top assembly (5) is arranged at the top of the fixed ring (401), a stirring rod (502) at the bottom side of the top cover (501) is positioned at the inner side of the main body (101), and a clamping block (5021) at the outer side of the stirring rod (502) is clamped with a connecting groove (2021) on the outer end rotating piece (202) of the separating plate (201).
2. The reaction kettle for sodium sulfate processing according to claim 1, wherein: the mounting mechanism (1) further comprises: a side groove (102) and a containing member (1021); the side grooves (102) are arranged in two groups, the side grooves (102) are symmetrically arranged at the inner ends of the two sides of the main body (101), and the side grooves (102) penetrate through the two ends of the main body (101); the holding piece (1021) is inserted into the inner end of the side groove (102), two sides of the holding piece (1021) penetrate through the side groove (102), pull rings are arranged at two ends of the holding piece (1021), the holding piece (1021) is of a hollow structure, and three groups of circular through holes are formed in the outer side of the holding piece (1021).
3. The reaction kettle for sodium sulfate processing according to claim 2, wherein: the mounting mechanism (1) comprises: an inner tank (103) and a push plate (1031); the inner groove (103) is formed in the bottom end of the inner side of the main body (101), the inner groove (103) penetrates through the front side of the main body (101), two ends of the inner groove (103) are respectively communicated with the side groove (102) through three groups of circular through holes, and the inner groove (103) is communicated with the inside of the containing piece (1021) through three groups of circular through holes; the push plate (1031) is arranged in the inner groove (103), and a screw rod is rotatably arranged at the bottom of the push plate (1031) and is in threaded connection with the main body (101).
4. The reaction kettle for sodium sulfate processing according to claim 1, wherein: the filter assembly (2) comprises: a separation plate (201) and a movable groove (2011); round holes are formed in the separating plate (201) at equal intervals, the round holes penetrate through two sides of the separating plate (201), and a cylindrical protruding structure is arranged at the top of the separating plate (201); the movable groove (2011) is formed in the inner side of the separation plate (201), the movable groove (2011) is communicated with a round hole in the separation plate (201), and two ends of the movable groove (2011) penetrate through the separation plate (201) through rectangular through grooves.
5. The reaction kettle for sodium sulfate processing according to claim 4, wherein: the filter assembly (2) comprises: a rotating member (202) and a connecting groove (2021); the rotating piece (202) is arranged at the top of the separating plate (201), the rotating piece (202) is rotationally connected with a cylindrical protruding structure at the upper end of the separating plate (201), and blades at two sides of the rotating piece (202) are attached to the top of the separating plate (201); the connecting groove (2021) is formed in the middle of the top of the rotating piece (202).
6. The reaction kettle for sodium sulfate processing according to claim 4, wherein: the filter assembly (2) comprises: a shutter (203) and a lever (2031); the flashboard (203) is rotatably arranged in a movable groove (2011) in the separating plate (201), circular through holes are formed in the flashboard (203) at equal intervals, the flashboard (203) is communicated with the circular through holes in the separating plate (201), and rectangular protruding blocks at two ends of the flashboard (203) are positioned at two sides of the movable groove (2011); two groups of control rods (2031) are arranged in total, and the control rods (2031) are inserted into rectangular protruding blocks at two ends of the flashboard (203).
7. The reaction kettle for sodium sulfate processing according to claim 1, wherein: the movable assembly (4) comprises: a fixing ring (401) and a connecting ring (4011); an annular guide rail is arranged in the fixed ring (401); the connecting ring (4011) is arranged on the inner side of the fixed ring (401), the connecting ring (4011) is in sliding connection with the guide rail in the fixed ring (401), and two groups of rectangular grooves are symmetrically arranged in the connecting ring (4011).
8. The reaction kettle for sodium sulfate processing as claimed in claim 7, wherein: the movable assembly (4) comprises: a mount (402) and a squeegee (403); the mounting pieces (402) are provided with two groups in total, the mounting pieces (402) are positioned on two sides of the bottom of the connecting ring (4011), the top of each mounting piece (402) is in sliding connection with a rectangular groove in the connecting ring (4011) through an elastic piece, and a T-shaped groove is formed in the bottom end of each mounting piece (402); the scrapers (403) are provided with two groups, the scrapers (403) are arranged on the outer side of the mounting piece (402), and the T-shaped blocks at the outer ends of the scrapers (403) are clamped with the T-shaped grooves in the mounting piece (402).
9. The reaction kettle for sodium sulfate processing according to claim 1, wherein: the top assembly (5) comprises: a top cover (501) and a fixing frame (5011); the upper end of the top cover (501) is provided with a charging window; the fixing frame (5011) is arranged at the middle position of the top cover (501), the bottom of the fixing frame (5011) penetrates through the middle side of the top cover (501), and a motor is arranged in the fixing frame (5011).
10. The reaction kettle for sodium sulfate processing according to claim 9, wherein: the top assembly (5) comprises: a stirring rod (502) and a clamping block (5021); the stirring rod (502) is rotatably arranged at the lower end of the fixing frame (5011), the stirring rod (502) is positioned at the bottom side of the top cover (501), the stirring rod (502) is connected with the bottom of the motor, and stirring blades are arranged at the lower end of the stirring rod (502); the clamping block (5021) is arranged at the bottom side of the stirring rod (502).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310668231.9A CN116392849B (en) | 2023-06-07 | 2023-06-07 | Reaction kettle for sodium sulfate processing |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310668231.9A CN116392849B (en) | 2023-06-07 | 2023-06-07 | Reaction kettle for sodium sulfate processing |
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| Publication Number | Publication Date |
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| CN116392849A true CN116392849A (en) | 2023-07-07 |
| CN116392849B CN116392849B (en) | 2023-08-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202310668231.9A Active CN116392849B (en) | 2023-06-07 | 2023-06-07 | Reaction kettle for sodium sulfate processing |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1175659A (en) * | 1966-05-02 | 1969-12-23 | Inveta A G Fur Forschung Und P | Process and Apparatus for Reflux Crystallization |
| JPH05103919A (en) * | 1991-10-15 | 1993-04-27 | Ngk Insulators Ltd | Multi-functional filter |
| CN108328628A (en) * | 2018-03-23 | 2018-07-27 | 杨奕颉 | A kind of sodium sulfite produciton equipment |
| CN216572590U (en) * | 2021-09-29 | 2022-05-24 | 余耀强 | Reagent agitating unit for chemical production convenient to observe |
| CN115364514A (en) * | 2022-09-13 | 2022-11-22 | 毛小明 | Preparation method and preparation system of edible salt |
| CN218516523U (en) * | 2022-10-17 | 2023-02-24 | 易如可信科技(北京)有限公司 | Environment-friendly fire extinguishing agent production device |
-
2023
- 2023-06-07 CN CN202310668231.9A patent/CN116392849B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1175659A (en) * | 1966-05-02 | 1969-12-23 | Inveta A G Fur Forschung Und P | Process and Apparatus for Reflux Crystallization |
| JPH05103919A (en) * | 1991-10-15 | 1993-04-27 | Ngk Insulators Ltd | Multi-functional filter |
| CN108328628A (en) * | 2018-03-23 | 2018-07-27 | 杨奕颉 | A kind of sodium sulfite produciton equipment |
| CN216572590U (en) * | 2021-09-29 | 2022-05-24 | 余耀强 | Reagent agitating unit for chemical production convenient to observe |
| CN115364514A (en) * | 2022-09-13 | 2022-11-22 | 毛小明 | Preparation method and preparation system of edible salt |
| CN218516523U (en) * | 2022-10-17 | 2023-02-24 | 易如可信科技(北京)有限公司 | Environment-friendly fire extinguishing agent production device |
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| Publication number | Publication date |
|---|---|
| CN116392849B (en) | 2023-08-04 |
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