CN116219555A - Degumming processing system and method for fibrilia - Google Patents
Degumming processing system and method for fibrilia Download PDFInfo
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- CN116219555A CN116219555A CN202211721104.2A CN202211721104A CN116219555A CN 116219555 A CN116219555 A CN 116219555A CN 202211721104 A CN202211721104 A CN 202211721104A CN 116219555 A CN116219555 A CN 116219555A
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- 238000000034 method Methods 0.000 title claims abstract description 47
- 244000025254 Cannabis sativa Species 0.000 claims abstract description 54
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 claims abstract description 54
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 claims abstract description 54
- 235000009120 camo Nutrition 0.000 claims abstract description 54
- 235000005607 chanvre indien Nutrition 0.000 claims abstract description 54
- 239000011487 hemp Substances 0.000 claims abstract description 54
- 238000003825 pressing Methods 0.000 claims abstract description 24
- 239000000835 fiber Substances 0.000 claims abstract description 20
- 238000011068 loading method Methods 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 37
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 30
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 18
- 238000010025 steaming Methods 0.000 claims description 17
- 238000004061 bleaching Methods 0.000 claims description 16
- 238000010009 beating Methods 0.000 claims description 14
- 238000002791 soaking Methods 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 12
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 10
- 239000000839 emulsion Substances 0.000 claims description 9
- 102000004190 Enzymes Human genes 0.000 claims description 8
- 108090000790 Enzymes Proteins 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 8
- 238000007906 compression Methods 0.000 claims description 7
- 238000010411 cooking Methods 0.000 claims description 7
- 239000012535 impurity Substances 0.000 claims description 7
- 230000006835 compression Effects 0.000 claims description 6
- 239000003599 detergent Substances 0.000 claims description 6
- 239000003814 drug Substances 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 238000002386 leaching Methods 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 230000007935 neutral effect Effects 0.000 claims description 5
- 239000003292 glue Substances 0.000 claims description 4
- 239000012071 phase Substances 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 244000198134 Agave sisalana Species 0.000 claims description 3
- 240000008564 Boehmeria nivea Species 0.000 claims description 3
- 240000000491 Corchorus aestuans Species 0.000 claims description 3
- 235000011777 Corchorus aestuans Nutrition 0.000 claims description 3
- 235000010862 Corchorus capsularis Nutrition 0.000 claims description 3
- 240000000797 Hibiscus cannabinus Species 0.000 claims description 3
- 240000006240 Linum usitatissimum Species 0.000 claims description 3
- 235000004431 Linum usitatissimum Nutrition 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 230000003247 decreasing effect Effects 0.000 claims description 3
- 239000012530 fluid Substances 0.000 claims description 3
- 239000003921 oil Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 239000012808 vapor phase Substances 0.000 claims description 3
- 239000011790 ferrous sulphate Substances 0.000 claims description 2
- 235000003891 ferrous sulphate Nutrition 0.000 claims description 2
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 2
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 239000002351 wastewater Substances 0.000 abstract description 3
- 239000000084 colloidal system Substances 0.000 description 4
- 238000011049 filling Methods 0.000 description 4
- 239000007789 gas Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000722949 Apocynum Species 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 239000010902 straw Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C1/00—Treatment of vegetable material
- D01C1/04—Bacteriological retting
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/66—Disintegrating fibre-containing textile articles to obtain fibres for re-use
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- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Molecular Biology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Textile Engineering (AREA)
- Preliminary Treatment Of Fibers (AREA)
- Treatment Of Fiber Materials (AREA)
Abstract
The invention discloses a degumming processing system for fibrilia, which comprises a wet start machine, a feeding machine and a yarn pressing machine, wherein the wet start machine comprises a feeding curtain, a stripping structure and a first conveying mechanism, the feeding curtain is obliquely upwards arranged on one side of the stripping structure, and the other side of the stripping structure is connected with the first conveying mechanism; the feeding machine comprises a clapping roller positioned at one side of the top of the first conveying mechanism, a flat curtain horizontally arranged under the clapping roller and an inclined curtain with one end arranged at one end of the flat curtain far away from the first conveying mechanism, and the other end of the inclined curtain leans against the yarn pressing machine; the yarn pressing machine comprises a second conveying curtain horizontally connected to the tail end of the inclined curtain, a hemp collecting opening positioned right below the second conveying curtain, a yarn cage positioned below the hemp collecting opening and a pressing rod positioned above the yarn cage, wherein the pressing rod is suitable for compacting hemp fibers falling into the yarn cage. The invention also provides a degumming process method of the fibrilia, which changes the traditional fibrilia knocking process into a process of secondarily loading into a cage, reduces the discharge of waste water, improves the production efficiency, reduces the total production cost and improves the product quality.
Description
Technical Field
The invention relates to the technical field of textile processing, in particular to a degumming processing system and a degumming processing method for fibrilia.
Background
The surface of the fibrilia contains a large amount of colloid, the fibrilia is coarse and hard due to the existence of the colloid, the degummed fibrilia is required to be degummed before processing and use, and the residual gum rate and breaking strength of the degummed fibrilia influence the processing value of the fibrilia, so that the degummed fibrilia is an important point of processing.
The traditional hemp degumming process method is a chemical degumming method, a physical degumming method, a biological enzyme degumming method and the like. The chemical degumming method uses sodium hydroxide as a treating agent, so that the alkali consumption is high, and the degumming wastewater has great environmental pollution; the physical degumming method is mainly mechanical degumming, and the current stage treatment comprises the methods of manual hemp scraping, ultrasonic wave, steam explosion and the like, but only partial colloid can be removed, so the method is often used as an auxiliary method; the biological enzyme degumming method utilizes the characteristics of specificity and high efficiency of different enzymes to remove the external colloid of the fiber, and has better compound use effect of a plurality of enzymes, but the biological enzyme degumming method has low degumming rate and long time consumption.
In addition, the traditional fibrilia production process flow is as follows: the process flow of steaming, bleaching and beating hemp is long, the labor is more, the labor intensity is high, and the degumming uniformity is poor; and the loss rate after cooking is large, and uniformity of loading density and bleaching uniformity during cooking and bleaching cannot be ensured.
Disclosure of Invention
In view of the foregoing drawbacks of the prior art, a first object of the present invention is to provide a degumming processing system for fibrilia, comprising a wet start, a feeder and a yarn presser, wherein:
the wet start machine comprises a feeding curtain, a stripping structure and a first conveying mechanism, wherein the feeding curtain is obliquely upwards arranged on one side of the stripping structure, and the other side of the stripping structure is connected with the first conveying mechanism;
the feeding machine comprises a beating roller positioned at one side of the top of the first conveying mechanism, a flat curtain horizontally arranged under the beating roller and an inclined curtain with one end arranged at one end of the flat curtain far away from the first conveying mechanism, and the other end of the inclined curtain leans against the yarn pressing machine;
the yarn pressing machine comprises a second conveying curtain horizontally connected to the tail end of the inclined curtain, a hemp collecting opening located right below the second conveying curtain, a yarn cage located below the hemp collecting opening and a pressing rod located right above the yarn cage, wherein the pressing rod is suitable for compacting hemp fibers falling into the yarn cage.
Preferably, the stripping structure comprises a plurality of pairs of horizontally arranged roller, stripping rollers arranged between each pair of roller, a drain bottom horizontally arranged under the roller and the stripping rollers, and a first hemp rod collecting port arranged under the drain bottom, wherein the hemp fibers are output after rolling and drafting by the roller and are stripped by the stripping rollers, and colloidal particles and hemp rods in the hemp fibers fall into the drain bottom and the first hemp rod collecting port.
Preferably, the first conveying mechanism comprises a conveying curtain horizontally arranged, a lifting curtain connected to the tail end of the conveying curtain and far away from the stripping structure, and a uniform roller arranged on one side above the lifting curtain, wherein one end of the conveying curtain far away from the lifting curtain is closely adjacent to the lower side of the stripping roller so as to receive the fibrilia stripped by the stripping roller and fall onto the conveying curtain, the lifting curtain is used for lifting the fibrilia on the conveying curtain into the feeding machine, and the uniform roller is used for carrying out uniform distribution conveying on the fibrilia conveyed into the feeding machine.
A second object of the present invention is to provide a degumming process method for a fibrilia, using the degumming processing system for a fibrilia as described above, the degumming process method comprising the steps of:
S 100 : vapor phase cooking: soaking raw hemp in water for 2-4 hr, loading into a cage, placing into a gas-phase steaming tank, steaming under 0.6-1.8MPa for 2-30min, releasing steam, and taking out hemp fiber from the steaming tank;
S 200 : pre-degumming: adding proper amount of water into the steamer, adding the soaked raw hemp when the water in the steamer is burned to 85-100 ℃, then adding pre-degummed liquid medicine when the water temperature is 150 ℃, continuously steaming for 40 minutes, cooling the water temperature to 90 ℃ after steaming, taking out the raw hemp, and soaking in cold water for 1.5-2.5 hours;
S 300 : secondary cage: feeding the obtained dispersed activated raw hemp into a wet start machine, sequentially removing glue impurities adsorbed on the surface of hemp fibers through a feeding machine and a yarn pressing machine, finally feeding the raw hemp into a yarn cage again, and beating cakes by adopting a compression bar;
S 400 : bleaching: degumming the fibrilia obtained after beating cakes in the boiling and bleaching process by biological enzyme, and bleaching by hydrogen peroxide, wherein a plurality of drying processes with decreasing temperature are adopted in the drying process;
S 500 : soaking oil: adding mechanical oil, sodium hydroxide or potassium hydroxide and a detergent into water, stirring uniformly to prepare emulsion, soaking the degummed fibrilia in the emulsion, and preserving the temperature for 0.5-3 h at 60-100 ℃.
Preferably, in step S 200 Wherein the pre-degumming liquid medicine comprises ethanol, water and sulfuric acid, the volume fraction of the ethanol is 60-98%, and the concentration of the sulfuric acid is 0.4-0.8g/L.
Preferably, in step S 300 In the middle feeding process, the yarn cage rotates continuously at the speed of 3-5 revolutions per minute, and the compression bar moves up and down to compact and homogenize fibrilia; and meanwhile, continuously spraying water into the yarn cage from top to bottom for leaching, wherein the leaching water temperature is 50-80 ℃.
Preferably, in step S 500 The emulsion is prepared from (by weight) mechanical oil 6-30 g, sodium hydroxide or potassium hydroxide 2-10 g, detergent 2-12 g and water 3-12 kg.
Preferably, in step S 100 Wherein the weight ratio of the fibrilia to the treatment fluid is 1:10-30, the concentration of sodium hydroxide is 3-6 g/L, the temperature is 60-80 ℃, the treatment time is 5-20 min, and the pH value is neutral by water washing.
Preferably, in step S 200 Wherein the weight ratio of the fibrilia to the treatment liquid is 1:10-30, the pH value is 4-6, the concentration of anhydrous ferrous sulfate is 8-10 g/L, the concentration of hydrogen peroxide is 7-10 g/L, the treatment temperature is 50-80 ℃, the treatment time is 30-60 min, and the pH value is neutral by washing with water.
Preferably, the hemp fiber is hemp, flax, ramie, kendir, jute, sisal or kenaf.
Compared with the prior art, the degumming process of the fibrilia has the following advantages:
the invention changes the production modes of cage filling, steaming, bleaching, beating, secondary cage filling and oil soaking in the traditional degumming process into the following steps: the improved secondary cage loading is used for effectively loosening fibrilia through a set of device of opening, impurity removal and cage loading combination, so that the influence of poor local degumming caused by unevenness during primary cage loading can be effectively avoided, and the effective restoration is carried out during subsequent bleaching.
Drawings
FIG. 1 is a schematic diagram of a degummed processing system for fibrilia in accordance with one embodiment of the present invention;
fig. 2 is a schematic flow chart of a degumming process method for fibrilia according to an embodiment of the present invention.
Reference numerals illustrate:
1-starting up in a wet state;
11-feeding curtain; 12-peeling the structure; 121-roller; 122-stripping roller; 123-leaking bottom; 124-a first hemp stalk collection port; 13-a first conveying mechanism; 131-conveying curtain, 132-lifting curtain; 133-a uniform roller; 134-viewing window; 135-a second hemp stalk collection port;
2-a feeder;
21-a falling roller; 22-flat curtain; 23-inclined curtain;
3-a yarn pressing machine;
31-a second conveyor curtain; 32-collecting the hemp opening; 33-gauze cage; 34-compression bar.
Detailed Description
The following description of the embodiments of the present invention will be made apparent and fully in view of the accompanying drawings, in which some, but not all embodiments of the invention are shown. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
In addition, the technical features of the different embodiments of the present invention described below may be combined with each other as long as they do not collide with each other.
Referring to fig. 1, an embodiment of the present invention provides a degumming processing system for fibrilia, which includes a wet start machine 1, a feeder 2 and a yarn pressing machine 3, wherein:
the wet start machine 1 comprises a feeding curtain 11, a stripping structure 12 and a first conveying mechanism 13, wherein the feeding curtain 11 is obliquely upwards arranged on one side of the stripping structure 12, and the other side of the stripping structure 12 is connected with the first conveying mechanism 13.
The feeder 2 comprises a roller 21, a flat curtain 22 and a slanted curtain 23, wherein:
the doffing roller 21 is located at one side of the top of the first conveying mechanism 13 and is used for doffing and loosening the fibrilia on the first conveying mechanism 13, the flat curtain 22 is horizontally arranged right below the doffing roller 21 and is used for receiving the fibrilia fallen by the doffing roller 21, one end of the inclined curtain 23 is arranged at one end of the flat curtain 22 far away from the first conveying mechanism 13, the other end of the inclined curtain 23 is inclined and leaned against the yarn pressing machine 3, and degummed fibrilia is conveyed into the yarn pressing machine 3 through the inclined curtain 23.
The yarn presser 3 comprises a second conveying curtain 31, a collecting opening 32, a yarn cage 33 and a pressing rod 34, wherein:
the second conveying curtain 31 is horizontally connected to the tail end of the inclined curtain 23 to receive the fibrilia conveyed by the inclined curtain 23, the hemp collecting opening 32 is located right below the second conveying curtain 31 to further collect colloidal particle impurities in the fibrilia, the yarn cage 33 is located below the hemp collecting opening 32, degummed fibrilia falls into the yarn cage 33, the pressing rod 34 is located right above the yarn cage 33, and the pressing rod 34 is suitable for compacting the fibrilia falling into the yarn cage 33.
Specifically, referring to fig. 1, in an embodiment of the present invention, the stripping structure 12 includes a plurality of pairs of horizontally disposed roller 121, stripping roller 122, drain bottom 123 and first straw collection port 124, wherein:
the stripping roller 122 is located between each pair of roller rollers 121, pick teeth are uniformly arranged on the outer surfaces of the stripping rollers 122 and used for picking and rotating the degummed fibrilia rolled by the roller rollers 121 and scattering the degummed fibrilia, the drain bottom 123 is horizontally arranged right below the roller rollers 121 and the stripping rollers 122 and used for receiving colloidal particles, fibrilia impurities and the like falling by the stripping rollers 122, the first fibrilia collecting opening 124 is arranged right below the drain bottom 123, the fibrilia is output after rolling and drafting by the roller rollers 121 and is peeled off by the stripping rollers 122, and colloidal particles and fibrilia rods in the fibrilia fall into the drain bottom 123 and the first fibrilia collecting opening 124.
Specifically, referring to fig. 1, in the embodiment of the present invention, the first conveying mechanism 13 includes a conveying curtain 131, a lift curtain 132, and a uniform roller 133, wherein:
the conveying curtain 131 is horizontally arranged, one end of the conveying curtain 131 is located between the stripping roller 122 and the bottom 123 to receive the fibrilia picked by the stripping roller 122 and fall into the upper surface of the conveying curtain 131, the other end of the conveying curtain is connected with the bottom end of the lifting curtain 132 to facilitate conveying the fibrilia on the conveying curtain 131 to the lifting curtain 132, the lifting curtain 132 is connected to the tail end of the conveying curtain 131 and far away from the stripping structure 12, and the lifting curtain 132 is obliquely upwards arranged, preferably, the inclination angle in the embodiment is about 45 degrees.
Thus, the homogenizing roller 133 is disposed on one side above the lifting curtain 132, and one end of the conveying curtain 131 away from the lifting curtain 132 is adjacent to the lower side of the peeling roller 122 to receive the fibrilia peeled by the peeling roller 122 and fall onto the conveying curtain 131, the lifting curtain 132 is used for lifting the fibrilia on the conveying curtain 131 into the feeder 2, and the homogenizing roller 133 is used for uniformly distributing and conveying the fibrilia conveyed into the feeder 2.
A second hemp stalk collecting port 135 is also provided at the bottom between the conveying curtain 131 and the lifting curtain 132 for collecting colloidal particles produced by further degumming. The first conveying mechanism 13 is also provided with an observation window 134, and the degummed conveying condition inside the first conveying mechanism 13 is conveniently observed through the observation window 134.
Referring to fig. 2, the embodiment of the invention further provides a degumming process method for a fibrilia, which adopts the degumming processing system for a fibrilia, and comprises the following steps:
S 100 : vapor phase cooking: soaking raw hemp in water for 2-4 hr, loading into a cage, placing into a gas phase steaming tank, steaming under 0.6-1.8MPa for 2-30min, releasing steam, and steaming hemp fiberTaking out from the tank;
S 200 : pre-degumming: adding proper amount of water into the steamer, adding the soaked raw hemp when the water in the steamer is burned to 85-100 ℃, then adding pre-degummed liquid medicine when the water temperature is 150 ℃, continuously steaming for 40 minutes, cooling the water temperature to 90 ℃ after steaming, taking out the raw hemp, and soaking in cold water for 1.5-2.5 hours;
S 300 : and (3) secondary cage loading: feeding the obtained dispersed activated raw hemp into a wet start machine 1, sequentially removing glue impurities adsorbed on the surface of hemp fibers through a feeding machine 2 and a yarn pressing machine 3, finally feeding the raw hemp into a yarn cage 33 again, and beating cakes by adopting a compression bar 34;
in the step, the traditional disc beating process is changed into the secondary cage loading process, so that not only can the waste water discharge, labor and the like be reduced, but also the degumming uniformity can be improved, the product quality is improved, and the total production time is shortened.
S 400 : bleaching: degumming the fibrilia obtained after beating cakes in the boiling and bleaching process by biological enzyme, and bleaching by hydrogen peroxide, wherein a plurality of drying processes with decreasing temperature are adopted in the drying process;
S 500 : soaking oil: adding mechanical oil, sodium hydroxide or potassium hydroxide and a detergent into water, stirring uniformly to prepare emulsion, soaking the degummed fibrilia in the emulsion, and preserving the temperature for 0.5-3 h at 60-100 ℃.
Therefore, the degumming process in the embodiment of the invention changes the production modes of cage filling, cooking, bleaching, beating, secondary cage filling and oil soaking in the traditional degumming process into the following modes: the improved secondary cage loading is used for effectively loosening fibrilia through a set of devices of opening, impurity removal and cage loading combination, so that the influence of poor local degumming caused by unevenness during primary cage loading can be effectively avoided, and the effective restoration is carried out during subsequent bleaching.
In particular to this step, in step S 100 Wherein the weight ratio of fibrilia to the treatment fluid in the gas phase cooking process is 1:10-30, the concentration of sodium hydroxide is 3-6 g/L, the temperature is 60-80 ℃, and the fibrilia is washed until the pH value is neutral.
In particular in the present stepIn step S 200 Wherein the pre-degumming liquid medicine comprises ethanol, water and sulfuric acid, the volume fraction of the ethanol is 60-98%, and the concentration of the sulfuric acid is 0.4-0.8g/L.
In particular to this step, in step S 300 In the middle, during feeding, the yarn cage 33 rotates continuously at the speed of 3-5 revolutions per minute, and the compression bar 34 moves up and down to compact and homogenize fibrilia; simultaneously, water is continuously sprayed into the yarn cage 33 from top to bottom for leaching, and the leaching water temperature is 50-80 ℃.
In particular to this step, in step S 500 The emulsion is prepared from (by weight) mechanical oil 6-30 g, sodium hydroxide or potassium hydroxide 2-10 g, detergent 2-12 g and water 3-12 kg.
In the step, the hemp fiber is hemp, flax, ramie, apocynum, jute, sisal or kenaf.
Although the present disclosure is disclosed above, the scope of the present disclosure is not limited thereto. Various changes and modifications may be made by one skilled in the art without departing from the spirit and scope of the disclosure, and these changes and modifications will fall within the scope of the invention.
Claims (10)
1. A degumming processing system for fibrilia, which is characterized by comprising a wet start machine, a feeding machine and a yarn pressing machine, wherein:
the wet start machine comprises a feeding curtain, a stripping structure and a first conveying mechanism, wherein the feeding curtain is obliquely upwards arranged on one side of the stripping structure, and the other side of the stripping structure is connected with the first conveying mechanism;
the feeding machine comprises a beating roller positioned at one side of the top of the first conveying mechanism, a flat curtain horizontally arranged under the beating roller and an inclined curtain with one end arranged at one end of the flat curtain far away from the first conveying mechanism, and the other end of the inclined curtain leans against the yarn pressing machine;
the yarn pressing machine comprises a second conveying curtain horizontally connected to the tail end of the inclined curtain, a hemp collecting opening located right below the second conveying curtain, a yarn cage located below the hemp collecting opening and a pressing rod located right above the yarn cage, wherein the pressing rod is suitable for compacting hemp fibers falling into the yarn cage.
2. The degummed processing system of claim 1, wherein said stripping structure comprises a plurality of pairs of horizontally disposed roller pairs, a stripping roller positioned between each pair of roller pairs, a bottom drain horizontally disposed directly below said roller pairs and said stripping roller pairs, and a first hemp stalk collection opening positioned directly below said bottom drain, wherein said hemp fibers are output after being drawn by said roller pairs and stripped by said stripping roller pairs, and wherein said hemp fibers have said glue particles and hemp stalks falling into said bottom drain and said first hemp stalk collection opening.
3. The degummed fiber processing system of claim 2, wherein the first conveyor mechanism comprises a horizontally disposed conveyor curtain, a lift curtain connected to an end of the conveyor curtain and remote from the stripping structure, and a uniformity roller disposed on a side above the lift curtain, wherein an end of the conveyor curtain remote from the lift curtain is immediately below the stripping roller to receive the separated fibers from the stripping roller and drop the separated fibers onto the conveyor curtain, the lift curtain is used for lifting the fibers on the conveyor curtain into the feeder, and the uniformity roller is used for uniformly distributing and conveying the fibers conveyed into the feeder.
4. A process for degumming a fibrilia using the degumming processing system for a fibrilia according to claim 3, comprising the steps of:
S 100 : vapor phase cooking: soaking raw hemp in water for 2-4 hr, loading into a cage, placing into a gas-phase steaming tank, steaming under 0.6-1.8MPa for 2-30min, releasing steam, and taking out hemp fiber from the steaming tank;
S 200 : pre-degumming: adding proper amount of water into the steamer, adding the soaked raw hemp when the water in the steamer is burned to 85-100 ℃,then adding pre-degummed liquid medicine at water temperature of 150 ℃, continuously steaming for 40 minutes, cooling the water temperature to 90 ℃ after steaming, taking out the raw hemp, and soaking in cold water for 1.5-2.5 hours;
S 300 : and (3) secondary cage loading: feeding the obtained dispersed activated raw hemp into a wet start machine, sequentially removing glue impurities adsorbed on the surface of hemp fibers through a feeding machine and a yarn pressing machine, finally feeding the raw hemp into a yarn cage again, and beating cakes by adopting a compression bar;
S 400 : bleaching: degumming the fibrilia obtained after beating cakes in the boiling and bleaching process by biological enzyme, and bleaching by hydrogen peroxide, wherein a plurality of drying processes with decreasing temperature are adopted in the drying process;
S 500 : soaking oil: adding mechanical oil, sodium hydroxide or potassium hydroxide and a detergent into water, stirring uniformly to prepare emulsion, soaking the degummed fibrilia in the emulsion, and preserving the temperature for 0.5-3 h at 60-100 ℃.
5. The degumming process for a fibrilia according to claim 4, wherein: in step S 200 Wherein the pre-degumming liquid medicine comprises ethanol, water and sulfuric acid, the volume fraction of the ethanol is 60-98%, and the concentration of the sulfuric acid is 0.4-0.8g/L.
6. The degumming process for a fibrilia according to claim 4, wherein: in step S 300 In the middle feeding process, the yarn cage rotates continuously at the speed of 3-5 revolutions per minute, and the compression bar moves up and down to compact and homogenize fibrilia; and meanwhile, continuously spraying water into the yarn cage from top to bottom for leaching, wherein the leaching water temperature is 50-80 ℃.
7. The degumming process for a fibrilia according to claim 4, wherein: in step S 500 The emulsion is prepared from (by weight) mechanical oil 6-30 g, sodium hydroxide or potassium hydroxide 2-10 g, detergent 2-12 g and water 3-12 kg.
8. The process for degumming a fibrilia according to claim 4, whereinThe method comprises the following steps: in step S 100 Wherein the weight ratio of the fibrilia to the treatment fluid is 1:10-30, the concentration of sodium hydroxide is 3-6 g/L, the temperature is 60-80 ℃, the treatment time is 5-20 min, and the pH value is neutral by water washing.
9. The degumming process for a fibrilia according to claim 4, wherein: in step S 200 Wherein the weight ratio of the fibrilia to the treatment liquid is 1:10-30, the pH value is 4-6, the concentration of anhydrous ferrous sulfate is 8-10 g/L, the concentration of hydrogen peroxide is 7-10 g/L, the treatment temperature is 50-80 ℃, the treatment time is 30-60 min, and the pH value is neutral by washing with water.
10. The degumming process for a fibrilia according to claim 4, wherein: the fibrilia is hemp, flax, ramie, kendir, jute, sisal or kenaf.
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CN202211721104.2A CN116219555A (en) | 2022-12-30 | 2022-12-30 | Degumming processing system and method for fibrilia |
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CN202211721104.2A CN116219555A (en) | 2022-12-30 | 2022-12-30 | Degumming processing system and method for fibrilia |
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CN116695358A (en) * | 2023-06-20 | 2023-09-05 | 山东芦氏特种面料科技有限公司 | A cellulose fiber flame retardant phosphorus nitrogen fixing machine |
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