CN116159503A - Organic synthesis device with waste gas purification system and purification method thereof - Google Patents
Organic synthesis device with waste gas purification system and purification method thereof Download PDFInfo
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- CN116159503A CN116159503A CN202310151739.1A CN202310151739A CN116159503A CN 116159503 A CN116159503 A CN 116159503A CN 202310151739 A CN202310151739 A CN 202310151739A CN 116159503 A CN116159503 A CN 116159503A
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- 239000002912 waste gas Substances 0.000 title claims abstract description 100
- 238000003786 synthesis reaction Methods 0.000 title claims abstract description 59
- 238000000746 purification Methods 0.000 title claims abstract description 57
- 238000000034 method Methods 0.000 title claims abstract description 39
- 239000007789 gas Substances 0.000 claims abstract description 149
- 238000001914 filtration Methods 0.000 claims abstract description 135
- 239000000945 filler Substances 0.000 claims abstract description 100
- 239000002699 waste material Substances 0.000 claims abstract description 29
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 26
- 238000011049 filling Methods 0.000 claims abstract description 24
- 230000007246 mechanism Effects 0.000 claims abstract description 13
- 239000002245 particle Substances 0.000 claims abstract description 5
- 238000012856 packing Methods 0.000 claims description 45
- 238000003756 stirring Methods 0.000 claims description 42
- 238000005192 partition Methods 0.000 claims description 23
- 238000007599 discharging Methods 0.000 claims description 12
- 230000000694 effects Effects 0.000 claims description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 11
- 238000007789 sealing Methods 0.000 claims description 9
- 239000007921 spray Substances 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 7
- 230000000712 assembly Effects 0.000 claims description 6
- 238000000429 assembly Methods 0.000 claims description 6
- 238000010030 laminating Methods 0.000 claims description 6
- 230000000149 penetrating effect Effects 0.000 claims description 5
- 230000007306 turnover Effects 0.000 claims description 5
- 229920006395 saturated elastomer Polymers 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 230000001502 supplementing effect Effects 0.000 claims description 3
- 230000008569 process Effects 0.000 abstract description 23
- 230000008859 change Effects 0.000 description 8
- 210000001503 joint Anatomy 0.000 description 7
- 229910052799 carbon Inorganic materials 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 238000003032 molecular docking Methods 0.000 description 5
- 238000005096 rolling process Methods 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 238000013019 agitation Methods 0.000 description 3
- 230000001737 promoting effect Effects 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/06—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with moving adsorbents, e.g. rotating beds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
- B01D53/18—Absorbing units; Liquid distributors therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
- B01D2252/10—Inorganic absorbents
- B01D2252/103—Water
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
- B01D2253/10—Inorganic adsorbents
- B01D2253/102—Carbon
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/40—Further details for adsorption processes and devices
- B01D2259/40083—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption
- B01D2259/40084—Regeneration of adsorbents in processes other than pressure or temperature swing adsorption by exchanging used adsorbents with fresh adsorbents
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
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- Organic Chemistry (AREA)
- Treating Waste Gases (AREA)
Abstract
The invention relates to the technical field of organic synthesis devices, in particular to an organic synthesis device with an exhaust gas purification system and a purification method thereof, wherein the organic synthesis device with the exhaust gas purification system comprises the following components: and the top of the synthesis device main body is provided with an exhaust gas purifying mechanism for purifying the exhaust gas generated by the synthesis device main body. According to the organic synthesis device with the waste gas purification system and the purification method thereof, the waste gas purification mechanism is arranged, the waste gas purification container, the waste gas filtering component, the filling component and the filtering waste collection container are matched for use, the function of replacing the filtering filler is completed, the filtering filler filled with particles is directly discharged and filled, the whole process is in a closed environment, on one hand, the synthesis device main body is not shut down due to replacement of the filtering filler in the replacement process, and the delay of the organic synthesis process is avoided.
Description
Technical Field
The invention relates to the field of organic synthesis devices, in particular to an organic synthesis device with an exhaust gas purification system and a purification method thereof.
Background
Organic synthesis refers to the process of chemically making simple substances, simple inorganic substances or simple organic substances into relatively complex organic substances.
In the organic synthesis process, the materials are generally put into an organic synthesis device to perform sufficient reaction mixing, and in the organic synthesis process of some medicines, some harmful exhaust gases are generated, so that people can install an exhaust gas purification system on the organic synthesis device to purify the harmful exhaust gases.
In the related art, an organic synthesis device with an exhaust gas purification system for pharmaceutical use is disclosed, such as CN113350963a, comprising a purification tube; the inside of the purifying pipe is hollow, and the bottom of the purifying pipe is communicated with an exhaust pipe of the organic synthesis equipment; the upper end and the lower end of the conversion frame are respectively connected with the outer side of the purifying pipe, and the manual mechanism is connected inside the conversion frame; the assembly connecting pipes are arranged at two positions in total and are connected with the conversion frame.
The prior art adopts active carbon to filterable type of waste gas, needs periodic change active carbon plate, and in the change process, although has kept the purge tube leakproofness, but because the change process is in the external environment, still can not avoid waste gas to reveal away in the manual operation in-process of staff, simultaneously, whole change operation is comparatively loaded down with trivial details to at filterable in-process, because the storage mode of active carbon plate is simple filling mode, and set up the air vent at the both ends of active carbon plate, make the gas can form the shortest distance through at the in-process of passing through, cause time and the space of gas and active carbon contact limited, be unfavorable for the abundant filtration to gas.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides an organic synthesis device with an exhaust gas purification system and a purification method thereof.
In order to achieve the above purpose, the invention adopts the following technical scheme: an organic synthesis device with an exhaust gas purification system, comprising: the synthesis device comprises a synthesis device main body, wherein the top of the synthesis device main body is provided with an exhaust gas purification mechanism for purifying exhaust gas generated by the synthesis device main body, the exhaust gas purification mechanism comprises a support frame, an exhaust gas purification container is fixedly arranged at the upper end of the support frame, the top of the exhaust gas purification container is communicated with a spray pipe fitting, an air inlet at the bottom of the exhaust gas purification container is communicated with a filtered waste collection container fixedly arranged at the lower end of the support frame through a pipeline, and the outer side of the filtered waste collection container is communicated with an exhaust port at the top of the synthesis device main body through a pipeline;
An exhaust gas filtering component for filtering and purifying the exhaust gas entering the exhaust gas purifying container is arranged in the exhaust gas purifying container, a filtering filler for filtering the exhaust gas is filled in the exhaust gas filtering component, and a filling component for supplementing the filtering filler into the exhaust gas filtering component is also arranged on the exhaust gas purifying container;
when the filtering effect of the filtering filler is saturated, the filtering filler in the waste gas filtering component is discharged downwards into the filtering waste material collecting container through the waste gas filtering component, and then new filtering filler is supplemented into the waste gas filtering component through the filling component, so that the automatic replacement function of the filtering filler in the waste gas purifying container is realized.
Preferably, the exhaust gas filtering component comprises a circular top plate horizontally and fixedly installed on the inner wall of the exhaust gas purifying container, two exhaust gas discharge slots are formed in the top of the circular top plate in a penetrating manner at positions deviating from the circle center, a separation screen plate is fixedly installed in the exhaust gas discharge slots far away from one side of the filling component, a rotating motor is fixedly installed at the circle center of the top of the circular top plate, a first circular plate is fixedly installed at the output end of the rotating motor after penetrating through the bottom of the circular top plate in a rotating manner, the upper end face of the first circular plate is attached to the lower end face of the circular top plate, a plurality of exhaust gas circulation slots which are uniformly distributed in a circumferential array are formed in the top of the first circular plate in a penetrating manner, and the exhaust gas discharge slots moving to the positions of the two exhaust gas circulation slots are all communicated with the exhaust gas circulation slots at the corresponding positions;
The bottom of first circular plate has the second circular plate through separating member fixed mounting, first circular plate with the outside of second circular plate all with exhaust gas purification container's inside wall closely laminates, the separating member will first circular plate with the space between the second circular plate evenly cuts apart into a plurality of sectorial filtration packing storage areas, the bottom of second circular plate corresponds a plurality of filtration packing storage area position link up and has seted up the row's material notch, the bottom of second circular plate is provided with a plurality of be used for right row's silo mouth carries out shutoff's shutoff subassembly.
Preferably, the partition member comprises a central column body fixedly installed between the first circular plate and the second circular plate, a plurality of partition plates distributed in a circumferential array are fixedly installed on the outer side of the central column body, one partition plate is a solid plate, and a plurality of waste gas passing holes are uniformly formed in the rest partition plates.
Preferably, the plugging assembly comprises a sliding baffle plate slidably mounted at the bottom of the second circular plate, a tension spring is fixedly mounted between one side of the sliding baffle plate, which is close to the center of the circle of the second circular plate, and the second circular plate, a magnetic block is fixedly mounted on one side of the sliding baffle plate, which is far away from the circle of the second circular plate, a first electromagnet is fixedly mounted on the inner side wall of the waste gas purifying container, and after the magnetic block is exactly aligned with the first electromagnet, a magnetic force for attracting the magnetic block is generated through electrifying the first electromagnet, so that the sliding baffle plate slides;
And a plurality of waste gas inlet holes are uniformly formed in the top of the sliding baffle plate, which is close to the position of the partition plate, which is a solid plate, and waste gas enters the filtering filler storage area above the waste gas inlet holes, sequentially passes through the remaining filtering filler storage areas along the circumferential direction, and finally flows out of the waste gas circulation notch.
Preferably, the exhaust gas filtering component further comprises a plurality of stirring assemblies for stirring the filter filler in the filter filler storage area, two overturning grooves are symmetrically formed in the bottom wall of the filter filler storage area, one stirring assembly is correspondingly arranged on each overturning groove, each stirring assembly comprises a stirring piece and a connecting bracket, the stirring pieces are rotatably arranged in the overturning grooves, the connecting brackets are fixedly arranged on the outer sides of the second circular plates, a first bevel gear is rotatably arranged at the lower ends of the connecting brackets, a limiting groove is formed in one side, close to the second circular plates, of the first bevel gear, a rotating shaft, far away from one end of the second circular plates, rotates to penetrate through the outer sides of the second circular plates, and then is fixedly provided with a limiting block which is slidably arranged in the limiting groove, and a supporting spring is fixedly arranged between the limiting block and the limiting groove;
The upper end of linking bridge has seted up the sliding tray, the meshing has the second bevel gear on the first bevel gear, the axis of rotation outside of second bevel gear with sliding tray sliding connection, fixed cover about the second bevel gear outside is equipped with spacing ring, spacing ring with linking bridge's side slip laminating, the top fixed mounting of second bevel gear axis of rotation has the wheel that rolls, waste gas purification container inner wall side is close to the ring channel has been seted up in the wheel position that rolls, roll the outside of wheel with the laminating of ring channel inside wall, the linking bridge first bevel gear the second bevel gear all is located in the ring channel.
Preferably, the exhaust gas filtering component further comprises a driving component for driving the stirring component to rotate, the driving component comprises a plurality of butt joint blocks and an electric push rod fixedly installed in the annular groove, the butt joint blocks are correspondingly and fixedly installed on one side, away from the second circular plate, of the first bevel gear, an installation seat is fixedly installed at the telescopic end of the electric push rod, two micro motors are symmetrically and fixedly installed on the installation seat, one side, close to the second circular plate, of each micro motor is fixedly installed with a pushing plate, one end, away from each micro motor, of each pushing plate is provided with an arc-shaped notch matched with a rotating shaft of the second bevel gear, one end, close to each butt joint block, of each micro motor rotating shaft is fixedly installed with two limiting pins, and one side, away from each first bevel gear, of each butt joint block is provided with a butt joint notch matched with an output shaft of each micro motor.
Preferably, the filling component comprises a storage container and a guide ring body, the storage container is fixedly arranged at the top of the waste gas purifying container, the guide ring body is fixedly arranged at the back of the top of the circular top plate and is communicated with one of the waste gas discharge slots, a discharge port at the bottom of the storage container is communicated with a guide pipeline with a telescopic function, the bottom end of the guide pipeline is slidingly extended to the upper end of the guide ring body, a guide plug is communicated with the upper end of the guide ring body, and a sealing plug with a cross gap is horizontally and fixedly arranged on the inner side wall of the guide ring body;
the outer side of the guide plug and the top end of the guide ring body are fixedly provided with second electromagnets, the outer side of the guide pipeline is sleeved with a connecting spring, and the upper end and the lower end of the supporting spring are fixedly connected with the guide pipeline and the top end of the guide plug respectively;
the two electromagnets are electrified to generate attractive magnetic force, so that the guide plug moves downwards and penetrates through the sealing plug.
Preferably, one filtering filler storage area is arranged between the two exhaust gas discharge slots, and the discharge slot is positioned at the middle position of the bottom wall of the filtering filler storage area.
Preferably, the bottom wall of the exhaust gas purifying container is provided with a conical structure, and the filter filler is circular activated carbon particles.
A purification method of an exhaust gas purification system, comprising the steps of:
s1, introducing waste gas generated by a synthesis device main body into a filtering waste collection container through a pipeline, and then entering a waste gas purifying container through the filtering waste collection container;
s2, the waste gas enters the waste gas filtering component, flows in the waste gas filtering component along the circumferential direction, fully contacts with the filter fillers in the filter filler storage areas at different positions, and filters the waste gas;
and S3, finally, discharging the waste gas from the upper end of the waste gas filtering component, and discharging the waste gas from a spraying pipe fitting at the top end of the waste gas purifying container.
Compared with the prior art, the invention has the following beneficial effects:
through setting up this exhaust purification mechanism, except possessing the effect to waste gas purification, through waste gas purification container, waste gas filtering part, filling part and filtration waste collection container cooperation use, accomplish the change function to the filtration packing, through directly discharging and filling the filtration packing of granule dress, and whole process all is in airtight environment, on the one hand, in the change process, can not shut down the synthetic device main part because of filtration packing changes, avoid delaying organic synthesis process, simultaneously, still avoided the problem that waste gas outwards revealed; on the other hand, the method of directly replacing the filter packing is adopted, so that the replacement step is simplified, and the automatic operation can be realized in the replacement process, thereby being beneficial to accelerating the replacement speed of the filter packing and reducing the workload of staff;
Through setting up this exhaust gas filtering component and mainly being used to carry out filtration to waste gas, wherein, through using first circular plate, second circular plate and separator cooperation, form a plurality of evenly distributed's filter filler storage area, can make waste gas pass through the filter filler storage area of different positions in proper order along circumferencial direction, be favorable to increasing waste gas and filter filler contact chance for the contact time of filter filler and waste gas is longer, and then helps promoting the purifying effect of filter filler to waste gas.
Drawings
Fig. 1 is a flow chart of a purification method with an exhaust gas purification system provided by the invention.
Fig. 2 is a schematic structural diagram of an organic synthesis device with an exhaust gas purification system according to the present invention.
Fig. 3 is a partial cutaway view of an exhaust gas purifying mechanism provided by the present invention.
Fig. 4 is a partial enlarged view of the region a shown in fig. 3.
Fig. 5 is a partial enlarged view of the region B shown in fig. 3.
Fig. 6 is a schematic structural view of the packing member and the exhaust gas filtering member provided by the present invention.
Fig. 7 is an exploded view of an exhaust gas filtering member provided by the present invention.
Fig. 8 is a schematic structural view of a second circular plate according to the present invention.
Fig. 9 is a schematic structural view of an agitation assembly according to the present invention.
Fig. 10 is a partial enlarged view of the region C shown in fig. 9.
Fig. 11 is a partial cutaway view of an agitation assembly provided by the present invention.
Fig. 12 is a partial cutaway view of a filler component provided by the present invention.
In the figure: 1. A synthesis device body; 2. an exhaust gas purifying mechanism; 21. a support frame; 22. an exhaust gas purifying vessel; 23. spraying the pipe fitting; 24. a filtration waste collection vessel; 25. an exhaust gas filtering member; 251. a circular top plate; 252. an exhaust gas discharge slot; 2521. a separation screen; 253. a rotating motor; 254. a first circular plate; 255. an exhaust gas flow slot; 256. a partition; 2561. a central column; 2562. a partition plate; 2563. an exhaust gas passing hole; 257. a second circular plate; 258. a filter packing storage area; 259. a plugging assembly; 2591. a sliding baffle; 2592. a tension spring; 2593. a magnetic block; 2594. a first electromagnet; 2595. an exhaust gas inlet; 2510. a discharge slot; 2511. a turnover groove; 26. a loading member; 261. a storage container; 262. a material guiding ring body; 263. a material guiding pipeline; 264. a material guiding plug; 265. a sealing plug; 266. a second electromagnet; 267. a connecting spring; 27. an agitation assembly; 271. an agitating member; 272. a connecting bracket; 273. a first bevel gear; 274. a limit groove; 275. a limiting block; 276. a support spring; 277. a rolling wheel; 278. a second bevel gear; 279. a sliding groove; 2710. a limit circular ring; 28. an annular groove; 29. a drive assembly; 291. a butt joint block; 292. an electric push rod; 293. a mounting base; 294. a micro motor; 295. a pushing plate; 296. an arc-shaped notch; 297. and a butt joint notch.
Description of the embodiments
The following description is presented to enable one of ordinary skill in the art to make and use the invention. The preferred embodiments in the following description are by way of example only and other obvious variations will occur to those skilled in the art.
Referring to fig. 1 to 12 in combination, the organic synthesis apparatus with an exhaust gas purifying system and the purifying method thereof include: the synthesis device comprises a synthesis device main body 1, wherein an exhaust gas purifying mechanism 2 for purifying exhaust gas generated by the synthesis device main body 1 is arranged at the top of the synthesis device main body 1, the exhaust gas purifying mechanism 2 comprises a support frame 21, an exhaust gas purifying container 22 is fixedly arranged at the upper end of the support frame 21, a spraying pipe fitting 23 is communicated with the top of the exhaust gas purifying container 22, a filtering waste collecting container 24 fixedly arranged at the lower end of the support frame 21 is communicated with an air inlet at the bottom end of the exhaust gas purifying container 22 through a pipeline, and the outer side of the filtering waste collecting container 24 is communicated with an air outlet at the top of the synthesis device main body 1 through a pipeline;
an exhaust gas filtering component 25 for filtering and purifying the exhaust gas entering the exhaust gas purifying container 22 is arranged in the exhaust gas purifying container 22, a filtering filler for filtering the exhaust gas is filled in the exhaust gas filtering component 25, and a filling component 26 for supplementing the filtering filler into the exhaust gas filtering component 25 is also arranged on the exhaust gas purifying container 22;
When the filtering action of the filtering filler is saturated, the filtering filler in the filtering filler is discharged downwards into the filtering waste collection container 24 through the waste gas filtering component 25, and then new filtering filler is supplemented into the waste gas filtering component 25 through the filling component 26, so that the automatic replacement function of the filtering filler in the waste gas purifying container 22 is realized.
In order to solve the problem of outward leakage of waste gas in the process of replacing filter fillers, when the organic synthesis device provided by the invention is used, waste gas generated by a synthesis device main body 1 firstly enters a filter waste collection container 24 through a pipeline, then enters a waste gas purification container 22 from the filter waste collection container 24, then enters a waste gas filtering part 25, the filtered waste gas is filtered through the filter fillers in the waste gas filtering part 25, the filtered waste gas flows into a spray pipe fitting 23 through the pipeline, the spray pipe fitting 23 continuously sprays the passed waste gas, and finally the sprayed waste gas is discharged through the spray pipe fitting 23, so that the waste gas is purified;
when the filtering effect of the filtering filler reaches saturation and needs to be replaced, the internal filtering filler is directly discharged through the waste gas filtering component 25, the discharged filtering filler flows into a filtering filler collecting container along a pipeline to be temporarily stored, and then, the new filtering filler is continuously filled into the waste gas filtering component 25 through a filling component 26, so that the replacement operation of the filtering filler is realized;
A waste discharge port is arranged at the bottom of the filtering waste collection container 24, and after the filtering waste in the filtering waste collection container 24 reaches a certain amount, the stored filtering filler can be manually cleaned out from the waste discharge port in the shut-down state of the synthesis device main body 1;
by arranging the waste gas purifying mechanism 2, besides the function of purifying waste gas, the waste gas purifying container 22, the waste gas filtering part 25, the filling part 26 and the filtering waste collection container 24 are matched for use, so that the function of replacing the filtering filler is completed, the filtering filler filled with particles is directly discharged and filled, and the whole process is in a closed environment, on one hand, in the replacement process, the synthesis device main body 1 is not shut down because the filtering filler is replaced, the organic synthesis process is prevented from being delayed, and meanwhile, the problem of outward leakage of waste gas is also avoided; on the other hand, the mode of directly replacing the filter packing is adopted, the replacement step is simplified, and the automatic operation can be realized in the replacement process, so that the replacement speed of the filter packing is increased, and the workload of staff is reduced.
As an embodiment of the present invention, the exhaust gas filtering component 25 includes a circular top plate 251 horizontally and fixedly installed on the inner wall of the exhaust gas purifying container 22, two exhaust gas discharge slots 252 are formed through the top of the circular top plate 251 at positions deviating from the center of the circle, a separation screen 2521 is fixedly installed inside the exhaust gas discharge slots 252 at a side far from the loading component 26, a rotating motor 253 is fixedly installed at the center of the top of the circular top plate 251, an output end of the rotating motor 253 rotates and penetrates through the bottom of the circular top plate 251, a first circular plate 254 is fixedly installed, an upper end surface of the first circular plate 254 is attached to a lower end surface of the circular top plate 251, a plurality of exhaust gas circulation slots 255 uniformly distributed in a circumferential array are formed through the top of the first circular plate 254, and the exhaust gas discharge slots 252 moving to the positions of the two exhaust gas circulation slots 255 are all communicated with the exhaust gas circulation slots 255 at corresponding positions;
The bottom of first circular plate 254 has second circular plate 257 through separating member 256 fixed mounting, first circular plate 254 with the outside of second circular plate 257 all with exhaust purification container 22's inside wall closely laminates, separating member 256 will the space between first circular plate 254 with the second circular plate 257 evenly cuts apart into a plurality of sectorial filter filler storage areas 258, the bottom of second circular plate 257 corresponds a plurality of filter filler storage areas 258 position link up and have seted up discharge slot 2510, the bottom of second circular plate 257 is provided with a plurality of shutoff subassemblies 259 that are used for carrying out shutoff to discharge slot 2510.
In the process of filtering the waste gas by using the waste gas filtering component 25, the waste gas flows upwards from the lower end of the waste gas purifying container 22, enters into the corresponding filtering filler storage area 258 above the plugging component 259 from the bottom of the plugging component 259, contacts with the filtering filler in the filtering filler, filters the passing waste gas by the filtering filler, then passes through the residual filtering filler storage area 258 one by one along the circumferential direction, and finally is discharged upwards from the waste gas discharge notch 252, thus completing the filtering treatment of the waste gas;
As an embodiment of the present invention, the partition 256 includes a central cylinder 2561 fixedly installed between the first circular plate 254 and the second circular plate, a plurality of partitions 2562 distributed in a circumferential array are fixedly installed on the outer side of the central cylinder 2561, one of the partitions 2562 is a solid plate, and a plurality of exhaust gas passing holes 2563 are uniformly formed in the remaining partitions 2562.
In order to realize the function that the above-mentioned exhaust gas sequentially passes through the plurality of filter packing storage areas 258 in the circumferential direction in the exhaust gas filtering member 25, the partition 256 is provided to divide the space between the first circular plate 254 and the second circular plate 257, and the exhaust gas firstly enters the filter packing storage areas 258 where the partition 2562, which is a solid plate, is located during the circulation between the filter packing storage areas 258, and then flows into the next filter packing storage area through the partition 2562 with the exhaust gas passing holes 2563 at the side, thus continuously passes through the filter packing storage areas at different positions, and finally is discharged upward from the exhaust gas discharging slot 252;
through setting up this exhaust gas filtering component 25 mainly used and carrying out filtration treatment to waste gas, wherein, through using first circular plate 254, second circular plate 257 and separator 256 cooperation, form a plurality of evenly distributed's filter filler storage area 258, can make waste gas pass through the filter filler storage area 258 of different positions in proper order along the circumferencial direction, be favorable to increasing waste gas and filter filler contact chance for filter filler and waste gas's contact time is longer, and then helps promoting the purifying effect of filter filler to waste gas.
As an embodiment of the present invention, the plugging assembly 259 includes a sliding plate 2591 slidably mounted at the bottom of the second circular plate 257, an extension spring 2592 is fixedly mounted between one side of the sliding plate 2591 near the center of the second circular plate 257 and the second circular plate 257, a magnetic block 2593 is fixedly mounted on one side of the sliding plate 2591 away from the circular shape of the second circular plate 257, a first electromagnet 2594 is fixedly mounted on the inner side wall of the exhaust gas purifying container 22, and after the magnetic block 2593 is exactly aligned with the first electromagnet 2594, a magnetic force attracting the magnetic block 2593 is generated by energizing the first electromagnet 2594, so that the sliding plate 2591 slides;
a plurality of exhaust gas inlet holes 2595 are uniformly formed in the top of the sliding block 2591 near the position of the partition plate 2562, which is a solid plate, and exhaust gas enters the upper filter packing storage area 258 through the exhaust gas inlet holes 2595, then sequentially passes through the remaining filter packing storage area 258 along the circumferential direction, and finally flows out from the exhaust gas circulation slots 255.
In order to realize the filter filler discharging function of the filter filler storage area 258 with saturated filter function, the filter filler storage area 258 is blocked by arranging the blocking component 259, when the filter filler in the filter filler storage area is required to be discharged, the waste gas filtering component 25 is in a static state and just aligns the first electromagnet 2594 with one of the blocking components 259, at the moment, the first electromagnet 2594 is electrified to generate magnetic force attracted to the magnetic block 2593, the sliding baffle 2591 can be pulled outwards to slide, the extension spring 2592 is stretched, the discharge slot 2510 is gradually opened, the filter filler in the filter filler storage area 258 is directly discharged downwards through the discharge slot 2510, after the set time is reached, the first electromagnet 2594 is powered off, the sliding baffle 2591 starts to slide and reset under the elastic force of the extension spring 2592, and finally the discharge slot 2510 is blocked, so that the discharging operation of the filter filler storage area 258 is completed;
The plugging assembly 259 is mainly used for controlling the discharge port 2510 to be conducted and closed, the sliding baffle 2591 is driven to slide by utilizing the magnetic attraction effect of the first electromagnet 2594 and the magnetic block 2593, the sliding baffles 2591 at different positions can be respectively driven to be opened by one first electromagnet 2594, the structure of the plugging assembly 259 is simplified, and the use cost of the plugging assembly 259 is saved.
As an embodiment of the present invention, the exhaust gas filtering component 25 further includes a plurality of stirring assemblies 27 for stirring the filtering filler in the filtering filler storage area 258, two turning slots 2511 are symmetrically formed on the bottom wall of the filtering filler storage area 258, one stirring assembly 27 is correspondingly disposed on the turning slots 2511, the stirring assembly 27 includes a stirring member 271 and a connecting bracket 272, the stirring member 271 is rotatably mounted in the turning slots 2511, the connecting bracket 272 is fixedly mounted on the outer side of the second circular plate 257, a first bevel gear 273 is rotatably mounted at the lower end of the connecting bracket 272, a limiting slot 274 is formed on one side of the first bevel gear 273, which is close to the second circular plate 257, a limiting block 275 is fixedly mounted after the rotating shaft of one end of the stirring member 271, which is far from the second circular plate 257, rotates to penetrate the outer side of the second circular plate 257, the limiting block 275 is slidably mounted in the limiting slot 274, a supporting spring 276 is fixedly mounted between the limiting block 275 and the limiting block 274, the limiting block 274 is a six-prismatic block, and the first bevel gear 273 is rotatably driven by the limiting block 271, and the first bevel gear 271 can be horizontally rotated along the rotating shaft.
The upper end of linking bridge 272 has seted up slide groove 279, the meshing has the second bevel gear 278 on the first bevel gear 273, the axis of rotation outside of the 278 of second bevel gear with slide groove 279 sliding connection, the fixed cover is equipped with spacing ring 2710 about the second bevel gear 278 outside, spacing ring 2710 with the side slip laminating of linking bridge 272, the top fixed mounting of second bevel gear 278 axis of rotation has the roll wheel 277, waste gas purification container 22 inner wall side is close to roll wheel 277 position has seted up ring channel 28, roll wheel 277's outside with ring channel 28 inside wall laminating, linking bridge 272 first bevel gear 273 second bevel gear 278 all is located in the ring channel 28.
In the process of filtering the exhaust gas by using the filter packing, in order to make the filter packing fully contact with the exhaust gas, the stirring assembly 27 is arranged to stir the filter packing, when stirring is performed, the rotating motor 253 rotates to drive the first circular plate 254, the partition 256 and the second circular plate 257 to rotate together, at this time, the rolling wheel 277 synchronously rolls along the inner side wall of the annular groove 28 along with the second circular plate 257, the second bevel gear 278 drives the first bevel gear 273 to rotate through the rolling action of the rolling wheel 277, the stirring piece 271 rotates in the turnover groove 2511 along with the first bevel gear 273, and the filter packing can be stirred through the continuous rotation of the stirring piece 271, so that the placement state of the filter packing is changed;
Through setting up this stirring subassembly 27, can realize the automatic stirring function to the filter media, after the filter media uses a period, through driving first circular plate 254, separator 256 and the synchronous rotation of second circular plate 257, impel the roll wheel 277 to drive stirring piece 271 rotation, and utilize stirring effect that stirring piece 271, can place the state to the filter media and adjust, help increasing filter media and comprehensive contact of waste gas, avoid waste gas to contact with the filter media of the same position all the time, and then help promoting the filter effect of filter media.
As an embodiment of the present invention, the exhaust gas filtering component 25 further includes a driving component 29 configured to drive the stirring component 27 to rotate, where the driving component 29 includes a plurality of docking blocks 291 and an electric push rod 292 fixedly installed in the annular groove 28, the docking blocks 291 are correspondingly and fixedly installed on a side of the first bevel gear 273 away from the second circular plate 257, a mounting seat 293 is fixedly installed at a telescopic end of the electric push rod 292, two micro motors 294 are symmetrically and fixedly installed on the mounting seat 293, a pushing plate 295 is fixedly installed on a side of the micro motor 294 close to the second circular plate 257, an arc notch 296 adapted to a rotation shaft of the second bevel gear 278 is provided at an end of the pushing plate 295 away from the micro motor 294, two limit pins are fixedly installed at an end of the micro motor 294 close to the rotation shaft of the docking block 291, and a docking notch 297 adapted to an output shaft of the micro motor 294 is provided at a side of the docking block 291 away from the first bevel gear 273.
During the filter media discharge process, to facilitate subsequent re-addition of filter media to filter media storage area 258, exhaust gas filter element 25 is controlled to rest, but to facilitate filter media discharge by providing drive assembly 29 to agitate assembly 27 for continued rotation due to the limited size of the notch of discharge slot 2510;
when the driving assembly 29 is matched with the stirring assembly 27 for use, at the moment, the two stirring assemblies 27 are just aligned with the driving assembly 29, then, the electric push rod 292 stretches to drive the mounting seat 293 and the two micro motors 294 to approach the butting block 291, the output ends of the micro motors 294 are enabled to be in contact with the butting block 291, at the moment, the output shafts of the micro motors 294 may not be aligned with the butting grooves 297, the electric push rod 292 continues to stretch to enable the butting block 291 and the first bevel gear 273 to be pressed and slide along the rotating shaft surface of the stirring member 271, the supporting springs 276 are compressed, in the process, the arc-shaped notch 296 at the end part of the pushing plate 295 is attached to the rotating shaft of the second bevel gear 278, the second bevel gear 278 can be pushed to slide on the connecting bracket 272, the rolling wheel 277 is further driven to be separated from the side wall of the second bevel gear 278, then, the electric push rod 292 stops stretching, at the moment, the rotating through the rotating shaft of the micro motors 294 is enabled to rotate on the side surfaces of the butting block 291 until the rotating shafts of the micro motors 294 are aligned with the butting grooves on the butting block 291, and under the elastic force of the supporting springs 276, the rotating shafts of the micro motors 294 can drive the second bevel gear 294 to rotate with the second bevel gear 278;
While under the operation of the plugging assembly 259, the discharge slot 2510 is opened, the filter charges are discharged downwards through the discharge slot 2510, and under the stirring action of the stirring member 271, the filter charges are promoted to move, so as to help to promote the discharge speed of the filter charges, as much as possible, after the set time is reached, the electric push rod 292 starts to be shortened, the mounting seat 293 and the micro motor 294 are gradually reset, the rotation shaft of the micro motor 294 is separated from the butting block 291, then the first circular plate 254, the partition 256 and the second circular plate 257 are driven to rotate again by the rotation motor 253, the two stirring assemblies 27 on the next filter charge storage area 258 are aligned with the driving assembly 29 again, the driving assembly 29 is butted with the two stirring assemblies 27 on the next set, and the filter charges are assisted to be discharged, so that the repeated operation is that the rotation direction of the micro motor 294 drives the two stirring members to be in the direction of the partition 2562 to the discharge slot 2510, so as to promote the filter charges to move towards the discharge slot 2510.
As an embodiment of the present invention, the filling unit 26 includes a storage container 261 and a guide ring 262, the storage container 261 is fixedly mounted on the top of the exhaust gas purifying container 22, the guide ring 262 is fixedly mounted on the top of the circular top plate 251 and is communicated with one of the exhaust gas discharge slots 252, a discharge port at the bottom of the storage container 261 is communicated with a guide pipe 263 having a telescopic function, a guide plug 264 is communicated at the bottom end of the guide pipe 263 and extends to the upper end of the guide ring 262 in a sliding manner, and a sealing plug 265 with a cross slit is horizontally and fixedly mounted on the inner side wall of the guide ring 262, so that exhaust gas can be prevented from flowing out of the exhaust gas circulation slot 255 by adopting the sealing plug 265;
The outer side of the guide plug 264 and the top end of the guide ring body 262 are fixedly provided with second electromagnets 266, the outer side of the guide pipe 263 is sleeved with a connecting spring 267, and the upper end and the lower end of the supporting spring 276 are fixedly connected with the guide pipe 263 and the top end of the guide plug 264 respectively;
the attractive magnetic force generated by the two electromagnets after the electromagnets are electrified causes the guide plug 264 to move downwards and penetrate the sealing plug 265.
After the filter filler is discharged, the filling part 26 is required to be used for continuously replenishing new filter filler into the filter filler storage area 258, in the process of filling the filter filler which is too difficult to fill, the discharged filter filler storage area 258 rotates to the position below the filling part 26, just the exhaust gas circulation notch 255 is aligned with and communicated with the exhaust gas discharge notch 252, at the moment, the two second electromagnets 266 are electrified and generate magnetic force which is mutually attracted, the guide pipeline 263 and the guide plug 264 can be driven to move downwards, and the supporting spring 276 is synchronously lengthened, at the moment, the bottom end of the guide plug 264 is of a tip structure and can smoothly penetrate through a cross gap on the sealing plug 265, then, a valve on the guide pipeline 263 is opened, so that the filter filler in the storage area 261 is discharged by the guide plug 264, and finally falls into the filter filler storage area 258 below through the exhaust gas discharge notch 252 until the set filling amount is reached, at the moment, the filler inside the filter filler storage area 258 is not full, the condition that the stirring part is difficult to stir is avoided, then, the two second electromagnets 266 lose the magnetic force effect and the attraction effect is lost, and the elastic force of the connecting spring 267 can be used for connecting the guide pipeline 263 to stretch, the guide pipeline 263 can be separated from the filter filler storage area 258, the filter filler can be continuously rotated until the filter filler is completely rotates to the position of the round filler storage area 258, and the filter filler is completely rotates, and the filter filler storage area is completely filled by rotating the round filler storage area 258, and the filter filler is completely separated by rotating by the sealing material, and the filter filler is filled by the filter filler, and the filter filler is filled by the filler, and has the filling is filled by the filler, and is filled;
Through setting up this filling part 26 and waste gas filter part 25 cooperation and using, realized the automatic discharging and the automatic charging operation of filter packing, on the one hand, can accomplish the change operation to filter packing, on the other hand, in discharging and charging process, evenly operate each filter packing one by one, can make whole filter packing change in-process, there is the filter packing all the time in the filter packing storage area 258 to exist for waste gas all the time with the filter packing, avoid appearing the filter packing neutral gear, and then help maintaining the filter effect of waste gas filter part 25 during the filter packing.
As an embodiment of the present invention, the two exhaust gas discharge slots 252 are spaced apart by one of the filter packing storage areas 258, and the discharge slot 2510 is provided at a middle position of the bottom wall of the filter packing storage area 258.
As an embodiment of the present invention, the bottom wall of the exhaust gas purifying container 22 is provided with a conical structure, and the filter packing is made of round activated carbon particles, which can facilitate the movement of the filter packing and the discharge of the filter packing.
A purification method of an exhaust gas purification system, comprising the steps of:
S1, introducing waste gas generated by a synthesis device main body 1 into a filtering waste collection container 24 through a pipeline, and then entering a waste gas purifying container 22 through the filtering waste collection container 24;
s2, the waste gas enters the waste gas filtering component 25, flows in the waste gas filtering component 25 along the circumferential direction, fully contacts with the filter fillings in the filter filling storage areas 258 at different positions, and filters the waste gas;
and S3, finally, discharging the waste gas from the upper end of the waste gas filtering component 25, and discharging the waste gas from the spray pipe fitting 23 at the top end of the waste gas purifying container 22.
The foregoing has shown and described the basic principles, principal features and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the foregoing embodiments, but rather, the foregoing embodiments and description illustrate the principles of the invention, and that various changes and modifications may be effected therein without departing from the spirit and scope of the invention as defined by the appended claims and their equivalents.
Claims (10)
1. An organic synthesis device with an exhaust gas purification system, comprising: the synthesis device comprises a synthesis device main body (1), wherein an exhaust gas purifying mechanism (2) for purifying exhaust gas generated by the synthesis device main body (1) is arranged at the top of the synthesis device main body (1), the exhaust gas purifying mechanism (2) comprises a support frame (21), an exhaust gas purifying container (22) is fixedly arranged at the upper end of the support frame (21), a spray pipe fitting (23) is communicated with the top of the exhaust gas purifying container (22), and the synthesis device is characterized in that a filtering waste collection container (24) fixedly arranged at the lower end of the support frame (21) is communicated with an air inlet at the bottom end of the exhaust gas purifying container (22) through a pipeline, and the outer side of the filtering waste collection container (24) is communicated with an air outlet at the top of the synthesis device main body (1) through a pipeline;
An exhaust gas filtering component (25) for filtering and purifying the exhaust gas entering the exhaust gas purifying container (22) is arranged in the exhaust gas purifying container (22), a filtering filler for filtering the exhaust gas is filled in the exhaust gas filtering component (25), and a filling component (26) for supplementing the filtering filler into the exhaust gas filtering component (25) is also arranged on the exhaust gas purifying container (22);
when the filtering effect of the filtering filler is saturated, the filtering filler in the filtering filler is discharged downwards into the filtering waste collecting container (24) through the waste filtering component (25), and then new filtering filler is supplemented into the waste filtering component (25) through the filling component (26), so that the automatic replacement function of the filtering filler in the waste purifying container (22) is realized.
2. An organic synthesis device with an exhaust gas purification system according to claim 1, wherein the exhaust gas filtering component (25) comprises a circular top plate (251) horizontally and fixedly installed on the inner wall of the exhaust gas purification container (22), two exhaust gas discharge slots (252) are formed in a penetrating manner at the top of the circular top plate (251) at the deviated circle center position, a separation screen plate (2521) is fixedly installed in the interior of the exhaust gas discharge slots (252) at the side far away from the filling component (26), a rotating motor (253) is fixedly installed at the circle center position of the top of the circular top plate (251), a first circular plate (254) is fixedly installed after the output end of the rotating motor (253) rotates to penetrate through the bottom of the circular top plate (251), the upper end face of the first circular plate (254) is attached to the lower end face of the circular top plate (251), a plurality of exhaust gas circulation slots (255) which are uniformly distributed in a circumferential array are formed in a penetrating manner at the top of the first circular plate (254), and the exhaust gas discharge slots (252) which are moved to the positions of the two circulation slots (255) are communicated with the corresponding exhaust gas circulation slots (255);
The bottom of first circular plate (254) is through separating member (256) fixed mounting has second circular plate (257), first circular plate (254) with the outside of second circular plate (257) all with the inside wall of exhaust purification container (22) closely laminates, separating member (256) will first circular plate (254) with space between second circular plate (257) evenly cuts apart into a plurality of sectorial filter filler storage areas (258), the bottom of second circular plate (257) corresponds a plurality of filter filler storage area (258) position link up and have seted up discharge notch (2510), the bottom of second circular plate (257) is provided with a plurality of be used for right discharge notch (2510) shutoff subassembly (259).
3. The organic synthesis device with an exhaust gas purification system according to claim 2, wherein the partition member (256) comprises a central column (2561) fixedly installed between the first circular plate (254) and the second circular plate, a plurality of partition plates (2562) distributed in a circumferential array are fixedly installed on the outer side of the central column (2561), one of the partition plates (2562) is a solid plate, and a plurality of exhaust gas passing holes (2563) are uniformly formed in the rest of the partition plates (2562).
4. An organic synthesis device with an exhaust gas purification system according to claim 3, wherein the plugging assembly (259) comprises a sliding baffle (2591) slidingly mounted at the bottom of the second circular plate (257), an extension spring (2592) is fixedly mounted between one side of the sliding baffle (2591) close to the center of the second circular plate (257) and the second circular plate (257), a magnetic block (2593) is fixedly mounted on one side of the sliding baffle (2591) away from the circular shape of the second circular plate (257), a first electromagnet (2594) is fixedly mounted on the inner side wall of the exhaust gas purification container (22), and after the magnetic block (2593) is aligned with the first electromagnet (2594), a magnetic force attracting the magnetic block (2593) is generated by electrifying the first electromagnet (2594), so that the sliding baffle (2591) slides;
a plurality of exhaust gas inlet holes (2595) are uniformly formed in the top of the sliding baffle plate (2591) close to the position of the partition plate (2562) which is a solid plate, exhaust gas enters the upper filter packing storage areas (258) from the exhaust gas inlet holes (2595), sequentially passes through the rest filter packing storage areas (258) along the circumferential direction, and finally flows out from the exhaust gas circulation notch (255).
5. The organic synthesis device with the exhaust gas purification system according to claim 2, wherein the exhaust gas filtering component (25) further comprises a plurality of stirring assemblies (27) for stirring the filter packing in the filter packing storage area (258), two turnover grooves (2511) are symmetrically formed in the bottom wall of the filter packing storage area (258), one stirring assembly (27) is correspondingly arranged on the turnover groove (2511), the stirring assembly (27) comprises stirring pieces (271) and connecting brackets (272), the stirring pieces (271) are rotatably arranged in the turnover grooves (2511), the connecting brackets (272) are fixedly arranged on the outer sides of the second circular plates (257), first bevel gears (273) are rotatably arranged at the lower ends of the connecting brackets (272), limit grooves (274) are formed in one sides, close to the second circular plates (257), of the first bevel gears (273), the rotary shafts, far from one ends of the second circular plates (257), penetrate through the second circular plates (257), and are fixedly arranged between the limit blocks (274) and the limit blocks (275) and the limit blocks (274) are fixedly arranged in the limit grooves (274);
The upper end of linking bridge (272) has seted up sliding tray (279), meshing has second bevel gear (278) on first bevel gear (273), the axis of rotation outside of second bevel gear (278) with sliding tray (279) sliding connection, fixed cover is equipped with spacing ring (2710) about second bevel gear (278) outside, spacing ring (2710) with the laminating of side slip of linking bridge (272), the top fixed mounting of second bevel gear (278) axis of rotation has roll wheel (277), exhaust purification container (22) inner wall side is close to roll wheel (277) position and has seted up ring channel (28), roll the outside of wheel (277) with ring channel (28) inside wall laminating, linking bridge (272) first bevel gear (273) second bevel gear (278) all are located in ring channel (28).
6. The organic synthesis device with an exhaust gas purification system according to claim 5, wherein the exhaust gas filtering component (25) further comprises a driving component (29) for driving the stirring component (27) to rotate, the driving component (29) comprises a plurality of butting blocks (291) and an electric push rod (292) fixedly installed in the annular groove (28), the butting blocks (291) are correspondingly and fixedly installed on one side, far away from the second circular plate (257), of the first bevel gear (273), a mounting seat (293) is fixedly installed at the telescopic end of the electric push rod (292), two micro motors (294) are symmetrically and fixedly installed on the mounting seat (293), a pushing plate (295) is fixedly installed on one side, close to the second circular plate (257), of the micro motors (294), one end, far away from the micro motors (291), of the pushing plate (295), is provided with an arc-shaped notch (296) matched with a rotating shaft of the second bevel gear (278), and two butting notches (291) are installed on one end, close to the rotating shaft of the micro motors (294), of the butting blocks (291), and one end, far away from the corresponding mini bevel gear (278).
7. The organic synthesis device with an exhaust gas purification system according to claim 2, wherein the filling component (26) comprises a storage container (261) and a guide ring body (262), the storage container (261) is fixedly arranged at the top of the exhaust gas purification container (22), the guide ring body (262) is fixedly arranged behind the top of the circular top plate (251) and is communicated with one of the exhaust gas discharge slots (252), a discharge hole at the bottom of the storage container (261) is communicated with a guide pipeline (263) with a telescopic function, the bottom end of the guide pipeline (263) is slidingly extended to the upper end of the guide ring body (262) and is communicated with a guide plug (264), and a sealing plug (265) with a cross gap is horizontally and fixedly arranged on the inner side wall of the guide ring body (262);
the outer side of the guide plug (264) and the top end of the guide ring body (262) are fixedly provided with second electromagnets (266), the outer side of the guide pipeline (263) is sleeved with a connecting spring (267), and the upper end and the lower end of the supporting spring (276) are fixedly connected with the guide pipeline (263) and the top end of the guide plug (264) respectively;
The two electromagnets are electrified to generate attractive magnetic force, so that the guide plug (264) moves downwards and penetrates through the sealing plug (265).
8. An organic synthesis device with an exhaust gas purification system according to claim 2, wherein two of the exhaust gas discharge slots (252) are separated by one of the filter packing storage areas (258), the discharge slot (2510) being located in a middle position of the bottom wall of the filter packing storage area (258).
9. An organic synthesis device with an exhaust gas purification system according to claim 1, wherein the bottom wall of the exhaust gas purification vessel (22) is arranged in a conical configuration and the filter packing is circular activated carbon particles.
10. A purification method of an exhaust gas purification system, suitable for an organic synthesis apparatus with an exhaust gas purification system according to any one of claims 1 to 9, comprising the steps of:
s1, introducing waste gas generated by a synthesis device main body (1) into a filtering waste collection container (24) through a pipeline, and then introducing the waste gas into a waste gas purifying container (22) through the filtering waste collection container (24);
S2, the waste gas enters the waste gas filtering component (25), flows in the waste gas filtering component (25) along the circumferential direction, fully contacts with filter fillers in filter filler storage areas (258) at different positions, and filters the waste gas;
and S3, finally, discharging the waste gas from the upper end of the waste gas filtering component (25), and discharging the waste gas from a spray pipe fitting (23) at the top end of the waste gas purifying container (22).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310151739.1A CN116159503A (en) | 2023-02-22 | 2023-02-22 | Organic synthesis device with waste gas purification system and purification method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310151739.1A CN116159503A (en) | 2023-02-22 | 2023-02-22 | Organic synthesis device with waste gas purification system and purification method thereof |
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| Publication Number | Publication Date |
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| CN116159503A true CN116159503A (en) | 2023-05-26 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202310151739.1A Withdrawn CN116159503A (en) | 2023-02-22 | 2023-02-22 | Organic synthesis device with waste gas purification system and purification method thereof |
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| CN (1) | CN116159503A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117101587A (en) * | 2023-10-08 | 2023-11-24 | 山东利兴新材料科技股份有限公司 | Reaction unit is used in ethylene carbonate production |
| CN117815878A (en) * | 2024-01-24 | 2024-04-05 | 昆山鹿城垃圾发电有限公司 | Comprehensive wet decomposition smoke treatment and separation equipment for household garbage |
-
2023
- 2023-02-22 CN CN202310151739.1A patent/CN116159503A/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117101587A (en) * | 2023-10-08 | 2023-11-24 | 山东利兴新材料科技股份有限公司 | Reaction unit is used in ethylene carbonate production |
| CN117101587B (en) * | 2023-10-08 | 2024-07-19 | 山东利兴新材料科技股份有限公司 | Reaction unit is used in ethylene carbonate production |
| CN117815878A (en) * | 2024-01-24 | 2024-04-05 | 昆山鹿城垃圾发电有限公司 | Comprehensive wet decomposition smoke treatment and separation equipment for household garbage |
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