CN116042336A - Method for brewing grape wine rich in procyanidine - Google Patents

Method for brewing grape wine rich in procyanidine Download PDF

Info

Publication number
CN116042336A
CN116042336A CN202310257638.2A CN202310257638A CN116042336A CN 116042336 A CN116042336 A CN 116042336A CN 202310257638 A CN202310257638 A CN 202310257638A CN 116042336 A CN116042336 A CN 116042336A
Authority
CN
China
Prior art keywords
grape
procyanidine
pulp
wine
fermentation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202310257638.2A
Other languages
Chinese (zh)
Inventor
鲁祥云
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sifram Wine Group Co ltd
Original Assignee
Sifram Wine Group Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sifram Wine Group Co ltd filed Critical Sifram Wine Group Co ltd
Priority to CN202310257638.2A priority Critical patent/CN116042336A/en
Publication of CN116042336A publication Critical patent/CN116042336A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G1/00Preparation of wine or sparkling wine
    • C12G1/02Preparation of must from grapes; Must treatment and fermentation
    • C12G1/0203Preparation of must from grapes; Must treatment and fermentation by microbiological or enzymatic treatment
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G1/00Preparation of wine or sparkling wine
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G2200/00Special features
    • C12G2200/21Wine additives, e.g. flavouring or colouring agents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Biochemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Molecular Biology (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention belongs to the field of wine brewing, and in particular relates to a method for brewing a wine rich in procyanidine, which comprises the following steps: step 1, preprocessing; step 2, pulp fermentation; step 3, ventilation; step 4, separating; step 5, temperature-controlled fermentation; step 6: filtering and changing barrels; step 7, adding anthocyanin; and 8, storing, pretreating, performing vacuum freeze drying on grape skin and grape seeds by a vacuum dryer, and then grinding the grape skin and the grape seeds into powder respectively, and extracting procyanidine powder from the powder. In the process of brewing the wine, the procyanidine in grape seeds and grape skin in grape residues generated by brewing is extracted, the extracted procyanidine is prepared into powder, and the procyanidine is prepared into powder and added into the wine after the sterilization of the wine is finished, so that the procyanidine in the wine is prevented from being damaged by high temperature, and the procyanidine content in the wine is improved.

Description

Method for brewing grape wine rich in procyanidine
Technical Field
The invention belongs to the field of wine brewing, and particularly relates to a method for brewing a wine rich in procyanidine.
Background
The wine is a fruit wine brewed by using grapes as raw materials, has higher alcohol content than beer and lower alcohol content than white wine, is rich in nutrition, has obvious health care effect, contains procyanidine which is considered to be one of the most effective natural antioxidants, can remove free radicals in human bodies, has the antioxidant capacity of 50 times of that of vitamin E and 20 times of that of vitamin C, and is beneficial to deferring aging after frequent drinking of the wine.
In the current grape wine brewing process, grape skin and grape seeds are reserved after grape is slightly crushed and directly made, procyanidine in grape skin and grape seeds is mixed in fermented fruit juice, after the fruit juice is fermented into grape wine, the grape is sterilized by a bus sterilization method, the bus sterilization method needs to heat the grape wine to 68-70 ℃ for 30 minutes, the procyanidine is a thermosensitive active ingredient, the procyanidine is damaged due to the fact that the environment temperature is too high, and therefore the procyanidine content of the produced grape wine is low.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a method for brewing grape wine rich in procyanidine.
The technical scheme adopted by the invention is as follows:
a method for brewing grape wine rich in procyanidine comprises the following steps:
step 1, pretreatment: selecting high-quality grapes, cleaning, taking grape skin and grape seeds out of pulp, vacuum freeze-drying the grape skin and the grape seeds by a vacuum dryer, grinding the grape skin and the grape seeds into powder, and extracting procyanidine powder from the powder;
step 2, pulp fermentation: repeatedly crushing the pretreated grape pulp by a crushing roller to further crush fibers in the grape pulp, and then placing the crushed pulp and juice into a fermentation tank for primary fermentation to naturally ferment the pulp and juice in the fermentation tank so as to separate out nutrient substances in the pulp;
step 3, ventilation: the air exchanging device is arranged on the fermentation tank, and air exchanging is carried out in the fermentation tank at regular time, so that the quality of the grapes is prevented from being reduced due to the fact that pulp on the upper layer of the fermentation tank is air-dried;
step 4, separation: separating grape juice in the fermentation tank by squeezing with filter cloth, separating grape juice from pulp and fiber, filtering and squeezing for several times, placing grape juice in a standing tank for waiting for the impurities in the interior to settle, and finally standing the upper layer of the tank to obtain clean grape juice primary pulp;
step 5: and (3) temperature control fermentation: placing the upper layer grape juice primary pulp which is placed in a standing tank and clarified in a fermentation tank for secondary fermentation, adding fermentation yeast into the fermentation tank, and controlling the temperature in the fermentation tank to ferment the grape juice primary pulp at constant temperature;
step 6, filtering and barrel changing: after the temperature control fermentation is finished, the grape juice primary pulp is changed into grape wine, and the grape wine is taken out of the fermentation tank, filtered and sterilized and poured into a oak barrel;
step 7, adding anthocyanin: adding procyanidine powder into oak barrel to mix procyanidine into wine;
step 8, storing: and placing the oak barrel filled with the wine in a wine cellar for storing the wine for constant temperature storage.
Further, the pretreatment method of the grapes in the step 1 comprises the following steps:
step one, drying and pulverizing: cleaning separated grape skin and grape seed to remove pulp attached to the surface, vacuum freezing and quick drying cleaned grape seed and grape skin, grinding grape seed and grape skin, and sieving to obtain grape seed powder and grape skin powder;
step two, extracting: extracting procyanidine from grape seed powder and grape skin powder by extraction method to obtain procyanidine powder.
Further, the pulp fermentation temperature in the step 2 is as follows: the pulp fermentation time is 20-24 ℃, and the pulp fermentation time is as follows: 3 days;
the temperature of the temperature-controlled fermentation in the step 5 is 20-22 ℃, and the time of the temperature-controlled fermentation is as follows: 7-15 days.
Further, the ventilation device in the step 3 is set to ventilate every 3 hours, and air is introduced into the fermentation tank after the gas in the fermentation tank is exhausted through the ventilation device.
Further, the grape variety for wine brewing is Cabernet Sauvignon.
Further, in the pretreatment step, grape skin and grape seeds are placed in a vacuum drying oven for vacuum freeze drying, and the process conditions of the vacuum freeze drying are as follows: the temperature is-20 ℃ to-10 ℃ and the time is 0.5-2h, the pressure is less than 100Pa, the grape skin and the grape seeds are removed by 30-55% through vacuum freeze drying, and the procyanidine in the grape skin and the grape seeds is kept.
The invention has the beneficial effects that:
the invention provides a grape wine brewing method rich in procyanidine, which is characterized in that procyanidine in grape seeds and grape skin in grape residues produced by brewing is extracted in a grape wine brewing process, the extracted procyanidine is prepared into powder, and the procyanidine is added into grape wine after the sterilization of the grape wine is finished, so that the procyanidine in the grape wine is prevented from being damaged at high temperature, and the content of procyanidine in the grape wine is improved.
Drawings
Fig. 1 is a flow chart of a method for brewing grape wine rich in procyanidins.
Detailed Description
The principles and features of the present invention are described below with reference to the drawings, the examples are illustrated for the purpose of illustrating the invention and are not to be construed as limiting the scope of the invention.
As shown in figure 1, the method for brewing the grape wine rich in procyanidine comprises the following steps of:
step 1, pretreatment: selecting high-quality grapes, cleaning, taking grape skin and grape seeds out of pulp, vacuum freeze-drying the grape skin and the grape seeds by a vacuum dryer, grinding the grape skin and the grape seeds into powder, and extracting procyanidine powder from the powder;
step 2, pulp fermentation: repeatedly crushing the pretreated grape pulp by a crushing roller to further crush fibers in the grape pulp, and then placing the crushed pulp and juice into a fermentation tank for primary fermentation to naturally ferment the pulp and juice in the fermentation tank so as to separate out nutrient substances in the pulp;
step 3, ventilation: the air exchanging device is arranged on the fermentation tank, and air exchanging is carried out in the fermentation tank at regular time, so that the quality of the grapes is prevented from being reduced due to the fact that pulp on the upper layer of the fermentation tank is air-dried;
step 4, separation: separating grape juice in the fermentation tank by squeezing with filter cloth, separating grape juice from pulp and fiber, filtering and squeezing for several times, placing grape juice in a standing tank for waiting for the impurities in the interior to settle, and finally standing the upper layer of the tank to obtain clean grape juice primary pulp;
step 5: and (3) temperature control fermentation: placing the upper layer grape juice primary pulp which is placed in a standing tank and clarified in a fermentation tank for secondary fermentation, adding fermentation yeast into the fermentation tank, and controlling the temperature in the fermentation tank to ferment the grape juice primary pulp at constant temperature;
step 6, filtering and barrel changing: after the temperature control fermentation is finished, the grape juice primary pulp is changed into grape wine, and the grape wine is taken out of the fermentation tank, filtered and sterilized and poured into a oak barrel;
step 7, adding anthocyanin: adding procyanidine powder into oak barrel to mix procyanidine into wine;
step 8, storing: and placing the oak barrel filled with the wine in a wine cellar for storing the wine for constant temperature storage.
Specifically, the pretreatment method of the grapes in the step 1 comprises the following steps:
step one, drying and pulverizing: cleaning separated grape skin and grape seed to remove pulp attached to the surface, vacuum freezing and quick drying cleaned grape seed and grape skin, grinding grape seed and grape skin, and sieving to obtain grape seed powder and grape skin powder;
step two, extracting: extracting procyanidine from grape seed powder and grape skin powder by extraction method to obtain procyanidine powder.
Specifically, the pulp fermentation temperature in the step 2 is as follows: the pulp fermentation time is 20-24 ℃, and the pulp fermentation time is as follows: 3 days;
the temperature of the temperature-controlled fermentation in the step 5 is 20-22 ℃, and the time of the temperature-controlled fermentation is as follows: 7-15 days.
Specifically, the ventilation device in the step 3 is set to ventilate every 3 hours, and air is introduced into the fermentation tank after the gas in the fermentation tank is exhausted through the ventilation device.
Specifically, the grape variety for brewing the wine is Cabernet Sauvignon.
Specifically, the process conditions of vacuum freeze drying in the pretreatment step are as follows: the temperature is-20 ℃ to-10 ℃ and the time is 0.5-2h, the pressure is less than 100Pa, the grape skin and the grape seeds are removed by 30-55% through vacuum freeze drying, and the procyanidine in the grape skin and the grape seeds is kept.
The procyanidine content, total sugar content and total acid content of the wine brewed in the examples were tested in the invention, and the test results are shown in Table 1.
TABLE 1 anthocyanin, total sugar and Total acid content of wine
Figure BDA0004130231000000051
The procyanidine content in the wine is detected by spectrophotometry, namely, the method of qualitative and quantitative analysis is carried out on the detected substance by measuring the light absorption degree of the substance at a specific wavelength or within a specific wavelength range;
the total sugar content of the wine is measured by an online glucose meter;
the total acid content of the wine is measured by a wine acidity tester;
the above comparative examples were measured for procyanidine content, total sugar content, total acid content from commercially available Cabernet Sauvignon dry red wine.
The foregoing description of the preferred embodiments of the invention is not intended to limit the invention to the precise form disclosed, and any such modifications, equivalents, and alternatives falling within the spirit and scope of the invention are intended to be included within the scope of the invention.

Claims (6)

1. A method for brewing grape wine rich in procyanidins, which is characterized by comprising the following steps:
step 1, pretreatment: selecting high-quality grapes, cleaning, taking grape skin and grape seeds out of pulp, vacuum freeze-drying the grape skin and the grape seeds by a vacuum dryer, grinding the grape skin and the grape seeds into powder, and extracting procyanidine powder from the powder;
step 2, pulp fermentation: repeatedly crushing the pretreated grape pulp by a crushing roller to further crush fibers in the grape pulp, and then placing the crushed pulp and juice into a fermentation tank for primary fermentation to naturally ferment the pulp and juice in the fermentation tank so as to separate out nutrient substances in the pulp;
step 3, ventilation: the air exchanging device is arranged on the fermentation tank, and air exchanging is carried out in the fermentation tank at regular time, so that the quality of the grapes is prevented from being reduced due to the fact that pulp on the upper layer of the fermentation tank is air-dried;
step 4, separation: separating grape juice in the fermentation tank by squeezing with filter cloth, separating grape juice from pulp and fiber, filtering and squeezing for several times, placing grape juice in a standing tank for waiting for the impurities in the interior to settle, and finally standing the upper layer of the tank to obtain clean grape juice primary pulp;
step 5: and (3) temperature control fermentation: placing the upper layer grape juice primary pulp which is placed in a standing tank and clarified in a fermentation tank for secondary fermentation, adding fermentation yeast into the fermentation tank, and controlling the temperature in the fermentation tank to ferment the grape juice primary pulp at constant temperature;
step 6, filtering and barrel changing: after the temperature control fermentation is finished, the grape juice primary pulp is changed into grape wine, and the grape wine is taken out of the fermentation tank, filtered and sterilized and poured into a oak barrel;
step 7, adding anthocyanin: adding procyanidine powder into oak barrel to mix procyanidine into wine;
step 8, storing: and placing the oak barrel filled with the wine in a wine cellar for storing the wine for constant temperature storage.
2. The method for brewing procyanidine-rich wine according to claim 1, wherein: the pretreatment method of the grapes in the step 1 comprises the following steps:
step one, drying and pulverizing: cleaning separated grape skin and grape seed to remove pulp attached to the surface, vacuum freezing and quick drying cleaned grape seed and grape skin, grinding grape seed and grape skin, and sieving to obtain grape seed powder and grape skin powder;
step two, extracting: extracting procyanidine from grape seed powder and grape skin powder by extraction method to obtain procyanidine powder.
3. The method for brewing procyanidine-rich wine according to claim 1, wherein: the pulp fermentation temperature in the step 2 is as follows: the pulp fermentation time is 20-24 ℃, and the pulp fermentation time is as follows: 3 days;
the temperature of the temperature-controlled fermentation in the step 5 is 20-22 ℃, and the time of the temperature-controlled fermentation is as follows: 7-15 days.
4. The method for brewing procyanidine-rich wine according to claim 1, wherein: and (3) the ventilation equipment in the step (3) is set to ventilate every 3 hours, and air is introduced into the fermentation tank after the air in the fermentation tank is exhausted through the ventilation equipment.
5. The method for brewing procyanidine-rich wine according to claim 1, wherein: the grape variety for brewing the wine is Cabernet Sauvignon.
6. The method for brewing procyanidine-rich wine according to claim 1, wherein: the process conditions of vacuum freeze drying in the pretreatment step are as follows: the temperature is-20 ℃ to-10 ℃ and the time is 0.5-2h, the pressure is less than 100Pa, the grape skin and the grape seeds are removed by 30-55% through vacuum freeze drying, and the procyanidine in the grape skin and the grape seeds is kept.
CN202310257638.2A 2023-03-14 2023-03-14 Method for brewing grape wine rich in procyanidine Pending CN116042336A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202310257638.2A CN116042336A (en) 2023-03-14 2023-03-14 Method for brewing grape wine rich in procyanidine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202310257638.2A CN116042336A (en) 2023-03-14 2023-03-14 Method for brewing grape wine rich in procyanidine

Publications (1)

Publication Number Publication Date
CN116042336A true CN116042336A (en) 2023-05-02

Family

ID=86129796

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202310257638.2A Pending CN116042336A (en) 2023-03-14 2023-03-14 Method for brewing grape wine rich in procyanidine

Country Status (1)

Country Link
CN (1) CN116042336A (en)

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1570073A (en) * 2004-05-09 2005-01-26 秦皇岛一品红酒业有限公司 Protoanthocyanin adding wine
CN102433236A (en) * 2012-01-06 2012-05-02 杨琳 Method for making proanthocyanidin-rich wine and product thereof
CN104694333A (en) * 2015-03-17 2015-06-10 黑龙江绿知都生物科技开发有限公司 Brewing process of blueberry brandy
CN107057906A (en) * 2017-05-08 2017-08-18 乌鲁木齐上善元生物科技有限公司 A kind of grape wine and its production method rich in OPC
CN107400590A (en) * 2017-09-28 2017-11-28 久为利华(天津)文化发展有限公司 Wine-making technique rich in anthocyanidin
TW201803978A (en) * 2017-10-03 2018-02-01 王志豪 Alcoholic beverages with anthocyanin and the method of the same
CN208055302U (en) * 2018-02-05 2018-11-06 中宁县华葡农林科技有限公司 One kind being based on Production of Wine installation for fermenting
CN115404138A (en) * 2022-10-31 2022-11-29 西夫拉姆酒业集团有限公司 Method for brewing grape wine rich in procyanidine

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1570073A (en) * 2004-05-09 2005-01-26 秦皇岛一品红酒业有限公司 Protoanthocyanin adding wine
CN102433236A (en) * 2012-01-06 2012-05-02 杨琳 Method for making proanthocyanidin-rich wine and product thereof
CN104694333A (en) * 2015-03-17 2015-06-10 黑龙江绿知都生物科技开发有限公司 Brewing process of blueberry brandy
CN107057906A (en) * 2017-05-08 2017-08-18 乌鲁木齐上善元生物科技有限公司 A kind of grape wine and its production method rich in OPC
CN107400590A (en) * 2017-09-28 2017-11-28 久为利华(天津)文化发展有限公司 Wine-making technique rich in anthocyanidin
TW201803978A (en) * 2017-10-03 2018-02-01 王志豪 Alcoholic beverages with anthocyanin and the method of the same
CN208055302U (en) * 2018-02-05 2018-11-06 中宁县华葡农林科技有限公司 One kind being based on Production of Wine installation for fermenting
CN115404138A (en) * 2022-10-31 2022-11-29 西夫拉姆酒业集团有限公司 Method for brewing grape wine rich in procyanidine

Similar Documents

Publication Publication Date Title
CN110923080A (en) Flavor enhancing brewing process for fresh grape brandy
CN105695277B (en) A kind of preparation method of matrimony vine Spirit
CN110564561A (en) Fruit wine aroma enhancement brewing process using cutinase
CN110885730A (en) Production method of Chinese wolfberry fruit wine
JPH01502474A (en) Improved method for obtaining alcoholic beverages from plant juices
CN107325906B (en) Preparation method of spine grape wine
CN111607472A (en) Dry red wine and its production process
Musteaţă et al. Capitalization of secondary wine products-an opportunity for the wine sector of republic of Moldova and Romania
CN116042336A (en) Method for brewing grape wine rich in procyanidine
CN106967555B (en) Production method of passion fruit-sugarcane mixed fruit wine
CN115404138A (en) Method for brewing grape wine rich in procyanidine
CN113549517A (en) Low-temperature preparation method of roxburgh rose fermented wine
CN110699201A (en) Brewing method of vitis davidii brandy
Moldovan et al. Effect of maceration conditions on chemical composition and colour characteristics of Merlot wines
CN112094714A (en) Preparation method of mulberry wine
CN109852506A (en) A kind of production technology of the reinforced claret of nutrition
CN103881885A (en) Method for improving non-biological stability of alcoholic drink mixed with fruit juice
CN111218368A (en) Chrysanthemum and medlar health wine
CN115161138B (en) Method for improving fragrance of dry red wine
CN111100776A (en) Production method of dry red cranberry wine
CN113073018B (en) White wine and multi-parameter-based preparation method
CN107245370B (en) Preparation method of spiny grape seed oil
CN108913419B (en) White gourd wine and brewing method thereof
CN111621387A (en) Production method of fen-flavor hawthorn distilled liquor
CN106929275A (en) A kind of production method of blueberry wine

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination