CN115948081A - Aerogel interior wall coating with purification function - Google Patents

Aerogel interior wall coating with purification function Download PDF

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Publication number
CN115948081A
CN115948081A CN202210021845.3A CN202210021845A CN115948081A CN 115948081 A CN115948081 A CN 115948081A CN 202210021845 A CN202210021845 A CN 202210021845A CN 115948081 A CN115948081 A CN 115948081A
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stirring barrel
aerogel
stirring
ring
purification function
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CN115948081B (en
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张忠伦
王明铭
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China Building Materials Science Innovation Technology Research Institute Shandong Co ltd
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China Building Materials Science Innovation Technology Research Institute Shandong Co ltd
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Abstract

The invention relates to the technical field of aerogel coatings, and discloses an aerogel inner wall coating for a purification function, wherein a preparation device of the aerogel inner wall coating for the purification function comprises a stirring barrel, a processing bin is arranged in the stirring barrel, the stirring barrel is connected in the processing bin in a sliding manner, an adjusting device is connected in the stirring barrel in a sliding manner, and the adjusting device is usedIn pushing the liquid in the stirring barrel, the adjusting device comprises a pushing disc which is connected in the stirring barrel in a sliding manner. The invention modifies SiO 2 The aerogel slurry is prepared by preparing raw materials such as aerogel powder dispersing agent, wetting agent, deionized water and the like, and modified SiO is added into the components 2 Aerogel powder for the aerogel interior wall coating that the preparation obtained possesses the function of adsorbing purification formaldehyde, and this aerogel interior wall coating thermal insulation performance is good, in addition, can each composition of fast dispersion mixture through the device, realizes having purification performance with aerogel coating's rapid preparation.

Description

Aerogel interior wall coating with purification function
Technical Field
The invention relates to the technical field of aerogel coatings, in particular to an aerogel inner wall coating with a purification function.
Background
The aerogel coating is the best heat insulation coating at present, is a product at a real nano-pore level, and is known to mainly realize infinite length of a pore wall link by heat conduction, heat radiation and heat convection through a nano-pore structure, so that a heat conduction path is long enough, a conduction path is narrow enough, and heat conduction is not passed; by adding proper anti-radiation components into the coating formula, the anti-radiation thermal property can be greatly improved; because the aperture of the nano-pore is small enough and is smaller than the free path of air molecules, air convection cannot effectively occur; therefore, the nano-grade heat insulation material has excellent comprehensive heat insulation performance, wherein the aerogel heat insulation coating is prepared by using the unique nano-structure and the selective characteristic to solar spectrum of SiO2 aerogel, using the SiO2 aerogel as a main filler, using water as a solvent, using a stabilizer to uniformly disperse the SiO2 aerogel to prepare slurry, selecting styrene-acrylic emulsion as a matrix, mixing the styrene-acrylic emulsion and other additives to prepare the water-based heat insulation coating, applying the water-based heat insulation coating to the surface of a building material, forming a compact vacuum layer on the surface of a coated object, effectively shielding infrared heat radiation and blocking ultraviolet rays, and reducing the heat exchange between the inside and the outside of the coated object. Compared with the traditional heat-insulating coating, the preparation method is simple and easy to implement, environment-friendly and energy-saving, has excellent heat-insulating effect, can adsorb and purify formaldehyde, and has the functions of fire prevention, flame retardance, sound insulation, noise reduction and condensed water discharge.
However, the existing aerogel coating for purification function needs a long processing time during preparation and processing, and because a plurality of raw materials are gradually added into the stirring barrel, the raw materials may not be well mixed, and further the stirring and mixing time needs to be prolonged, so that the problems of long processing time and low processing efficiency are caused, and therefore, the device can fully mix with the stock solution in the stirring barrel uniformly and quickly after the raw materials are gradually added into the stirring barrel.
Disclosure of Invention
The invention provides a aerogel inner wall coating for a purification function, which has the advantages of high processing efficiency and good mixing effect, and solves the problems that the existing aerogel coating for the purification function in the background art needs longer processing time during preparation and processing, and because a plurality of raw materials are gradually added into a stirring barrel, the raw materials can not be well mixed, and further the stirring and mixing time needs to be prolonged, so that the processing time is long, and the processing efficiency is slow.
The invention provides the following technical scheme: the aerogel interior wall coating with the purification function comprises the following components in parts by weight:
150 parts of aerogel slurry;
3 parts of phosphite ester;
30 parts of deionized water;
5 parts of organic acid;
10 parts of odorless styrene-acrylic emulsion;
2 parts of polyvinylpyrrolidone;
and 3 parts of sodium alginate.
Wherein: the aerogel slurry is prepared by the following components in parts by weight (unit: g):
modified SiO 2 60-80 parts of aerogel powder (with the function of adsorbing and purifying formaldehyde); 3-5 parts of wetting agent; 10-20 parts of a stabilizer; 350-400 parts of deionized water; 5-10 parts of dispersing agent.
The preparation process of the aerogel slurry comprises the following steps:
(1) placing the dispersing agent, the wetting agent and the deionized water into a stirring tank, and carrying out homogeneous dispersion on a high-speed dispersion machine at the rotating speed of 300r/min for 5min;
(2) adding the stabilizer into a stirring tank, uniformly stirring at the rotating speed of 1500r/min, and slowly adding SiO while stirring 2 An aerogel;
(3) after the aerogel is added, dispersing for 15min at a high speed of 2000r/min, then ultrasonically dispersing for 30min, and finally, grinding for 3 hours by replacing a grinding disc of a high-speed dispersion machine with 3000 r/min. Obtaining the aerogel slurry.
The invention also provides a preparation method of the aerogel interior wall coating with the purification function,
s1, placing aerogel slurry, deionized water and phosphite ester into a stirring barrel, and dispersing the aerogel slurry, the deionized water and the phosphite ester at a low speed through the stirring barrel;
s2, on the basis of the S1, adding polyvinylpyrrolidone and the primarily dispersed raw materials into the stirring barrel for fusion, raising the temperature in the stirring barrel to 40-45 ℃, and mixing the polyvinylpyrrolidone, the aerogel slurry, deionized water and phosphite ester through high-speed stirring;
s3, on the basis of the S2, adding sodium alginate and the odorless styrene-acrylic emulsion into the stirring barrel again, stirring at a low speed, and reacting at 45 ℃ for half an hour;
and S4, on the basis of the S3, adding organic acid into the stirring barrel, uniformly dispersing for 60 minutes at 800 revolutions per minute, and thus obtaining the aerogel coating.
In addition, the invention also provides an aerogel thermal insulation coating, and the preparation of the aerogel thermal insulation coating comprises the following components in parts by weight (unit: g):
100-150 parts of aerogel slurry; 2.5-3.0 parts of leveling agent; 300-350 parts of odorless styrene-acrylic emulsion; 1.0-1.5 parts of thickening agent; 3-6 parts of a dispersant; 2-4 parts of a curing agent; 2-4 parts of a defoaming agent;
and sequentially adding the raw materials into a stirring tank, and uniformly dispersing for 60min at a rotating speed of 800r/min on a high-speed dispersion machine to obtain the aerogel heat-insulating coating.
The invention also provides a preparation device of the aerogel inner wall coating with the purification function, wherein a processing bin is arranged inside the stirring barrel, the stirring barrel is connected inside the processing bin in a sliding manner, an adjusting device is connected inside the stirring barrel in a sliding manner and used for pushing liquid inside the stirring barrel, and the adjusting device comprises a push disc connected inside the stirring barrel in a sliding manner;
still be provided with first shrinkage pool on the agitator, first shrinkage pool is linked together with the inside in processing storehouse, be provided with first check valve on the push away dish, the internally mounted of first shrinkage pool has the second check valve, push away the dish and be used for the inside liquid of the first shrinkage pool of negative pressure extraction to the lower extreme that pushes away the dish, improved machining efficiency greatly through the agitator and the cooperation that pushes away the dish, shortened process time.
As an alternative to the purification function aerogel interior wall coating of the present invention, wherein: the first one-way valve comprises a second concave hole formed in the push disc, a second vertical hole communicated with the second concave hole is further formed in the push disc, a second sealing disc used for sealing the second concave hole is connected to the inside of the second concave hole in a sliding mode, a second short rod is installed at the lower end of the second sealing disc, a second spring is installed on the outer surface of the second short rod, and the second spring is connected with the push disc;
there is the second check valve including setting up the first perpendicular hole on the agitator, first perpendicular hole is linked together with first shrinkage pool, the inside sliding connection of first shrinkage pool has the first sealed dish that is used for sealing up first shrinkage pool, still install first quarter butt on the first sealed dish, the surface mounting of first quarter butt has first spring, first spring is connected with the agitator, and through the up-and-down motion that pushes away the dish, can let the liquid of processing storehouse bottom constantly get into the inside of agitator, lets from this that the stoste that has not taken place the reaction constantly be carried the upper end of agitator, makes things convenient for follow-up emergence reaction.
As an alternative to the purification function aerogel interior wall coating of the present invention, wherein: the stirring barrel is also provided with a motor, an output shaft of the motor is provided with a transmission sleeve, a force storage component is also arranged in the stirring barrel, a round rod is arranged on the force storage component, and the round rod penetrates through the push disc and is in threaded connection with the push disc;
round bar sliding connection is in the inside of transmission cover, be provided with first extension piece on the round bar, the internally mounted of transmission cover has first extension piece, first extension piece sliding connection is in the inside of first helicla flute, still install the slider on the pushing tray, the inner wall of agitator is provided with the square groove, slider sliding connection is in the inside of square groove, and through the cooperation of round bar and pushing tray, the realization pushes away the automatic upwards slip of dish.
As an alternative to the purification function aerogel interior wall coating of the present invention, wherein: the inner wall of the transmission sleeve is also provided with a circular groove, a bearing ring is rotatably connected inside the circular groove, and the bearing ring is connected with the first extending block;
the power storage component comprises a supporting sleeve installed on the stirring barrel, a torque spring is installed inside the supporting sleeve, the round rod is connected to the inside of the supporting sleeve in a rotating mode and is connected with the torque spring, a vertical groove communicated with the first spiral groove is further formed in the round rod, a second spiral groove communicated with the vertical groove is further formed in the round rod, the first extending block is used for being connected to the inside of the connecting rod and the second spiral groove in a sliding mode, and under the cooperation of the bearing ring and the vertical groove, the pushing disc can be pushed for many times in a short time to enable the raw liquid after reaction to flow to the middle position of the stirring barrel and absorb the raw liquid, which is not reacted at the lower end of the processing bin, to be conveyed to the upper end of the stirring barrel to wait for reaction.
As an alternative to the purification function aerogel interior wall coating of the present invention, wherein: the mixing device comprises a stirring barrel, a processing bin and a mixing component, wherein the stirring barrel is provided with the mixing component, the mixing component is used for stirring liquid and comprises a beating ring which is connected to the outer surface of the stirring barrel in a sliding mode, the inner wall of the stirring barrel is provided with a circular ring, the circular ring and the beating ring divide the interior of the processing bin into three spaces, the space at the upper end of the circular ring is a flowing bin, the space between the circular ring and the beating ring is a mixing bin, and the space at the lower end of the beating ring is a processing bin;
the ring is provided with a first through hole, the beating ring is provided with a second through hole, the first through hole and the second through hole are used for circulating liquid, and stock solution pushed out subsequently through the pushing disc is mixed with the reacted stock solution in an impacting manner, so that the raw materials in the reacted stock solution are completely reacted, and the processing efficiency is improved.
As an alternative to the purification function aerogel interior wall coating of the present invention, wherein: the lower end of the beating ring is provided with a circulating pipe, the inside of the circulating pipe is connected with a flat plate in a sliding mode, a circulating groove is formed in the flat plate, the flat plate is used for sealing the circulating pipe, a trapezoidal groove is further formed in the inner wall of the stirring barrel, the flat plate is used for being connected to the inside of the trapezoidal groove in a sliding mode, an elastic sheet is further installed on the beating ring and is connected with the flat plate, all reacted stock solution can be pushed to impact the first through hole through the beating ring, the stock solution pushed out subsequently by the pushing disc is mixed with the reacted stock solution in an impacting mode, and the reaction is complete.
As an alternative to the purification function aerogel interior wall coating of the present invention, wherein: the beating ring is also provided with a supporting ring sleeve, the inside of the supporting ring sleeve is rotatably connected with a rotating shaft, the rotating shaft is connected with a stirring blade in a sliding way, the stirring blade is used for stirring liquid in the mixing bin, and the rotating shaft is also provided with a fourth spring which is connected with the stirring blade;
the rotation axis runs through first through-hole, still be provided with the third helicla flute on the rotation axis, still install the second on the inner wall of agitator and stretch out the piece, the second stretches out piece sliding connection and in the inside of third helicla flute, and it is rotatory to utilize the rotation axis to drive the stirring leaf, and the stock solution stirring that mixes the storehouse inside is driven through the stirring leaf mixes to improve the device's machining efficiency.
As an alternative to the purification function aerogel interior wall coating of the present invention, wherein: the stirring barrel is further provided with an adjusting groove, a second sealing plate is connected to the inner wall of the stirring barrel in a sliding mode, a welding plate is installed at the lower end of the second sealing plate and connected with a striking ring, an adjusting sleeve is installed at the lower end of the welding plate, an L-shaped plate is connected to the inside of the adjusting sleeve in a sliding mode, the pushing disc is used for extruding the L-shaped plate to slide, a first sealing plate is further installed at the lower end of the L-shaped plate and connected to the inner wall of the stirring barrel in a sliding mode, a third spring is further installed in the inner wall of the stirring barrel and connected with the first sealing plate;
the lower extreme of agitator still installs the support section of thick bamboo, the internally mounted of support section of thick bamboo has the pneumatic cylinder, install the slide bar on the pneumatic cylinder, the slide bar runs through the support section of thick bamboo and is connected with the agitator, the slide bar is used for promoting the agitator and goes up and down, through hitting the rotatory mixed stoste of ring and stirring leaf and the stoste of taking place the reaction, still can remain the raw materials in the stoste of avoiding taking place the reaction.
The invention has the following beneficial effects:
1. the aerogel inner wall coating with the purification function is prepared by modifying SiO 2 The aerogel slurry is prepared by preparing raw materials such as aerogel powder dispersing agent, wetting agent, deionized water and the like, and modified SiO is added into the components 2 Aerogel powder for the aerogel interior wall coating that the preparation obtained possesses the function of adsorbing purification formaldehyde, and formaldehyde purification rate is greater than 90%, and coefficient of heat conductivity is less than or equal to 0.035W/(m.k), and infrared light transmittance is less than or equal to 30%, and this aerogel interior wall coating heat preservation heat-proof quality is good, and specific parameter is as follows:
Figure RE-GDA0003534669820000081
2. promote the inside liquid of agitator through the pushing disk and flow into the inside in processing storehouse, one of them, the liquid cover that pushes away through the pushing disk is reacting the upper end of stoste, let remain the raw materials in reacting the stoste and react with the stoste once more, its two, because the pushing disk is after pushing away partly liquid, the inside liquid of its agitator is clean stoste, make things convenient for next time raw materials to contact with the stoste, so reciprocal, can make the inside stoste of processing storehouse mix with the quick contact of raw materials, and then the device has improved machining efficiency through the cooperation of agitator and pushing disk greatly, processing time has been shortened.
3. This aerogel interior wall coating for purification performance, up-and-down motion through pushing away the dish, can let the liquid of processing storehouse bottom constantly get into the inside of agitator, from this let the stoste that has not been taken place the reaction constantly by the upper end of being carried the agitator, make things convenient for the follow-up reaction that takes place, make the device pass through the cooperation of the sealed dish of second and first sealed dish, further improvement mixing efficiency, with this improvement machining efficiency, the aerogel composition is difficult to the dispersion, can each composition of fast dispersion mixture through the device, the realization has aerogel coating for purification performance's quick preparation.
4. This aerogel interior wall coating for purification performance, through the inside of agitator first stretch out piece sliding connection at the second helicla flute of upwards sliding, make the round bar rotatory, push away the dish on the round bar can upwards slide and promote the inside liquid of agitator, make the device under the cooperation of bearing ring and vertical groove, let the former liquid that pushes away after the dish can the short time promote the emergence reaction flow to the intermediate position of agitator and absorb the former liquid that the processing storehouse lower extreme was not taken place the reaction and carry the upper end of agitator and wait for taking place the reaction.
Drawings
Fig. 1 is a schematic view of the overall structure of the present invention.
Fig. 2 is a sectional view of the mixing tank of the present invention.
Fig. 3 is a schematic structural diagram of the adjusting device of the present invention.
FIG. 4 is a schematic view of a portion of the structure shown in FIG. 3A according to the present invention.
Fig. 5 is a schematic structural view of the support sleeve and the torsion spring of the present invention.
FIG. 6 is a schematic view of a portion of the structure shown in FIG. 5B according to the present invention.
Fig. 7 is a schematic structural view of the hybrid component of the present invention.
FIG. 8 is a partial structural view of FIG. 7 at C according to the present invention.
In the figure: 1. a stirring barrel; 2. a support cylinder; 3. a motor; 4. an adjustment device; 6. a processing bin; 7. a mixing component; 10. a hydraulic cylinder; 11. a slide bar; 12. a stirring barrel; 13. a first recess; 14. a second recess; 15. a first vertical hole; 16. a second vertical hole; 18. a first sealing disk; 19. a first short bar; 20. a first spring; 21. a second sealing disk; 22. a second spring; 23. a second short bar; 41. a transmission sleeve; 42. a connecting rod; 44. pushing a disc; 45. a first helical groove; 46. a first extension block; 47. a round bar; 48. a square groove; 49. a slider; 50. a circular groove; 51. a bearing ring; 52. a vertical slot; 53. a second helical groove; 54. a support sleeve; 55. a torque spring; 61. a flow bin; 62. a mixing bin; 63. a processing bin; 71. an adjustment groove; 72. an L-shaped plate; 73. an adjusting sleeve; 74. a first sealing plate; 75. a third spring; 76. welding the plate; 77. A second sealing plate; 78. a circular ring; 79. a first through hole; 80. a second through hole; 81. striking a ring; 82. supporting the loop; 83. a trapezoidal groove; 84. a flat plate; 85. a spring plate; 86. a circulation tank; 87. a rotating shaft; 88. a third helical groove; 89. a second extension block; 90. a fourth spring; 91. A flow-through tube; 92. stirring the leaves.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The aerogel interior wall coating with the purification function comprises the following components in parts by weight:
150 parts of aerogel slurry;
3 parts of phosphite ester;
30 parts of deionized water;
5 parts of organic acid;
10 parts of odorless styrene-acrylic emulsion;
2 parts of polyvinylpyrrolidone;
3 parts of sodium alginate;
the raw materials are stirred and mixed to prepare the aerogel inner wall coating with the purification function.
Wherein: the aerogel slurry is prepared by the following components in parts by weight (unit: g):
modified SiO 2 60-80 parts of aerogel powder (with the function of adsorbing and purifying formaldehyde); 3-5 parts of a wetting agent; 10-20 parts of a stabilizer; 350-400 parts of deionized water; 5-10 parts of dispersing agent.
The preparation process of the aerogel slurry comprises the following steps:
(1) placing the dispersing agent, the wetting agent and the deionized water into a stirring tank, and carrying out homogeneous dispersion on a high-speed dispersion machine at the rotating speed of 300r/min for 5min;
(2) adding the stabilizer into a stirring tank, uniformly stirring at the rotating speed of 1500r/min, and slowly adding SiO while stirring 2 An aerogel;
(3) after the aerogel is added, dispersing for 15min at a high speed of 2000r/min, then ultrasonically dispersing for 30min, and finally, grinding for 3 hours by replacing a grinding disc of a high-speed dispersion machine with 3000 r/min. Obtaining the aerogel slurry.
In addition, the invention also provides an aerogel thermal insulation coating, and the preparation of the aerogel thermal insulation coating comprises the following components in parts by weight (unit: g):
100-150 parts of aerogel slurry; 2.5-3.0 parts of leveling agent; 300-350 parts of odorless styrene-acrylic emulsion; 1.0-1.5 parts of thickening agent; 3-6 parts of a dispersant; 2-4 parts of a curing agent; 2-4 parts of a defoaming agent;
and sequentially adding the raw materials into a stirring tank, and uniformly dispersing for 60min at a rotating speed of 800r/min on a high-speed dispersion machine to obtain the aerogel heat-insulating coating.
Example 2
The invention also provides a preparation method of the aerogel interior wall coating with the purification function,
s1, placing a dispersing agent, a wetting agent and deionized water into a stirring tank, carrying out homogeneous dispersion on a high-speed dispersion machine at a rotating speed of 300r/min for 5min, adding a stabilizing agent into the stirring tank, uniformly stirring at a rotating speed of 1500r/min, and slowly adding SiO while stirring 2 After the aerogel is added, dispersing for 15min at a high speed at a rotating speed of 2000r/min, then dispersing for 30min by ultrasonic, finally, grinding for 3 hours at a speed of 3000r/min by replacing a grinding disc of a high-speed dispersion machine to obtain aerogel slurry, putting the aerogel slurry, deionized water and phosphite ester into a stirring barrel 1, and dispersing the aerogel slurry, the deionized water and the phosphite ester at a low speed through the inside of the stirring barrel 1;
s2, on the basis of the S1, adding polyvinylpyrrolidone and the primarily dispersed raw materials into the stirring barrel 1 for fusion, raising the temperature in the stirring barrel 1 to 40-45 ℃, and mixing the polyvinylpyrrolidone, the aerogel slurry, deionized water and phosphite ester through high-speed stirring;
s3, on the basis of the S2, adding sodium alginate and the odorless styrene-acrylic emulsion into the stirring barrel 1 again, stirring at a low speed, and reacting at 45 ℃ for half an hour;
and S4, on the basis of the S3, uniformly dispersing the organic acid in the stirring barrel 1 for 60 minutes at 800 revolutions per minute to obtain the aerogel coating.
Example 3
The invention also provides a preparation device of the aerogel inner wall coating with the purification function, and particularly, referring to fig. 1-3, a processing bin 6 is arranged inside a stirring barrel 1, the stirring barrel 12 is connected inside the processing bin 6 in a sliding manner, an adjusting device 4 is connected inside the stirring barrel 12 in a sliding manner, the adjusting device 4 is used for pushing liquid inside the stirring barrel 12, and the adjusting device 4 comprises a push disc 44 connected inside the stirring barrel 12 in a sliding manner;
a first concave hole 13 is further formed in the stirring barrel 12, the first concave hole 13 is communicated with the interior of the processing bin 6, a first one-way valve is arranged on the pushing disc 44, a second one-way valve is mounted in the first concave hole 13, and the pushing disc 44 is used for extracting liquid in the first concave hole 13 to the lower end of the pushing disc 44 under negative pressure;
the lower extreme of agitator 1 still installs a support section of thick bamboo 2, and the internally mounted of a support section of thick bamboo 2 has pneumatic cylinder 10, installs slide bar 11 on the pneumatic cylinder 10, and slide bar 11 runs through a support section of thick bamboo 2 and is connected with agitator 12, and slide bar 11 is used for promoting agitator 12 and goes up and down.
The existing aerogel coating needs longer processing time during preparation and processing, and because a plurality of raw materials are gradually added into the stirring barrel 1, the raw materials can be mixed not well, and further the stirring and mixing time needs to be prolonged, so that the problems of long processing time and low processing efficiency are caused, therefore, in order to solve the problems that the raw materials can be fully mixed uniformly and quickly with the stock solution in the stirring barrel 1 after being gradually added into the stirring barrel 1, the stirring barrel 12 is arranged in the stirring barrel 1, the raw materials which enter the stirring barrel 1 can flow to the lower end of the stirring barrel 12 after contacting with the stock solution through the upward sliding of the stirring barrel 12, the stock solution which does not contact with the raw materials can flow to the upper end of the stirring barrel 12, and the stock solution can uniformly contact with the raw materials; the processing efficiency is greatly improved and the processing time is shortened through the matching of the stirring barrel 12 and the pushing disc 44.
Uniform contact stirring: according to fig. 2, by inputting the raw material into the inside of the stirring barrel 1, the raw material floats on the upper end surface of the stirring barrel 12, then the motor 3 drives the transmission sleeve 41 and the connecting rod 42 to drive the stirring barrel 12 to rotate, and the stirring barrel 12 is utilized to stir and mix, because the raw material is difficult to contact with the stock solution at the bottom of the stirring barrel 1, the hydraulic cylinder 10 pushes the sliding rod 11 to slide upwards, the sliding rod 11 pushes the stirring barrel 12 to slide upwards, so that a part of the volume of the stirring barrel 12 can be separated from the stock solution, and then a gap can exist between the lower end of the stirring barrel 12 and the stirring barrel 1, so that the stock solution and the stock solution which is over-reacted can flow to the middle position of the stirring barrel 12.
Subsequently, as shown in fig. 3, the pushing disc 44 inside the stirring barrel 12 slides upwards, so that the pushing disc 44 pushes the liquid inside the stirring barrel 12 to flow into the processing bin 6, firstly, the liquid pushed out by the pushing disc 44 covers the reacted stock solution, and the raw material remaining in the reacted stock solution reacts with the stock solution again, secondly, after a part of liquid is pushed out by the pushing disc 44, the liquid inside the stirring barrel 12 is clean stock solution, so that the next time the raw material contacts with the stock solution conveniently, and in such a reciprocating way, the stock solution inside the processing bin 6 and the raw material are rapidly contacted and mixed, and further, the device greatly improves the processing efficiency by matching the stirring barrel 12 and the pushing disc 44, and shortens the processing time.
Example 4
Through the up-and-down movement of the pushing disc 44, the liquid at the bottom of the processing bin 6 can continuously enter the stirring barrel 12, so that the unreacted raw liquid is continuously conveyed to the upper end of the stirring barrel 12, and the subsequent reaction is facilitated, the embodiment is an improvement made on the basis of the embodiment 3, specifically, referring to fig. 1-4, the first check valve comprises a second concave hole 14 arranged on the pushing disc 44, a second vertical hole 16 communicated with the second concave hole 14 is further arranged on the pushing disc 44, a second sealing disc 21 for sealing the second concave hole 14 is slidably connected inside the second concave hole 14, a second short rod 23 is arranged at the lower end of the second sealing disc 21, a second spring 22 is arranged on the outer surface of the second short rod 23, and the second spring 22 is connected with the pushing disc 44;
the second check valve is including setting up first perpendicular hole 15 on agitator 12, and first perpendicular hole 15 is linked together with first shrinkage pool 13, and the inside sliding connection of first shrinkage pool 13 has a first sealed dish 18 that is used for sealed first shrinkage pool 13, still installs first quarter butt 19 on the first sealed dish 18, and the surface mounting of first quarter butt 19 has first spring 20, and first spring 20 is connected with agitator 12.
And (3) reciprocating replacement: according to fig. 4, when the pushing disc 44 slides upwards, the liquid on the upper end of the pushing disc 44 is buckled on the pushing disc 44, so that the pushing disc 44 becomes a sealing body, and the liquid in the stirring barrel 12 can be pushed out by the upward sliding of the pushing disc 44, at this time, a negative pressure is generated in the space between the pushing disc 44 and the bottom of the stirring barrel 12, and the first sealing disc 18 is extracted by the negative pressure to slide upwards, so that the liquid at the bottom of the processing bin 6 can enter the lower end of the pushing disc 44 through the first vertical hole 15 and the first concave hole 13;
then, the pushing disc 44 slides downwards, so that liquid at the lower end of the pushing disc 44 can extrude the first sealing disc 18 to seal the first concave hole 13, and the liquid can only extrude and open the second sealing disc 21, so that the second sealing disc 21 slides out of the second concave hole 14, the liquid flows to the upper end of the pushing disc 44 through the second vertical hole 16 and the second concave hole 14, and through the up-and-down movement of the pushing disc 44, the liquid at the bottom of the processing bin 6 can continuously enter the inner part of the stirring barrel 12, so that the unreacted raw liquid is continuously conveyed to the upper end of the stirring barrel 12, and the subsequent reaction is facilitated, so that the device further improves the mixing efficiency through the matching of the second sealing disc 21 and the first sealing disc 18, and the processing efficiency is improved.
Example 5
The automatic upward sliding of the push tray 44 is realized by the matching of the round rod 47 and the push tray 44, and the embodiment is an improvement made on the basis of the embodiment 4, specifically, referring to fig. 1-4, the stirring barrel 1 is further provided with the motor 3, the output shaft of the motor 3 is provided with the transmission sleeve 41, the stirring barrel 12 is further internally provided with a force accumulation component, the force accumulation component is provided with the round rod 47, and the round rod 47 penetrates through the push tray 44 and is in threaded connection with the push tray 44;
round bar 47 sliding connection is provided with first piece 46 of stretching out in the inside of driving sleeve 41 on the round bar 47, and the internally mounted of driving sleeve 41 has first piece 46 of stretching out, and first piece 46 sliding connection of stretching out still installs slider 49 in the inside of first helicla flute 45 on the pushing disc 44, and the inner wall of agitator 12 is provided with square groove 48, and slider 49 sliding connection is in the inside of square groove 48.
Automatic sliding: according to fig. 3, a first spiral groove 45 is further disposed on the round bar 47, when the stirring barrel 12 slides upwards, the round bar 47 on the stirring barrel 12 can drive the sliding connection to the inside of the transmission sleeve 41, and the sliding connection is made to the inside of the first spiral groove 45 through the first extending block 46, so that the round bar 47 can rotate, because the round bar 47 is in threaded connection with the pushing disc 44, and the sliding block 49 on the pushing disc 44 is also in sliding connection to the inside of the square groove 48, so that the round bar 47 can only drive the pushing disc 44 to slide upwards, and further, the pushing disc 44 can automatically slide upwards.
Example 6
Under the matching of the bearing ring 51 and the vertical groove 52, the pushing disc 44 can conveniently push the reacted stock solution for multiple times in a short time, and the embodiment is an improvement on the basis of embodiment 5, specifically, referring to fig. 1 to 6, the inner wall of the transmission sleeve 41 is further provided with a circular groove 50, the inside of the circular groove 50 is rotatably connected with the bearing ring 51, and the bearing ring 51 is connected with the first protruding block 46;
the power accumulating part comprises a supporting sleeve 54 arranged on the stirring barrel 12, a torque spring 55 is arranged inside the supporting sleeve 54, a round rod 47 is rotatably connected inside the supporting sleeve 54 and connected with the torque spring 55, a vertical groove 52 communicated with the first spiral groove 45 is further arranged on the round rod 47, a second spiral groove 53 communicated with the vertical groove 52 is further arranged on the round rod 47, and the first extending block 46 is used for being connected inside the connecting rod 42 and the second spiral groove 53 in a sliding mode.
And (4) layering again: according to fig. 5 and 6, the bearing ring 51 of the first protruding block 46 is rotatably connected to the inside of the circular groove 50, and the circular rod 47 is further provided with a vertical groove 52 and a second spiral groove 53, when the first protruding block 46 is slidably connected to the inside of the first spiral groove 45, so that the circular rod 47 rotates, the circular rod 47 drives the torque spring 55 to rotate, the torque spring 55 stores the rotational force through the torque spring 55, and then when the first protruding block 46 is slidably connected to the inside of the vertical groove 52, because the circular rod 47 only abuts against two sides of the first protruding block 46 at this time, so that the torque spring 55 releases the compressed force, the circular rod 47 drives the circular rod 47 to rotate in the opposite direction through the torque spring 55, the circular rod 47 drives the first protruding block 46 and the bearing ring 51 to rotate, so that the pushing plate 44 connected to the circular rod 47 slides downwards, the liquid at the bottom is conveyed to the upper end of the pushing plate 44 through the pushing plate 44, and then the first protruding block 46 is slidably connected to the inside of the second spiral groove 53 by sliding the stirring barrel 12, so that the circular rod 47 rotates;
the pushing disc 44 on the round rod 47 slides upwards and pushes the liquid inside the stirring barrel 12, so that the device can make the pushing disc 44 push the reacted raw liquid to flow to the middle position of the stirring barrel 12 and suck the unreacted raw liquid at the lower end of the processing bin 6 to the upper end of the stirring barrel 12 for waiting for reaction for many times in a short time under the cooperation of the bearing ring 51 and the vertical groove 52.
Example 7
The stock solution subsequently pushed out by the push disc 44 is mixed with the reacted stock solution by impact, so that the raw materials in the reacted stock solution are completely reacted, and the processing efficiency is improved, the embodiment is an improvement on the basis of the embodiment 6, specifically, referring to fig. 1-7, the mixing part 7 is further mounted on the stirring barrel 12, the mixing part 7 is used for stirring the liquid, the mixing part 7 comprises a striking ring 81 connected to the outer surface of the stirring barrel 12 in a sliding manner, a circular ring 78 is further mounted on the inner wall of the stirring barrel 1, the interior of the processing bin 6 is divided into three spaces by the circular ring 78 and the striking ring 81, the space at the upper end of the circular ring 78 is the flow bin 61, the space between the circular ring 78 and the striking ring 81 is the mixing bin 62, and the space at the lower end of the striking ring 81 is the processing bin 63;
the ring 78 is provided with a first through hole 79, the striking ring 81 is provided with a second through hole 80, and the first through hole 79 and the second through hole 80 are both used for circulating liquid.
Stirring and mixing: according to fig. 7, the pushing disc 44 pushes the reacted stock solution to the upper end surface of the circular ring 78, the reacted stock solution flows to the upper end of the striking ring 81 through the first through hole 79, the reacted stock solution flows to the inside of the processing bin 63 through the second through hole 80 on the striking ring 81, the striking ring 81 is slid upwards to completely react the raw material in the stock solution, so that the striking ring 81 pushes a part of the reacted stock solution to impact the first through hole 79, and the first through hole 79 is ejected, so that the stock solution subsequently pushed out by the pushing disc 44 is mixed with the impacted reacted stock solution, and the raw material in the reacted stock solution completely reacts, thereby improving the processing efficiency.
Example 8
The beating ring 81 can push all the reacted stock solution to impact the first through hole 79, so that the stock solution subsequently pushed out by the pushing disc 44 is mixed with the reacted stock solution by impact, and the reaction is complete, the embodiment is an improvement made on the basis of the embodiment 7, specifically, referring to fig. 1-8, the lower end of the beating ring 81 is provided with a circulating pipe 91, the inside of the circulating pipe 91 is slidably connected with a flat plate 84, the flat plate 84 is provided with a circulating groove 86, the flat plate 84 is used for sealing the circulating pipe 91, the inner wall of the stirring barrel 1 is further provided with a trapezoidal groove 83, the flat plate 84 is used for being slidably connected inside the trapezoidal groove 83, the beating ring 81 is further provided with a spring sheet 85, and the spring sheet 85 is connected with the flat plate 84.
Increase the impact mixing effect: according to fig. 8, since the second through hole 80 formed on the striking ring 81 allows a part of the reacted raw liquid to flow into the processing bin 63, in order to allow the raw material in the reacted raw liquid to be fully reacted, a circulating pipe 91 is installed at the lower end of the striking ring 81, according to fig. 8, when the striking ring 81 slides upwards, a flat plate 84 abutting against the inner wall of the stirring barrel 1 on the circulating pipe 91 is slidably connected inside the trapezoidal groove 83, so that the circulating groove 86 is not overlapped with the hole on the circulating pipe 91, the flat plate 84 seals the circulating pipe 91, the striking ring 81 becomes a sealed body, and the striking ring 81 can push all the reacted raw liquid to impact the first through hole 79, so that the raw liquid subsequently pushed out by the pushing disc 44 is mixed with the reacted raw liquid, and the reaction is completely completed.
Example 9
The rotating shaft 87 is used for driving the stirring blade 92 to rotate, and the stirring blade 92 is used for driving the stock solution in the mixing bin 62 to stir and mix, so as to improve the processing efficiency of the device, in the embodiment, the improvement is made on the basis of the embodiment 8, specifically, please refer to fig. 1-8, the beating ring 81 is further provided with a supporting ring sleeve 82, the inside of the supporting ring sleeve 82 is rotatably connected with the rotating shaft 87, the rotating shaft 87 is slidably connected with the stirring blade 92, the stirring blade 92 is used for stirring the liquid in the mixing bin 62, the rotating shaft 87 is further provided with a fourth spring 90, and the fourth spring 90 is connected with the stirring blade 92;
the rotating shaft 87 penetrates through the first through hole 79, a third spiral groove 88 is further formed in the rotating shaft 87, a second extending block 89 is further mounted on the inner wall of the stirring barrel 1, and the second extending block 89 is connected inside the third spiral groove 88 in a sliding mode.
Rotating and stirring: according to fig. 8, a supporting ring sleeve 82 is further installed on the striking ring 81, a rotating shaft 87 is rotatably connected inside the supporting ring sleeve 82, when the striking ring 81 drives the rotating shaft 87 to slide upwards, the supporting ring is slidably connected inside a third spiral groove 88 through a second extending block 89, so that the rotating shaft 87 rotates, the rotating shaft 87 drives the stirring blade 92 to rotate, and the stirring blade 92 drives the stock solution inside the mixing bin 62 to stir and mix, so as to improve the processing efficiency of the device;
it should be noted that the stirring blade 92 is slidably connected to the rotating shaft 87, so that when the hitting ring 81 slides upward, the stirring blade 92 will abut against the circular ring 78 and slide downward, so as to avoid the hitting ring 81 from being locked, and ensure the hitting ring 81 to rotate and move upward.
Example 10
The raw liquid and the reacted raw liquid are mixed by rotating the beating ring 81 and the stirring blade 92, so that raw materials can be prevented from remaining in the reacted raw liquid, the embodiment is an improvement made on the basis of embodiment 9, specifically, please refer to fig. 1 to 8, an adjusting groove 71 is further arranged on the stirring barrel 12, a second sealing plate 77 is connected in the inner wall of the stirring barrel 12 in a sliding manner, a welding plate 76 is mounted at the lower end of the second sealing plate 77, the welding plate 76 is connected with the beating ring 81, an adjusting sleeve 73 is mounted at the lower end of the welding plate 76, an L-shaped plate 72 is slidably connected inside the adjusting sleeve 73, the pushing disc 44 is used for extruding the L-shaped plate 72 to slide, a first sealing plate 74 is further mounted at the lower end of the L-shaped plate 72, the first sealing plate 74 is slidably connected in the inner wall of the stirring barrel 12, a third spring 75 is further mounted in the inner wall of the stirring barrel 12, and the third spring 75 is connected with the first sealing plate 74.
Liquid pushing and mixing: according to fig. 8, when the pushing disc 44 slides upwards, the pushing disc 44 will abut against the L-shaped plate 72, so that the L-shaped plate 72 slides upwards, at this time, the pushing disc 44 will push the stock solution to flow to the flowing bin 61 and the mixing bin 62, and then when the L-shaped plate 72 abuts against the adjusting sleeve 73, the adjusting sleeve 73 will drive the welding plate 76 to slide upwards, the striking ring 81 will be driven by the welding plate 76 to slide upwards, and the striking ring 81 and the stirring blades 92 will rotate to mix the stock solution and the reacted stock solution, so as to avoid the stock solution which has undergone the reaction from remaining in the stock solution which has undergone the reaction;
it should be noted that a second sealing plate 77 is mounted on the welding plate 76, and a first sealing plate 74 is mounted on the L-shaped plate 72, and the regulating groove 71 is sealed by the second sealing plate 77 and the first sealing plate 74, so that the inside of the agitating barrel 12 is not flowed when the liquid at the mixing bin 62 is not flowed.
It should be noted that, in this document, relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the technical principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.

Claims (10)

1. The aerogel interior wall coating for the purification function is characterized in that: the paint comprises the following components in parts by weight:
150 parts of aerogel slurry;
3 parts of phosphite ester;
30 parts of deionized water;
5 parts of organic acid;
10 parts of odorless styrene-acrylic emulsion;
2 parts of polyvinylpyrrolidone;
and 3 parts of sodium alginate.
2. The method for preparing the aerogel interior wall coating material for purification function according to claim 1, wherein:
s1, placing aerogel slurry, deionized water and phosphite ester into a stirring barrel (1), and dispersing the aerogel slurry, the deionized water and the phosphite ester at a low speed through the inside of the stirring barrel (1);
s2, on the basis of the S1, adding polyvinylpyrrolidone into the stirring barrel (1) to be fused with the primarily dispersed raw materials, raising the temperature in the stirring barrel (1) to 40-45 ℃, and mixing the polyvinylpyrrolidone, the aerogel slurry, deionized water and phosphite ester through high-speed stirring;
s3, on the basis of the S2, adding sodium alginate and the odorless styrene-acrylic emulsion into the stirring barrel (1) again, stirring at a low speed, and reacting at 45 ℃ for half an hour;
and S4, on the basis of the S3, adding organic acid into the stirring barrel (1) and uniformly dispersing for 60 minutes at 800 revolutions per minute to obtain the aerogel coating.
3. The apparatus for preparing an aerogel interior wall coating material for purification function according to claim 2, wherein: a processing bin (6) is arranged inside the stirring barrel (1), the stirring barrel (12) is connected inside the processing bin (6) in a sliding mode, an adjusting device (4) is connected inside the stirring barrel (12) in a sliding mode, the adjusting device (4) is used for pushing liquid inside the stirring barrel (12), and the adjusting device (4) comprises a pushing disc (44) connected inside the stirring barrel (12) in a sliding mode;
still be provided with first shrinkage pool (13) on agitator (12), first shrinkage pool (13) is linked together with the inside in processing storehouse (6), be provided with first check valve on push away dish (44), the internally mounted of first shrinkage pool (13) has the second check valve, push away dish (44) and be used for the inside liquid of negative pressure extraction first shrinkage pool (13) to the lower extreme that pushes away dish (44).
4. The apparatus for preparing an aerogel interior wall coating material for purification function according to claim 3, wherein: the first one-way valve comprises a second concave hole (14) formed in a push disc (44), a second vertical hole (16) communicated with the second concave hole (14) is further formed in the push disc (44), a second sealing disc (21) used for sealing the second concave hole (14) is connected to the inside of the second concave hole (14) in a sliding mode, a second short rod (23) is installed at the lower end of the second sealing disc (21), a second spring (22) is installed on the outer surface of the second short rod (23), and the second spring (22) is connected with the push disc (44);
there is second check valve including setting up first perpendicular hole (15) on agitator (12), first perpendicular hole (15) are linked together with first shrinkage pool (13), the inside sliding connection of first shrinkage pool (13) has first sealed dish (18) that are used for sealed first shrinkage pool (13), still install first quarter butt (19) on first sealed dish (18), the surface mounting of first quarter butt (19) has first spring (20), first spring (20) are connected with agitator (12).
5. The apparatus for preparing an aerogel interior wall coating material for purification function as set forth in claim 3, wherein: the stirring device is characterized in that a motor (3) is further mounted on the stirring barrel (1), a transmission sleeve (41) is mounted on an output shaft of the motor (3), a force accumulation part is further mounted inside the stirring barrel (12), a round rod (47) is mounted on the force accumulation part, and the round rod (47) penetrates through the push disc (44) and is in threaded connection with the push disc (44);
round bar (47) sliding connection is in the inside of transmission cover (41), be provided with first piece (46) of stretching out on round bar (47), the internally mounted of transmission cover (41) has first piece (46) of stretching out, first piece (46) sliding connection of stretching out is in the inside of first helicla flute (45), still install slider (49) on pushing away dish (44), the inner wall of agitator (12) is provided with square groove (48), slider (49) sliding connection is in the inside of square groove (48).
6. The apparatus for preparing an aerogel interior wall coating material for purification function according to claim 5, wherein: the inner wall of the transmission sleeve (41) is further provided with a circular groove (50), a bearing ring (51) is rotatably connected inside the circular groove (50), and the bearing ring (51) is connected with the first extending block (46);
the power storage component comprises a support sleeve (54) installed on the stirring barrel (12), a torque spring (55) is installed inside the support sleeve (54), a round rod (47) is rotatably connected inside the support sleeve (54) and connected with the torque spring (55), a vertical groove (52) communicated with a first spiral groove (45) is further formed in the round rod (47), a second spiral groove (53) communicated with the vertical groove (52) is further formed in the round rod (47), and a first extending block (46) is used for being connected inside a connecting rod (42) and the second spiral groove (53) in a sliding mode.
7. The apparatus for preparing an aerogel interior wall coating material for purification function according to claim 3, wherein: the stirring barrel (12) is further provided with a mixing component (7), the mixing component (7) is used for stirring liquid, the mixing component (7) comprises a beating ring (81) which is connected to the outer surface of the stirring barrel (12) in a sliding mode, the inner wall of the stirring barrel (1) is further provided with a circular ring (78), the circular ring (78) and the beating ring (81) divide the interior of the processing bin (6) into three spaces, the space at the upper end of the circular ring (78) is a flowing bin (61), the space between the circular ring (78) and the beating ring (81) is a mixing bin (62), and the space at the lower end of the beating ring (81) is a processing bin (63);
be provided with first through-hole (79) on ring (78), be provided with second through-hole (80) on beating ring (81), first through-hole (79) all are used for circulating liquid with second through-hole (80).
8. The apparatus for preparing an aerogel interior wall coating material for purification function as set forth in claim 7, wherein: the lower end of the beating ring (81) is provided with a circulating pipe (91), the inside of the circulating pipe (91) is connected with a flat plate (84) in a sliding mode, a circulating groove (86) is formed in the flat plate (84), the flat plate (84) is used for sealing the circulating pipe (91), a trapezoidal groove (83) is further formed in the inner wall of the stirring barrel (1), the flat plate (84) is used for being connected to the inside of the trapezoidal groove (83) in a sliding mode, an elastic sheet (85) is further installed on the beating ring (81), and the elastic sheet (85) is connected with the flat plate (84).
9. The apparatus for preparing an aerogel interior wall coating material for purification function according to claim 7, wherein: the beating ring (81) is further provided with a supporting ring sleeve (82), the supporting ring sleeve (82) is connected with a rotating shaft (87) in a rotating mode, the rotating shaft (87) is connected with a stirring blade (92) in a sliding mode, the stirring blade (92) is used for stirring liquid in the mixing bin (62), the rotating shaft (87) is further provided with a fourth spring (90), and the fourth spring (90) is connected with the stirring blade (92);
rotation axis (87) run through first through-hole (79), still be provided with third helicla flute (88) on rotation axis (87), still install the second on the inner wall of agitator (1) and stretch out piece (89), piece (89) sliding connection is stretched out to the second in the inside of third helicla flute (88).
10. The apparatus for preparing an aerogel interior wall coating material for purification function according to claim 9, wherein: the stirring device is characterized in that an adjusting groove (71) is further arranged on the stirring barrel (12), a second sealing plate (77) is connected to the inner wall of the stirring barrel (12) in a sliding manner, a welding plate (76) is installed at the lower end of the second sealing plate (77), the welding plate (76) is connected with a striking ring (81), an adjusting sleeve (73) is installed at the lower end of the welding plate (76), an L-shaped plate (72) is connected to the inner portion of the adjusting sleeve (73) in a sliding manner, the push disc (44) is used for extruding the L-shaped plate (72) to slide, a first sealing plate (74) is further installed at the lower end of the L-shaped plate (72), the first sealing plate (74) is connected to the inner wall of the stirring barrel (12) in a sliding manner, a third spring (75) is further installed in the inner wall of the stirring barrel (12), and the third spring (75) is connected with the first sealing plate (74);
support section of thick bamboo (2) are still installed to the lower extreme of agitator (1), the internally mounted of support section of thick bamboo (2) has pneumatic cylinder (10), install slide bar (11) on pneumatic cylinder (10), slide bar (11) run through support section of thick bamboo (2) and are connected with agitator (12), slide bar (11) are used for promoting agitator (12) and go up and down.
CN202210021845.3A 2022-01-10 2022-01-10 Aerogel interior wall coating for purification function Active CN115948081B (en)

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