CN115901856A - Heat detection equipment - Google Patents

Heat detection equipment Download PDF

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Publication number
CN115901856A
CN115901856A CN202211688289.1A CN202211688289A CN115901856A CN 115901856 A CN115901856 A CN 115901856A CN 202211688289 A CN202211688289 A CN 202211688289A CN 115901856 A CN115901856 A CN 115901856A
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heat
liquid
storage tank
liquid storage
combustion
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王岩
张清军
李元景
陈志强
李荐民
刘耀红
郝中原
赵晓琳
刘鹏
李鸽
罗丛
李广勤
魏来
杨内
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Tsinghua University
Nuctech Co Ltd
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Tsinghua University
Nuctech Co Ltd
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Priority to CN202211688289.1A priority Critical patent/CN115901856A/en
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Abstract

The utility model provides a heat detection device, which is applied to the technical field of energy sources and comprises a combustion device, an ignition laser, a temperature measuring meter and a control module, wherein the combustion device is provided with a combustion cavity, the combustion cavity is provided with an irradiation port, and a crucible for bearing a coal sample is suitable to be placed in the combustion cavity; the ignition laser is arranged above the combustion device and emits laser to the coal sample in the combustion cavity through the irradiation hole of the combustion cavity so as to ignite the coal sample; the temperature meter is used for detecting the temperature of a heat exchange medium exchanging heat with the heat in the combustion chamber and generating a temperature signal; the control module is in communication connection with the temperature meter to receive the temperature signal. The heat detection equipment has the advantages of convenience in experiment and accurate result.

Description

热量检测设备Heat detection equipment

技术领域technical field

本公开涉及能源技术领域,更具体地,涉及一种热量检测设备。The disclosure relates to the field of energy technology, and more specifically, to a heat detection device.

背景技术Background technique

随着工业化发展到今天,煤炭能源日益趋于紧张,为了获得更高的燃烧效率,需要对煤炭的热量指标进行测量,以充分的利用煤炭能源。现有技术中的氧弹热量计使用电热丝或棉线作为引燃物质,在最终热量计量时需要扣除该不稳定燃烧热背景。而且在多次样本测量时,需要更换氧弹,不同的氧弹由于制造差异热阻不一致,造成使用不同氧弹测量的样本的测量时间有所区别,导致散热时间有所区别。另外不同氧弹校准后误差不一致,从而导致样本与样本之间的测量误差不一致,导致热量分析时变得困难且准确度降低。With the development of industrialization, coal energy is becoming more and more scarce. In order to obtain higher combustion efficiency, it is necessary to measure the heat index of coal to make full use of coal energy. Oxygen bomb calorimeters in the prior art use heating wires or cotton threads as ignition substances, and the unstable combustion heat background needs to be deducted in the final calorie measurement. In addition, when multiple samples are measured, the oxygen bomb needs to be replaced. Different oxygen bombs have inconsistent thermal resistance due to manufacturing differences, resulting in differences in the measurement time of samples measured with different oxygen bombs, resulting in differences in heat dissipation time. In addition, the errors after calibration of different oxygen bombs are inconsistent, resulting in inconsistent measurement errors between samples, making thermal analysis difficult and reducing accuracy.

发明内容Contents of the invention

为解决现有技术中的上述问题,本公开实施例提出一种热量检测设备,所述热量检测设备具有便于实验和结果准确的优点。In order to solve the above-mentioned problems in the prior art, an embodiment of the present disclosure proposes a heat detection device, which has the advantages of convenient experimentation and accurate results.

本公开的一个方面提供了一种热量检测设备,用于测量煤的热量指标,热量检测设备包括燃烧装置、引燃激光器、温度测量计和控制模块,所述燃烧装置具有燃烧腔,所述燃烧腔开设有照射口,所述燃烧腔内适于放置承载煤样的坩埚;所述引燃激光器设于所述燃烧装置的上方,通过所述燃烧腔的照射口向所述燃烧腔内的煤样发射激光以引燃该煤样;所述温度测量计用于探测与所述燃烧腔内的热量进行换热的换热介质的温度,并生成温度信号;所述控制模块与所述温度测量计通讯连接以接收所述温度信号。One aspect of the present disclosure provides a heat detection device for measuring the heat index of coal. The heat detection device includes a combustion device, an ignition laser, a temperature gauge and a control module. The combustion device has a combustion chamber, and the combustion The cavity is provided with an irradiation port, and the crucible for carrying coal samples is suitable for placing in the combustion cavity; The sample emits laser light to ignite the coal sample; the temperature measuring instrument is used to detect the temperature of the heat exchange medium that exchanges heat with the heat in the combustion chamber, and generates a temperature signal; the control module and the temperature measurement Meter communication connection to receive the temperature signal.

根据本公开实施例的热量检测设备,通过设置引燃激光器可以便于引燃煤样,由于引燃激光器的热量较稳定,在最终热量计量时需要扣除的热量容易计量,使得热量指标的计算较为准确。而且在多次煤样样本测量时,无需更换引燃激光器,使得不同煤样样本的测量时间相同以及散热时间相同,有利于实验的顺利进行。由于无需更换引燃激光器,每次引入的热量误差一致性好,从而导致样本与样本之间的测量误差一致,便于热量分析且结果准确度较高。According to the heat detection equipment of the embodiment of the present disclosure, setting the ignition laser can facilitate the ignition of the coal sample. Since the heat of the ignition laser is relatively stable, the heat that needs to be deducted in the final heat measurement is easy to measure, so that the calculation of the heat index is more accurate. . Moreover, when coal samples are measured for many times, there is no need to replace the ignition laser, so that the measurement time and heat dissipation time of different coal samples are the same, which is conducive to the smooth progress of the experiment. Since there is no need to replace the ignition laser, the heat error introduced each time is consistent, resulting in consistent measurement errors between samples, which is convenient for thermal analysis and has high accuracy of results.

在一些实施例中,所述热量检测设备还包括第一储液箱,所述第一储液箱围设于所述燃烧腔外,所述第一储液箱内通入换热液体,所述温度测量计的探头设于所述第一储液箱内实时测量所述第一储液箱内的所述换热液体的温度,并生成温度信号。In some embodiments, the heat detection device further includes a first liquid storage tank, the first liquid storage tank surrounds the combustion chamber, and a heat exchange liquid is passed into the first liquid storage tank, so that The probe of the temperature measuring meter is set in the first liquid storage tank to measure the temperature of the heat exchange liquid in the first liquid storage tank in real time, and generate a temperature signal.

在一些实施例中,所述第一储液箱为环状储液箱,所述第一储液箱包括第一盛液部和第一中空部,所述第一盛液部内通入换热液体,所述燃烧装置的至少部分设于所述第一中空部,所述热量检测设备还包括换热管,所述换热管设于所述第一盛液部内,所述换热管的一端与所述燃烧腔连通,所述换热管的另一端与外部环境连通。In some embodiments, the first liquid storage tank is an annular liquid storage tank, the first liquid storage tank includes a first liquid storage part and a first hollow part, and the heat exchange Liquid, at least part of the combustion device is set in the first hollow part, the heat detection device also includes a heat exchange tube, the heat exchange tube is set in the first liquid containing part, the heat exchange tube One end communicates with the combustion chamber, and the other end of the heat exchange tube communicates with the external environment.

在一些实施例中,所述热量检测设备还包括搅拌桨,所述搅拌桨可转动地设于所述第一盛液部内。In some embodiments, the heat detection device further includes a stirring paddle, and the stirring paddle is rotatably arranged in the first liquid containing part.

在一些实施例中,所述热量检测设备还包括:循环泵,所述循环泵与所述第一盛液部连通;制冷模块,所述制冷模块与所述循环泵连通,所述循环泵将所述第一盛液部中的所述换热液体抽至所述制冷模块;第二储液箱,所述第二储液箱与所述制冷模块连通,所述制冷模块将制冷后的换热液体输入至所述第二储液箱,所述第二储液箱与所述第一盛液部连通,以将流入所述第二储液箱的换热液体流入所述第一盛液部。In some embodiments, the heat detection device further includes: a circulation pump, the circulation pump communicates with the first liquid containing part; a refrigeration module, the refrigeration module communicates with the circulation pump, and the circulation pump The heat exchange liquid in the first liquid storage part is pumped to the refrigeration module; the second liquid storage tank is connected to the refrigeration module, and the refrigeration module stores the cooled exchange The hot liquid is input into the second liquid storage tank, and the second liquid storage tank communicates with the first liquid storage part, so that the heat exchange liquid flowing into the second liquid storage tank flows into the first liquid storage part department.

在一些实施例中,所述第二储液箱包括第二盛液部和由底部向上凹入所述第二盛液部的第二中空部,所述第二盛液部与所述制冷模块连通,所述制冷模块将制冷后的换热液体输入至所述第二盛液部,所述第二盛液部与所述第一盛液部连通,所述第一储液箱和所述燃烧装置的至少部分设于所述第二中空部。In some embodiments, the second liquid storage tank includes a second liquid storage part and a second hollow part recessed upward from the bottom into the second liquid storage part, and the second liquid storage part is connected to the refrigeration module connected, the refrigeration module inputs the refrigerated heat exchange liquid to the second liquid storage part, the second liquid storage part communicates with the first liquid storage part, and the first liquid storage tank and the At least part of the combustion device is provided in the second hollow portion.

在一些实施例中,所述热量检测设备还包括隔热件,所述隔热件设于所述第二中空部,且位于所述第一盛液部的环形外壁与所述第二盛液部的环形内壁之间。In some embodiments, the heat detection device further includes a heat insulating element, the heat insulating element is arranged in the second hollow part, and is located between the annular outer wall of the first liquid containing part and the second liquid containing part. between the annular inner walls of the

在一些实施例中,所述热量检测设备还包括支撑组件,所述第一储液箱、所述第二储液箱和所述燃烧装置设于所述支撑组件,所述支撑组件具有进气口,所述进气口和所述燃烧腔连通,煤样燃烧所需气体通过所述进气口进入所述燃烧腔。In some embodiments, the heat detection device further includes a support assembly, the first liquid storage tank, the second liquid storage tank and the combustion device are arranged on the support assembly, and the support assembly has an air intake The air inlet communicates with the combustion chamber, and the gas required for coal sample combustion enters the combustion chamber through the air inlet.

在一些实施例中,所述支撑组件包括:支架;支撑座,所述支撑座设于所述支架,所述支撑座包括第一支撑部和第二支撑部,所述第二支撑部的支撑面高于所述第一支撑部的支撑面,所述第二储液箱和所述第一储液箱设于所述第一支撑部,所述第二支撑部的部分伸入所述第二中空部,且所述第二支撑部的支撑面与所述第一储液箱的底部平齐,所述燃烧装置的底部设于所述第二支撑部的支撑面上,所述燃烧装置的底部具有贯通口,所述贯通口与所述第二支撑部的所述进气口连通。In some embodiments, the support assembly includes: a bracket; a support base, the support base is arranged on the bracket, the support base includes a first support part and a second support part, and the support of the second support part The surface is higher than the support surface of the first support part, the second liquid storage tank and the first liquid storage tank are arranged on the first support part, and part of the second support part extends into the first support part. Two hollow parts, and the support surface of the second support part is flush with the bottom of the first liquid storage tank, the bottom of the combustion device is set on the support surface of the second support part, and the combustion device There is a through-hole at the bottom of the body, and the through-hole communicates with the air inlet of the second support part.

在一些实施例中,所述热量检测设备还包括:弹性件,所述弹性件设于第二支撑部;托盘,所述托盘设于所述弹性件,所述承载煤样的坩埚适于放置在所述托盘内;防尘罩,当将所述防尘罩罩设于所述坩埚时,所述弹性件处于压缩状态;激光管,所述激光管的一端设于所述坩埚且与煤样正对,所述激光管的另一端穿过所述防尘罩与所述照射口正对。In some embodiments, the heat detection device further includes: an elastic member, the elastic member is arranged on the second supporting part; a tray, the tray is arranged on the elastic member, and the crucible carrying the coal sample is suitable for placing In the tray; a dust cover, when the dust cover is set on the crucible, the elastic member is in a compressed state; a laser tube, one end of the laser tube is set on the crucible and connected to the coal The other end of the laser tube passes through the dust cover and faces the irradiation port.

在一些实施例中,所述热量检测设备还包括驱动件和传动件,所述传动件的一端与所述驱动件连接,所述传动件的另一端与所述第二储液箱连接,所述驱动件适于驱动所述传动件带动所述第二储液箱以及设于所述第二中空部内的所述第一储液箱和所述燃烧装置与所述支撑座分离和连接。In some embodiments, the heat detection device further includes a driving element and a transmission element, one end of the transmission element is connected to the driving element, and the other end of the transmission element is connected to the second liquid storage tank, so The driving member is suitable for driving the transmission member to drive the second liquid storage tank, the first liquid storage tank and the combustion device disposed in the second hollow part to separate from and connect to the support base.

在一些实施例中,所述热量检测设备还包括:玻璃盖板,所述玻璃盖板倾斜设于所述照射口以封堵所述照射口,所述引燃激光器发射的激光透过所述玻璃盖板照射于煤样;探测器,所述探测器与所述玻璃盖板水平,且与所述玻璃盖板的照射面相对设置。In some embodiments, the heat detection device further includes: a glass cover, the glass cover is obliquely arranged on the irradiation opening to block the irradiation opening, the laser light emitted by the ignition laser passes through the The glass cover plate is irradiated on the coal sample; the detector is horizontal to the glass cover plate and set opposite to the irradiated surface of the glass cover plate.

本公开的附加方面和优点将在下面的描述中部分给出,部分将从下面的描述中变得明显,或通过本公开的实践了解到。Additional aspects and advantages of the disclosure will be set forth in part in the description which follows, and in part will be obvious from the description, or may be learned by practice of the disclosure.

附图说明Description of drawings

为了更完整地理解本公开及其优势,现在将参考结合附图的以下描述,其中:For a more complete understanding of the present disclosure and its advantages, reference should now be made to the following description taken in conjunction with the accompanying drawings, in which:

图1是根据本公开实施例的热量检测设备的结构示意图;FIG. 1 is a schematic structural diagram of a heat detection device according to an embodiment of the present disclosure;

图2是根据本公开实施例的热量检测设备的剖视图;2 is a cross-sectional view of a heat detection device according to an embodiment of the present disclosure;

图3是根据本公开实施例的激光在穿过玻璃盖板和空气的界面时,发生部分反射的示意图;3 is a schematic diagram of partial reflection of laser light passing through an interface between a glass cover and air according to an embodiment of the present disclosure;

图4是根据本公开实施例的煤质分析系统的结构示意图。Fig. 4 is a schematic structural diagram of a coal quality analysis system according to an embodiment of the present disclosure.

附图标记:Reference signs:

煤质分析系统1000,坩埚100d,Coal quality analysis system 1000, crucible 100d,

热量检测设备100b,heat detection device 100b,

燃烧装置1b,燃烧腔11b,Combustion device 1b, combustion chamber 11b,

温度测量计2b,第一储液箱3b,第一盛液部3lb,Temperature measuring gauge 2b, first liquid storage tank 3b, first liquid containing part 3lb,

换热管4b,搅拌桨5b,循环泵6b,抽水管6lb,制冷模块7b,第二储液箱8b,第二盛液部8lb,隔热件9b,Heat exchange tube 4b, stirring paddle 5b, circulation pump 6b, water suction pipe 6lb, refrigeration module 7b, second liquid storage tank 8b, second liquid containing part 8lb, heat insulation 9b,

支撑组件l0b,支架l0lb,支撑座102b,第一支撑部1021b,第二支撑部1022b,进气口10221b,Support assembly l0b, bracket l0lb, support seat 102b, first support portion 1021b, second support portion 1022b, air inlet 10221b,

引燃激光器20b,弹性件30b,托盘40b,防尘罩50b,激光管60b,Ignition laser 20b, elastic member 30b, tray 40b, dust cover 50b, laser tube 60b,

驱动件70b,传动件80b,玻璃盖板90b,探测器ll0b,衰减器120b,挡板130b,控制模块140b,Drive 70b, transmission 80b, glass cover 90b, detector 110b, attenuator 120b, baffle 130b, control module 140b,

加热炉l00a,载物架100e,设备仓1e,电器仓2e。Heating furnace l00a, carrier 100e, equipment warehouse 1e, electrical warehouse 2e.

具体实施方式Detailed ways

以下,将参照附图来描述本公开的实施例。但是应该理解,这些描述只是示例性的,而并非要限制本公开的范围。此外,在以下说明中,省略了对公知结构和技术的描述,以避免不必要地混淆本公开的概念。另外,本公开以下提供的各个实施例以及实施例中的技术特征可以以任意方式相互组合。Hereinafter, embodiments of the present disclosure will be described with reference to the drawings. It should be understood, however, that these descriptions are exemplary only, and are not intended to limit the scope of the present disclosure. Also, in the following description, descriptions of well-known structures and techniques are omitted to avoid unnecessarily obscuring the concept of the present disclosure. In addition, the various embodiments provided below in the present disclosure and the technical features in the embodiments can be combined with each other in any manner.

在此使用的术语仅仅是为了描述具体实施例,而并非意在限制本公开。此外,在此使用的术语“包括”、“包含”等表明了所述特征、步骤、操作和/或部件的存在,但是并不排除存在或添加一个或多个其他特征、步骤、操作或部件。在此使用的所有术语(包括技术和科学术语)具有本领域技术人员通常所理解的含义,除非另外定义。应注意,这里使用的术语应解释为具有与本说明书的上下文相一致的含义,而不应以理想化或过于刻板的方式来解释。The terminology used herein is for the purpose of describing particular embodiments only, and is not intended to be limiting of the present disclosure. In addition, the terms "comprising", "comprising", etc. used herein indicate the existence of stated features, steps, operations and/or components, but do not exclude the existence or addition of one or more other features, steps, operations or components . All terms (including technical and scientific terms) used herein have the meaning commonly understood by one of ordinary skill in the art, unless otherwise defined. It should be noted that the terms used herein should be interpreted to have a meaning consistent with the context of this specification, and not be interpreted in an idealized or overly rigid manner.

随着工业化发展到今天,煤炭能源日益趋于紧张,为了获得更高的燃烧效率,需要对煤炭的热量指标进行测量,以充分的利用煤炭能源。现有技术中的氧弹热量计使用电热丝或棉线作为引燃物质,在最终热量计量时需要扣除该不稳定燃烧热背景。而且在多次样本测量时,需要更换氧弹,不同的氧弹由于制造差异热阻不一致,造成使用不同氧弹测量的样本的测量时间有所区别,导致散热时间有所区别。另外不同氧弹校准后误差不一致,从而导致样本与样本之间的测量误差不一致,导致热量分析时变得困难且准确度降低。With the development of industrialization, coal energy is becoming more and more scarce. In order to obtain higher combustion efficiency, it is necessary to measure the heat index of coal to make full use of coal energy. Oxygen bomb calorimeters in the prior art use heating wires or cotton threads as ignition substances, and the unstable combustion heat background needs to be deducted in the final calorie measurement. In addition, when multiple samples are measured, the oxygen bomb needs to be replaced. Different oxygen bombs have inconsistent thermal resistance due to manufacturing differences, resulting in differences in the measurement time of samples measured with different oxygen bombs, resulting in differences in heat dissipation time. In addition, the errors after calibration of different oxygen bombs are inconsistent, resulting in inconsistent measurement errors between samples, making thermal analysis difficult and reducing accuracy.

下面参考图1-图4描述根据本公开实施例的热量检测设备100b和煤质分析系统1000。The following describes a heat detection device 100b and a coal quality analysis system 1000 according to an embodiment of the present disclosure with reference to FIGS. 1-4 .

如图1-图3所示,根据本公开实施例的热量检测设备100b,用于测量煤的热量指标,热量检测设备100b可以包括燃烧装置1b、引燃激光器20b、温度测量计2b和控制模块140b。燃烧装置1b具有燃烧腔11b,燃烧腔11b开设有照射口,燃烧腔11b内适于放置承载煤样的坩埚100d;引燃激光器20b设于燃烧装置1b的上方,通过燃烧腔11b的照射口向燃烧腔11b内的煤样发射激光以引燃该煤样;温度测量计2b用于探测与燃烧腔11b内的热量进行换热的换热介质的温度,并生成温度信号,温度测量计2b与控制模块140b通讯连接。As shown in Figures 1-3, a heat detection device 100b according to an embodiment of the present disclosure is used to measure the heat index of coal, and the heat detection device 100b may include a combustion device 1b, an ignition laser 20b, a thermometer 2b and a control module 140b. The combustion device 1b has a combustion chamber 11b, and the combustion chamber 11b is provided with an irradiation port, and the combustion chamber 11b is suitable for placing a crucible 100d carrying a coal sample; an ignition laser 20b is arranged above the combustion device 1b, and passes through the irradiation port of the combustion chamber 11b to The coal sample in the combustion chamber 11b emits laser light to ignite the coal sample; the thermometer 2b is used to detect the temperature of the heat exchange medium that exchanges heat with the heat in the combustion chamber 11b, and generates a temperature signal. The thermometer 2b and The control module 140b is connected in communication.

其中,设置引燃激光器20b可以便于引燃煤样,温度测量计2b可以测量煤样燃烧前的换热介质的温度,并生成温度信号传输至控制模块140b,温度测量计2b可以测量煤样燃烧后的换热介质的温度,并生成温度信号传输至控制模块140b,控制模块140b根据煤样燃烧前的换热介质的温度、煤样燃烧后的换热介质的温度和引燃激光器20b引入的热量即可计算出煤的热量指标。Among them, setting the ignition laser 20b can facilitate the ignition of the coal sample, the temperature measuring instrument 2b can measure the temperature of the heat exchange medium before the coal sample is burned, and generate a temperature signal and transmit it to the control module 140b, and the temperature measuring instrument 2b can measure the temperature of the coal sample burning The temperature of the heat exchange medium after burning, and generate a temperature signal and transmit it to the control module 140b. The control module 140b is based on the temperature of the heat exchange medium before coal sample combustion, the temperature of the heat exchange medium after coal sample combustion, and the The heat can be used to calculate the heat index of coal.

另外,煤样引燃使用引燃激光器20b完成,重复性好且不需要维护。在一些实验数据中,以80%光衰(引燃激光器20b寿命特性)计算,单次分析点燃5分钟,可使用超过3.8万次。以32个样本/天计算,可使用1200天以上。在允许误差为1%时,每周使用标准样本校准一次即可,直至激光能量无法点燃煤样。上述实验数据仅以举例说明,并不能理解为对本公开的限制。In addition, the ignition of the coal sample is completed using the ignition laser 20b, which has good repeatability and does not require maintenance. In some experimental data, calculated on the basis of 80% light decay (the lifetime characteristics of the ignition laser 20b), a single analysis of ignition for 5 minutes can be used more than 38,000 times. Based on 32 samples/day, it can be used for more than 1200 days. When the allowable error is 1%, it is enough to use the standard sample to calibrate once a week until the laser energy cannot ignite the coal sample. The above experimental data are for illustration only, and should not be construed as limiting the present disclosure.

根据本公开实施例的热量检测设备100b,通过设置引燃激光器20b可以便于引燃煤样,由于引燃激光器20b的热量较稳定,在最终热量计量时需要扣除的热量容易计量,使得热量指标的计算较为准确。而且在多次煤样样本测量时,无需更换引燃激光器20b,使得不同煤样样本的测量时间相同以及散热时间相同,有利于实验的顺利进行。由于无需更换引燃激光器20b,每次引入的热量误差一致性好,从而导致样本与样本之间的测量误差一致,便于热量分析且结果准确度较高。According to the calorie detection device 100b of the embodiment of the present disclosure, the coal sample can be easily ignited by setting the ignition laser 20b. Since the heat of the ignition laser 20b is relatively stable, the heat that needs to be deducted in the final calorie measurement is easy to measure, so that the calorie index The calculation is more accurate. Moreover, when coal samples are measured for many times, there is no need to replace the ignition laser 20b, so that the measurement time and heat dissipation time of different coal samples are the same, which is conducive to the smooth progress of the experiment. Since there is no need to replace the ignition laser 20b, the heat error introduced each time is consistent, resulting in consistent measurement errors between samples, which is convenient for heat analysis and has high accuracy of results.

根据本公开的一些实施例,如图1和图2所示,热量检测设备l00b还可以包括第一储液箱3b,第一储液箱3b围设于燃烧腔11b外,第一储液箱3b内通入换热液体,温度测量计2b的探头设于第一储液箱3b内实时测量第一储液箱3b内的换热液体的温度,并生成温度信号。由此,燃烧腔11b内燃烧煤样的热量可以传递到换热液体中,温度测量计2b可以实时测量换热液体的温度并将温度信号传输至控制模块140b,控制模块140b通过分析换热前换热液体的温度和换热后换热液体的温度即可得到煤样的热量指标。According to some embodiments of the present disclosure, as shown in FIG. 1 and FIG. 2 , the heat detection device 100b may further include a first liquid storage tank 3b, the first liquid storage tank 3b is arranged outside the combustion chamber 11b, and the first liquid storage tank The heat exchange liquid is passed into 3b, and the probe of the thermometer 2b is set in the first liquid storage tank 3b to measure the temperature of the heat exchange liquid in the first liquid storage tank 3b in real time, and generate a temperature signal. Thus, the heat of the coal sample burned in the combustion chamber 11b can be transferred to the heat exchange liquid, and the temperature measuring instrument 2b can measure the temperature of the heat exchange liquid in real time and transmit the temperature signal to the control module 140b. The heat index of the coal sample can be obtained from the temperature of the heat exchange liquid and the temperature of the heat exchange liquid after heat exchange.

在本公开的一些实施例中,如图2所示,第一储液箱3b为环状储液箱,第一储液箱3b包括第一盛液部31b和第一中空部,第一盛液部31b内通入换热液体,燃烧装置1b的至少部分设于第一中空部,热量检测设备100b还包括换热管4b,换热管4b设于第一盛液部31b内,换热管4b的一端与燃烧腔11b连通,换热管4b的另一端与外部环境连通。这里,第一储液箱3b的内环壁面与燃烧装置1b的设于第一中空部的部分的壁面可以为同一壁面,也可以为不同壁面。当第一储液箱3b的内环壁面与燃烧装置1b的设于第一中空部的部分的壁面为同一壁面时,相当于燃烧装置1b的至少部分沉入换热液体。In some embodiments of the present disclosure, as shown in FIG. 2 , the first liquid storage tank 3b is an annular liquid storage tank, and the first liquid storage tank 3b includes a first liquid containing part 31b and a first hollow part, and the first containing The heat exchange liquid is passed into the liquid part 31b, at least a part of the combustion device 1b is arranged in the first hollow part, and the heat detection device 100b also includes a heat exchange tube 4b, and the heat exchange tube 4b is arranged in the first liquid containing part 31b for heat exchange. One end of the tube 4b communicates with the combustion chamber 11b, and the other end of the heat exchange tube 4b communicates with the external environment. Here, the inner ring wall surface of the first liquid storage tank 3b and the wall surface of the portion of the combustion device 1b provided in the first hollow portion may be the same wall surface or may be different wall surfaces. When the inner ring wall surface of the first liquid storage tank 3b is the same wall surface as the wall surface of the portion of the combustion device 1b disposed in the first hollow portion, it means that at least part of the combustion device 1b sinks into the heat exchange liquid.

由此,燃烧腔11b内燃烧煤样的热量可以进入换热管4b,通过换热管4b可以将热量换热到换热液体中,温度测量计2b可以实时测量换热液体的温度并将温度信号传输至控制模块140b,控制模块140b通过分析换热前换热液体的温度和换热后换热液体的温度即可得到煤样的热量指标。其中,第二储液箱8b的第一中空部可以便于至少部分燃烧装置1b的设置,并且有利于实现将燃烧腔11b内的热量换热到第一盛液部31b内的换热液体中。Thus, the heat of burning coal samples in the combustion chamber 11b can enter the heat exchange tube 4b, and the heat can be exchanged into the heat exchange liquid through the heat exchange tube 4b, and the temperature measuring instrument 2b can measure the temperature of the heat exchange liquid in real time and set the temperature The signal is transmitted to the control module 140b, and the control module 140b can obtain the heat index of the coal sample by analyzing the temperature of the heat exchange liquid before heat exchange and the temperature of the heat exchange liquid after heat exchange. Wherein, the first hollow part of the second liquid storage tank 8b can facilitate the installation of at least part of the combustion device 1b, and facilitate heat exchange from the combustion chamber 11b to the heat exchange liquid in the first liquid storage part 31b.

根据本公开的一些实施例,如图2所示,热量检测设备100b还包括搅拌桨5b,搅拌桨5b可转动地设于第一盛液部31b内。由此,搅拌桨5b可以均匀第一盛液部31b内换热液体的温度,使得测量结果更加准确。According to some embodiments of the present disclosure, as shown in FIG. 2 , the heat detection device 100b further includes a stirring paddle 5b, which is rotatably disposed in the first liquid containing portion 31b. Thus, the stirring paddle 5b can even out the temperature of the heat exchange liquid in the first liquid containing part 31b, so that the measurement result is more accurate.

在本公开的一些实施例中,如图1和图2所示,热量检测设备1O0b还包括循环泵6b、制冷模块7b和第二储液箱8b。循环泵6b与第一盛液部31b连通;制冷模块7b与循环泵6b连通,循环泵6b将第一盛液部31b中的换热液体抽至制冷模块7b;第二储液箱8b与制冷模块7b连通,制冷模块7b将制冷后的换热液体输入至第二储液箱8b,第二储液箱8b与第一盛液部31b连通,以将流入第二储液箱8b的换热液体流入第一盛液部31b。由此可以便于完成第一储液箱3b内的换热液体循环过程,使得可以对第一盛液部31b内的换热液体进行温度调节,使得换热前的换热液体温度可控,从而使得对煤样的热量指标的测量更加精确。In some embodiments of the present disclosure, as shown in FIG. 1 and FIG. 2 , the heat detection device 100b further includes a circulation pump 6b, a refrigeration module 7b and a second liquid storage tank 8b. The circulation pump 6b communicates with the first liquid storage part 31b; the refrigeration module 7b communicates with the circulation pump 6b, and the circulation pump 6b pumps the heat exchange liquid in the first liquid storage part 31b to the refrigeration module 7b; the second liquid storage tank 8b communicates with the refrigeration module 7b. The module 7b is connected, and the refrigeration module 7b inputs the refrigerated heat exchange liquid to the second liquid storage tank 8b, and the second liquid storage tank 8b communicates with the first liquid storage part 31b to transfer the heat exchange fluid flowing into the second liquid storage tank 8b. The liquid flows into the first liquid containing portion 31b. This can facilitate the completion of the heat exchange liquid circulation process in the first liquid storage tank 3b, so that the temperature of the heat exchange liquid in the first liquid storage part 31b can be adjusted, so that the temperature of the heat exchange liquid before heat exchange can be controlled, thereby It makes the measurement of the heat index of the coal sample more accurate.

而现有氧弹热量计无法在工作后自动恢复至测试前温度。由于受限于加水定量精度,因此更换水箱中的水会导致热容改变,在1天内需要重复换水校准。累计连续测量还会导致氧弹热量计内水箱与外水箱温差越来越大,脱离工况,无法连续运行。氧弹表面亲水的特性还导致更换氧弹时造成热量计内水箱水量下降,计量失准。However, the existing oxygen bomb calorimeter cannot automatically return to the temperature before the test after working. Due to the limitation of the quantitative accuracy of adding water, changing the water in the water tank will cause the heat capacity to change, and it is necessary to repeat the water changing calibration within 1 day. Accumulative continuous measurement will also lead to an increasing temperature difference between the inner water tank and the outer water tank of the oxygen bomb calorimeter, which is out of working condition and cannot operate continuously. The hydrophilic nature of the surface of the oxygen bomb also causes the water volume in the water tank in the calorimeter to drop when the oxygen bomb is replaced, resulting in inaccurate measurement.

在本公开一些具体的示例中,水循环过程使第二储液箱8b和第一储液箱3b之间的温差缩小以确保工况要求,主动制冷确保每次分析起始温度控制在±1℃范围内。例如,可以在第一储液箱3b内、第二储液箱8b内和环境中各有一个温度探头用于确认工况。由于搅拌桨5b的转轴和第一储液箱3b无法做到严格密封(密封后,密封垫和转轴摩擦生热,产热功率不恒定,无法准确计量造成误差),第一储液箱3b中的液体会随着蒸发而损失,造成计量值偏高。In some specific examples of the present disclosure, the water circulation process reduces the temperature difference between the second liquid storage tank 8b and the first liquid storage tank 3b to ensure the working conditions, and active refrigeration ensures that the initial temperature of each analysis is controlled within ±1°C within range. For example, there may be a temperature probe in the first liquid storage tank 3b, in the second liquid storage tank 8b and in the environment for confirming the working conditions. Since the rotating shaft of the stirring paddle 5b and the first liquid storage tank 3b cannot be strictly sealed (after sealing, the sealing pad and the rotating shaft generate heat due to friction, the heat production power is not constant, and errors cannot be accurately measured), the first liquid storage tank 3b The liquid will be lost with evaporation, resulting in high metered value.

在第一储液箱3b温度升高后(非分析状态),触发维护进程。在维护进程中会监测环境温度、第一储液箱3b温度、第二储液箱8b温度,启动半导体制冷和循环水泵将整体温度下降至环境温度附近,偏差在2度以内。再关闭半导体制冷,继续循环至第二储液箱8b和第一储液箱3b之间的温差不大于1度。在循环泵6b启动时,第一储液箱3b内的水位由水位检测器反馈,不足的部分由蠕动泵从底部蓄液箱抽取液体补齐,确保每次分析的换热液体量相等。底部蓄液箱中也有一个水位传感器,确保有液体可补。循环泵6b的抽水管61b的抽水端接近于第一盛液部31b的底端。After the temperature of the first liquid storage tank 3b rises (non-analysis state), the maintenance process is triggered. During the maintenance process, the ambient temperature, the temperature of the first liquid storage tank 3b, and the temperature of the second liquid storage tank 8b will be monitored, and the semiconductor refrigeration and circulating water pump will be started to reduce the overall temperature to around the ambient temperature, with a deviation within 2 degrees. Turn off the semiconductor refrigeration again, and continue to circulate until the temperature difference between the second liquid storage tank 8b and the first liquid storage tank 3b is not greater than 1 degree. When the circulation pump 6b is started, the water level in the first liquid storage tank 3b is fed back by the water level detector, and the insufficient part is made up by the liquid drawn from the bottom liquid storage tank by the peristaltic pump to ensure that the amount of heat exchange liquid analyzed each time is equal. There is also a water level sensor in the bottom reservoir to ensure there is fluid to replenish. The suction end of the water suction pipe 61b of the circulation pump 6b is close to the bottom end of the first liquid containing part 31b.

在一些示例中,热量检测设备100b还可以包括有独立的寿命测算代码,统计搅拌桨5b、循环泵6b等易损耗元件的寿命,并在其寿命临近预期结束时进行提醒更换。In some examples, the heat detection device 100b may also include an independent life measurement code to count the life of consumable components such as the stirring paddle 5b and the circulation pump 6b, and remind them to replace them when their life is approaching the expected end.

根据本公开的一些实施例,如图1和图2所示,第二储液箱8b包括第二盛液部81b和由底部向上凹入第二盛液部81b的第二中空部,第二盛液部81b与制冷模块7b连通,制冷模块7b将制冷后的换热液体输入至第二盛液部81b,第二盛液部81b与第一盛液部31b连通,第一储液箱3b和燃烧装置1b的至少部分设于第二中空部。由此,可以使得燃烧装置1b、第一储液箱3b和第二储液箱8b布局紧凑,从而减小热量检测设备100b的体积。According to some embodiments of the present disclosure, as shown in FIG. 1 and FIG. 2 , the second liquid storage tank 8b includes a second liquid storage part 81b and a second hollow part upwardly recessed from the bottom into the second liquid storage part 81b. The liquid storage part 81b communicates with the refrigeration module 7b, the refrigeration module 7b inputs the refrigerated heat exchange liquid to the second liquid storage part 81b, the second liquid storage part 81b communicates with the first liquid storage part 31b, and the first liquid storage tank 3b And at least part of the combustion device 1b is provided in the second hollow portion. Thus, the layout of the combustion device 1b, the first liquid storage tank 3b and the second liquid storage tank 8b can be made compact, thereby reducing the volume of the heat detection device 100b.

在本公开的一些实施例中,如图1和图2所示,热量检测设备100b还可以包括隔热件9b,隔热件9b设于第二中空部,且位于第一盛液部31b的环形外壁与第二盛液部81b的环形内壁之间。由此,在布局紧凑的前提下,隔热件9b可以隔绝至少部分第一盛液部31b流向第二盛液部81b的热量,减少第一盛液部31b内的热量散失,使得煤样完全燃烧后,温度测量计2b测量到的第一盛液部31b内换热液体的升高温度更接近于煤样的热量指标。In some embodiments of the present disclosure, as shown in FIG. 1 and FIG. 2 , the heat detection device 100b may further include a heat insulating member 9b, which is arranged in the second hollow part and located at the bottom of the first liquid containing part 31b. Between the annular outer wall and the annular inner wall of the second liquid containing portion 81b. Therefore, under the premise of a compact layout, the heat insulating member 9b can isolate at least part of the heat flowing from the first liquid containing part 31b to the second liquid containing part 81b, reducing the heat loss in the first liquid containing part 31b, so that the coal sample is completely After combustion, the elevated temperature of the heat exchange liquid in the first liquid containing part 31b measured by the temperature measuring instrument 2b is closer to the heat index of the coal sample.

根据本公开的一些实施例,如图1和图2所示,热量检测设备100b还可以包括支撑组件10b,第一储液箱3b、第二储液箱8b和燃烧装置1b设于支撑组件10b,支撑组件10b具有进气口10221b,进气口10221b和燃烧腔11b连通,煤样燃烧所需气体通过进气口10221b进入燃烧腔11b。由此,支撑组件10b可以便于第一储液箱3b、第二储液箱8b和燃烧装置1b的设置,进气口10221b可以便于煤样燃烧所需气体进入燃烧腔11b,有利于煤样燃烧。According to some embodiments of the present disclosure, as shown in FIG. 1 and FIG. 2 , the heat detection device 100b may further include a support assembly 10b, and the first liquid storage tank 3b, the second liquid storage tank 8b and the combustion device 1b are arranged on the support assembly 10b. The support assembly 10b has an air inlet 10221b, and the air inlet 10221b communicates with the combustion chamber 11b, and the gas required for coal sample combustion enters the combustion chamber 11b through the air inlet 10221b. Thus, the support assembly 10b can facilitate the setting of the first liquid storage tank 3b, the second liquid storage tank 8b and the combustion device 1b, and the air inlet 10221b can facilitate the gas required for coal sample combustion to enter the combustion chamber 11b, which is beneficial to the coal sample combustion .

根据本公开的一些实施例,如图1和图2所示,支撑组件10b包括支架101b和支撑座102b,支撑座102b设于支架101b,支撑座102b包括第一支撑部1021b和第二支撑部1022b,第二支撑部1022b的支撑面高于第一支撑部1021b的支撑面,第二储液箱8b和第一储液箱3b设于第一支撑部1021b,第二支撑部1022b的部分伸入第二中空部,且第二支撑部1022b的支撑面与第一储液箱3b的底部平齐,燃烧装置1b的底部设于第二支撑部1022b的支撑面上,燃烧装置1b的底部具有贯通口,贯通口与第二支撑部1022b的进气口10221b连通。可以理解的是,第二支撑部1022b的部分伸入第二中空部,且第二支撑部1022b的支撑面与第一储液箱3b的底部平齐,可以使得燃烧腔11b完全被第一储液箱3b包围,可以减少热量流失到第一储液箱3b以外的地方,使得对热量指标的测量更准确。According to some embodiments of the present disclosure, as shown in FIG. 1 and FIG. 2 , the support assembly 10b includes a bracket 101b and a support base 102b, the support base 102b is arranged on the bracket 101b, and the support base 102b includes a first support portion 1021b and a second support portion 1022b, the supporting surface of the second supporting part 1022b is higher than the supporting surface of the first supporting part 1021b, the second liquid storage tank 8b and the first liquid storage tank 3b are arranged on the first supporting part 1021b, and part of the second supporting part 1022b extends into the second hollow part, and the supporting surface of the second supporting part 1022b is flush with the bottom of the first liquid storage tank 3b, the bottom of the burning device 1b is arranged on the supporting surface of the second supporting part 1022b, and the bottom of the burning device 1b has The through opening communicates with the air inlet 10221b of the second support portion 1022b. It can be understood that part of the second support part 1022b extends into the second hollow part, and the support surface of the second support part 1022b is flush with the bottom of the first liquid storage tank 3b, so that the combustion chamber 11b can be completely covered by the first storage tank 3b. Surrounded by the liquid tank 3b, the loss of heat to places other than the first liquid storage tank 3b can be reduced, making the measurement of the heat index more accurate.

根据本公开的一些实施例,如图2所示,热量检测设备100b还可以包括弹性件30b、托盘40b、防尘罩50b和激光管60b。弹性件30b设于第二支撑部1022b;托盘40b设于弹性件30b,承载煤样的坩埚100d适于放置在托盘40b内;当将防尘罩50b罩设于坩埚100d时,弹性件30b处于压缩状态;激光管60b的一端设于坩埚100d且与煤样正对,激光管60b的另一端穿过防尘罩50b与照射口正对。由此,通过弹性件30b处于压缩状态时传递给坩埚100d的力使得坩埚100d可以与防尘罩50b很好地贴合,从而加强防尘罩50b的防尘效果。激光管60b可以将引燃激光器20b照射的激光光束引至煤样,使得在设置防尘罩50b防尘的同时不妨碍引燃激光器20b点燃煤样。According to some embodiments of the present disclosure, as shown in FIG. 2 , the heat detection device 100b may further include an elastic member 30b, a tray 40b, a dust cover 50b and a laser tube 60b. The elastic member 30b is arranged on the second supporting part 1022b; the tray 40b is arranged on the elastic member 30b, and the crucible 100d carrying the coal sample is suitable for being placed in the tray 40b; when the dustproof cover 50b is set on the crucible 100d, the elastic member 30b is in Compressed state: one end of the laser tube 60b is set on the crucible 100d and faces the coal sample, and the other end of the laser tube 60b passes through the dust cover 50b and faces the irradiation port. Thus, the force transmitted to the crucible 100d when the elastic member 30b is in a compressed state enables the crucible 100d to fit well with the dustproof cover 50b, thereby enhancing the dustproof effect of the dustproof cover 50b. The laser tube 60b can guide the laser beam irradiated by the ignition laser 20b to the coal sample, so that the dustproof cover 50b is set to prevent dust while not hindering the ignition of the coal sample by the ignition laser 20b.

根据本公开的一些实施例,如图1所示,热量检测设备100b还包括驱动件70b和传动件80b,传动件80b的一端与驱动件70b连接,传动件80b的另一端与第二储液箱8b连接,驱动件70b适于驱动传动件80b带动第二储液箱8b以及设于第二中空部内的第一储液箱3b和燃烧装置1b与支撑座102b分离和连接。According to some embodiments of the present disclosure, as shown in FIG. 1 , the heat detection device 100b further includes a driving member 70b and a transmission member 80b, one end of the transmission member 80b is connected to the driving member 70b, and the other end of the transmission member 80b is connected to the second liquid storage The tank 8b is connected, and the driving member 70b is adapted to drive the transmission member 80b to separate and connect the second liquid storage tank 8b and the first liquid storage tank 3b and the combustion device 1b disposed in the second hollow portion to the support seat 102b.

由此,当第二储液箱8b以及设于第二中空部内的第一储液箱3b和燃烧装置1b与支撑座102b分离时,可以便于将承载煤样的坩埚100d放置在托盘40b上,也可以便于将实验完成的坩埚100d从托盘40b上取走;当第二储液箱8b以及设于第二中空部内的第一储液箱3b和燃烧装置1b与支撑座102b连接时,可以保证实验环境,使得承载煤样的坩埚100d在燃烧腔11b内利完成实验。驱动件70b和传动件g0b可以便于实现第二储液箱8b以及设于第二中空部内的第一储液箱3b和燃烧装置1b与支撑座102b分离和连接。Thus, when the second liquid storage tank 8b, the first liquid storage tank 3b and the combustion device 1b disposed in the second hollow part are separated from the support base 102b, it is convenient to place the crucible 100d carrying the coal sample on the tray 40b, It is also convenient to take away the crucible 100d completed by the experiment from the tray 40b; when the second liquid storage tank 8b and the first liquid storage tank 3b and the combustion device 1b located in the second hollow part are connected with the support seat 102b, it can be ensured The experimental environment makes the crucible 100d carrying the coal sample complete the experiment in the combustion chamber 11b. The driving member 70b and the transmission member g0b can facilitate the separation and connection of the second liquid storage tank 8b, the first liquid storage tank 3b and the combustion device 1b disposed in the second hollow portion, and the support seat 102b.

根据本公开的一些实施例,如图2和图3所示,热量检测设备100b还包括玻璃盖板90b和探测器110b。玻璃盖板90b倾斜设于照射口以封堵照射口,引燃激光器20b发射的激光透过玻璃盖板90b照射于煤样;探测器110b与玻璃盖板90b水平,且与玻璃盖板90b的照射面相对设置。需要说明的是,为确保每次热量检测设备100b中煤样的引燃能量可计量,于是在照射口设置一块倾斜的玻璃盖板90b,例如玻璃盖板90b可以倾斜45°,45°仅为举例说明,并不能理解为对本公开的限制,引燃激光器20b照射的激光穿过与水平面呈45°角的玻璃盖板90b到达煤样表面将煤样引燃。激光在穿过玻璃盖板90b和空气的界面时,发生部分反射,其反射光的强度与透射强度成正比。此时使用的探测器110b例如可以为光电探测器,将反射光的功率统计并按时间进行积分,换算后可得到整个分析过程中激光引入的非燃烧热量,在最终热量计算中可精确扣除。According to some embodiments of the present disclosure, as shown in FIGS. 2 and 3 , the heat detection device 100b further includes a glass cover 90b and a detector 110b. The glass cover plate 90b is obliquely arranged at the irradiation port to block the irradiation port, and the laser light emitted by the ignition laser 20b is irradiated on the coal sample through the glass cover plate 90b; the detector 110b is horizontal to the glass cover plate 90b, and The irradiated surfaces are set opposite to each other. It should be noted that, in order to ensure that the ignition energy of the coal sample in the heat detection device 100b can be measured each time, an inclined glass cover plate 90b is arranged at the irradiation port. For example, the glass cover plate 90b can be inclined at 45°, which is only As an example, which should not be construed as a limitation to the present disclosure, the laser irradiated by the ignition laser 20b passes through the glass cover plate 90b at an angle of 45° to the horizontal plane and reaches the surface of the coal sample to ignite the coal sample. When the laser light passes through the interface between the glass cover plate 90b and the air, it is partially reflected, and the intensity of the reflected light is proportional to the transmitted intensity. The detector 110b used at this time may be, for example, a photodetector. The power of the reflected light is counted and integrated over time. After conversion, the non-combustion heat introduced by the laser during the entire analysis process can be obtained, which can be accurately deducted in the final heat calculation.

本公开能够避免引燃激光器20b光衰和环境温度变化造成的输出能量不一致的情况,在热量检测设备100b稳定时可避免反复校准,有利于自动化实现。玻璃盖板90b的作用除了反射部分激光用于能量检测外,还可保护引燃激光器20b透镜组免于煤烟吸附。其中,玻璃盖板90b的反射率可通过镀膜进行调整。在使用非镀膜玻璃时,其反射率可达10%左右。此时使用5W的激光,反射功率可达500mW左右。The present disclosure can avoid the inconsistency of the output energy caused by the light decay of the ignition laser 20b and the change of the ambient temperature, and can avoid repeated calibration when the heat detection device 100b is stable, which is beneficial to automatic realization. The function of the glass cover plate 90b is not only to reflect part of the laser light for energy detection, but also to protect the lens group of the ignition laser 20b from soot adsorption. Wherein, the reflectivity of the glass cover plate 90b can be adjusted by coating. When using non-coated glass, its reflectivity can reach about 10%. At this time, using a 5W laser, the reflected power can reach about 500mW.

在一些具体的实施例中,探测器110b与控制模块140b通讯连接,探测器110b将煤样的引燃能量信号传输至控制模块140b,控制模块140b在计算煤样热量时可以将煤样的引燃能量扣除,由此,进一步提高了本公开的热量检测设备100b的自动化程度。In some specific embodiments, the detector 110b communicates with the control module 140b, the detector 110b transmits the ignition energy signal of the coal sample to the control module 140b, and the control module 140b can calculate the coal sample's ignition energy signal The combustion energy is deducted, thereby further improving the degree of automation of the heat detection device 100b of the present disclosure.

根据本公开的一些实施例,如图3所示,在玻璃盖板90b与探测器110b之间设有衰减器120b和带有小孔的挡板130b,玻璃盖板90b、衰减器120b、挡板130b和探测器110b依次设置。由于高灵敏度探测器110b工作在非线性范围时,不利于能量精确统计。此时通过在玻璃盖板90b与探测器110b之间设置衰减器120b和带有小孔的挡板130b,可以使得探测器110b对反射光的功率统计更准确,进而更准确的计算出激光引入的非燃烧热量,从而使得热量检测设备100b对煤样的热量测量更准确。例如,衰减器120b可使用中性灰玻璃、偏振镜、凹透镜和小孔,在整个光学腔室内,所有内壁需发黑并进行哑光处理,尽量避免反射造成统计误差。According to some embodiments of the present disclosure, as shown in FIG. 3 , an attenuator 120b and a baffle 130b with a small hole are provided between the glass cover 90b and the detector 110b, the glass cover 90b, the attenuator 120b, the baffle The plate 130b and the detector 110b are arranged in sequence. Since the high-sensitivity detector 110b works in a nonlinear range, it is not conducive to accurate energy statistics. At this time, by setting the attenuator 120b and the baffle plate 130b with a small hole between the glass cover plate 90b and the detector 110b, the power statistics of the reflected light by the detector 110b can be made more accurate, and then the laser input can be calculated more accurately. non-combustion heat, so that the heat detection device 100b can measure the heat of the coal sample more accurately. For example, the attenuator 120b can use neutral gray glass, polarizers, concave lenses and small holes. In the entire optical cavity, all inner walls need to be blackened and matte treated to avoid statistical errors caused by reflection as much as possible.

根据本公开的一些实施例,如图3所示,带有小孔的挡板130b为间隔开的多个。由此,可以进一步使得探测器110b对反射光的功率统计更准确。According to some embodiments of the present disclosure, as shown in FIG. 3 , there are a plurality of baffles 130b with small holes spaced apart. Thereby, the power statistics of the reflected light by the detector 110b can be further made more accurate.

如图4所示,根据本公开实施例的煤质分析系统1000,包括M个加热炉100a、热量检测设备100b和载物架100e。As shown in FIG. 4 , a coal quality analysis system 1000 according to an embodiment of the present disclosure includes M heating furnaces 100a, heat detection equipment 100b and a carrier 100e.

其中,热量检测设备100b为根据如上所述的热量检测设备100b。每个加热炉100a用于测定至少一个煤质指标,M为大于等于1的整数,可以理解的是,煤质指标可以包括但不限于水分、灰分、挥发分和硫等。这里M可以为1,一个加热炉100a可以用于测定水分、灰分、挥发分和硫中的任意一个,或者一个加热炉100a可以用于同时测定水分和挥发分,或者一个加热炉100a可以用于同时测定灰分和硫;这里M也可以为2,两个加热炉100a可以用于测定水分、灰分、挥发分和硫中的任意两个,或者一个加热炉100a用于同时测定水分和挥发分,另一个加热炉100a用于同时测定灰分和硫;这里M还可以为3,三个加热炉100a可以分别用于测定水分、灰分、挥发分和硫中的任意三个;当然M还可以为4、5或者6等等,这里仅以举例说明,并不能理解为对本公开的限制。下面以M为2,一个加热炉100a用于同时测定水分和挥发分,另一个加热炉100a用于同时测定灰分和硫进行举例说明。Wherein, the heat detection device 100b is the heat detection device 100b as described above. Each heating furnace 100a is used to measure at least one coal quality index, and M is an integer greater than or equal to 1. It can be understood that the coal quality index may include but not limited to moisture, ash, volatile matter and sulfur. Here M can be 1, and one heating furnace 100a can be used for determining any one of moisture, ash, volatile matter and sulfur, or one heating furnace 100a can be used for simultaneously measuring moisture and volatile matter, or one heating furnace 100a can be used for Simultaneous determination of ash content and sulfur; here M also can be 2, two heating furnaces 100a can be used for measuring any two in moisture, ash content, volatile matter and sulfur, or one heating furnace 100a is used for measuring moisture and volatile matter simultaneously, Another heating furnace 100a is used to measure ash and sulfur at the same time; here M can also be 3, and three heating furnaces 100a can be used to measure any three in moisture, ash, volatile matter and sulfur respectively; Certainly M can also be 4 , 5 or 6, etc., are used here for illustration only, and should not be construed as limiting the present disclosure. In the following, M is 2, and one heating furnace 100a is used for simultaneous determination of moisture and volatile matter, and the other heating furnace 100a is used for simultaneous determination of ash content and sulfur for illustration.

测定水分的原理为:称取一定量的一般分析实验煤样,于加热炉内,在105℃~110℃下于空气或氮气流中干燥到质量恒定,根据煤样的质量损失计算煤样的水分质量分数。The principle of moisture determination is as follows: Weigh a certain amount of coal sample for general analysis experiment, dry it in the air or nitrogen flow in the heating furnace at 105 ° C ~ 110 ° C until the quality is constant, and calculate the coal sample weight according to the mass loss of the coal sample. Moisture mass fraction.

测定挥发分的原理为:称取一定量的一般分析实验煤样,于加热炉内,在(900±10)℃下隔绝空气加热7min,以减少的质量占煤样质量的质量分数,减去该煤样的水分质量分数作为煤样的挥发分质量分数。The principle of determining volatile matter is as follows: Weigh a certain amount of coal sample for general analysis experiment, heat it in a heating furnace at (900±10)°C for 7 minutes without air, and subtract the mass fraction of the coal sample mass from the reduced mass The moisture mass fraction of the coal sample is used as the volatile mass fraction of the coal sample.

在一些具体的示例中,每个加热炉100a包括炉体、加热装置、质量测定装置和控制组件。炉体具有加热腔,加热腔内适于放置承载煤样的坩埚,加热腔开设有通气口,测定对应的煤质指标所需气体通过通气口进入加热腔;加热装置设于加热腔内给煤样加热;质量测定装置的部分伸入加热腔实时测量承载煤样的坩埚的质量并生成质量信号。In some specific examples, each heating furnace 100a includes a furnace body, a heating device, a mass measuring device and a control assembly. The furnace body has a heating chamber, which is suitable for placing a crucible for carrying coal samples. The heating chamber is provided with a vent, and the gas required to measure the corresponding coal quality index enters the heating chamber through the vent; the heating device is set in the heating chamber to feed the coal. The sample is heated; the part of the mass measuring device extends into the heating chamber to measure the mass of the crucible carrying the coal sample in real time and generate a mass signal.

可以理解的是,当需要加热炉100a测定水分和挥发分时,可以向通气口通入氮气,控制组件与质量测定装置通讯连接,质量测定装置可以测量加热前的承载煤样的坩埚的质量并生成质量信号传输给控制组件,加热装置给煤样加热至105℃~110℃且煤样干燥到质量恒定时,质量测定装置可以测量此时的承载煤样的坩埚的质量并生成质量信号传输给控制组件,控制组件可以通过加热前的承载煤样的坩埚的质量和当前的承载煤样的坩埚的质量计算出质量损失,从而计算煤样的水分质量分数。It can be understood that, when the heating furnace 100a is required to measure moisture and volatile matter, nitrogen gas can be introduced into the air vent, and the control component is communicated with the mass measuring device, which can measure the mass of the crucible carrying the coal sample before heating and Generate a quality signal and transmit it to the control component. When the heating device heats the coal sample to 105°C-110°C and the coal sample is dried to a constant quality, the quality measuring device can measure the mass of the crucible carrying the coal sample at this time and generate a quality signal for transmission to the control unit. The control component can calculate the mass loss according to the mass of the crucible carrying the coal sample before heating and the current mass of the crucible carrying the coal sample, so as to calculate the moisture mass fraction of the coal sample.

加热装置继续给煤样加热至(900±10)℃,加热7min后,质量测定装置可以测量此时的承载煤样的坩埚的质量并生成质量信号传输给控制组件,控制组件可以用减少的质量占煤样质量的质量分数,减去该煤样的水分质量分数作为煤样的挥发分质量分数。The heating device continues to heat the coal sample to (900±10)°C. After heating for 7 minutes, the mass measuring device can measure the mass of the crucible carrying the coal sample at this time and generate a mass signal to transmit to the control component. The control component can use the reduced mass The mass fraction of the coal sample mass is subtracted from the moisture mass fraction of the coal sample as the volatile mass fraction of the coal sample.

加热炉100a对挥发分和硫的测定同理,这里不再赘述。The heating furnace 100a is the same for the determination of volatile matter and sulfur, so it will not be repeated here.

载物架100e包括设备仓1e和电器仓2e,M个加热炉100a和热量检测设备100b设于设备仓1e,控制模块140b设于电器仓2e。由此,可以实现将M个加热炉100a、热量检测设备100b和控制模块140b按功能分区放置,使得M个加热炉100a、热量检测设备100b和控制模块140b的布置整齐且互不干扰。The carrier 100e includes an equipment compartment 1e and an electrical appliance compartment 2e, M heating furnaces 100a and heat detection equipment 100b are located in the equipment compartment 1e, and a control module 140b is located in the electrical appliance compartment 2e. Thus, the M heating furnaces 100a, heat detection devices 100b and control modules 140b can be placed according to functional areas, so that the M heating furnaces 100a, heat detection devices 100b and control modules 140b are neatly arranged without interfering with each other.

根据本公开实施例的煤质分析系统1000,通过集成M个加热炉100a和热量检测设备100b,以及让控制组件对加热炉100a的质量信号进行分析,让控制模块140b对热量检测设备100b的温度信号进行分析,使得一人即可对煤质分析系统1000进行操作,测量完成后的数据自动上传,自动分析即可得到煤质指标和热量指标的综合数据。因此本公开的煤质分析系统1000集成度高便利性好,使用过程中节省人力物力。According to the coal quality analysis system 1000 of the embodiment of the present disclosure, by integrating M heating furnaces 100a and heat detection equipment 100b, and allowing the control component to analyze the quality signal of the heating furnace 100a, let the control module 140b monitor the temperature of the heat detection equipment 100b The signal is analyzed, so that one person can operate the coal quality analysis system 1000, and the data after the measurement is automatically uploaded, and the comprehensive data of the coal quality index and the heat index can be obtained through automatic analysis. Therefore, the coal quality analysis system 1000 of the present disclosure has high integration and good convenience, and saves manpower and material resources during use.

在本公开的描述中,需要理解的是,术语“中心”、“纵向”、“横向”、“长度”、“宽度”、“厚度”、“上”、“下”、“前”、“后”、“左”、“右”、“竖直”、“水平”、“顶”、“底”“内”、“外”、“顺时针”、“逆时针”、“轴向”、“径向”、“周向”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本公开和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本公开的限制。此外,限定有“第一”、“第二”的特征可以明示或者隐含地包括一个或者更多个该特征。在本公开的描述中,除非另有说明,“多个”的含义是两个或两个以上。In describing the present disclosure, it is to be understood that the terms "center", "longitudinal", "transverse", "length", "width", "thickness", "upper", "lower", "front", " Back", "Left", "Right", "Vertical", "Horizontal", "Top", "Bottom", "Inner", "Outer", "Clockwise", "Counterclockwise", "Axial", The orientations or positional relationships indicated by "radial", "circumferential", etc. are based on the orientations or positional relationships shown in the drawings, and are only for the convenience of describing the present disclosure and simplifying the description, rather than indicating or implying the referred devices or elements Must be in a particular orientation, constructed, and operate in a particular orientation, and thus should not be construed as limiting on the present disclosure. In addition, the features defined as "first" and "second" may explicitly or implicitly include one or more of these features. In the description of the present disclosure, unless otherwise specified, "plurality" means two or more.

在本公开的描述中,需要说明的是,除非另有明确的规定和限定,术语“安装”、“相连”、“连接”应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或一体地连接;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通。对于本领域的普通技术人员而言,可以具体情况理解上述术语在本公开中的具体含义。In the description of the present disclosure, it should be noted that unless otherwise specified and limited, the terms "installation", "connection" and "connection" should be understood in a broad sense, for example, it can be a fixed connection or a detachable connection. Connected, or integrally connected; it can be mechanically connected or electrically connected; it can be directly connected or indirectly connected through an intermediary, and it can be the internal communication of two components. Those of ordinary skill in the art can understand the specific meanings of the above terms in the present disclosure in specific situations.

在本说明书的描述中,参考术语“一个实施例”、“一些实施例”、“示意性实施例”、“示例”、“具体示例”、或“一些示例”等的描述意指结合该实施例或示例描述的具体特征、结构、材料或者特点包含于本公开的至少一个实施例或示例中。在本说明书中,对上述术语的示意性表述不一定指的是相同的实施例或示例。而且,描述的具体特征、结构、材料或者特点可以在任何的一个或多个实施例或示例中以合适的方式结合。In the description of this specification, references to the terms "one embodiment," "some embodiments," "exemplary embodiments," "example," "specific examples," or "some examples" are intended to mean that the implementation A specific feature, structure, material, or characteristic described by an embodiment or example is included in at least one embodiment or example of the present disclosure. In this specification, schematic representations of the above terms do not necessarily refer to the same embodiment or example. Furthermore, the specific features, structures, materials or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

尽管已经示出和描述了本公开的实施例,本领域的普通技术人员可以理解:在不脱离本公开的原理和宗旨的情况下可以对这些实施例进行多种变化、修改、替换和变型,本公开的范围由权利要求及其等同物限定。Although the embodiments of the present disclosure have been shown and described, those skilled in the art can understand that various changes, modifications, substitutions and variations can be made to these embodiments without departing from the principle and spirit of the present disclosure. The scope of the present disclosure is defined by the claims and their equivalents.

本领域技术人员可以理解,本公开的各个实施例和/或权利要求中记载的特征可以进行多种组合或/或结合,即使这样的组合或结合没有明确记载于本公开中。特别地,在不脱离本公开精神和教导的情况下,本公开的各个实施例和/或权利要求中记载的特征可以进行多种组合和/或结合。所有这些组合和/或结合均落入本公开的范围。Those skilled in the art can understand that various combinations and/or combinations of the features described in the various embodiments and/or claims of the present disclosure can be made, even if such combinations or combinations are not explicitly recorded in the present disclosure. In particular, without departing from the spirit and teaching of the present disclosure, the various embodiments of the present disclosure and/or the features described in the claims can be combined and/or combined in various ways. All such combinations and/or combinations fall within the scope of the present disclosure.

尽管已经参照本公开的特定示例性实施例示出并描述了本公开,但是本领域技术人员应该理解,在不背离所附权利要求及其等同物限定的本公开的精神和范围的情况下,可以对本公开进行形式和细节上的多种改变。因此,本公开的范围不应该限于上述实施例,而是应该不仅由所附权利要求来进行确定,还由所附权利要求的等同物来进行限定。While the present disclosure has been shown and described with reference to certain exemplary embodiments thereto, it should be understood by those skilled in the art that other modifications may be made without departing from the spirit and scope of the present disclosure as defined by the appended claims and their equivalents. Various changes in form and details have been made to this disclosure. Therefore, the scope of the present disclosure should not be limited to the above-described embodiments, but should be determined not only by the appended claims, but also by the equivalents of the appended claims.

Claims (12)

1. A heat detection apparatus for measuring a heat index of coal, comprising:
the combustion device is provided with a combustion cavity, the combustion cavity is provided with an irradiation port, and a crucible for bearing a coal sample is placed in the combustion cavity;
the ignition laser is arranged above the combustion device and emits laser to the coal sample in the combustion cavity through the irradiation port of the combustion cavity so as to ignite the coal sample;
the temperature measuring meter is used for detecting the temperature of a heat exchange medium exchanging heat with the heat in the combustion cavity and generating a temperature signal;
a control module in communication with the temperature gauge to receive the temperature signal.
2. The heat sensing device of claim 1, further comprising a first tank surrounding the combustion chamber, wherein a heat-exchange liquid is introduced into the first tank, and wherein a probe of the temperature meter is disposed in the first tank to measure the temperature of the heat-exchange liquid in the first tank in real time and generate a temperature signal.
3. The heat detecting apparatus according to claim 2, wherein the first liquid storage tank is an annular liquid storage tank, the first liquid storage tank includes a first liquid containing portion and a first hollow portion, a heat exchange liquid is introduced into the first liquid containing portion, at least a portion of the combustion device is disposed in the first hollow portion,
the heat detection equipment further comprises a heat exchange tube, the heat exchange tube is arranged in the first liquid containing part, one end of the heat exchange tube is communicated with the combustion cavity, and the other end of the heat exchange tube is communicated with the external environment.
4. The heat detecting apparatus according to claim 3, further comprising a paddle rotatably provided in the first liquid containing portion.
5. The heat detecting apparatus according to claim 3, further comprising:
the circulating pump is communicated with the first liquid containing part;
the refrigeration module is communicated with the circulating pump, and the circulating pump pumps the heat exchange liquid in the first liquid containing part to the refrigeration module;
the second liquid storage tank is communicated with the refrigeration module, the refrigeration module inputs the refrigerated heat exchange liquid into the second liquid storage tank, and the second liquid storage tank is communicated with the first liquid containing part so as to flow the heat exchange liquid flowing into the second liquid storage tank into the first liquid containing part.
6. The heat detecting apparatus according to claim 5, wherein the second liquid storage tank includes a second liquid containing portion and a second hollow portion recessed upward from a bottom of the second liquid containing portion, the second liquid containing portion communicates with the refrigerating module, the refrigerating module inputs the heat-exchange liquid after refrigeration to the second liquid containing portion, the second liquid containing portion communicates with the first liquid containing portion, and at least a part of the first liquid storage tank and the combustion device are disposed in the second hollow portion.
7. The heat detecting apparatus according to claim 6, further comprising a heat insulating member provided in the second hollow portion between the annular outer wall of the first liquid containing portion and the annular inner wall of the second liquid containing portion.
8. The heat detecting apparatus according to claim 6, further comprising a support assembly, wherein the first reservoir, the second reservoir and the combustion device are disposed on the support assembly, the support assembly has an air inlet, the air inlet is communicated with the combustion chamber, and a gas required for combustion of the coal sample enters the combustion chamber through the air inlet.
9. The heat sensing device of claim 8, wherein the support assembly comprises:
a support;
the supporting seat, the supporting seat is located the support, the supporting seat includes first supporting part and second supporting part, the holding surface of second supporting part is higher than the holding surface of first supporting part, the second liquid reserve tank with first liquid reserve tank is located first supporting part, the part of second supporting part stretches into well kenozooecium in the second, just the holding surface of second supporting part with the bottom parallel and level of first liquid reserve tank, burner's bottom is located on the holding surface of second supporting part, burner's bottom has the through hole, the through hole with the second supporting part the air inlet intercommunication.
10. The heat detecting apparatus according to claim 9, further comprising:
the elastic piece is arranged on the second supporting part;
the tray is arranged on the elastic piece, and the crucible for bearing the coal sample is suitable for being placed in the tray;
a dust cover, wherein when the dust cover is covered on the crucible, the elastic member is in a compressed state;
and one end of the laser tube is arranged on the crucible and is opposite to the coal sample, and the other end of the laser tube penetrates through the dust cover and is opposite to the irradiation port.
11. The heat detecting apparatus according to claim 9, further comprising a driving member and a driving member, wherein one end of the driving member is connected to the driving member, and the other end of the driving member is connected to the second liquid storage tank, and the driving member is adapted to drive the driving member to drive the second liquid storage tank and the first liquid storage tank and the combustion device disposed in the second hollow portion to be separated from and connected to the supporting base.
12. The heat detecting device according to any one of claims 1 to 11, characterized by further comprising:
the glass cover plate is obliquely arranged on the irradiation port to seal the irradiation port, and laser emitted by the ignition laser penetrates through the glass cover plate to irradiate the coal sample;
and the detector is horizontal to the glass cover plate and is opposite to the irradiation surface of the glass cover plate.
CN202211688289.1A 2022-12-27 2022-12-27 Heat detection equipment Pending CN115901856A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202211688289.1A CN115901856A (en) 2022-12-27 2022-12-27 Heat detection equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202211688289.1A CN115901856A (en) 2022-12-27 2022-12-27 Heat detection equipment

Publications (1)

Publication Number Publication Date
CN115901856A true CN115901856A (en) 2023-04-04

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202211688289.1A Pending CN115901856A (en) 2022-12-27 2022-12-27 Heat detection equipment

Country Status (1)

Country Link
CN (1) CN115901856A (en)

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