CN115890507A - Preparation method of grinding consumable suitable for high-rotation-speed and low-pressure grinding - Google Patents

Preparation method of grinding consumable suitable for high-rotation-speed and low-pressure grinding Download PDF

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CN115890507A
CN115890507A CN202211718867.1A CN202211718867A CN115890507A CN 115890507 A CN115890507 A CN 115890507A CN 202211718867 A CN202211718867 A CN 202211718867A CN 115890507 A CN115890507 A CN 115890507A
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grinding
low
slurry
consumable
pressure
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张瑞敏
董景涛
何晓艳
齐朝辉
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Hebei Siruien New Material Technology Co ltd
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Hebei Siruien New Material Technology Co ltd
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Abstract

The invention provides a preparation method of a grinding consumable suitable for high-rotation-speed and low-pressure grinding, which comprises the following specific steps: step S1:20-30% of thermosetting powder resin, 20-30% of unsaturated monomer, 60-70% of ceramic alumina abrasive, 1-2% of photoinitiator and 1-3% of surfactant are mixed according to a proportion and added into a container; step S2: the slurry with high shear viscosity is formed by high stirring in a dark place, and then the slurry is coated on the base material in a slit type extrusion coating mode; and step S3: contacting with a concave roller with a prismatic table structure, extruding by a compression roller, and shaping and curing under a UV light source; and step S4: the titanium alloy mobile phone middle frame is polished by matching mechanical grinding equipment under the conditions of low pressure, high revolution and low rotation speed, the total removal rate of the middle frame is high, the roughness is low after the middle frame is subjected to a coarse grinding-fine grinding process, and the titanium alloy polishing effect consistency of the polishing consumable material of the frustum pyramid result is good under the conditions of low pressure, high rotation speed and low rotation speed.

Description

Preparation method of grinding consumable suitable for high-rotation-speed and low-pressure grinding
Technical Field
The invention relates to the technical field of grinding consumable material preparation, in particular to a preparation method of a grinding consumable material suitable for high-rotation-speed and low-pressure grinding.
Background
The Pro iPhone adopts a stainless steel middle frame, and although the Pro iPhone has the characteristics of firmness and durability, the weight of the machine body is inevitably increased; the structure of iPhone 14Pro makes a major breakthrough, and the iPhone 14Pro series abandons stainless steel materials, instead adopts titanium alloy materials, the titanium alloy has stronger and durable characteristics, is not easy to bend, has lighter weight than stainless steel, has the defects of higher cost than stainless steel, higher processing difficulty of the titanium alloy, heat conductivity of the titanium alloy of 7.955W/m.K, which is 1/5 of iron and 1/10 of aluminum, so that the titanium alloy is gathered in a grinding area in the grinding process, and the temperature can reach over 1000 ℃, and under the high temperature, the titanium alloy and abrasive are easy to bond, diffuse and have strong chemical reaction, so that the grinding consumables are quickly worn, the integrity of the titanium alloy workpiece is damaged by the high temperature, the geometric precision of the workpiece is reduced, the processing yield is low, and parameters such as the material, hardness, granularity and the like of the grinding consumables are required to be accurately controlled.
In the prior art, mechanical equipment grinding is matched with grinding of the mobile phone middle frame, in order to grind the titanium alloy middle frame, the rotation number is increased to 5000-7000r/min from 1500-2500r/min, the pressure is very low and is approximately 5-10N, the removal rate of the middle frame needs to be 12-13um/min after the coarse grinding and fine grinding process, the roughness needs to reach Ra =0.03um after the fine grinding, and then the required effect can be achieved after 2 times of polishing. Therefore, development of titanium alloy polishing consumables which are matched with mechanical polishing equipment and suitable for high rotating speed and low pressure is urgent.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a preparation method of a grinding consumable material suitable for high-rotating-speed and low-pressure grinding.
In order to realize the purpose, the invention is realized by the following technical scheme: a preparation method of a grinding consumable suitable for high-rotation-speed and low-pressure grinding is specifically as follows:
step S1:20-30% of thermosetting powder resin, 20-30% of unsaturated monomer, 60-70% of ceramic alumina abrasive, 1-2% of photoinitiator and 1-3% of surfactant are mixed according to a proportion and added into a container;
step S2: the slurry with high shear viscosity is formed by high stirring in a dark place, and then the slurry is coated on the base material in a slit type extrusion coating mode;
and step S3: contacting with a concave roller with a prismatic table structure, extruding by a compression roller, and shaping and curing under a UV light source;
and step S4: and (3) further carrying out thermal aging by adding short wave infrared through a drying channel to obtain the prismatic table-shaped grinding consumable.
Further, in the step S1, the thermosetting powder resin is one or a mixture of epoxy powder resin, polyester powder resin, polyacrylic acid powder resin and polyurethane powder resin; the mesh number of the ceramic alumina abrasive is 400# -3000#; the monomer is one or a mixture of lauric acrylate, pentaerythritol triacrylate and tetrahydrofuran acrylate hexanediol diacrylate; the photoinitiator is2, 4, 6-trimethylbenzoyl-diphenyl phosphine oxide; the surfactant is one or more of Dow 15-S-5, 15-S-12 and 15-S-15.
Further, in the step S4, the specific batching process for the 600# grinding consumables is as follows:
a) Firstly, adding 2g (initiator TPO into pentaerythritol triacrylate to be fully dissolved, and then adding 15-S-15 into the initiator TPO to obtain uniform resin liquid;
b) Then, 550g of 600# ceramic alumina abrasive, 100g of 2500# ceramic alumina abrasive and 200g of epoxy resin powder coating are uniformly mixed;
c) Spraying the mixed resin liquid obtained in the step a) on the mixed resin liquid obtained in the step b), stirring while fully wetting and uniformly mixing to obtain high-viscosity slurry, wherein the temperature of the slurry is controlled to be 30-40 ℃ again, and the viscosity is controlled to be 25000-35000Pc.s;
d) And then transferring the slurry onto a polyester film substrate through a slit, extruding the polyester film substrate through a frustum roller, and carrying out setting curing and thermal curing by using a UV light source to obtain the No. 600 grinding consumable.
Further, in the step S4, the specific batching process for the 2500# grinding consumables is as follows:
a) Adding 3g of initiator TPO into pentaerythritol triacrylate to be fully dissolved, and adding 15-S-15 surfactant into the initiator TPO to obtain uniform resin liquid;
b) Then 650g of 2500# ceramic alumina abrasive, 300g of tetrahydrofuran acrylate and 100g of epoxy resin powder coating are uniformly mixed;
c) Spraying the mixed resin liquid obtained in the step a) on the mixed resin liquid obtained in the step b), stirring while fully wetting and uniformly mixing to obtain high-viscosity slurry, controlling the temperature of the slurry to be 30-40 ℃ again, and controlling the viscosity to be 25000-35000Pc.s;
d) And then transferring the slurry onto a polyester film substrate through a slit, extruding the polyester film substrate through a frustum roller, and carrying out shaping curing and thermosetting through a UV light source to obtain a 2500# grinding consumable.
Further, the 600# abrasive consumables are matched with a mechanical grinding device at the pressure F =10N, the rotation r =5500r/min and the time t =60s.
Further, 2500# abrasive consumables are matched with a mechanical grinding device under the conditions that the pressure is F =10N, the revolution r =5500r/min and the time t =60s.
The invention has the beneficial effects that:
1. according to the invention, the titanium alloy mobile phone middle frame is ground under the conditions of low pressure, high revolution and matched mechanical grinding equipment, and the total removal rate of the middle frame is high and the roughness is low after the middle frame is subjected to a coarse grinding-fine grinding process;
2. under the conditions of low pressure and high rotating speed, the grinding consumables of the frustum pyramid result have good titanium alloy grinding effect consistency;
3. according to the invention, by designing a small net wall gap, heat can be removed by chip removal, and heavy grinding marks can not be caused on a workpiece;
4. after the grinding is finished, the service life of a formula system is long and can reach about 30 times;
5. the grinding consumable of the invention is used for grinding the titanium alloy middle frame by matching with mechanical equipment, after CNC, the mechanical equipment matches with the consumable to achieve the required grinding effect through 1500# coarse grinding, 2500# fine grinding, 3000# polishing and 5000# polishing.
Drawings
Other features, objects and advantages of the invention will become more apparent upon reading of the detailed description of non-limiting embodiments with reference to the following drawings:
FIG. 1 is a schematic structural diagram of a mold in a method for preparing a polishing consumable material suitable for high-speed and low-pressure polishing according to the present invention;
FIG. 2 is a schematic diagram showing the change of the polishing area of the coating layer consuming the same height in the polishing consumable for high-speed and low-pressure polishing according to the present invention;
FIG. 3 is a schematic diagram showing the change of the polishing area of the coating layer consuming the same height in the polishing consumable for high-speed and low-pressure polishing according to the present invention;
FIG. 4 is a schematic diagram showing the variation of the polishing area of the coating layer consuming the same height in the polishing consumable for high-speed and low-pressure polishing according to the present invention;
FIG. 5 is a schematic diagram showing the variation of the polishing area of the coating layer consuming the same height in the polishing consumable for high-speed and low-pressure polishing according to the present invention.
FIG. 6 is a schematic diagram of the production of the polishing consumables suitable for high-speed and low-pressure polishing according to the present invention.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further explained by combining the specific embodiments.
In the present invention, referring to fig. 1, a mold with a frustum pyramid structure (as shown in fig. 1) is designed, wherein the length b1 of the bottom edge of the mold is =1.3-1.8mm, the height h is =0.45-0.55mm, the demolding angle α =80-86 °, and the partition wall gap c1=0-0.2mm. The shape breaks through the original pyramid structure (such as 3m patent 5152917), the grinding consumables obtained by the pyramid structure have the disadvantages of high coating consumption speed and high cross-sectional area change under the condition of high rotating speed, so that the pressure intensity change is large, and the effect difference of the ground workpieces is large; the grinding consumables obtained by the prismatic table structure have small difference of cross section area along with the consumption of the coating, the grinding pressure fluctuates in a small range, and the ground middle frame workpiece has good effect consistency.
Example 1: the mechanical equipment sets pressure F =10N, revolution r =5500r/min and time t =60s, and is matched with grinding consumables 1500# grinding sand paper in pyramid shape (shown in a specific figure 2) and frustum shape (shown in a specific figure 3); under the above conditions, the coating consumes h1=0.1mm, fig. 2 is a pyramid shape, fig. 3 is a newly designed frustum shape, and when the module consumes the same height h1, the shaded part in fig. 4 and fig. 5 is the change of the grinding area of the grinding block, the coating with the same thickness is consumed, and the change of the contact area and the pressure intensity, and the specific change data are shown in the following table:
Figure DEST_PATH_IMAGE001
from the above table, it can be seen that when the coating consumes the same height h1, the pressure intensity of the grinding consumables of the pyramid is changed greatly, and the grinding consumables of the frustum structure are not changed greatly, so the mold for designing and developing the frustum structure is designed.
2) The grinding consumable for grinding the titanium alloy is obtained by matching with the frustum structure and designing a proper formula system
Referring to fig. 6, a method for preparing a grinding consumable suitable for high-speed and low-pressure grinding includes the following specific steps:
step S1:20-30% of thermosetting powder resin, 20-30% of unsaturated monomer, 60-70% of ceramic alumina abrasive, 1-2% of photoinitiator and 1-3% of surfactant are mixed according to a proportion and added into a container;
step S2: the slurry with high shear viscosity is formed by high stirring in a dark place, and then the slurry is coated on the base material in a slit type extrusion coating mode;
and step S3: contacting with a concave roller with a prismatic table structure, extruding by a press roller, and shaping and curing under a UV light source;
and step S4: and further carrying out thermal aging by a drying channel and short wave infrared to obtain the prismatic table-shaped grinding consumable.
The thermosetting powder resin is one or a mixture of epoxy powder resin, polyester powder resin, polyacrylic acid powder resin and polyurethane powder resin; the mesh number of the ceramic alumina abrasive is 400# -3000#; the monomer is one or a mixture of lauric acrylate, pentaerythritol triacrylate and tetrahydrofuran acrylate hexanediol diacrylate; the photoinitiator is2, 4, 6-trimethylbenzoyl-diphenyl phosphine oxide; the surfactant is one or more of Dow 15-S-5, 15-S-12 and 15-S-15.
In the present invention, example 2:
epoxy resin powder coating: 200g (Di Si Man's Uralac P3170)
Pentaerythritol triacrylate (PETA): 200g (Saedoma)
Abrasive material of ceramic alumina # 600: 550g (Jiangsu Ruiker JIS600 #)
2500# ceramic alumina abrasive 100g (Jiangsu Ruike' er JIS2500 #)
Initiator TPO: 2g (Basff)
Surfactant 15-S-15 12g (Dow chemical)
The specific batching process for the 600# grinding consumable material is as follows:
a) Firstly, adding 2g (initiator TPO into pentaerythritol triacrylate to be fully dissolved, and then adding 15-S-15 into the initiator TPO to obtain uniform resin liquid;
b) Then, 550g of No. 600 ceramic alumina abrasive, 100g of No. 2500 ceramic alumina abrasive and 200g of epoxy resin powder coating are uniformly mixed;
c) Spraying the mixed resin liquid obtained in the step a) on the mixed resin liquid obtained in the step b), stirring while fully wetting and uniformly mixing to obtain high-viscosity slurry, controlling the temperature of the slurry to be 30-40 ℃ again, and controlling the viscosity to be 25000-35000Pc.s;
d) Transferring the slurry onto a polyester film substrate through a slit, extruding the polyester film substrate through a prismoid roller, and carrying out shaping curing and thermosetting through a UV light source to obtain a 600# grinding consumable;
example 3: dosing Process dosing and implementation according to example 2
Epoxy resin powder coating 100g (Uralac P3170 of Disman)
Tetrahydrofuran acrylate (THFA): 300g (sartomer)
2500# ceramic alumina abrasive 650g (Jiangsu Ruiker JIS2500 #)
Initiator TPO 3g (Basff)
Surfactant 15-S-15: 18g (Dow chemical)
The specific batching process for the 2500# grinding consumable material is as follows:
a) Adding 3g of initiator TPO into pentaerythritol triacrylate to be fully dissolved, and adding 15-S-15 surfactant into the initiator TPO to obtain uniform resin liquid;
b) Then, 650g of 2500# ceramic alumina abrasive, 300g of tetrahydrofuran acrylate and 100g of epoxy resin powder coating are uniformly mixed;
c) Spraying the mixed resin liquid obtained in the step a) on the mixed resin liquid obtained in the step b), stirring while fully wetting and uniformly mixing to obtain high-viscosity slurry, controlling the temperature of the slurry to be 30-40 ℃ again, and controlling the viscosity to be 25000-35000Pc.s;
d) And then transferring the slurry onto a polyester film substrate through a slit, extruding the polyester film substrate through a prismoid roller, and carrying out setting curing and thermocuring by using a UV light source to obtain the 2500# grinding consumable.
The 600# and 2500# abrasive consumables obtained in examples 2 and 3 respectively were used in conjunction with a mechanical grinding apparatus at a pressure of F =10N, a rotation number of r =5500r/min, and a time of t =60s, and the grinding effects were as follows:
Figure DEST_PATH_IMAGE002
the requirements for polishing titanium alloys can be met from the test data in the table above.
In the invention, when the abrasive material is prepared, firstly, 20-30% of thermosetting powder resin, 20-30% of unsaturated monomer, 60-70% of ceramic alumina abrasive material, 1-2% of photoinitiator and 1-3% of surfactant are mixed and added into a container according to a proportion; the slurry is protected from light and highly stirred to form slurry with high shear viscosity, and then the slurry is coated on the base material in a slit type extrusion coating mode; then contacting with a concave roller with a prismatic table structure, extruding by a compression roller, and shaping and curing under a UV light source; and finally, further carrying out thermal aging by a drying channel and short wave infrared to obtain the prismatic table-shaped grinding consumable.
The above formulas are all calculated by taking the numerical value of the dimension, the formula is a formula of the latest real situation obtained by collecting a large amount of data and performing software simulation, the preset parameters in the formula are set by the technicians in the field according to the actual situation, if the weight coefficient and the scale coefficient exist, the set size is a specific numerical value obtained by quantizing each parameter, the subsequent comparison is convenient, and as for the size of the weight coefficient and the scale coefficient, the proportional relation between the parameter and the quantized numerical value is not influenced.
In the above embodiments of the present application, the descriptions of the respective embodiments have respective emphasis, and for parts that are not described in detail in a certain embodiment, reference may be made to related descriptions of other embodiments.
As will be appreciated by one skilled in the art, embodiments of the present invention may be provided as a method, system, or computer program product. Accordingly, the present invention may take the form of an entirely hardware embodiment, an entirely software embodiment or an embodiment combining software and hardware aspects. Furthermore, the present invention may take the form of a computer program product embodied on one or more computer-usable storage media having computer-usable program code embodied in the medium.
Although the present invention has been described in detail with reference to the foregoing embodiments, it should be understood by those skilled in the art that the following descriptions are only illustrative and not restrictive, and that the scope of the present invention is not limited to the above embodiments: any person skilled in the art can modify or easily conceive the technical solutions described in the foregoing embodiments or equivalent substitutes for some technical features within the technical scope of the present disclosure; such modifications, changes or substitutions do not depart from the spirit and scope of the embodiments of the present invention, and they should be construed as being included therein. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.

Claims (6)

1. The preparation method of the grinding consumable suitable for high-rotation-speed and low-pressure grinding is characterized in that the preparation method comprises the following specific steps:
step S1:20-30% of thermosetting powder resin, 20-30% of unsaturated monomer, 60-70% of ceramic alumina abrasive, 1-2% of photoinitiator and 1-3% of surfactant are mixed and added into a container according to a proportion;
step S2: the slurry is protected from light and highly stirred to form slurry with high shear viscosity, and then the slurry is coated on the base material in a slit type extrusion coating mode;
and step S3: contacting with a concave roller with a prismatic table structure, extruding by a press roller, and shaping and curing under a UV light source;
and step S4: and further carrying out thermal aging by a drying channel and short wave infrared to obtain the prismatic table-shaped grinding consumable.
2. The preparation method of the grinding consumable material suitable for high-rotation-speed and low-pressure grinding according to claim 1, wherein in the step S1, the thermosetting powder resin is one or a mixture of epoxy powder resin, polyester powder resin, polyacrylic acid powder resin and polyurethane powder resin; the mesh number of the ceramic alumina abrasive is 400# -3000#; the monomer is one or a mixture of lauric acrylate, pentaerythritol triacrylate and tetrahydrofuran acrylate hexanediol diacrylate; the photoinitiator is2, 4, 6-trimethylbenzoyl-diphenyl phosphine oxide; the surfactant is one or more of Dow 15-S-5, 15-S-12 and 15-S-15.
3. The method for preparing a grinding consumable material suitable for high-speed and low-pressure grinding according to claim 2, wherein in the step S4, the specific material preparation process for the No. 600 grinding consumable material is as follows:
a) Firstly, adding 2g (initiator TPO into pentaerythritol triacrylate to fully dissolve, and then adding 15-S-15 into the initiator TPO to obtain uniform resin liquid;
b) Then, 550g of No. 600 ceramic alumina abrasive, 100g of No. 2500 ceramic alumina abrasive and 200g of epoxy resin powder coating are uniformly mixed;
c) Spraying the mixed resin liquid obtained in the step a) on the mixed resin liquid obtained in the step b), stirring while fully wetting and uniformly mixing to obtain high-viscosity slurry, controlling the temperature of the slurry to be 30-40 ℃ again, and controlling the viscosity to be 25000-35000Pc.s;
d) And then transferring the slurry onto a polyester film substrate through a slit, extruding the polyester film substrate through a frustum roller, and carrying out setting curing and thermal curing by using a UV light source to obtain the No. 600 grinding consumable.
4. The method for preparing a grinding consumable material suitable for high-speed and low-pressure grinding according to claim 3, wherein in the step S4, the specific blending process for the 2500# grinding consumable material is as follows:
a) Adding 3g of initiator TPO into pentaerythritol triacrylate to be fully dissolved, and adding 15-S-15 surfactant into the initiator TPO to obtain uniform resin liquid;
b) Then, 650g of 2500# ceramic alumina abrasive, 300g of tetrahydrofuran acrylate and 100g of epoxy resin powder coating are uniformly mixed;
c) Spraying the mixed resin liquid obtained in the step a) on the mixed resin liquid obtained in the step b), stirring while fully wetting and uniformly mixing to obtain high-viscosity slurry, wherein the temperature of the slurry is controlled to be 30-40 ℃ again, and the viscosity is controlled to be 25000-35000Pc.s;
d) And then transferring the slurry onto a polyester film substrate through a slit, extruding the polyester film substrate through a prismoid roller, and carrying out setting curing and thermocuring by using a UV light source to obtain the 2500# grinding consumable.
5. The method for preparing a grinding consumable material suitable for high-rotation-speed and low-pressure grinding according to claim 3, wherein the 600# grinding consumable material is matched with a mechanical grinding device under the conditions of pressure F =10N, r =5500r/min and time t =60s.
6. The method for preparing a grinding consumable suitable for high-speed and low-pressure grinding according to claim 4, wherein the 2500# grinding consumable is matched with a mechanical grinding device under the conditions of pressure F =10N, r =5500r/min and time t =60s.
CN202211718867.1A 2022-12-30 2022-12-30 Preparation method of grinding consumable suitable for high-rotation-speed and low-pressure grinding Pending CN115890507A (en)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020019199A1 (en) * 1999-04-23 2002-02-14 3M Innovative Properties Company Abrasive article suitable for abrading glass and glass ceramic workpieces
US20050060947A1 (en) * 2003-09-23 2005-03-24 3M Innovative Properties Company Compositions for abrasive articles
CN102123830A (en) * 2008-07-24 2011-07-13 3M创新有限公司 Abrasive material product, its production method and use method
CN104552043A (en) * 2014-12-17 2015-04-29 衢州学院 Manufacturing method for trapezoid microflute polishing thin film
CN105856089A (en) * 2016-06-01 2016-08-17 东莞市中微纳米科技有限公司 Grinding composite body and preparation method thereof
JP6317842B1 (en) * 2016-12-07 2018-04-25 マイクロ ケミカル コリア カンパニー リミテッド Polishing pad and manufacturing method thereof
CN108481217A (en) * 2018-03-26 2018-09-04 河北思瑞恩新材料科技有限公司 A kind of pyramid type solid grinding tool and preparation method for metallic mobile phone center of polishing

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020019199A1 (en) * 1999-04-23 2002-02-14 3M Innovative Properties Company Abrasive article suitable for abrading glass and glass ceramic workpieces
CN1348404A (en) * 1999-04-23 2002-05-08 3M创新有限公司 Abrasive article suitable for abrading glass and glass ceramic workpieces
US20050060947A1 (en) * 2003-09-23 2005-03-24 3M Innovative Properties Company Compositions for abrasive articles
CN102123830A (en) * 2008-07-24 2011-07-13 3M创新有限公司 Abrasive material product, its production method and use method
CN104552043A (en) * 2014-12-17 2015-04-29 衢州学院 Manufacturing method for trapezoid microflute polishing thin film
CN105856089A (en) * 2016-06-01 2016-08-17 东莞市中微纳米科技有限公司 Grinding composite body and preparation method thereof
JP6317842B1 (en) * 2016-12-07 2018-04-25 マイクロ ケミカル コリア カンパニー リミテッド Polishing pad and manufacturing method thereof
CN108481217A (en) * 2018-03-26 2018-09-04 河北思瑞恩新材料科技有限公司 A kind of pyramid type solid grinding tool and preparation method for metallic mobile phone center of polishing

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Application publication date: 20230404