CN115836695A - Preservation method of semi-finished dishes - Google Patents

Preservation method of semi-finished dishes Download PDF

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CN115836695A
CN115836695A CN202211605277.8A CN202211605277A CN115836695A CN 115836695 A CN115836695 A CN 115836695A CN 202211605277 A CN202211605277 A CN 202211605277A CN 115836695 A CN115836695 A CN 115836695A
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semi
zinc oxide
finished
nano zinc
finished dishes
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郑学斌
仰玲玲
刘艳萍
王池丽
肖瑀
许睿
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Hefei Technology College
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Hefei Technology College
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Abstract

The invention provides a fresh-keeping method of semi-finished dishes, which comprises the following steps: uniformly mixing the preservative emulsion containing the nano zinc oxide with semi-finished dishes, then carrying out low-temperature plasma treatment, and carrying out radio frequency sterilization treatment. The method adopts the method of combining the zinc oxide bactericide, the low-temperature plasma and the radio frequency sterilization for fresh-keeping treatment, not only can greatly prolong the fresh-keeping time of semi-finished dishes, but also can keep good edible quality of the semi-finished dishes after fresh keeping, and is particularly suitable for the fresh-keeping treatment of the semi-finished dishes of meat products.

Description

Preservation method of semi-finished dishes
Technical Field
The invention relates to the technical field of food preservation, in particular to a preservation method of semi-finished dishes.
Background
Semi-finished dish, also called prefabricated dish, is made up by using agricultural products of vegetables, domestic animals, fowls and aquatic products as raw material and adding various auxiliary materials through the processes of cutting, stirring, pickling, rolling, forming and flavouring. The semi-finished dish can be eaten after being simply cooked, so that the time for cooking is greatly saved, and the semi-finished dish is very suitable for fast-paced life style, and has good market potential and economic value.
With the rapid market introduction of semi-finished dishes and the development of related technologies, the quality requirements of people are gradually increased. Among many factors influencing the quality of semi-finished dishes, the sterilization and preservation technology of the semi-finished dishes has great influence on the texture, sensory quality and nutrition of the dishes besides raw materials, preprocessing technology and the like. At present, a high-temperature high-pressure sterilization method is commonly used as a preservation method of semi-finished dishes, although a satisfactory sterilization effect can be achieved and the storage period is prolonged, the method often has adverse effects on the texture and sensory quality of the semi-finished dishes, and the taste of the sterilized dishes is seriously reduced. Therefore, how to make semi-finished dishes have a long shelf life and maintain good sensory quality is an important research topic at present.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a method for preserving semi-finished dishes.
The invention provides a method for preserving semi-finished dishes, which comprises the following steps:
s1, uniformly mixing preservative emulsion containing nano zinc oxide with semi-finished dishes;
s2, placing the semi-finished dishes processed in the S1 into a reaction cavity of a dielectric barrier discharge type low-temperature plasma device, and performing sterilization treatment by adopting low-temperature plasma;
and S3, placing the semi-finished dish processed in the S2 into a radio frequency instrument for radio frequency sterilization treatment.
Preferably, in S1, the preservative emulsion containing nano zinc oxide comprises the following raw materials in percentage by mass: 0.1-0.2% of fatty acid modified nano zinc oxide, 0.3-0.5% of lecithin, 0.05-0.1% of ginger ethanol extract and the balance of water.
Preferably, the preparation method of the fatty acid modified nano zinc oxide comprises the following steps: adding stearic acid and nano zinc oxide into an ethanol solution, performing ultrasonic dispersion uniformly, performing reflux heating reaction, centrifuging, and drying to obtain the zinc oxide nanoparticle.
Preferably, the mass ratio of the stearic acid to the nano zinc oxide is (0.2-0.5): 10; the temperature of the reflux heating reaction is 60-100 ℃, and the time is 1-3h.
Preferably, the preparation method of the ginger ethanol extract comprises the following steps: mixing rhizoma Zingiberis recens dry powder with 60-95% ethanol solution, leaching, filtering, rotary evaporating the filtrate to remove solvent, and oven drying at 50-60 deg.C.
Preferably, the ratio of the ginger dry powder to the ethanol solution is 1g: (10-20) mL; the leaching temperature is 40-60 ℃, and the leaching time is 3-5h.
Preferably, in S1, the preparation method of the preservative emulsion containing nano zinc oxide comprises the following steps: mixing fatty acid modified nanometer zinc oxide, rhizoma Zingiberis recens extract and lecithin, ultrasonically dispersing at 40-50 deg.C, dripping the obtained mixture into water at 40-50 deg.C, and ultrasonically dispersing.
Preferably, in S1, the mass ratio of the preservative emulsion containing nano zinc oxide to semi-finished dishes is (0.03-0.05): 1000.
Preferably, in S2, the discharge power of the sterilization treatment by adopting low-temperature plasma is 200-400W, the treatment time is 1-2min, and the working gas is air.
Preferably, in S3, the distance between the plates subjected to radio frequency sterilization treatment is 140-180mm, and the sterilization time is 10-15min.
Preferably, the semi-finished food is a meat product.
Preferably, the semi-finished dish is western cold beef steak, sauced pork ribs or spicy beef sauce.
The invention has the following beneficial effects:
according to the invention, the method of adding the preservative emulsion containing nano zinc oxide, low-temperature plasma treatment and radio frequency sterilization is combined, wherein the nano zinc oxide is subjected to fatty acid coating treatment and is prepared into the emulsion together with natural antioxidant and lecithin, so that the nano zinc oxide can be well combined with fat in dishes, the antibacterial property and the antioxidant property of the dishes are improved, and the change of flavor in the long-term preservation process is favorably reduced; by adopting the combination of low-temperature plasma treatment and radio frequency sterilization methods and adjusting proper process parameters, the method not only can play a good sterilization effect, but also can reduce the influence on the texture and flavor change of dishes in the sterilization process, so that the dishes have good sensory quality and fresh-keeping effect. The invention can effectively prolong the preservation period of semi-finished dishes, reduce the influence of sterilization treatment on the internal texture and chemical component change of semi-finished dish products in the sterilization treatment and the preservation process and the reduction of edible sensory quality caused by the oxidative deterioration of fat in meat products in the preservation process, can still meet the requirement of food sanitation and safety on the colony number after being refrigerated for 8 months, can keep good flavor, and is particularly suitable for the preservation treatment of the semi-finished dishes of meat products.
Detailed Description
The technical solution of the present invention will be described in detail below with reference to specific examples.
In the following examples and comparative examples:
the preparation method of the ginger ethanol extract comprises the following steps: mixing 10g of ginger dry powder with 150mL of 75% ethanol solution by mass fraction, leaching for 4h at 50 ℃, filtering, performing rotary evaporation on the obtained filtrate to remove the solvent, and drying at 50 ℃ to obtain the ginger extract.
The preparation method of the fatty acid modified nano zinc oxide comprises the following steps: adding 0.04g of stearic acid and 1g of nano zinc oxide into 100mL of ethanol solution, performing ultrasonic dispersion uniformly, performing reflux heating reaction at 70 ℃ for 2h, centrifuging, and drying to obtain the zinc oxide nanoparticle.
Example 1
Frying the western cold beefsteak:
cleaning and slicing beef, uniformly coating a pickling material on the surface of the beef, pickling for 48h at 4 ℃, taking out the beef, standing at room temperature for 15min, and frying the beef on an electric furnace by using butter, wherein the pickling material is prepared from table salt, chilli powder, paprika powder and garlic powder in a mass ratio of 1:3, and (3).
The method for preserving the fried western cold beefsteak comprises the following steps:
s1, uniformly mixing preservative emulsion containing nano zinc oxide with western cold beefsteak according to a mass ratio of 0.04g; the preservative emulsion containing the nano zinc oxide comprises the following raw materials in percentage by mass: 0.15% of fatty acid modified nano zinc oxide, 0.4% of lecithin, 0.08% of ginger ethanol extract and the balance of water, and the preparation method comprises the following steps: mixing fatty acid modified nano zinc oxide, ginger extract and lecithin, performing ultrasonic dispersion at 45 ℃, then dropwise adding the obtained mixture into water at 45 ℃, and performing ultrasonic dispersion uniformly to obtain the product;
s2, placing the western cold steak processed in the S1 into a reaction cavity of a dielectric barrier discharge type low-temperature plasma device, taking air as working gas, and performing sterilization treatment for 1.5min by adopting low-temperature plasma under the condition of discharge power of 300W;
and S3, placing the western cold steak processed in the S2 in a radio frequency instrument, setting the distance between polar plates to be 160mm, carrying out radio frequency sterilization treatment for 12min, and then carrying out vacuum packaging.
Example 2
Decocting secretly made sauce chop:
adding salad oil into a pot, heating with slow fire, adding shallot for quick-frying, adding spareribs, frying to slight yellow, adding sauce prepared from crystal sugar, soybean paste and dark soy sauce, transferring to a marmite, adding garlic, ginger, long green pickled pepper, rod pepper, pickled pepper water, yellow rice wine, white vinegar and chicken powder, and cooking to obtain the pork, garlic, ginger, shallot, crystal sugar, long green pickled pepper, rod pepper, pickled pepper water, soybean paste, salad oil, dark soy sauce, yellow rice wine, white vinegar and chicken powder, wherein the mass ratio of the spareribs, garlic, ginger, shallot, long green pickled pepper, rod pepper, pickled pepper water to the yellow rice wine to the white rice wine to the chicken powder is 50:2:0.9:0.75:2.5:1:0.5:8:6.5:5:0.1:0.5:0.65:0.2.
the method for preserving the secretly-made sauced steak obtained by the decoction comprises the following steps:
s1, uniformly mixing preservative emulsion containing nano zinc oxide and secret sauce steaks according to a mass ratio of 0.05g; the preservative emulsion containing the nano zinc oxide comprises the following raw materials in percentage by mass: 0.2% of fatty acid modified nano zinc oxide, 0.5% of lecithin, 0.1% of ginger ethanol extract and the balance of water, and the preparation method comprises the following steps: mixing fatty acid modified nano zinc oxide, ginger extract and lecithin, performing ultrasonic dispersion at 50 ℃, then dropwise adding the obtained mixture into water at 50 ℃, and performing ultrasonic dispersion uniformly to obtain the product;
s2, arranging the special sauce processed in the S1 in a reaction cavity of a dielectric barrier discharge type low-temperature plasma device, and performing sterilization treatment for 2min by using low-temperature plasma under the condition of discharge power of 400W by taking air as working gas;
and S3, placing the secretly-made sauce steak processed in the step S2 in a radio frequency instrument, setting the distance between polar plates to be 180mm, carrying out radio frequency sterilization treatment for 15min, and then carrying out vacuum packaging.
Example 3
Boiling the spicy beef paste:
cutting beef into granules, pouring soybean oil into a pot, heating with slow fire, frying the beef in the pot, adding garlic seeds, hot pepper and soybean paste, and cooking to obtain the beef, garlic seeds, hot pepper, soybean oil and soybean paste, wherein the mass ratio of the beef, garlic seeds, hot pepper, soybean oil and soybean paste is 70.
The method for preserving the cooked spicy beef paste comprises the following steps:
s1, uniformly mixing preservative emulsion containing nano zinc oxide and 1kg of spicy beef paste according to the mass ratio of 0.03g; the preservative emulsion containing the nano zinc oxide comprises the following raw materials in percentage by mass: 0.1% of fatty acid modified nano zinc oxide, 0.3% of lecithin, 0.05% of ginger ethanol extract and the balance of water, and the preparation method comprises the following steps: mixing fatty acid modified nano zinc oxide, ginger extract and lecithin, performing ultrasonic dispersion at 40 ℃, then dropwise adding the obtained mixture into water at 40 ℃, and performing ultrasonic dispersion uniformly to obtain the product;
s2, placing the spicy beef paste processed in the S1 into a reaction cavity of a dielectric barrier discharge type low-temperature plasma device, and performing sterilization treatment for 1min by using low-temperature plasma under the condition of discharge power of 200W by taking air as working gas;
and S3, placing the spicy beef paste processed in the step S2 in a radio frequency instrument, setting the distance between polar plates to be 140mm, carrying out radio frequency sterilization treatment for 10min, and then carrying out vacuum packaging.
Comparative example 1
The method for preserving the fried western cold beefsteak comprises the following steps:
s1, uniformly mixing a water dispersion of nano zinc oxide with a solid content of 0.15% with 1kg of western cold beefsteak according to a mass ratio of 0.04g;
s2, placing the western cold steak processed in the S1 into a reaction cavity of a dielectric barrier discharge type low-temperature plasma device, taking air as working gas, and performing sterilization treatment for 1.5min by adopting low-temperature plasma under the condition of discharge power of 300W;
and S3, placing the western cold steak processed in the S2 in a radio frequency instrument, setting the distance between polar plates to be 160mm, carrying out radio frequency sterilization treatment for 12min, and then carrying out vacuum packaging.
The frying method of Xiliang beefsteak is the same as that of example 1.
Comparative example 2
The method for preserving the fried western cold beefsteak comprises the following steps:
s1, uniformly mixing preservative emulsion containing nano zinc oxide with western cold beefsteak according to a mass ratio of 0.04g; the preservative emulsion containing the nano zinc oxide comprises the following raw materials in percentage by mass: 0.15% of fatty acid modified nano zinc oxide, 0.4% of lecithin, 0.08% of ginger ethanol extract and the balance of water, and the preparation method comprises the following steps: mixing fatty acid modified nano zinc oxide, ginger extract and lecithin, performing ultrasonic dispersion at 45 ℃, then dropwise adding the obtained mixture into water at 45 ℃, and performing ultrasonic dispersion uniformly to obtain the product;
and S2, placing the western cold steak processed in the S1 in a radio frequency instrument, setting the distance between polar plates to be 160mm, carrying out radio frequency sterilization for 12min, and then carrying out vacuum packaging.
The frying method of Xiliang beefsteak is the same as that of example 1.
Comparative example 3
The method for preserving the fried western cold beefsteak comprises the following steps:
s1, uniformly mixing preservative emulsion containing nano zinc oxide with western cold beefsteak according to a mass ratio of 0.04g; the preservative emulsion containing the nano zinc oxide comprises the following raw materials in percentage by mass: 0.15% of fatty acid modified nano zinc oxide, 0.4% of lecithin, 0.08% of ginger ethanol extract and the balance of water, and the preparation method comprises the following steps: mixing fatty acid modified nano zinc oxide, ginger extract and lecithin, performing ultrasonic dispersion at 45 ℃, then dropwise adding the obtained mixture into water at 45 ℃, and performing ultrasonic dispersion uniformly to obtain the product;
and S2, placing the western cold steak processed in the S1 into a reaction cavity of a dielectric barrier discharge type low-temperature plasma device, taking air as working gas, carrying out sterilization treatment for 1.5min by adopting low-temperature plasma under the condition of discharge power of 300W, and then carrying out vacuum packaging.
The frying method of Xiliang beefsteak is the same as that of example 1.
Comparative example 4
The conventional high-temperature high-pressure fresh-keeping treatment of the fried western cold beefsteak comprises the following steps:
vacuum packaging West cold steak, placing in high temperature high pressure sterilizing pan, and sterilizing at 121 deg.C for 20 min.
The frying method of Xiliang beefsteak is the same as that of example 1.
Test examples
After the western cold steak after the preservation treatment of example 1 and comparative examples 1-4 is stored at 4 +/-1 ℃ for 8 months under the condition of keeping out of the sun, the total number of microbial colonies in the sample is detected according to GB 4789.1-2016 national food safety Standard food microbiology test, and the test results are shown in Table 1:
TABLE 1
Figure BDA0003998514220000081
The western-cold beefsteak which is not subjected to preservation treatment, is preserved for 8 months at 4 +/-1 ℃ under the condition of keeping out of the sun after being subjected to preservation treatment of example 1, comparative example 1 and comparative example 4, is subjected to sensory evaluation of tenderness (full score of 25), juiciness (full score of 25) and flavor (full score of 50), and the total score is 100. The evaluation results are shown in table 2:
TABLE 2
Example 1 Comparative example 1 Comparative example 4 Untreated with
Sensory Scoring (score) 81.2 69.5 54.8 93.7
The results of microbial colony quantity inspection and sensory evaluation show that the combination of the method of adding the preservative emulsion containing nano zinc oxide, low-temperature plasma treatment and radio frequency sterilization can effectively prolong the preservation period of semi-finished dishes, reduce the influence of sterilization treatment on the change of the internal texture and chemical components of semi-finished dish products in the sterilization treatment and preservation process and reduce the reduction of edible sensory quality caused by oxidative deterioration of fat in meat products in the preservation process, and can still meet the requirements of food sanitation and safety on the colony quantity after being refrigerated for 8 months, and the change of flavor is small; comparative example 1 only adopts a common nano zinc oxide aqueous dispersion, and has large flavor change after long-term storage because the bonding property with fat in meat products is not strong enough and the nano zinc oxide aqueous dispersion can not play a good role in antioxidation; comparative examples 2 and 3 only adopt one of low-temperature plasma treatment and radio frequency sterilization, the sterilization effect is not good enough, and the number of colonies after long-term storage is unqualified; comparative example 4 adopts conventional high-temperature high-pressure sterilization treatment, so that the sensory quality of the dish is greatly reduced.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (10)

1. A method for keeping semi-finished dishes fresh, which is characterized by comprising the following steps:
s1, uniformly mixing preservative emulsion containing nano zinc oxide with semi-finished dishes;
s2, placing the semi-finished dishes processed in the S1 into a reaction cavity of a dielectric barrier discharge type low-temperature plasma device, and performing sterilization treatment by adopting low-temperature plasma;
and S3, placing the semi-finished dish processed in the S2 into a radio frequency instrument for radio frequency sterilization treatment.
2. The method for preserving semi-finished dishes according to claim 1, wherein in S1, the preservative emulsion containing nano zinc oxide comprises the following raw materials by mass percent: 0.1-0.2% of fatty acid modified nano zinc oxide, 0.3-0.5% of lecithin, 0.05-0.1% of ginger ethanol extract and the balance of water.
3. The method for preserving semi-finished dishes according to claim 1, wherein the fatty acid-modified nano zinc oxide is prepared by: adding stearic acid and nano zinc oxide into an ethanol solution, performing ultrasonic dispersion uniformly, performing reflux heating reaction, centrifuging, and drying to obtain the zinc oxide nanoparticle.
4. The method for preserving semi-finished dishes according to claim 3, wherein the stearic acid and the nano zinc oxide are mixed in a mass ratio of (0.2-0.5): 10; the temperature of the reflux heating reaction is 60-100 ℃, and the time is 1-3h.
5. The method for preserving semi-finished dishes according to claim 1, wherein the ethanol extract of ginger is prepared by: mixing rhizoma Zingiberis recens dry powder with 60-95% ethanol solution, leaching, filtering, rotary evaporating the filtrate to remove solvent, and oven drying at 50-60 deg.C.
6. The method of claim 5, wherein the ratio of the dry ginger powder to the ethanol solution is 1g: (10-20) mL; the leaching temperature is 40-60 ℃, and the leaching time is 3-5h.
7. The method for preserving semi-finished dishes according to claim 2, wherein in S1, the nano-zinc oxide-containing preservative emulsion is prepared by the following steps: mixing fatty acid modified nanometer zinc oxide, rhizoma Zingiberis recens extract and lecithin, ultrasonically dispersing at 40-50 deg.C, dripping the obtained mixture into water at 40-50 deg.C, and ultrasonically dispersing.
8. The method for preserving semi-finished food as claimed in claim 1, wherein in S1, the mass ratio of the preservative emulsion containing nano zinc oxide to the semi-finished food is (0.03-0.05): 1000.
9. The method of claim 1, wherein in S2, the discharge power of the low temperature plasma for sterilization is 200-400W, the treatment time is 1-2min, and the working gas is air.
10. The method of claim 1, wherein in S3, the distance between the plates for RF sterilization is 140-180mm, and the sterilization time is 10-15min.
CN202211605277.8A 2022-12-14 2022-12-14 Preservation method of semi-finished dishes Withdrawn CN115836695A (en)

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Application publication date: 20230324