CN115389668B - Traditional Chinese medicine organic matter residue detection device based on gas phase detection method - Google Patents

Traditional Chinese medicine organic matter residue detection device based on gas phase detection method Download PDF

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Publication number
CN115389668B
CN115389668B CN202211045023.5A CN202211045023A CN115389668B CN 115389668 B CN115389668 B CN 115389668B CN 202211045023 A CN202211045023 A CN 202211045023A CN 115389668 B CN115389668 B CN 115389668B
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fixedly connected
base
footstock
wall
working
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CN115389668A (en
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李晓帆
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Suzhou Juxintang Pharmaceutical Co ltd
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Suzhou Juxintang Pharmaceutical Co ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/16Injection
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The utility model provides a detection device is remained to chinese-medicinal material organic matter based on vapor phase detection method, includes the base, fixedly connected with is a plurality of support columns that are mutual symmetry and set up on the up end of base, a plurality of the support column is kept away from each other and sets up, and is a plurality of the support column is kept away from the common fixedly connected with footstock of one end of base, be equipped with the fixed orifices on the footstock, fixedly connected with working cylinder on the inner wall of fixed orifices, fixedly connected with is a plurality of bracing pieces that are mutual symmetry and set up on a lateral wall of footstock base, a plurality of the bracing pieces are kept away from the common fixedly connected with footstock of one end of footstock, the footstock is just to the setting of working cylinder, be equipped with the pneumatic cylinder on the lateral wall that the footstock was kept away from to the footstock, be equipped with the hydraulic pressure post on the pneumatic cylinder. According to the invention, the user can more conveniently complete the sampling work of the traditional Chinese medicinal materials and the injection detection work of the samples, so that the use of the user is greatly facilitated.

Description

Traditional Chinese medicine organic matter residue detection device based on gas phase detection method
Technical Field
The invention relates to the technical field related to detection of traditional Chinese medicinal materials, in particular to a traditional Chinese medicinal material organic matter residue detection device based on a gas phase detection method.
Background
The traditional Chinese medicine is processed according to the theory of traditional Chinese medicine and the processing method of traditional Chinese medicine, can be directly used for the clinical medicine of traditional Chinese medicine, and has the problem of organic matter residue in the process of processing and producing the traditional Chinese medicine, so that the traditional Chinese medicine needs to be subjected to corresponding organic matter detection work, and a gas phase detection method, namely a gas chromatography detection method, is a method capable of detecting organic matters.
When the existing technology detects the organic matter residue of the traditional Chinese medicine by using a gas phase detection method, the traditional Chinese medicine needs to be sampled manually, which is very troublesome, and after the traditional Chinese medicine is sampled by using the medicine, the traditional Chinese medicine also needs to be sucked by a needle tube, and the sample is injected into corresponding equipment, so that the operation is very complicated, and the use of the traditional Chinese medicine by a user is greatly inconvenient.
Therefore, we propose a device for detecting organic residue in Chinese medicinal materials based on gas phase detection method to solve the above problems.
Disclosure of Invention
The invention aims to solve the problems in the prior art, and provides a traditional Chinese medicine organic matter residue detection device based on a gas phase detection method.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
the utility model provides a detection device is remained to chinese-medicinal material organic matter based on vapor phase detection method, includes the base, fixedly connected with is a plurality of support columns that are mutual symmetry and set up on the up end of base, a plurality of the support column is kept away from each other and sets up, a plurality of the support column is kept away from the common fixedly connected with footstock of one end of base, be equipped with the fixed orifices on the footstock, fixedly connected with working cylinder on the inner wall of fixed orifices, fixedly connected with is a plurality of supporting shoe that are mutual symmetry and set up on the lateral wall of footstock base, a plurality of the supporting shoe is kept away from the common fixedly connected with footstock of one end of footstock, the footstock is just to the working cylinder setting, be equipped with the pneumatic cylinder on the lateral wall of footstock is kept away from to the footstock, the one end that the pneumatic cylinder was kept away from to the pneumatic cylinder runs through the footstock setting, the one end fixedly connected with extrusion dish of pneumatic cylinder, the extrusion dish is the setting of matching with working cylinder, be equipped with the gridding plate on the inner wall of working cylinder, still be equipped with working device on the base.
Preferably, the working device comprises a plurality of supporting seats fixedly connected to the base, wherein the supporting seats are symmetrically arranged, one ends of the supporting seats far away from the base are respectively provided with a clamping groove, the clamping grooves are respectively internally provided with clamping blocks in a sliding manner, the clamping blocks are fixedly connected with fixing rings, the inner walls of the fixing rings are fixedly connected with working pipes, the working pipes are close to one side wall of the base and are provided with working holes, one side outer wall of each working pipe close to the base is fixedly connected with a conveying pipe, the conveying pipes are right opposite to the working holes, the base is also provided with a gas phase detector, one ends of the conveying pipes far away from the working holes are arranged on the gas phase detector, the conveying pipes are provided with butterfly valves, the butterfly valves are close to the gas phase detector, the outer walls of the conveying pipes are provided with micro motors, the output ends of the micro motors are arranged on the butterfly valves, and the working pipes are directly provided with control devices.
Preferably, the control device is close to a blanking hole arranged on a side wall of the working cylinder, which is close to the base, a blanking pipe is fixedly connected to the outer wall of one side of the working cylinder, which is close to the base, the blanking pipe is just opposite to the blanking hole, a lifting pipe is slidingly connected to the blanking pipe, a fixed disc is fixedly connected to the outer wall of the blanking pipe, the fixed disc is close to the working cylinder, a lifting disc is fixedly connected to the outer wall of the lifting pipe, the lifting disc is connected with the fixed disc through a plurality of lifting springs, a sealing disc is fixedly connected to the inner wall of the lifting pipe, a plurality of sealing holes which are arranged in a central symmetry manner are formed in the sealing disc, the sealing holes are mutually far away from each other, a hose is fixedly connected to one end of the lifting pipe, which is close to the base, a connecting pipe is fixedly connected to one end of the hose, which is far away from the lifting pipe, and the connecting pipe is slidingly connected to the inside the working pipe.
Preferably, a plurality of the clamping grooves are fixedly connected with magnet discs on the inner wall of one side, close to the base, of the clamping grooves, a plurality of the clamping blocks are fixedly connected with magnet blocks on the side wall, close to the base, of the clamping blocks, and the magnet blocks are respectively arranged in a mutually attracting mode with the magnet discs.
Preferably, a plurality of handles are fixedly connected to the side wall of the lifting disc.
Preferably, fixedly connected with bracing piece on the inner wall of lifter, fixedly connected with connecting rod on the lateral wall that the bracing piece is close to the base, the connecting rod runs through hose and connecting pipe setting, the one end fixedly connected with leak dish that the bracing piece was kept away from to the connecting rod.
Preferably, the outer wall of the connecting pipe is fixedly connected with a fixing sleeve, and the working pipe is arranged in the fixing sleeve in a sliding manner.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, a user can heat traditional Chinese medicinal materials and medicaments into the working cylinder, then the hydraulic cylinder is used for controlling the extrusion plate to descend and matched with the grid plate, so that the sampling treatment work of the traditional Chinese medicinal materials can be smoothly completed, and then the lower working tube and other structures can be used for conveniently adding samples into the gas phase detection instrument, so that the detection work of organic matter residues by the user is greatly facilitated.
Drawings
FIG. 1 is a front structural sectional view of a traditional Chinese medicine organic matter residue detection device based on a gas phase detection method;
FIG. 2 is an enlarged view of the structure A of FIG. 1;
FIG. 3 is an enlarged view of the structure B of FIG. 1;
fig. 4 is an enlarged view of the C structure of fig. 1.
In the figure: 1 a base, 2 a support column, 3 a top seat, 4 a fixed port, 5 a working cylinder, 6 a support block, 7 a top disc, 8 a hydraulic cylinder, 9 a hydraulic cylinder, 10 an extrusion disc, 11 a grid plate, 12 a support seat, 13 a clamping groove, 14 a clamping block, 15 a fixed ring, 16 a working tube, 17 a working hole, 18 a gas phase detector, 19 a butterfly valve, 20 a micro motor, 21 a blanking port, 22 a blanking tube, 23 a lifting tube, 24 a fixed disc, 25 a lifting disc, 26 a sealing disc, 27 a sealing hole, 28 a hose, 29 a connecting tube, 30 a magnet disc, 31 a magnet block, 32 a handle, 33 a support rod, 34 a connecting rod, 35 a leak disc, 36 a fixed sleeve, 37 a conveying tube and 38 a lifting spring.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments.
Referring to FIGS. 1-4, a detection device for residue of organic matters in Chinese medicinal materials based on a gas phase detection method comprises a base 1, a plurality of supporting columns 2 which are symmetrically arranged are fixedly connected to the upper end face of the base 1, a plurality of supporting columns 2 are arranged far away from each other, one end of each supporting column 2 far away from the base 1 is fixedly connected with a top seat 3, a fixed port 4 is arranged on the top seat 3, a working cylinder 5 is fixedly connected to the inner wall of the fixed port 4, a plurality of supporting blocks 6 which are symmetrically arranged are fixedly connected to one side wall of the base 1 of the top seat 3, one end of each supporting block 6 far away from the top seat 3 is fixedly connected with a top disc 7, the top disc 7 is opposite to the working cylinder 5, a side wall of each top disc 7 far away from the top seat 3 is provided with a hydraulic cylinder 8, a hydraulic cylinder 9 is provided with a pressing disc 10, one end of each hydraulic cylinder 9 far away from each hydraulic cylinder 8 is fixedly connected with a pressing disc 10, each pressing disc 10 is matched with the working cylinder 5, a grid plate 11 is arranged on the inner wall of the working cylinder 5, one side wall of the base 1 is further provided with a plurality of supporting blocks 6 which are symmetrically arranged, one end of each supporting blocks 6 far away from the top seat 3 is fixedly connected with a plurality of magnetic blocks 31 which are fixedly connected to one side wall 13 which is fixedly connected with one side of the base 13, a plurality of magnetic blocks 13 which are fixedly connected to one side of the base 13, a plurality of the magnetic blocks are fixedly connected to one side 13 which are fixedly connected to one side of the base 13, one side of the magnetic blocks 13 is far away from the magnetic base 13, one side 13 is fixedly connected to one side 13 is far away from one side 13, and one side 13 is far away from each magnetic base 13 is fixedly connected to one side 13, and each magnetic blocks 13 is arranged in each magnetic base 13 is far away 13 is 13, and each magnetic base is 13 is connected to each and is 13, the fixed state is more stably maintained;
the clamping blocks 14 are fixedly connected with the fixing ring 15 together, the inner wall of the fixing ring 15 is fixedly connected with the working tube 16, a side wall of the working tube 16, which is close to the base 1, is provided with a working hole 17, the outer wall of one side, which is close to the base 1, of the working tube 16 is fixedly connected with a conveying tube 37, the conveying tube 37 is arranged opposite to the working hole 17, the base 1 is also provided with a gas phase detector 18, the gas phase detector 18 is a device in the prior art and can carry out organic matter residue detection work, one end, which is far away from the working hole 17, of the conveying tube 37 is arranged on the gas phase detector 18, the conveying tube 37 is provided with a butterfly valve 19, the butterfly valve 19 is arranged close to the gas phase detector 18, the outer wall of the conveying tube 37 is provided with a micro motor 20, the output end of the micro motor 20 is arranged on the butterfly valve 19, the working tube 16 and the working tube 5 are directly provided with a control device, the control device is arranged close to a blanking port 21 arranged on one side wall, which is close to the base 1, of the working tube 5 is fixedly connected with a blanking tube 22, the blanking tube 22 is arranged opposite to the blanking port 21, the blanking tube 22 is connected with a lifting tube 23 in a sliding manner, the outer wall 22 is fixedly connected with a lifting disc 25, which is fixedly connected with a lifting disc 25, and is fixedly connected with a lifting disc 25, which is fixedly connected with the lifting disc 25, and the lifting disc is provided with the lifting disc 25;
the lifting disc 25 is connected with the fixed disc 24 through a plurality of lifting springs 38, the sealing disc 26 is fixedly connected to the inner wall of the lifting tube 23, a plurality of sealing holes 27 which are arranged in a central symmetry mode are fixedly connected to the sealing disc 26, the sealing holes 27 are arranged away from each other, one end of the lifting tube 23, which is close to the base 1, is fixedly connected with the flexible tube 28, one end of the flexible tube 28, which is far away from the lifting tube 23, is fixedly connected with the connecting tube 29, the connecting tube 29 is arranged in the working tube 16, the outer wall of the connecting tube 29 is fixedly connected with the fixing sleeve 36, the working tube 16 is arranged in the fixing sleeve 36, the connecting tube 29 and the working tube 16 can be connected in a stable and sealed mode by means of the fixing sleeve 36, the supporting rod 33 is fixedly connected to the inner wall of the lifting tube 23, the connecting rod 33 is close to one side wall of the base 1, the connecting rod 34 penetrates through the flexible tube 28 and the connecting tube 29, one end, which is far away from the supporting rod 33, of the connecting tube 35 is fixedly connected with the connecting tube 35, the lifting tube 23 can lift the sample solvent and the preset solvent, which can fall down along with the lifting tube 23, the sample solvent can be stirred, the sample can be detected in a well, and the sample can be detected in the gas phase, and the sample can be fully fused in the sample can be detected.
In the use process of the invention, firstly, a proper working tube 16 is selected, then the working tube 16 and the fixed ring 15 are moved, so that a plurality of clamping blocks 14 are respectively inserted into a plurality of clamping grooves 13, then a plurality of magnet blocks 31 are respectively adsorbed with a plurality of magnet discs 30, thus, the preliminary fixing work of the working tube 16 and the fixed ring 15 is completed, then the connection work of a conveying tube 37 and a gas phase detector 18 is completed, then a certain amount of corresponding solvent can be poured into the working tube 16, so that the solvents fill the conveying tube 37 and part of the working tube 16, then a connecting tube 29 can be inserted into the working tube 16, and a fixed sleeve 36 is sleeved on the working tube 16, thus, the connection work of the connecting tube 29 and the working tube 16 can be completed, meanwhile, a leak disc 35 can be inserted into the working tube 16, then a user can place the Chinese medicinal materials needing to be detected into the working tube 5, and add corresponding medicaments into the working tube 5, and simultaneously the hydraulic cylinder 8 can be started;
the hydraulic cylinder 8 can control the hydraulic cylinder 9 to push the extrusion disk 10 to lift when working, so the extrusion disk 10 can be matched with the grid plate 11 to extrude traditional Chinese medicine materials, then the traditional Chinese medicine materials are fully fused with the medicine materials to obtain samples, the hydraulic cylinder 8 can be closed after the treatment work is completed, and the lifting disk 25 is pulled by the handle 32, so the lifting disk 25 can overcome the elasticity of the lifting spring 38 to drive the lifting pipe 23 to descend, the lifting pipe 23 can enable the sealing disk 26 to be far away from the blanking pipe 22 when descending, the sealing hole 27 on the sealing disk 26 can be prevented from being blocked, then the sample medicine materials can be smoothly dropped into the working pipe 16 to be fused with preset solvents, the situation that when a user controls the lifting pipe 23 to ascend and descend can be informed, the loophole disk 35 can be pushed to ascend and descend through the supporting rod 33 and the connecting rod 34, so the fusion of the dropped sample medicine materials and the preset medicine materials can be accelerated, then the user can control the micro motor 20 to start the micro motor 19, the mixed medicine materials can enter the gas phase detector 18 to complete the detection work, the whole work does not need to be smoothly transferred by the needle tube, and the whole work is greatly convenient for the user.
The foregoing is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art, who is within the scope of the present invention, should make equivalent substitutions or modifications according to the technical scheme of the present invention and the inventive concept thereof, and should be covered by the scope of the present invention.

Claims (4)

1. The utility model provides a chinese-medicinal material organic matter remains detection device based on vapor phase detection method, includes base (1), its characterized in that, fixedly connected with is a plurality of support columns (2) that are mutual symmetry setting on the up end of base (1), a plurality of support columns (2) are keeping away from each other and set up, a plurality of support columns (2) are kept away from one end of base (1) fixedly connected with footstock (3) jointly, be equipped with fixed port (4) on footstock (3), fixedly connected with working cylinder (5) on the inner wall of fixed port (4), fixedly connected with is a plurality of supporting shoe (6) that are mutual symmetry setting on one lateral wall of footstock (3) base (1), a plurality of supporting shoe (6) are kept away from one end fixedly connected with footstock (7) jointly of footstock (3), footstock (7) are just set up working cylinder (5), be equipped with pneumatic cylinder (8) on one lateral wall that footstock (3) were kept away from to footstock (7), be equipped with pneumatic cylinder (9) on pneumatic cylinder (8), fixedly connected with pneumatic cylinder (10) that one end (10) were kept away from to footstock (8) are kept away from to one side of footstock (8), a grid plate (11) is arranged on the inner wall of the working cylinder (5), and a working device is further arranged on the base (1); the working device comprises a plurality of supporting seats (12) fixedly connected to a base (1), wherein the supporting seats (12) are symmetrically arranged, one ends of the supporting seats (12) far away from the base (1) are respectively provided with a clamping groove (13), the clamping grooves (13) are respectively internally and slidably connected with clamping blocks (14), the clamping blocks (14) are fixedly connected with a fixing ring (15) together, a working tube (16) is fixedly connected to the inner wall of the fixing ring (15), a working hole (17) is formed in one side wall of the working tube (16) close to the base (1), a conveying tube (37) is fixedly connected to the outer wall of one side of the working tube (16) close to the base (1), the conveying tube (37) is just opposite to the working hole (17), a gas phase detector (18) is further arranged on the base (1), one end of the conveying tube (37) far away from the working hole (17) is arranged on the gas phase detector (18), a motor (19) is arranged on the conveying tube (37), a butterfly valve motor (19) is arranged on the outer wall of the micro butterfly valve (20) close to the motor (19), the working tube (16) and the working cylinder (5) are directly provided with a control device; the control device is close to a blanking port (21) formed in one side wall of the working cylinder (5) close to the base (1), a blanking pipe (22) is fixedly connected to the outer wall of one side of the working cylinder (5) close to the base (1), the blanking pipe (22) is opposite to the blanking port (21), a lifting pipe (23) is connected to the blanking pipe (22) in a sliding mode, a fixed disc (24) is fixedly connected to the outer wall of the blanking pipe (22), the fixed disc (24) is arranged close to the working cylinder (5), a lifting disc (25) is fixedly connected to the outer wall of the lifting pipe (23), a sealing disc (26) is fixedly connected to the inner wall of the lifting pipe (23), a plurality of sealing holes (27) which are arranged in a central symmetry mode are formed in a mutually-distant mode, one end, close to the base (1), of the lifting pipe (23) is fixedly connected with a lifting disc (25), one end, close to the lifting tube (28) is connected to the connecting tube (29), and the hose (29) is connected to the inner end, which is fixedly connected with the lifting tube (16); the inner wall of the lifting pipe (23) is fixedly connected with a supporting rod (33), a connecting rod (34) is fixedly connected to one side wall, close to the base (1), of the supporting rod (33), the connecting rod (34) penetrates through the hose (28) and the connecting pipe (29), and one end, far away from the supporting rod (33), of the connecting rod (34) is fixedly connected with a leak disc (35).
2. The device for detecting organic matter residues in a traditional Chinese medicine based on a gas phase detection method according to claim 1, wherein a plurality of magnet plates (30) are fixedly connected to the inner wall of one side of the clamping grooves (13) close to the base (1), a plurality of magnet blocks (31) are fixedly connected to one side wall of the clamping blocks (14) close to the base (1), and the magnet blocks (31) are respectively attracted to the magnet plates (30).
3. The device for detecting organic matter residues in a traditional Chinese medicine based on a gas phase detection method according to claim 1, wherein a plurality of handles (32) are fixedly connected to the side wall of the lifting disc (25).
4. The device for detecting organic matter residues in traditional Chinese medicinal materials based on a gas phase detection method according to claim 1, wherein a fixing sleeve (36) is fixedly connected to the outer wall of the connecting pipe (29), and the working pipe (16) is slidably connected in the fixing sleeve (36).
CN202211045023.5A 2022-08-30 2022-08-30 Traditional Chinese medicine organic matter residue detection device based on gas phase detection method Active CN115389668B (en)

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