CN115350623A - Rapid emulsification and dispersion device and process for binaphthol processing - Google Patents
Rapid emulsification and dispersion device and process for binaphthol processing Download PDFInfo
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- CN115350623A CN115350623A CN202211276663.7A CN202211276663A CN115350623A CN 115350623 A CN115350623 A CN 115350623A CN 202211276663 A CN202211276663 A CN 202211276663A CN 115350623 A CN115350623 A CN 115350623A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/93—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with rotary discs
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/43—Mixing liquids with liquids; Emulsifying using driven stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/21—Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by their rotating shafts
- B01F27/2124—Shafts with adjustable length, e.g. telescopic shafts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/805—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis wherein the stirrers or the receptacles are moved in order to bring them into operative position; Means for fixing the receptacle
- B01F27/806—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis wherein the stirrers or the receptacles are moved in order to bring them into operative position; Means for fixing the receptacle with vertical displacement of the stirrer, e.g. in combination with means for pivoting the stirrer about a vertical axis in order to co-operate with different receptacles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/40—Mounting or supporting mixing devices or receptacles; Clamping or holding arrangements therefor
- B01F35/42—Clamping or holding arrangements for mounting receptacles on mixing devices
Abstract
The invention relates to the technical field of binaphthol processing, and discloses a rapid emulsifying and dispersing device and a rapid emulsifying and dispersing process for binaphthol processing, wherein the device comprises the following components: the device comprises a ground platform, a controller, a clamp holder, a bottom dispersing mechanism, a container mechanism, a material injection mechanism and a pump station; the controller is fixedly arranged on the right side of the top of the platform; the clamp holder is fixedly arranged on the front side of the top of the platform; the bottom dispersion mechanism is arranged on the front side of the platform; the container mechanism is placed on the inner side of the clamp holder and is positioned above the bottom dispersing mechanism; the material injection mechanism is fixedly arranged at the top of the platform; the pump station is arranged on the rear side of the top end of the platform. This quick emulsification dispersion devices of binaphthol processing can realize that the bottom stretches into the mode and emulsifies the dispersion, makes the dispersion impeller contact the bottom filler more easily and makes its emulsification dispersion more easily to can realize filling more deep input, avoid it directly to float at the liquid surface, can make the improvement emulsification dispersion effect.
Description
Technical Field
The invention relates to the technical field of binaphthol processing, in particular to a device and a process for quickly emulsifying and dispersing binaphthol.
Background
Binaphthol is a typical chiral compound, has strong plane asymmetry, is easy to be resolved into high-purity enantiomers, and has been successfully applied to inducing some asymmetric synthetic reactions, the chiral compound is a special kind of organic compound, is an optical rotation compound formed by containing one or more asymmetric atoms, some chiral compounds are excellent plant growth hormone, herbicide and pesticide, and play a great role in crop culture, so that the synthesis and analysis of the chiral compound are different from the high-technology field of general chemical industry technology and are also the field with very active chemical frontier at present, the supply of chemical reagents in China has become the bottleneck of developing chemical research, the chiral chemical reagents and related compounds are more so and almost completely depend on imports, and therefore, the research on the synthesis of the representative chiral compound binaphthol is significant;
in the prior art, the invention with the similar application number of CN113041926A is adopted for emulsification and dispersion in the production process of binaphthol, and discloses an emulsification and dispersion machine which comprises a fixed base, a kettle body and an emulsification and dispersion mechanism; the kettle body is fixed on the upper end surface of the fixed base through the shock absorption support, the upper end surface of the fixed base is also provided with an electric telescopic column, the top of the electric telescopic column is provided with a support arm, and the lower end surface of the support arm is provided with a kettle cover for covering the kettle body; the material emulsifying and dispersing device is high in material emulsifying and dispersing efficiency and emulsifying quality, materials in the kettle body can be further crushed, and the materials in the kettle body form internal circulation, so that the emulsifying and dispersing uniformity is improved, and the emulsifying and dispersing efficiency and the emulsifying quality are further improved.
Disclosure of Invention
The invention aims to provide a rapid emulsification and dispersion device and a rapid emulsification and dispersion process for processing binaphthol, which are used for at least solving the problems that all emulsification and dispersion machines in the prior art adopt a lifting dispersion plate to extend into the bottom of a solution from the top for dispersion, the dispersion mode is not easy to contact the bottom of the solution, so that part of fillers with higher density cannot be fully emulsified and dispersed after sinking, and part of fillers with lower density directly float on the surface of a liquid surface, so that the fillers cannot be fully emulsified and dispersed.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a fast emulsification dispersion devices of binaphthol processing, includes: the device comprises a ground platform, a controller, a clamp holder, a bottom dispersing mechanism, a container mechanism, a material injection mechanism and a pump station;
the controller is fixedly arranged on the right side of the top of the platform; the clamp holder is fixedly arranged on the front side of the top of the platform; the bottom dispersing mechanism is arranged on the front side of the platform; the container mechanism is placed on the inner side of the holder and is positioned above the bottom dispersing mechanism; the material injection mechanism is fixedly arranged at the top of the platform; the pump station sets up the top rear side of platform, pump station and controller electric connection.
Preferably, in order to realize bottom emulsification and dispersion, the bottom dispersion mechanism comprises: the device comprises a bottom dispersion mechanism box body, a funnel, a lifting module, a driving module, a sealing cylinder, a first magnetic chuck, a dispersion disc, a liquid storage box, a pressure pump and a liquid discharge valve; the bottom dispersion mechanism box body is embedded in the front side of the platform along the up-down direction; the funnel is arranged at an opening at the top of the inner cavity of the box body of the bottom dispersing mechanism; the lifting module is arranged on the rear side of the top end of the bottom dispersion mechanism box body in the vertical direction and is electrically connected with the controller; the driving module is arranged at the lifting end of the lifting module, the output end of the driving module extends into the inner cavity of the funnel, and the driving module is electrically connected with the controller; the number of the sealing cylinders is two, and the two sealing cylinders are respectively connected to the upper side and the lower side of the output end of the driving module in a rotating manner through bearings along the up-down direction; the first magnetic sucker is arranged at the center of the top end of the sealing cylinder above the first magnetic sucker; the dispersion disc is arranged at the output end of the driving module and is positioned at the inner sides of the upper sealing cylinder and the lower sealing cylinder; the liquid storage tank is arranged on the rear side of the bottom end of the inner cavity of the bottom dispersion mechanism box body in the left-right direction, and a liquid inlet hole of the liquid storage tank is connected with the bottom of the inner cavity of the funnel through a guide pipe; the pressurizing pump is fixedly arranged at the top end of the liquid storage tank, a liquid inlet pipe of the pressurizing pump extends into the inner cavity of the liquid storage tank, and the pressurizing pump is electrically connected with the controller; and the liquid discharge valve is arranged at the top end of the right side of the outer wall of the box body of the bottom dispersing mechanism and is in threaded connection with the liquid outlet pipe of the pressure pump.
Preferably, in order to cooperate to achieve bottom emulsification dispersion, the container mechanism comprises: the device comprises a storage barrel, a connecting barrel, a sealing seat, a sealing ring, a second magnetic chuck, a liquid inlet valve, a magnet ring, a cone and a take-up and pay-off module; the storage barrel is clamped at the inner side of the clamp along the up-down direction; the connecting cylinder is embedded in the center of the bottom end of the inner cavity of the storage barrel in the vertical direction; the sealing seat is inserted at the top end of the connecting cylinder; the sealing ring is arranged on the outer side of the bottom end of the sealing seat along the circumferential direction; the second magnetic chuck is arranged at the center of the bottom end of the sealing seat; the number of the liquid inlet valves is two, and the two liquid inlet valves are respectively screwed at openings on the front side and the rear side of the top end of the storage barrel; the number of the magnet rings is two, and the two magnet rings are respectively arranged at the top end of the inner cavity of the storage barrel and positioned at the outer sides of the bottoms of the two liquid inlet valves; the number of the cones is two, and the two cones are respectively adsorbed at the bottoms of the two magnet rings; the wire winding and unwinding module is arranged at the top end of the inner cavity of the storage barrel, an inner steel wire of the wire winding and unwinding module extends into the inner cavity of the storage barrel and is connected with the outer walls of the two cones respectively, and the wire winding and unwinding module is electrically connected with the controller.
Preferably, the inner diameter of the connecting cylinder is matched with the outer diameter of the sealing cylinder.
Preferably, the inner diameter of the sealing ring is matched with the outer diameter of the connecting cylinder.
Preferably, in order to realize deeper feeding of the filler, the material injection mechanism comprises: the device comprises a material injection mechanism shell, a liquid storage tank, a three-way electromagnetic valve, a telescopic connecting pipe, a pressure storage tank, an electromagnetic valve and an air pump; the shell of the material injection mechanism is arranged at the top end of the platform through a bracket along the front-back direction; the number of the liquid storage tanks is two, the two liquid storage tanks are respectively arranged at the left end and the right end of the rear side of the inner cavity of the shell of the material injection mechanism, and liquid inlets at the top ends of the two liquid storage tanks are respectively connected with a liquid outlet pipe of a pump station; the number of the three-way electromagnetic valves is two, the two three-way electromagnetic valves are respectively arranged at the left end and the right end of the front side of the bottom end of the shell of the material injection mechanism, liquid inlet holes of the two three-way electromagnetic valves are respectively connected with liquid outlets of a left liquid storage tank and a right liquid storage tank through guide pipes, and the three-way electromagnetic valves are electrically connected with the controller; the number of the telescopic connecting pipes is two, and the two telescopic connecting pipes are respectively arranged at liquid outlets at the bottom of the three-way electromagnetic valve; the number of the pressure storage tanks is two, and the two pressure storage tanks are respectively arranged at the left end and the right end of the front side of the inner cavity of the shell of the material injection mechanism along the up-down direction; the electromagnetic valves are embedded in the middle of the inner cavities of the left pressure storage tank and the right pressure storage tank respectively, and are electrically connected with the controller; the air pump is arranged at the bottom end of the inner cavity of the shell of the material injection mechanism and is electrically connected with the controller.
Preferably, the air outlet pipe of the air pump is respectively connected with the top ends of the upper part and the lower part of the inner cavities of the left pressure storage tank and the right pressure storage tank which are separated by the electromagnetic valve.
The processing technology of the device comprises the following steps:
the method comprises the following steps: the working personnel fills base materials into the container mechanism in advance, the container mechanism is hoisted to the inner side of the clamper, the clamper clamps the storage barrel at the top of the bottom dispersion mechanism box body, the telescopic connecting pipe is connected with the liquid inlet valves at two sides, the control controller starts the pump station to inject the filler into the liquid storage tanks respectively from the pump station to realize the pre-filling of the filler,
step two: the lifting module drives the driving module to move upwards, the top sealing cylinder enables the sealing seat to move upwards from the inner side of the connecting cylinder to the top under the coordination of the second magnetic sucker, and the bottom sealing cylinder seals the inner cavity of the connecting cylinder;
step three: drive module drive dispersion impeller rotates inside the storage bucket to emulsify the dispersion operation to the inside material of storage bucket:
step four: compressed air is filled into the upper side and the lower side of an inner cavity of the pressure storage tank through an air outlet pipe by an air pump, the compressed air at the bottom of the pressure storage tank enters the storage barrel through a three-way electromagnetic valve, a telescopic connecting pipe and a liquid inlet valve, and a steel wire in the wire unwinding and winding module is unwound, so that a cone is pushed by the compressed air to be downwards inserted into the liquid level of a base material in the storage barrel;
step five: the pre-filled filler in the liquid storage tank enters the three-way electromagnetic valve, the pressure air at the top of the inner cavity of the pressure storage tank pushes the filler to be injected into the storage barrel, and the filler is enabled to be instantly broken along the cone under the action of the compressed air to penetrate into the bottom of the liquid level of the base material to further enable the filler and the base material to be easily dispersed by the dispersion disc at the bottom of the base material;
step six: after emulsification is finished, the wire winding and unwinding module winds an internal steel wire of the wire winding and unwinding module to enable a cone body to be attracted and fixed by a magnet ring on a corresponding position to enable the cone body to reset, the lifting module is shortened to enable the driving module to drive the upper sealing barrel and the lower sealing barrel to sequentially move downwards out of the connecting barrel, the top sealing barrel enables the sealing seat to be downwards inserted into the top of the connecting barrel again under the matching of the first magnetic sucker and the second magnetic sucker, the sealing ring seals a connecting gap between the sealing seat and the connecting barrel, so that the bottom of the storage barrel is sealed, and the container mechanism can be taken out of the clamp holder;
step seven: the liquid that sealed section of thick bamboo took out gets into to the funnel in to get into the liquid reserve tank through the pipeline under the funnel, staff's accessible controller control force (forcing) pump is handled by the discharge valve discharge with the liquid that the liquid reserve tank is inside to be collected.
Compared with the prior art, the invention has the beneficial effects that:
1. drive module rebound through lifting module to make drive module drive about both sides sealed section of thick bamboo insert to the connecting cylinder inner chamber, first magnetic chuck and second magnetic chuck magnetism attract mutually, and make a top sealed section of thick bamboo with the sealed seat from the inboard top that makes progress of connecting cylinder under the cooperation of second magnetic chuck, bottom sealed section of thick bamboo inserts the connecting cylinder inner chamber and seals the connecting cylinder inner chamber, drive module drive dispersion impeller rotates in storage bucket is inside, in order to emulsify the dispersion operation to the inside material of storage bucket:
2. compressed air is filled into the upper side and the lower side of an inner cavity of a pressure storage tank through an air pump, the compressed air at the bottom of the pressure storage tank enters a storage barrel through a three-way electromagnetic valve, a telescopic connecting pipe and a liquid inlet valve, a cone is pushed by the compressed air to be downwards inserted into the liquid level of a base material in the storage barrel, the compressed air at the top of the inner cavity of the pressure storage tank pushes filler in the three-way electromagnetic valve to be injected into the storage barrel through the telescopic connecting pipe and the liquid inlet valve, and the filler is enabled to penetrate into the bottom of the liquid level of the feed material along a gap of the liquid level of the base material instantaneously broken by the cone under the action of the compressed air, so that the filler and the base material are more easily dispersed by a dispersion disc at the bottom of the base material, a wire take-up and pay-off module winds up an internal steel wire to enable the cone and is magnetically attracted and fixed by a magnet ring at a corresponding position to enable the cone to reset, and is convenient to use next time;
3. the driving module drives the upper sealing cylinder and the lower sealing cylinder to move out of the connecting cylinder through the lifting module, the top sealing cylinder enables the sealing seat to be downwards inserted into the top of the connecting cylinder again under the matching of the first magnetic sucker and the second magnetic sucker, and the sealing ring seals a connecting gap between the sealing seat and the connecting cylinder;
thereby can realize that the bottom stretches into the mode and emulsify the dispersion, make the dispersion impeller contact the bottom filler more easily and make its emulsification dispersion more easily to can realize filling more deep input, avoid it directly to float on the liquid surface, can make and improve emulsification dispersion effect.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is an exploded view of the bottom dispersion mechanism of FIG. 1;
FIG. 3 is an exploded view of the container mechanism of FIG. 1;
fig. 4 is an exploded view of the injection mechanism of fig. 1.
In the figure: 1. the device comprises a platform, 2, a controller, 3, a gripper, 4, a bottom dispersing mechanism, 41, a bottom dispersing mechanism box body, 42, a funnel, 43, a lifting module, 44, a driving module, 45, a sealing barrel, 46, a first magnetic sucker, 47, a dispersing disk, 48, a liquid storage box, 49, a pressure pump, 410, a liquid discharge valve, 5, a container mechanism, 51, a storage barrel, 52, a connecting barrel, 53, a sealing seat, 54, a sealing ring, 55, a second magnetic sucker, 56, a liquid inlet valve, 57, a magnet ring, 58, a cone, 59, a take-up and pay-off line module, 6, an injection mechanism, 61, an injection mechanism shell, 62, a liquid storage tank, 63, a three-way electromagnetic valve, 64, a telescopic connecting pipe, 65, a pressure storage tank, 66, an electromagnetic valve, 67, an air pump, 7 and a pump station.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Referring to fig. 1-4, the present invention provides a technical solution: the utility model provides a quick emulsification dispersion devices of binaphthol processing, includes: the device comprises a platform 1, a controller 2, a holder 3, a bottom dispersing mechanism 4, a container mechanism 5, a material injection mechanism 6 and a pump station 7; the controller 2 is fixedly arranged on the right side of the top of the platform 1; the clamp 3 is fixedly arranged on the front side of the top of the platform 1, the clamp 3 is driven in an electric or manual mode according to actual requirements, and the clamp 3 can clamp and fix the outer part of the storage barrel 51 in the container mechanism 5; the bottom dispersing mechanism 4 is arranged on the front side of the platform 1; the container mechanism 5 is placed inside the gripper 3 and above the bottom dispersion mechanism 4; the material injection mechanism 6 is fixedly arranged at the top of the platform 1; pump station 7 sets up the top rear side at platform 1, pump station 7 and 2 electric connection of controller, and pump station 7 can be controlled by staff operation control ware 2, and the staff can pour into the filler into pump station 7 to pour into liquid storage pot 62 into respectively by pump station 7 into, realize that the filler prefills.
Preferably, as shown in fig. 2, the bottom dispersing mechanism 4 further includes: a bottom dispersion mechanism box body 41, a funnel 42, a lifting module 43, a driving module 44, a sealing barrel 45, a first magnetic sucker 46, a dispersion disc 47, a liquid storage box 48, a pressure pump 49 and a liquid discharge valve 410; the bottom dispersion mechanism box body 41 is embedded in the front side of the platform 1 along the up-down direction;
in order to collect the liquid brought out by the up-and-down movement of the sealing cylinder 45, the funnel 42 is arranged at the top opening of the inner cavity of the bottom dispersion mechanism box body 41;
in order to realize the height position adjustment of the sealing cylinder 45 and the dispersion disc 47, the lifting module 43 is arranged at the rear side of the top end of the bottom dispersion mechanism box body 41 along the up-down direction, the lifting module 43 is electrically connected with the controller 2, the lifting module 43 can be controlled by the controller 2 operated by a worker, and the lifting module 43 can drive the driving module 44 to lift to a specified height position; the driving module 44 is arranged at the lifting end of the lifting module 43, the output end of the driving module 44 extends into the inner cavity of the funnel 42, the driving module 44 is electrically connected with the controller 2, the driving module 44 can be controlled by the controller 2 operated by a worker, and the driving module 44 can drive the dispersion disc 47 to rotate in the storage barrel 51; the number of the sealing cylinders 45 is two, and the two sealing cylinders 45 are respectively connected to the upper side and the lower side of the output end of the driving module 44 in the vertical direction through bearings in a rotating manner; the first magnetic chuck 46 is provided at the top center position of the upper sealing cylinder 45; the dispersion disc 47 is arranged at the output end of the driving module 44 and is positioned at the inner sides of the upper sealing cylinder 45 and the lower sealing cylinder 45;
in order to realize the collection and discharge treatment of the liquid in the funnel 42, the liquid storage tank 48 is installed at the rear side of the bottom end of the inner cavity of the bottom dispersion mechanism box body 41 along the left-right direction, and a liquid inlet hole of the liquid storage tank 48 is connected with the bottom of the inner cavity of the funnel 42 through a guide pipe; the pressure pump 49 is fixedly arranged at the top end of the liquid storage box 48, a liquid inlet pipe of the pressure pump 49 extends into the inner cavity of the liquid storage box 48, the pressure pump 49 is electrically connected with the controller 2, the pressure pump 49 can be driven to be controlled by the controller 2 operated by a worker, and the pressure pump 49 can discharge liquid in the liquid storage box 48 through a liquid outlet pipe in the pressure pump 49 and the liquid outlet valve 410; the drain valve 410 is arranged at the top end of the right side of the outer wall of the bottom dispersion mechanism box body 41, the drain valve 410 is in threaded connection with the liquid outlet pipe of the pressure pump 49, and the drain valve 410 can be connected with an external collection container.
Preferably, as shown in fig. 3, the connection portion of the internal components of the container means 5 should be sealed to prevent the internal liquid from leaking out, and the container means 5 includes: the device comprises a storage barrel 51, a connecting barrel 52, a sealing seat 53, a sealing ring 54, a second magnetic chuck 55, a liquid inlet valve 56, a magnet ring 57, a cone 58 and a take-up and pay-off module 59; the bucket 51 is held inside the holder 3 in the up-down direction;
in order to realize the extension of the bottom dispersing mechanism 4 from the lower part of the storage barrel 51, the connecting cylinder 52 is embedded in the center of the bottom end of the inner cavity of the storage barrel 51 along the up-down direction; the sealing seat 53 is inserted at the top end of the connecting cylinder 52, and the sealing seat 53 can be fixedly connected with the top of the connecting cylinder 52 in a clamping or magnetic suction manner; the seal ring 54 is circumferentially arranged outside the bottom end of the seal seat 53; the second magnetic chuck 55 is arranged at the bottom center of the sealing seat 53, and the second magnetic chuck 55 can magnetically attract the first magnetic chuck 46 to realize the connection between the sealing seat 53 and the top sealing cylinder 45;
in order to realize the effect that the cone 58 breaks the liquid level, the number of the liquid inlet valves 56 is two, and the two liquid inlet valves 56 are respectively screwed at the front and rear openings at the top end of the storage barrel 51; the number of the magnet rings 57 is two, and the two magnet rings 57 are respectively arranged at the top end of the inner cavity of the storage barrel 51 and positioned at the outer sides of the bottoms of the two liquid inlet valves 56; the number of the cones 58 is two, and the two cones 58 are respectively adsorbed at the bottoms of the two magnet rings 57; receive and release line module 59 and set up on the inner chamber top of storage bucket 51, the inner wire that receives and releases line module 59 extends into storage bucket 51 and is connected with two cone 58 outer walls respectively, receive and release line module 59 and controller 2 electric connection, receive and release line module 59 can be controlled by staff operation control ware 2, the inside winding of receive and release line module 59 has the rolling of the inside steel wire of steel wire accessible be connected with cone 58 and relaxs the realization and control the recycling of cone 58.
Preferably, the inner diameter of the connecting cylinder 52 is adapted to the outer diameter of the sealing cylinder 45, and when the top sealing cylinder 45 and the dispersion disc 47 extend into the storage barrel 51, the bottom sealing cylinder 45 is inserted into the inner cavity of the connecting cylinder 52 and the bottom sealing cylinder 45 is kept inserted into the connecting cylinder 52 and seals the inner cavity of the connecting cylinder 52 while the dispersion disc 47 rotates in the storage barrel 51.
Preferably, the inner diameter of the sealing ring 54 is adapted to the outer diameter of the connecting cylinder 52, so that the sealing ring 54 seals the connecting gap between the sealing seat 53 and the connecting cylinder 52, thereby sealing the bottom of the storage barrel 51.
As a preferable scheme, further, as shown in fig. 4, the material injection mechanism 6 includes: a material injection mechanism shell 61, a liquid storage tank 62, a three-way electromagnetic valve 63, a telescopic connecting pipe 64, a pressure storage tank 65, an electromagnetic valve 66 and an air pump 67; the material injection mechanism shell 61 is arranged at the top end of the platform 1 through a bracket along the front-back direction;
in order to realize the pre-storage of the fillers, the number of the liquid storage tanks 62 is two, the two liquid storage tanks 62 are respectively arranged at the left end and the right end of the rear side of the inner cavity of the shell 61 of the material injection mechanism, and liquid inlets at the top ends of the two liquid storage tanks 62 are respectively connected with a liquid outlet pipe of the pump station 7; the number of the three-way electromagnetic valves 63 is two, the two three-way electromagnetic valves 63 are respectively arranged at the left end and the right end of the front side of the bottom end of the material injection mechanism shell 61, liquid inlet holes of the two three-way electromagnetic valves 63 are respectively connected with liquid outlets of the left liquid storage tank 62 and the right liquid storage tank 62 through guide pipes, the three-way electromagnetic valves 63 are electrically connected with the controller 2, and the three-way electromagnetic valves 63 can realize the mutual communication among the liquid storage tanks 62, the telescopic connecting pipe 64 and the pressure storage tank 65; the number of the telescopic connecting pipes 64 is two, and the two telescopic connecting pipes 64 are respectively arranged at liquid outlets at the bottom of the three-way electromagnetic valve 63;
in order to realize that compressed air on the upper side and the lower side inside the pressure storage tanks 65 respectively realize the pushing of the cone 58 and the material in sequence, the number of the pressure storage tanks 65 is two, and the two pressure storage tanks 65 are respectively arranged at the left end and the right end of the front side of the inner cavity of the material injection mechanism shell 61 along the up-down direction; the number of the electromagnetic valves 66 is two, the two electromagnetic valves 66 are respectively embedded in the middle of the inner cavities of the left pressure storage tank 65 and the right pressure storage tank 65, the electromagnetic valves 66 are electrically connected with the controller 2, the electromagnetic valves 66 can be controlled by operating the controller 2 by workers, and the electromagnetic valves 66 can control compressed air on the upper side and the lower side of the pressure storage tanks 65; the air pump 67 sets up in the inner chamber bottom of annotating material mechanism shell 61, and air pump 67 and controller 2 electric connection, and the air pump 67 can be controlled by staff operation control ware 2, and the air pump 67 can be gone into compressed air pump to the pressure storage jar 65 inside.
Preferably, the air outlet pipe of the air pump 67 is connected to the top ends of the upper and lower portions of the inner cavities of the left and right pressurized storage tanks 65, which are separated by the electromagnetic valve 66, so as to store the compressed air in the upper and lower portions of the pressurized storage tanks 65.
A dispersing process of a binaphthol processing rapid emulsifying and dispersing device comprises the following specific steps:
the staff fills the base material into the container mechanism 5 in advance, and hoist the container mechanism 5 to the inner side of the holder 3, the staff makes the holder 3 hold the storage barrel 51 at the top of the bottom dispersion mechanism box 41, and connect the telescopic connection pipe 64 with the two-side liquid inlet valve 56, the control controller 2 starts the pump station 7, the filler is injected into the liquid storage tank 62 by the pump station 7, the pre-filling of the filler is realized, the control controller 2 starts the lifting module 43 and the driving module 44 in sequence, the lifting module 43 drives the driving module 44 to move upwards, and the driving module 44 drives the upper and lower two-side sealing barrels 45 to be inserted into the inner cavity of the connecting barrel 52, the first magnetic suction cup 46 and the second magnetic suction cup 55 attract each other magnetically, and the top sealing barrel 45 makes the sealing seat 53 from the inner side of the connecting barrel 52 to the top under the cooperation of the second magnetic suction cup 55, the bottom sealing barrel 45 is inserted into the inner cavity of the connecting barrel 52 and seals the inner cavity of the connecting barrel 52, the driving module 44 drives the dispersion disc 47 to rotate in the storage barrel 51, so as to perform the emulsification dispersion operation on the materials in the storage barrel 51:
when the filling operation needs to be performed on the interior of the storage barrel 51, the worker controls the controller 2 to start the air pump 67, the telescopic connecting pipe 64, the coiling and uncoiling line module 59 and the electromagnetic valve 66, the air pump 67 fills compressed air to the upper side and the lower side of the inner cavity of the pressure storage tank 65 through an air outlet pipe, the three-way electromagnetic valve 63 controls the communication between the pressure storage tank 65 and the telescopic connecting pipe 64, so that the compressed air at the bottom of the pressure storage tank 65 enters the storage barrel 51 through the three-way electromagnetic valve 63, the telescopic connecting pipe 64 and the liquid inlet valve 56, the steel wire in the coiling and uncoiling line module 59 is uncoiled, the cone 58 is pushed by the compressed air to be downwards inserted into the liquid level of the base material in the storage barrel 51, meanwhile, the pre-filled filler in the liquid storage tank 62 enters the three-way electromagnetic valve 63, the electromagnetic valve 66 is opened, so that the top pressure air in the inner cavity of the pressure storage tank 65 pushes the filler in the three-way electromagnetic valve 63 to be injected into the storage barrel 51 through the telescopic connecting pipe 64 and the liquid inlet valve 56, the filler is pushed by the compressed air to be deep into the bottom of the liquid level of the base material along the gap of the cone 58 under the action of the compressed air to be conveniently dispersed by the magnetic attraction dispersion disc 47 at the bottom of the base material, the coiling and uncoiling line module 59 makes the cone 58 to make the cone 58 and the cone 58 be conveniently used for magnetic attraction of the magnetic attraction dispersion disc 57 at the upper position of the bottom of the cone 58, so that the cone 58 and the magnetic attraction dispersion disc 47 at the magnetic attraction dispersion disc 58 is conveniently and the magnetic attraction of the bottom of the magnetic attraction dispersion disc 58 and the bottom of the magnetic attraction dispersion disc;
after emulsification is finished, the worker controls the controller 2 to start the lifting module 43, the lifting module 43 shortens to make the driving module 44 drive the upper and lower two-side sealing cylinders 45 to move downwards out of the connecting cylinder 52 in sequence, and makes the top sealing cylinder 45 to make the sealing seat 53 inserted downwards again to the top of the connecting cylinder 52 under the cooperation of the first magnetic sucker 46 and the second magnetic sucker 55, and makes the sealing ring 54 seal the connecting gap between the sealing seat 53 and the connecting cylinder 52, thereby realizing the bottom sealing of the storage cylinder 51, the container mechanism 5 can be taken out of the clamper 3, the taken liquid enters the funnel 42 and enters the liquid storage box 48 through the pipeline below the funnel 42, and the worker can control the pressure pump 49 to discharge the liquid collected inside the liquid storage box 48 through the liquid discharge valve 410 for processing.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. The utility model provides a binaphthol processing rapid emulsification dispersion devices which characterized in that includes:
a platform (1);
the controller (2) is fixedly arranged on the right side of the top of the platform (1);
the clamp holder (3) is fixedly arranged on the front side of the top of the platform (1);
a bottom dispersion mechanism (4) arranged on the front side of the platform (1);
a container mechanism (5) placed inside the gripper (3) and above the bottom dispersion mechanism (4);
the material injection mechanism (6) is fixedly arranged at the top of the platform (1);
and the pump station (7) is arranged on the rear side of the top end of the platform (1), and the pump station (7) is electrically connected with the controller (2).
2. The rapid emulsifying and dispersing device for processing binaphthol as claimed in claim 1, wherein the bottom dispersing mechanism (4) comprises:
a bottom dispersion mechanism box body (41) embedded in the front side of the platform (1);
the hopper (42) is arranged at the opening of the top of the inner cavity of the bottom dispersion mechanism box body (41);
the lifting module (43) is arranged on the rear side of the top end of the bottom dispersion mechanism box body (41), and the lifting module (43) is electrically connected with the controller (2);
the driving module (44) is arranged at the lifting end of the lifting module (43), the output end of the driving module (44) extends into the inner cavity of the funnel (42), and the driving module (44) is electrically connected with the controller (2);
the number of the sealing cylinders (45) is two, and the two sealing cylinders (45) are respectively connected to the upper side and the lower side of the output end of the driving module (44) in a rotating mode through bearings;
a first magnetic chuck (46) provided at the top center of the sealing cylinder (45);
the dispersion disc (47) is arranged at the output end of the driving module (44) and is positioned at the inner sides of the upper sealing cylinder (45) and the lower sealing cylinder (45);
the liquid storage box (48) is arranged on the rear side of the bottom end of the inner cavity of the bottom dispersion mechanism box body (41), and a liquid inlet hole of the liquid storage box (48) is connected with the bottom of the inner cavity of the funnel (42) through a guide pipe;
the pressure pump (49) is fixedly installed at the top end of the liquid storage box (48), a liquid inlet pipe of the pressure pump (49) extends into the inner cavity of the liquid storage box (48), and the pressure pump (49) is electrically connected with the controller (2);
and the liquid discharge valve (410) is arranged at the top end of the right side of the outer wall of the bottom dispersion mechanism box body (41), and the liquid discharge valve (410) is in threaded connection with a liquid outlet pipe of the pressure pump (49).
3. The rapid emulsifying and dispersing device for processing binaphthol as claimed in claim 2, wherein said container mechanism (5) comprises:
a storage bucket (51) clamped inside the clamp (3);
the connecting cylinder (52) is embedded in the center of the bottom end of the inner cavity of the storage barrel (51);
the sealing seat (53) is inserted at the top end of the connecting cylinder (52);
a seal ring (54) disposed circumferentially outside the bottom end of the seal seat (53);
the second magnetic sucker (55) is arranged at the center of the bottom end of the sealing seat (53);
the number of the liquid inlet valves (56) is two, and the two liquid inlet valves (56) are respectively screwed at openings on the front side and the rear side of the top end of the storage barrel (51);
the number of the magnet rings (57) is two, and the two magnet rings (57) are respectively arranged at the top end of the inner cavity of the storage barrel (51) and positioned at the outer sides of the bottoms of the two liquid inlet valves (56);
the number of the cones (58) is two, and the two cones (58) are respectively adsorbed at the bottoms of the two magnet rings (57);
receive and release line module (59), set up in the inner chamber top of bucket (51), the inside steel wire of receive and release line module (59) extends into the inner chamber of bucket (51) and respectively with two cone (58) outer wall connection, receive and release line module (59) and controller (2) electric connection.
4. The rapid emulsifying and dispersing device for binaphthol processing according to claim 3, wherein the inner diameter of the connecting cylinder (52) is adapted to the outer diameter of the sealing cylinder (45).
5. The rapid emulsifying and dispersing device for binaphthol processing according to claim 4, wherein the inner diameter of the sealing ring (54) is matched with the outer diameter of the connecting cylinder (52).
6. The rapid emulsification and dispersion device for processing binaphthol as claimed in claim 5, wherein the material injection mechanism (6) comprises:
the material injection mechanism shell (61) is arranged at the top end of the platform (1) through a bracket;
the number of the liquid storage tanks (62) is two, the two liquid storage tanks (62) are respectively arranged at the left end and the right end of the rear side of the inner cavity of the material injection mechanism shell (61), and liquid inlets at the top ends of the two liquid storage tanks (62) are respectively connected with a liquid outlet pipe of the pump station (7);
the quantity of the three-way electromagnetic valves (63) is two, the two three-way electromagnetic valves (63) are respectively arranged at the left end and the right end of the front side of the bottom end of the material injection mechanism shell (61), liquid inlet holes of the two three-way electromagnetic valves (63) are respectively connected with liquid outlets of the left liquid storage tank (62) and the right liquid storage tank (62) through guide pipes, and the three-way electromagnetic valves (63) are electrically connected with the controller (2);
the number of the telescopic connecting pipes (64) is two, and the two telescopic connecting pipes (64) are respectively arranged at liquid outlets at the bottom of the three-way electromagnetic valve (63);
the number of the pressure storage tanks (65) is two, and the two pressure storage tanks (65) are respectively arranged at the left end and the right end of the front side of the inner cavity of the material injection mechanism shell (61);
the number of the electromagnetic valves (66) is two, the two electromagnetic valves (66) are respectively embedded in the middle of the inner cavities of the left pressure storage tank (65) and the right pressure storage tank (65), and the electromagnetic valves (66) are electrically connected with the controller (2);
the air pump (67) is arranged at the bottom end of the inner cavity of the material injection mechanism shell (61), and the air pump (67) is electrically connected with the controller (2).
7. The rapid emulsifying and dispersing device for processing binaphthol as claimed in claim 6, wherein the outlet of the air pump (67) is connected to the top ends of the upper and lower portions of the left and right pressurized storage tanks (65) whose inner chambers are partitioned by the electromagnetic valve (66).
8. The dispersing process of the rapid emulsifying and dispersing device for processing binaphthol according to claim 7, which is characterized by comprising the following steps:
the method comprises the following steps: a worker fills base materials into the container mechanism (5) in advance, the container mechanism (5) is hoisted to the inner side of the clamp holder (3), the clamp holder (3) clamps the storage barrel (51) at the top of the bottom dispersion mechanism box body (41), the telescopic connecting pipe (64) is connected with the liquid inlet valves (56) on the two sides, the controller (2) starts the pump station (7), and the filler is respectively injected into the liquid storage tank (62) through the pump station (7), so that the pre-filling of the filler is realized;
step two: the lifting module (43) drives the driving module (44) to move upwards, the top sealing cylinder (45) enables the sealing seat (53) to move upwards from the inner side of the connecting cylinder (52) to the top under the matching of the second magnetic sucker (55), and the bottom sealing cylinder (45) seals the inner cavity of the connecting cylinder (52);
step three: the driving module (44) drives the dispersion disc (47) to rotate inside the storage barrel (51) so as to emulsify and disperse materials inside the storage barrel (51):
step four: compressed air is filled into the upper side and the lower side of an inner cavity of the pressure storage tank (65) by an air pump (67) through an air outlet pipe, the compressed air at the bottom of the pressure storage tank (65) enters the storage barrel (51) through a three-way electromagnetic valve (63), a telescopic connecting pipe (64) and a liquid inlet valve (56), and a steel wire in the wire coiling and uncoiling module (59) is uncoiled, so that the cone (58) is pushed by the compressed air to be downwards inserted into the liquid level of the base material in the storage barrel (51);
step five: the pre-filled filler in the liquid storage tank (62) enters the three-way electromagnetic valve (63), the pressure air at the top of the inner cavity of the pressure storage tank (65) pushes the filler to be injected into the storage barrel (51), and the filler is enabled to penetrate into the bottom of the liquid level of the feeding material along the liquid level gap of the base material instantaneously broken by the cone (58) under the action of the compressed air, so that the filler and the base material are more easily dispersed by the dispersion disc (47) at the bottom of the base material;
step six: after emulsification is finished, a wire coiling and uncoiling module (59) winds steel wires in the wire coiling and uncoiling module to enable a cone (58) to be attracted and fixed by an upper magnetic ring (57) at a corresponding position to reset the cone (58), a lifting module (43) is shortened to enable a driving module (44) to drive upper and lower sealing cylinders (45) to move downwards out of a connecting cylinder (52) in sequence, a top sealing cylinder (45) is enabled to be matched with a first magnetic sucker (46) and a second magnetic sucker (55) to enable a sealing seat (53) to be inserted downwards to the top of the connecting cylinder (52) again, a sealing ring (54) is enabled to seal a connecting gap between the sealing seat (53) and the connecting cylinder (52), further bottom sealing of a storage barrel (51) is achieved, and a container mechanism (5) can be taken out of a clamp holder (3);
step seven: the liquid brought out by the sealing barrel (45) enters the funnel (42) and enters the liquid storage box (48) through a pipeline below the funnel (42), and a worker can control the pressurizing pump (49) to discharge the liquid collected in the liquid storage box (48) through the liquid discharge valve (410) for treatment through the controller (2).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211276663.7A CN115350623A (en) | 2022-10-19 | 2022-10-19 | Rapid emulsification and dispersion device and process for binaphthol processing |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202211276663.7A CN115350623A (en) | 2022-10-19 | 2022-10-19 | Rapid emulsification and dispersion device and process for binaphthol processing |
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| CN114471211A (en) * | 2022-01-24 | 2022-05-13 | 黑龙江中医药大学 | Preparation device and method of traditional Chinese medicine shampoo for conditioning scalp psoriasis |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107261930A (en) * | 2017-06-27 | 2017-10-20 | 台山市兰宝磨具有限公司 | A kind of powder crushes charging mixing arrangement |
| CN109261049A (en) * | 2018-10-29 | 2019-01-25 | 南京高正农用化工有限公司 | Agriculture chemical compounding mixing arrangement |
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