CN115327015A - Continuous light hydrocarbon chromatographic analysis method, system, computer equipment and computer readable storage medium - Google Patents

Continuous light hydrocarbon chromatographic analysis method, system, computer equipment and computer readable storage medium Download PDF

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CN115327015A
CN115327015A CN202210874394.8A CN202210874394A CN115327015A CN 115327015 A CN115327015 A CN 115327015A CN 202210874394 A CN202210874394 A CN 202210874394A CN 115327015 A CN115327015 A CN 115327015A
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宋晓晟
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SHANGHAI OUSHEN TECHNOLOGY CO LTD
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SHANGHAI OUSHEN TECHNOLOGY CO LTD
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    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/88Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/88Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G01N2030/884Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds
    • G01N2030/8854Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds involving hydrocarbons

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Abstract

The application relates to a continuous light hydrocarbon chromatographic analysis method, a system, computer equipment and a computer readable storage medium, which relate to the technical field of light hydrocarbon analysis and comprise the following steps: obtaining pure sample gas, obtaining collected sample gas, purifying and distributing the collected sample gas to form pure sample gas, and outputting the pure sample gas; separating pure sample gas, namely separating the pure sample gas through a chromatographic column to obtain and output various monomer hydrocarbon gases; identifying the monomer hydrocarbon, namely mixing the monomer hydrocarbon gas with a preset gas, outputting a mixed gas, identifying data of the mixed gas, and outputting the data of the mixed gas; analyzing the monomer hydrocarbon, periodically acquiring data of the mixed gas, and analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; determining sample data, acquiring the peak-out time of the monomer hydrocarbon from the sample data and outputting, and analyzing and outputting peak data according to the peak-out time. This application has the effect of carrying out the analysis to the lighter hydrocarbons in the oil well in real time.

Description

Continuous light hydrocarbon chromatographic analysis method, system, computer equipment and computer readable storage medium
Technical Field
The present application relates to the field of light hydrocarbon analysis technologies, and in particular, to a continuous light hydrocarbon chromatography method, system, computer device, and computer-readable storage medium.
Background
Light hydrocarbons are important components of petroleum and natural gas. Light hydrocarbon mainly refers to 8 monomer hydrocarbons of C1-C8. The existing method for analyzing light hydrocarbon applied to oil gas exploration is generally carried back to a laboratory for analysis after field sampling, and the timeliness of analysis cannot be guaranteed.
With respect to the related art in the above, the inventors consider that: because the light hydrocarbon in the oil well is dynamically changed, the light hydrocarbon in the oil well needs to be analyzed in real time, and if the light hydrocarbon is taken back to a laboratory for analysis after sampling, the phenomenon of analysis lag easily occurs.
Disclosure of Invention
In order to analyze light hydrocarbons in an oil well in real time and obtain an analysis result in real time, the application provides a continuous light hydrocarbon chromatographic analysis method, a continuous light hydrocarbon chromatographic analysis system, computer equipment and a computer-readable storage medium.
In a first aspect, the continuous light hydrocarbon chromatographic analysis method provided by the application adopts the following technical scheme:
the continuous light hydrocarbon chromatographic analysis method comprises the following steps:
a pure sample gas obtaining step, namely obtaining collected sample gas, purifying and distributing the collected sample gas to form pure sample gas, and outputting the pure sample gas;
a pure sample gas separation step, wherein the pure sample gas is separated through a chromatographic column, and a plurality of monomer hydrocarbon gases are obtained and output;
a monomer hydrocarbon identification step, namely mixing a monomer hydrocarbon gas with a preset gas, outputting a mixed gas, identifying data of the mixed gas, and outputting the data of the mixed gas;
a monomer hydrocarbon analysis step, namely periodically acquiring data of the mixed gas, and analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas as sample data, acquiring and outputting the peak emergence time of the monomer hydrocarbon from the sample data, and analyzing and outputting peak data according to the peak emergence time.
By adopting the technical scheme, the data of the mixed gas is periodically acquired to form the data of periodically analyzing the mixed gas, so that the related data of the monomer hydrocarbon can be periodically output, and the aim of analyzing the monomer hydrocarbon in the oil well in real time is fulfilled.
Optionally, the pure sample gas obtaining step includes:
degassing, namely, after drilling fluid is obtained, outputting gas after the drilling fluid is treated by a degasser;
and a filtering step, namely receiving the gas output by the degasser, filtering the gas by a filter element to form a pure sample gas, and outputting the pure sample gas.
By adopting the technical scheme, the mixed gas contained in the drilling fluid is partially separated by the degasser, and the gas part is output, wherein substances such as mud and the like mainly comprising the weight of the drilling fluid are separated and discarded; then through filtering impurity among the gas part, form pure sample gas to this pure sample gas carries out the analysis as the sample gas of gathering, thereby can more accurately carry out the analysis to the gas in the well drilling, acquire data such as more accurate monomer hydrocarbon.
Optionally, the step of analyzing the monomeric hydrocarbon comprises:
acquiring a first group of mixed gas data, and analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; then determining retention time, and obtaining and outputting the peak-out time of the monomer hydrocarbon within the retention time;
after the first group of mixed gas data is analyzed and an analysis result is output, acquiring a second group of mixed gas data, and analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; and then determining the retention time, and acquiring and outputting the peak time of the monomer hydrocarbon within the retention time.
By adopting the technical scheme, the gas analysis time is close to the cycle time of the mixed gas acquisition, so that after the first group of mixed gas data is analyzed, the data of the second mixed gas is analyzed, the same data analysis equipment can be adopted, the cost is reduced, and the difference of different equipment in mixed gas data analysis is reduced.
Optionally, in the two groups of mixed gases, the proportion of the pure sample gas to the set gas is different.
By adopting the technical scheme, the sample gas with different concentrations can be obtained, the analysis of various monomer hydrocarbons is biased, and the analysis data can be more accurate.
Optionally, the step of identifying the monomeric hydrocarbon comprises:
a step of obtaining mixed gas, in which pure sample gas is mixed with hydrogen, and then the mixture is ignited and combusted under the combustion supporting of air to generate and output new gas;
and identifying new gas, acquiring new gas generated by combustion, and identifying the data of the monomer hydrocarbon through an identifier.
By adopting the technical scheme, the obtained pure gas is mixed with combustion-supporting materials such as hydrogen, air and the like and then ignited, so that the mixed gas is combusted, new gas is generated, the generated new gas is subjected to component analysis through the identifier, and data is obtained.
Optionally, the pure sample gas separation step includes:
dividing the pure sample gas into two parts, separating the gas through two chromatographic columns respectively, and outputting the separated gas respectively;
the monomer hydrocarbon identification step is used for identifying the gases output by the two chromatographic columns respectively and outputting data of two groups of mixed gases;
and the monomer hydrocarbon analysis step periodically acquires data of two groups of mixed gases, and analyzes and outputs the data.
Through adopting above-mentioned technical scheme, through being divided into two parts with the pure sample gas of same time collection, can be when the analysis monomer hydrocarbon, periodically gather two sets of mist's data respectively, then analyze, twice analysis can be partial to some extent to ensure accuracy, high efficiency and the integrality of data.
In a second aspect, the continuous light hydrocarbon chromatographic analysis system provided by the application adopts the following technical scheme:
the continuous light hydrocarbon chromatographic analysis system is applied to the continuous light hydrocarbon chromatographic analysis method and comprises the following steps:
the pure sample gas acquisition module is used for acquiring the collected sample gas, purifying and distributing the collected sample gas to form pure sample gas and outputting the pure sample gas;
the pure sample gas separation module is used for separating the pure sample gas to obtain and output a plurality of monomer hydrocarbon gases;
the monomer hydrocarbon identification module is used for mixing the monomer hydrocarbon gas with preset gas, outputting mixed gas, identifying data of the mixed gas and outputting the data of the mixed gas;
the monomer hydrocarbon analysis module periodically acquires data of the mixed gas and analyzes and determines the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas as sample data, acquiring and outputting the peak emergence time of the monomer hydrocarbon from the sample data, and analyzing and outputting peak data according to the peak emergence time.
By adopting the technical scheme, the data of the mixed gas are periodically acquired to form the data of periodically analyzing the mixed gas, so that the related data of the monomer hydrocarbon can be periodically output, and the aim of analyzing the monomer hydrocarbon in the oil well in real time is fulfilled.
In a third aspect, the present application provides a computer device, which adopts the following technical solution:
a computer device comprising a memory and a processor, the memory having stored thereon a computer program which can be loaded by the processor and which performs the above-mentioned method.
By adopting the technical scheme, the intelligent terminal is used, the data of the mixed gas are periodically acquired, and the data of the mixed gas are periodically analyzed, so that the relevant data of the monomer hydrocarbon can be periodically output, and the aim of analyzing the monomer hydrocarbon in the oil well in real time is fulfilled.
In a fourth aspect, the present application provides a computer-readable storage medium, which adopts the following technical solutions:
a computer-readable storage medium storing a computer program that can be loaded by a processor and executes the above-mentioned method.
By adopting the technical scheme, the storage medium is provided with the computer program of the fire-based fire extinguisher selection method, and the data of the mixed gas is periodically acquired to form the data of the periodically analyzed mixed gas, so that the related data of the monomer hydrocarbon can be periodically output, and the aim of analyzing the monomer hydrocarbon in the oil well in real time is fulfilled.
In summary, the present application includes at least one of the following beneficial technical effects:
1. the data of the mixed gas is periodically acquired to form data for periodically analyzing the mixed gas, so that the related data of the monomer hydrocarbon can be periodically output, and the aim of analyzing the monomer hydrocarbon in the oil well in real time is fulfilled;
2. the pure sample gas collected at the same time is divided into two parts, so that the data of two groups of mixed gas can be periodically and respectively collected when the monomer hydrocarbon is analyzed, and then the analysis is carried out, and the two analyses can be biased, so that the accuracy, the high efficiency and the integrity of the data are ensured;
3. the time of gas analysis is close to the cycle time of mixed gas acquisition, so that after the data of the first group of mixed gas is analyzed, the data of the second mixed gas is analyzed, the same data analysis equipment can be adopted, the cost is reduced, and the difference of different equipment in mixed gas data analysis is reduced.
Drawings
FIG. 1 is a schematic representation of the steps of a continuous light hydrocarbon chromatographic method according to an embodiment of the present application;
FIG. 2 is a schematic diagram of the continuous light hydrocarbon chromatographic analysis system according to an embodiment of the present application;
FIG. 3 is a schematic interface diagram of a monomeric hydrocarbon analysis module of a continuous light hydrocarbon chromatography system according to an embodiment of the present application;
fig. 4 is a schematic structural diagram of a computer device according to an embodiment of the present application.
In the figure, 1, a pure sample gas acquisition module; 2. a pure sample gas separation module; 3. a monomeric hydrocarbon identification module; 4. a monomeric hydrocarbon analysis module.
Detailed Description
The present application is described in further detail below with reference to fig. 1-4.
In order to accurately find the condition of an oil well and provide effective information for workers to find a water flooded layer and evaluate the oil and gas properties in time for the possibility of oil and gas containing in a logging abnormal well section, the water-bearing property of a reservoir and the degree of secondary oxidative bacterial degradation of hydrocarbons, and the like, in the related technology, the C1-C5 monomeric hydrocarbon is explored, and the related data of the C6-C8 monomeric hydrocarbon is developed, wherein the related data comprises the components and the proportion of the C6-C8 monomeric hydrocarbon and the parameters and indexes formed by combining the data.
Therefore, the application provides a continuous light hydrocarbon chromatographic analysis method, which can be used for identifying and analyzing C6-C8 monomer hydrocarbon existing in an oil well, can quickly and periodically provide effective C6-C8 related data, and is convenient for workers to check information of the current well section of the oil well.
The embodiment of the application discloses a continuous light hydrocarbon chromatographic analysis method, which comprises the following steps with reference to fig. 1:
s100: and obtaining a pure sample gas.
The pure sample gas refers to a pure gas from which impurities are removed. In the embodiment of the application, the sample gas in the oil well needs to be collected firstly, and then the collected sample gas is subjected to purification treatment and distribution. The purification treatment is to form pure sample gas from the collected sample gas and then output the pure sample gas. Dispensing is understood here to mean dividing the purified sample gas into a plurality of portions for subsequent processing.
S200: and (5) a pure sample gas separation step.
Because the gas composition in the oil well is more, and the analysis is mainly used for obtaining the composition ratio of C5-C8 in the sample gas, the separation is needed. In the embodiment of the application, a chromatographic column is used for separating pure sample gas, and a plurality of monomer hydrocarbon gases are obtained and output.
The various monomeric hydrocarbon gases, C1-C5 monomeric hydrocarbons, separated here can be analyzed by other prior art equipment and the results exported, while the C6-C8 monomeric hydrocarbons need to be processed before further analysis.
S300: and (4) identifying the monomer hydrocarbon.
In order to analyze the components, the proportion and other related data of the monomer hydrocarbon more quickly, the step is to output mixed gas after mixing the monomer hydrocarbon gas with preset gas in a real-time process; and then identifying the data of the mixed gas, outputting the data of the mixed gas, and simultaneously outputting various combined parameters, indexes and the like, thereby facilitating the analysis of the next step.
S400: and (4) analyzing the monomer hydrocarbon.
This step first requires the acquisition of the plurality of data generated and output in step S300, followed by analysis.
Since the time required for the identification step of the monomer hydrocarbon is long, in order to realize the periodic output data of 60S, in the embodiment of the present application, when the analysis is performed in step S400, the next group of mixed gas is subjected to the identification of the monomer hydrocarbon in step S300, so that the time for outputting the analysis data can be saved, and the periodic output data can be formed.
When data of the mixed gas is periodically acquired, the peak height, the minimum peak area and the minimum fluctuation of the mixed gas need to be analyzed and determined. And then determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas as sample data, acquiring and outputting the peak time of the monomer hydrocarbon from the sample data, and analyzing and outputting the peak data according to the peak time.
Further, the specific steps of S100 are as follows:
s101: and (4) degassing. Since the gas in the well is contaminated with various impurities and some other gas not intended to be detected in this application, etc., after the drilling fluid has been obtained, it is common to treat the obtained drilling fluid via a degasser, which outputs the gas after the treatment. It is to be understood that the gas output here comprises mainly monomeric hydrocarbon gas as well as part of the other gases, i.e. the gas after the preliminary treatment is obtained in this case.
S102: and (5) filtering. The degasser outputs gas, inputs the gas into the filter element, forms pure sample gas after filtering the gas by the filter element, and outputs the pure sample gas.
It should be understood that the filter element described herein may be one of a variety of gas filters, and in particular, may be used by those skilled in the art with the appropriate filter element selected for the actual filtering needs, as is well known in the art.
The step S300 comprises the following steps:
s301: and acquiring mixed gas.
Mixing pure sample gas with hydrogen, igniting and burning under the combustion supporting of air and other gases, and generating and outputting new gas in the burning process. Wherein, hydrogen is the setting gas set in the embodiment of the application, and the technicians in the field can also set according to the detection requirements.
The step of mixing the pure sample gas and the hydrogen comprises the step of mixing two parts of pure sample gas with the hydrogen respectively, wherein the proportion of the two mixed gases is different, so that the output related data is not completely the same, the subsequent identification and analysis steps are more convenient, and the analysis data can be more comprehensively obtained.
S302: and identifying new gas.
The new gases generated by combustion were obtained and the data for the monomeric hydrocarbons identified by the identifier in the examples of this application. It should be understood that the data of the monomeric hydrocarbon as used herein only refers to information such as the ratio of the individual monomeric hydrocarbons. Authentication by an authenticator is also a well known technique to those skilled in the art and will not be described in detail here.
S400 comprises the following specific steps:
s401: a first set of mixed gas data is acquired.
Because two groups of components are set for analysis when identifying gas composition data, one group is firstly used for analysis. The analysis here consists essentially of determining the peak height, minimum peak area and minimum fluctuation of the mixed gas. And then determining the retention time, and acquiring and outputting the peak-appearing time of the monomer hydrocarbon within the retention time so as to obtain the relevant data of the monomer hydrocarbon.
S402: a second set of mixed gas data is acquired.
After the first group of mixed gas data is analyzed and an analysis result is output, acquiring a second group of mixed gas data, analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas in the same way as the first group of mixed gas data; and determining the retention time, and acquiring and outputting the peak time of the monomer hydrocarbon within the retention time.
It is noted that, in general, a time required from the identification of one set of data to the analysis of the data is about 120s, and in order to form a 60s cycle, the first set of mixed gas is subjected to 60s before the identification and analysis of the second set of data is started. The periodic collection, separation, identification and analysis are carried out by taking the cycle as a period.
More importantly, the collection and the data identification analysis are separately performed, namely, the collection is performed by the lower computer, and the data identification analysis is performed by the upper computer, so that the collection and the data identification analysis can be performed independently, and the aim of periodically outputting identification analysis data can be conveniently fulfilled.
The upper computer and the lower computer can be connected by a communication line, such as a communication line adopted by a communication protocol such as RS 485. In the host computer of this application, can also insert the output interface of other analytic data, be convenient for more detailed analysis.
The implementation principle of the embodiment of the application is as follows: the data of the mixed gas are periodically acquired to form the data of periodically analyzing the mixed gas, so that the related data of the monomer hydrocarbon can be periodically output, and the aim of analyzing the monomer hydrocarbon in the oil well in real time is fulfilled.
The embodiment of the application also discloses a continuous light hydrocarbon chromatographic analysis system, which is applied to the continuous light hydrocarbon chromatographic analysis method, and the system is referred to fig. 2, and comprises a pure sample gas acquisition module 1, a pure sample gas separation module 2, a monomer hydrocarbon identification module 3 and a monomer hydrocarbon analysis module 4.
The pure sample gas acquisition module 1 is used for acquiring the collected sample gas and outputting the pure sample gas. Wherein gather sample gas, can set up to common sampling tool or well drilling tool in this application embodiment, this application does not improve because can select by the present technical staff style of calligraphy, only need can export sample gas can.
And then outputting the sample gas for purification treatment and distribution to form pure sample gas and outputting the pure sample gas. Here, the treatment can be carried out by degassers and filters and a pure sample gas is output.
Pure sample gas separation module 2 is used for separating pure sample gas, can set up to the chromatographic column in this application embodiment for obtain and output multiple monomer hydrocarbon gas, and separate C1-C5 monomer hydrocarbon and C6-C8 monomer hydrocarbon, this application mainly carries out the analysis to C6-C8 monomer hydrocarbon.
It should be noted that the pure sample gas acquisition module 1 and the pure sample gas separation module 2 are both arranged as a lower computer, that is to say, can be arranged on site, and are convenient for rapidly acquiring pure sample gas and performing necessary separation.
The monomer hydrocarbon identification module 3 is used for mixing the monomer hydrocarbon gas with a preset gas to output a mixed gas, identifying data of the mixed gas, and outputting the data of the mixed gas, and can be actually implemented by an identifier, which is also well known by the technology of the person skilled in the art.
Referring to fig. 2 and 3, the monomer hydrocarbon analysis module 4 periodically obtains data of the mixed gas, which may be implemented in a software manner in the embodiment of the present application, and can achieve the purpose of analyzing and determining the peak height, the minimum peak area, and the minimum fluctuation of the mixed gas.
In the analysis process, the determined peak height, the minimum peak area and the minimum fluctuation of the mixed gas are used as sample data, the peak emergence time of the monomer hydrocarbon is obtained from the sample data and output, and the peak data is analyzed and output according to the peak emergence time, so that the related data of the sample gas is output.
It should be noted that the single hydrocarbon identification module 3 and the single hydrocarbon analysis module 4 are both arranged as an upper computer and are respectively arranged with a lower computer mainly used for collection to form two independent parts, which do not interfere with each other, so that collection and data identification and analysis can be respectively and independently performed, and therefore, the purpose of periodically outputting identification and analysis data can be conveniently realized.
The upper computer and the lower computer can be connected by a communication line, such as a communication line adopted by a communication protocol such as RS 485.
The implementation principle of the embodiment of the application is as follows: the data of the mixed gas are periodically acquired to form the data of periodically analyzing the mixed gas, so that the related data of the monomer hydrocarbon can be periodically output, and the aim of analyzing the monomer hydrocarbon in the oil well in real time is fulfilled.
The embodiment of the application also discloses computer equipment.
Those skilled in the art will appreciate that the configuration shown in fig. 4 is a block diagram of only a portion of the configuration associated with the present application and does not constitute a limitation on the devices to which the present application applies, and that a particular device may include more or less components than those shown, or may combine certain components, or have a different arrangement of components.
The apparatus comprises a memory in which the computer program is stored and a processor which, when executing the computer program, carries out the steps in the method embodiments described above.
The embodiment of the application also discloses a computer readable storage medium, which stores a computer program, and the computer program realizes the steps in the above method embodiments when being executed by a processor.
It will be understood by those skilled in the art that all or part of the processes of the methods of the embodiments described above can be implemented by hardware instructions of a computer program, which can be stored in a non-volatile computer-readable storage medium, and when executed, can include the processes of the embodiments of the methods described above. Any reference to memory, storage, database or other medium used in the embodiments provided herein can include at least one of non-volatile and volatile memory. Non-volatile Memory may include Read-Only Memory (ROM), magnetic tape, floppy disk, flash Memory, optical storage, or the like. Volatile Memory can include Random Access Memory (RAM) or external cache Memory. By way of illustration and not limitation, RAM can take many forms, such as Static Random Access Memory (SRAM) or Dynamic Random Access Memory (DRAM), for example. The embodiments of the present invention are preferred embodiments of the present application, and the protection scope of the present application is not limited thereby, wherein like parts are denoted by like reference numerals. Therefore, the method comprises the following steps: all equivalent changes made according to the structure, shape and principle of the present application shall be covered by the protection scope of the present application.

Claims (9)

1. The continuous light hydrocarbon chromatographic analysis method is characterized by comprising the following steps:
a pure sample gas obtaining step, namely obtaining collected sample gas, purifying and distributing the collected sample gas to form pure sample gas, and outputting the pure sample gas;
a pure sample gas separation step, wherein the pure sample gas is separated through a chromatographic column, and a plurality of monomer hydrocarbon gases are obtained and output;
a monomer hydrocarbon identification step, namely mixing a monomer hydrocarbon gas with a preset gas, outputting a mixed gas, identifying data of the mixed gas, and outputting the data of the mixed gas;
a monomer hydrocarbon analysis step, namely periodically acquiring data of the mixed gas, and analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas as sample data, acquiring and outputting the peak time of the monomer hydrocarbon from the sample data, and analyzing and outputting the peak data according to the peak time.
2. The continuous light hydrocarbon chromatographic analysis method according to claim 1, wherein the pure sample gas obtaining step comprises:
a degassing step, namely, after the drilling fluid is obtained, gas is output after the drilling fluid is treated by a degasser;
and a filtering step, namely receiving the gas output by the degasser, filtering the gas by a filtering piece to form a pure sample gas, and outputting the pure sample gas.
3. The continuous light hydrocarbon chromatographic analysis method according to claim 2, wherein the monomeric hydrocarbon analysis step comprises:
acquiring a first group of mixed gas data, and analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; then determining retention time, and obtaining and outputting the peak-out time of the monomer hydrocarbon within the retention time;
after the first group of mixed gas data is analyzed and the analysis result is output, acquiring a second group of mixed gas data, and analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; and then determining the retention time, and acquiring and outputting the peak time of the monomer hydrocarbon within the retention time.
4. The continuous light hydrocarbon chromatographic analysis method according to claim 3, wherein the ratio of the pure sample gas to the set gas in the two groups of mixed gas is different.
5. The continuous light hydrocarbon chromatographic analysis method according to claim 2, wherein the step of identifying the monomeric hydrocarbon comprises:
a step of obtaining mixed gas, in which pure sample gas is mixed with hydrogen, and then is ignited and combusted under the combustion supporting of air to generate and output new gas;
and identifying new gas, acquiring new gas generated by combustion, and identifying the data of the monomer hydrocarbon through an identifier.
6. The continuous light hydrocarbon chromatographic analysis method of claim 1,
the pure sample gas separation step comprises the following steps:
dividing the pure sample gas into two parts, separating the gas through two chromatographic columns respectively, and outputting the separated gas;
the monomer hydrocarbon identification step is used for identifying the gases output by the two chromatographic columns respectively and outputting data of two groups of mixed gases;
and the monomer hydrocarbon analysis step periodically acquires data of the two groups of mixed gases, and analyzes and outputs the data.
7. A continuous light hydrocarbon chromatographic analysis system for use in the continuous light hydrocarbon chromatographic analysis method according to any one of claims 1 to 6, comprising:
the pure sample gas acquisition module (1) is used for acquiring the collected sample gas, purifying and distributing the collected sample gas to form pure sample gas and outputting the pure sample gas;
the pure sample gas separation module (2) is used for separating the pure sample gas to obtain and output a plurality of monomer hydrocarbon gases;
the monomer hydrocarbon identification module (3) is used for outputting mixed gas after mixing the monomer hydrocarbon gas with preset gas, identifying the data of the mixed gas and outputting the data of the mixed gas;
the monomer hydrocarbon analysis module (4) is used for periodically acquiring data of the mixed gas and analyzing and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas; and determining the peak height, the minimum peak area and the minimum fluctuation of the mixed gas as sample data, acquiring and outputting the peak emergence time of the monomer hydrocarbon from the sample data, and analyzing and outputting peak data according to the peak emergence time.
8. A computer device comprising a memory and a processor, the memory having stored thereon a computer program which can be loaded by the processor and which executes the method according to any one of claims 1 to 6.
9. A computer-readable storage medium, in which a computer program is stored which can be loaded by a processor and which executes the method of any one of claims 1 to 6.
CN202210874394.8A 2022-07-23 2022-07-23 Continuous light hydrocarbon chromatographic analysis method, system, computer equipment and computer readable storage medium Pending CN115327015A (en)

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