CN115318083A - Tail gas purification processing system of dichlorophenol production - Google Patents

Tail gas purification processing system of dichlorophenol production Download PDF

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Publication number
CN115318083A
CN115318083A CN202210830365.1A CN202210830365A CN115318083A CN 115318083 A CN115318083 A CN 115318083A CN 202210830365 A CN202210830365 A CN 202210830365A CN 115318083 A CN115318083 A CN 115318083A
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fixed mounting
tail gas
air
water treatment
air duct
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袁娇
朱席
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Individual
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/77Liquid phase processes
    • B01D53/78Liquid phase processes with gas-liquid contact
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/46Removing components of defined structure
    • B01D53/68Halogens or halogen compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B9/00Cleaning hollow articles by methods or apparatus specially adapted thereto 
    • B08B9/08Cleaning containers, e.g. tanks
    • B08B9/0804Cleaning containers having tubular shape, e.g. casks, barrels, drums
    • B08B9/0808Cleaning containers having tubular shape, e.g. casks, barrels, drums by methods involving the use of tools, e.g. by brushes, scrapers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/20Halogens or halogen compounds
    • B01D2257/202Single element halogens
    • B01D2257/2025Chlorine
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2258/00Sources of waste gases
    • B01D2258/02Other waste gases

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mechanical Engineering (AREA)
  • Gas Separation By Absorption (AREA)

Abstract

The invention relates to the technical field of chemical processes, in particular to a tail gas purification treatment system for dichlorophenol production, which comprises a base, a water treatment tank fixedly arranged at the upper end of the base, a tank cover hinged on the water treatment tank, an air inlet arranged in the tank cover, and a transition tank fixedly arranged at the upper end of the base; the upper cavity and the lower cavity are arranged inside the water treatment tank; the air guide mechanism is arranged inside the water treatment tank. According to the invention, through arranging the lower cavity, the air guide tube, the air guide port and other mechanisms, tail gas enters the upper cavity from the air inlet, is guided into the air guide tube from the air guide port under the flow guidance of the flow guidance equipment, the tail gas in the air guide tube is sprayed into water from the spray head through the air pipe at the lower end, the air guide tube rotates under the action of the driving equipment, and the tail gas in the air guide tube diffuses to the periphery of the water, so that the contact area of the tail gas and the water is increased, and the quick absorption of the tail gas is realized.

Description

Tail gas purification processing system of dichlorophenol production
Technical Field
The invention relates to the technical field of chemical processes, in particular to a tail gas purification treatment system for dichlorophenol production.
Background
Diclofenac sodium is a third-generation non-steroidal potent anti-inflammatory analgesic, and is clinically used for various rheumatic arthritis, postoperative pain, fever caused by various reasons, and the like. The existing diclofenac sodium is prepared by the following steps: the method comprises the steps of preparing dichlorophenol by taking cyclohexanone as a raw material, preparing diphenylamine by taking dichlorophenol as a raw material and preparing diclofenac sodium by taking diphenylamine as a raw material, wherein the preparation of dichlorophenol by taking cyclohexanone as a raw material is an important ring.
The method for preparing dichlorophenol by taking cyclohexanone as a raw material mostly adopts the steps of introducing chlorine into the cyclohexanone in a chlorination reaction kettle to produce tetrachloro cyclic ketone, and then heating and decomposing the tetrachloro cyclic ketone into dichlorophenol in a dehydrochlorination reaction kettle, so that more acidic waste gas can be generated in the process, most of chlorine gas and hydrogen chloride gas cannot be directly discharged into air, the environment can be seriously polluted, and the serious waste of resources can be caused. In the prior art, generally, the tail gas is cleaned by adopting solvents such as dilute hydrochloric acid after being treated by water, and finally, an alkaline solution is utilized for final absorption treatment.
Therefore, a tail gas purification treatment system for dichlorophenol production is provided.
Disclosure of Invention
The invention aims to provide a tail gas purification treatment system for dichlorophenol production, which aims to solve the problem of insufficient absorption in the water treatment of the tail gas produced by dichlorophenol in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a tail gas purification treatment system for dichlorophenol production comprises a base, a water treatment tank fixedly mounted at the upper end of the base, a tank cover hinged on the water treatment tank, an air inlet arranged in the tank cover, and a transition tank fixedly mounted at the upper end of the base; the upper cavity and the lower cavity are arranged inside the water treatment tank; the air guide mechanism is arranged in the water treatment tank.
Preferably, the air guide mechanism is including rotating the air duct of installing on the lower chamber roof, set up the air guide mouth that two symmetries set up on the lateral wall of air duct upper end, the lower extreme fixed mounting of air duct has the gas-supply pipe that several symmetries set up, several fixed mounting has a plurality of shower nozzles on the lateral wall of gas-supply pipe.
Through setting up mechanisms such as cavity of resorption, air duct, air guide port, tail gas gets into the epicoele from the air inlet, in the leading-in air duct of follow-up air guide port under the water conservancy diversion of water conservancy diversion equipment, tail gas in the air duct is spouted to aquatic by the shower nozzle at the gas-supply pipe through the lower extreme, and at drive arrangement, motor, actuating lever subassembly effect down the air duct is rotary motion promptly, and tail gas in the air duct is to the diffusion all around of water for tail gas and water's area of contact increase realizes the quick absorption to tail gas.
Preferably, the top fixed mounting of case lid has the motor, the mid-rotation of case lid installs the actuating lever, the output shaft of motor and the top fixed connection of actuating lever, the bottom of actuating lever and the top fixed connection of air duct, fixed mounting has the flabellum on the actuating lever, fixed mounting has the groove of gathering on the roof of lower chamber, the inside in the groove of gathering is located to the air guide mouth.
Through setting up mechanisms such as motor, actuating lever, flabellum, above-mentioned water conservancy diversion equipment is subassembly such as motor 12, actuating lever 13, flabellum 14, and the output shaft of motor drives the actuating lever and rotates after the starter motor, and the flabellum is rotary motion under the effect of actuating lever, and the flabellum forms the air current in the inside of epicoele, forms the negative pressure in the position that is close to the air inlet, and the tail gas that gets into from the air inlet flows down along with the air current, and tail gas gathers in gathering groove department to it is leading-in to the trachea to be accelerateed by the air guide mouth department.
Preferably, the middle part of the air duct is fixedly provided with a first crushing blade, the lower end of the air duct is fixedly provided with two fixing blocks, a second crushing blade is movably arranged between the two fixing blocks, and a first spring is fixedly connected between the two fixing blocks and the second crushing blade.
Through setting up first broken blade, the fixed block, mechanisms such as the broken blade of second, the air duct rotates under the drive of actuating lever, first broken blade on the air duct is rotatory along with the rotation of air duct, carry out the breakage to shower nozzle department spun tail gas bubble, make tail gas in the bubble can not be because of the isolation of bubble and water contact, the broken blade of second is blown the broken blade of second by the gas under the effect of bottom tail gas bubble when the broken blade of second follows the air duct pivoted, make reciprocating motion about the first spring, the contact of bubble and water accelerates.
Preferably, the inside fixed mounting of air duct has first dead lever, the upper end fixed mounting of first dead lever has the telescopic link, the flexible end fixed mounting of telescopic link has the piston, the second spring has been cup jointed on the telescopic link, and the both ends of second spring are fixed connection respectively on first dead lever and piston.
Through setting up first dead lever, the telescopic link, mechanisms such as piston, contain toxic gases such as chlorine in the tail gas, chlorine and water's reaction is reversible reaction, chlorine is very easily dissolved in water, chlorine in the air duct is after air duct end and water reaction, water is by the air duct end get into in the air duct, tail gas gets into in the air duct fast and makes all be full of chlorine in the whole air duct, water can flow back to in the epicoele, the piston is rebound under the ascending force effect of rivers, and form sealedly between the air duct inner wall, make tail gas can not get into the aquatic in the cavity of resorption, tail gas can not in time be handled.
Preferably, the upper end fixed mounting of base has the air pump, the gas transmission mouth end fixedly connected with intake pipe of air pump, the inside fixed mounting of intake pipe has the check valve, the terminal fixed mounting of gas transmission mouth of intake pipe is on the lateral wall of water treatment tank, the inside fixed mounting of water treatment tank has a plurality of heat-conducting plates, and is a plurality of the lateral wall of water treatment tank is run through to the one end of heat-conducting plate and extends to its outside, and is a plurality of equal fixed mounting has two fin on the lateral wall of heat-conducting plate.
Through setting up the air pump, the intake pipe, mechanisms such as heat-conducting plate, chlorine and water reaction are exothermic, get into the aquatic along with tail gas gradually, make the temperature increasingly high, along with the rising of temperature, the treatment effect of tail gas reduces, utilize numerical control among the prior art to make the air pump can be interrupted a few minutes after blowing in a period of cold air, prevent that the atmospheric pressure in the water treatment box is too big, the speed that the air pump blew the air is slower, after opening the air pump, the air pump blew external cold air into the cavity of water treatment box in, make the temperature in the cavity reduce, derive the temperature of aquatic under the effect of heat-conducting plate, fin on the heat-conducting plate makes the heat on the heat-conducting plate expand fast and scatter, the speed that the temperature reduces with higher speed.
Preferably, a conductive block and two second fixing rods are fixedly mounted on the top wall of the lower cavity, the two second fixing rods are respectively arranged on two sides of the conductive block, a floating ball is slidably mounted between the two second fixing rods, an alarm is fixedly mounted on one side of the water treatment tank, and the conductive block, the floating ball and the alarm are all electrically connected with a power supply through wires.
Through setting up mechanisms such as conducting block, second dead lever, floater, the aquatic is along with getting into gradually of tail gas, and the concentration of solution is higher and higher, and along with the increase of solution concentration, the buoyancy that the floater received is bigger and bigger, and the floater highly risees gradually in solution, and when floater and conducting block contacted each other, the circuit at here was put through, has the electric current to pass through in the siren, and the siren sends out the police dispatch newspaper, and the concentration of reminding the staff solution is too high, needs to change the water of handling tail gas.
Preferably, the opposite side fixed mounting of water treatment tank has the blast pipe, the terminal fixed mounting of blast pipe is in one side of transition box, the top fixed mounting of transition box has the muffler, the one end fixed mounting of muffler is at the opposite side of water treatment tank, rotate on the inner wall of transition box and install the pivot, fixed mounting has the impeller in the pivot, the port department of blast pipe is located to the impeller, fixed mounting has the worm wheel in the pivot, rotate on the diapire of transition box and install the worm, worm wheel and worm intermeshing.
Through arranging mechanisms such as an exhaust pipe, a gas return pipe and a rotating shaft, redundant tail gas in the lower cavity after water treatment rises to the position above the water surface, the tail gas in the transition box flows back into the upper cavity along with the air flow to be treated again by negative pressure formed in the upper cavity, the impeller rotates under the air flow formed by the exhaust pipe and the gas return pipe, the rotating shaft rotates under the driving of the impeller, the worm wheel on the rotating shaft rotates along with the rotation of the rotating shaft, the worm and the worm wheel are meshed with each other, the worm wheel rotates along with the rotation of the rotating shaft to drive subsequent equipment, after water treatment is completed, all working procedures are stopped, and the redundant tail gas flows into a subsequent existing alkali treatment device through an air outlet pipe on the side wall of the transition box to be treated.
Preferably, the top fixed mounting of worm has reciprocal lead screw, the top of reciprocal lead screw is rotated and is installed on the roof of transition case, the inside movable mounting of transition case has annular scraper blade, the inside fixed mounting of annular scraper blade has screw nut, screw nut cup joints on reciprocal lead screw.
Through setting up reciprocal lead screw, annular scraper blade, mechanism such as lead screw nut, reciprocal lead screw rotates under the drive of worm, reciprocating motion is to the lead screw nut who cup joints on the reciprocal lead screw, lead screw nut fixed mounting is in the inside of annular scraper blade, annular scraper blade is at the gag lever post of its upper end and the mutual block of spout on the transition incasement wall, can receive the restriction when making annular scraper blade rotatory under the interact of gag lever post and spout, thereby make annular scraper blade do reciprocating motion from top to bottom in the transition incasement, tail gas can have the drop of water to get into in the transition incasement after the aquatic by the way, tail gas drop of water on the annular scraper blade to the transition incasement wall strikes off, prevent to glue glutinous tail gas solution on the inner wall and volatilize the diffusion again after long-time.
Preferably, the air duct, the air delivery pipe and the nozzle are made of aluminum alloy.
The aluminum alloy has the characteristics of oxidation resistance and the like, so that the air guide pipe, the air delivery pipe and the spray head cannot be corroded due to acid solution generated by dissolving tail gas in water, and the service life of the air guide pipe, the air delivery pipe and the spray head is prolonged.
Compared with the prior art, the invention has the following beneficial effects:
1. through setting up mechanisms such as cavity of resorption, air duct, air guide port, tail gas gets into the epicoele from the air inlet, in the leading-in air duct of air guide port under the water conservancy diversion of water conservancy diversion equipment, tail gas in the air duct is spouted to aquatic by the shower nozzle through the gas-supply pipe of lower extreme, and rotary motion is done to the air duct under drive arrangement's effect, and tail gas in the air duct is to the diffusion all around of water for the area of contact increase of tail gas and water realizes the quick absorption to tail gas.
2. Through setting up mechanisms such as motor, actuating lever, flabellum, the output shaft of motor drives the actuating lever and rotates behind the starter motor, and the flabellum is rotary motion under the effect of actuating lever, and the flabellum forms the air current in the inside of epicoele, forms the negative pressure in the position that is close to the air inlet, and the tail gas that gets into from the air inlet flows down along with the air current, and tail gas gathers in gathering groove department to it is leading-in to the air guide pipe to be accelerateed by air guide department.
3. Through setting up first broken blade, the fixed block, mechanisms such as the broken blade of second, the air duct rotates under the drive of actuating lever, first broken blade on the air duct is rotatory along with the rotation of air duct, carry out the breakage to shower nozzle department spun tail gas bubble, make tail gas in the bubble can not be because of the isolation of bubble and water contact, the broken blade of second is blown the broken blade of second by the gas under the effect of bottom tail gas bubble when the broken blade of second follows the air duct pivoted, make reciprocating motion about the first spring, the contact of bubble and water accelerates.
4. Through setting up mechanisms such as first dead lever, telescopic link, piston, contain toxic gases such as chlorine in the tail gas, chlorine and water's reaction is reversible reaction, and chlorine is very easily dissolved in water, and chlorine in the air duct is terminal after reacting with water at the air duct, and water is by the air duct terminal entering air duct in, and tail gas gets into in the air duct fast makes all be full of chlorine in the whole air duct, and water may flow back to in the epicoele for tail gas can not get into the aquatic in the cavity of resorption, and tail gas can not in time be handled.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a front cross-sectional view of the present invention;
FIG. 3 is a top cross-sectional view of the transition box of the present invention;
FIG. 4 is a sectional top view of the water treatment tank of the present invention;
FIG. 5 is an enlarged view of the structure at A in FIG. 2 according to the present invention;
FIG. 6 is an enlarged view of the structure of FIG. 2 at B in accordance with the present invention;
fig. 7 is an enlarged view of the structure at C in fig. 2 according to the present invention.
In the figure: 1. a base; 2. a water treatment tank; 3. a box cover; 4. an air inlet; 5. a transition box; 6. an upper chamber; 7. a lower cavity; 8. an air duct; 9. an air guide port; 10. a gas delivery pipe; 11. a spray head; 12. a motor; 13. a drive rod; 14. a fan blade; 15. a collecting groove; 16. a first crushing blade; 17. a fixed block; 18. a second crushing blade; 19. a first spring; 20. a first fixing lever; 21. a telescopic rod; 22. a piston; 23. a second spring; 24. an air pump; 25. an air inlet pipe; 26. a one-way valve; 27. a heat conducting plate; 28. a heat sink; 29. a conductive block; 30. a second fixing bar; 31. a floating ball; 32. an alarm; 33. an exhaust pipe; 34. an air return pipe; 35. a rotating shaft; 36. an impeller; 37. a worm gear; 38. a worm; 39. a reciprocating screw; 40. an annular brush plate; 41. a lead screw nut.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1 to 7, the present invention provides a system for purifying and treating tail gas from dichlorophenol production, which has the following technical scheme:
a tail gas purification treatment system for dichlorophenol production comprises a base 1, a water treatment tank 2 fixedly mounted at the upper end of the base 1, a tank cover 3 hinged on the water treatment tank 2, an air inlet 4 arranged in the tank cover 3, and a transition tank 5 fixedly mounted at the upper end of the base 1; an upper chamber 6 and a lower chamber 7 which are arranged inside the water treatment tank 2; and the air guide mechanism is arranged inside the water treatment tank 2.
As an embodiment of the present invention, referring to fig. 1, the air guide mechanism includes an air guide tube 8 rotatably installed on the top wall of the lower chamber 7, two symmetrically arranged air guide ports 9 are formed on the side wall of the upper end of the air guide tube 8, several symmetrically arranged air guide tubes 10 are fixedly installed at the lower end of the air guide tube 8, and a plurality of nozzles 11 are fixedly installed on the side walls of the air guide tubes 10.
Through setting up cavity of resorption 7, the air duct 8, lead mechanisms such as gas port 9, tail gas gets into in the epicoele 6 from air inlet 4, follow in leading-in air duct 8 of gas port 9 under the water conservancy diversion of follow-up water conservancy diversion equipment, tail gas in the air duct 8 is spouted to aquatic by shower nozzle 11 at the gas-supply pipe 10 through the lower extreme, at drive arrangement, motor 12 promptly, rotary motion is done to air duct 8 under the effect of the 13 subassemblies of actuating lever, tail gas in the air duct 8 is to diffusion all around of water, make the increase of tail gas and water area of contact, realize the quick absorption to tail gas, guarantee that tail gas fully receives the washing effect, and then guarantee that subsequent pickling and alkali wash process can go on smoothly.
Referring to fig. 1, the diversion apparatus according to an embodiment of the present invention includes a motor 12 fixedly mounted on the top of a case cover 3, a driving rod 13 rotatably mounted in the middle of the case cover 3, an output shaft of the motor 12 fixedly connected to the top end of the driving rod 13, a bottom end of the driving rod 13 fixedly connected to the top end of an air duct 8, a fan blade 14 fixedly mounted on the driving rod 13, a collecting groove 15 fixedly mounted on the top wall of a lower chamber 7, and an air duct 9 disposed inside the collecting groove 15.
Through setting up motor 12, actuating lever 13, flabellum 14 etc. mechanism, above-mentioned diversion equipment is motor 12, actuating lever 13, flabellum 14 etc. subassembly, the output shaft of motor 12 drives actuating lever 13 and rotates after motor 12 is started, flabellum 14 is rotary motion under the effect of actuating lever 13, flabellum 14 forms the air current in the inside of upper chamber 6, form the negative pressure in the position that is close to air inlet 4, tail gas that gets into from air inlet 4 flows down along with the air current, tail gas gathers in groove 15 department and gathers to lead in to the trachea 8 by leading the gas port 9 department with higher speed.
As an embodiment of the invention, referring to fig. 1, a first crushing blade 16 is fixedly installed in the middle of the air duct 8, two fixing blocks 17 are fixedly installed at the lower end of the air duct 8, a second crushing blade 18 is movably installed between the two fixing blocks 17, and a first spring 19 is fixedly connected between the two fixing blocks 17 and the second crushing blade 18.
Through setting up first broken blade 16, the fixed block 17, mechanisms such as the broken blade of second 18, air duct 8 rotates under the drive of actuating lever 13, first broken blade 16 on the air duct 8 is rotatory along with air duct 8's rotation, break 11 department spun tail gas bubbles of shower nozzle, make tail gas in the bubble can not be because of the isolation of bubble and water contact, the broken blade of second 18 follows air duct 8 pivoted while under the effect of bottom tail gas bubble and receive the broken blade of gas-blowing second 18, make first spring 19 reciprocating motion from top to bottom, the contact of bubble and water accelerates.
Referring to fig. 1, as an embodiment of the present invention, a first fixing rod 20 is fixedly installed inside the air duct 8, an expansion rod 21 is fixedly installed at an upper end of the first fixing rod 20, a piston 22 is fixedly installed at an expansion end of the expansion rod 21, a second spring 23 is sleeved on the expansion rod 21, and two ends of the second spring 23 are respectively fixedly connected to the first fixing rod 20 and the piston 22.
Because the tail gas contains toxic gases such as chlorine and the like, the reaction of the chlorine and the water is a reversible reaction, when the tail gas is introduced, the flow is small, the chlorine is very soluble in water, the chlorine in the gas guide tube 8 can possibly react with the water at the tail end of the gas guide tube 8, the water enters the gas guide tube 8 from the tail end of the gas guide tube 8, and the tail gas quickly enters the gas guide tube 8 and even enters the upper cavity 6; therefore, by arranging the first fixing rod 20, the telescopic rod 21, the piston 22 and other mechanisms, when water may flow back into the upper chamber 6, the piston 22 moves upwards under the action of the ascending force of water flow and forms a seal with the inner wall of the air duct 8, so that the air duct 8 is closed, and the situation of water backflow is avoided; until a large amount of tail gas enters, the piston 22 moves downwards under the action of air pressure, the air duct 8 is sealed and removed, and the tail gas enters the water in the lower cavity 7 in a large amount and is fully washed.
Referring to fig. 1, an air pump 24 is fixedly mounted at the upper end of a base 1, an air inlet pipe 25 is fixedly connected to an air delivery port end of the air pump 24, a check valve 26 is fixedly mounted inside the air inlet pipe 25, an end of the air delivery port of the air inlet pipe 25 is fixedly mounted on a side wall of a water treatment tank 2, a plurality of heat conduction plates 27 are fixedly mounted inside the water treatment tank 2, one end of each heat conduction plate 27 penetrates through the side wall of the water treatment tank 2 and extends to the outside of the water treatment tank, and two cooling fins 28 are fixedly mounted on the side walls of the heat conduction plates 27.
Through the arrangement of the mechanisms such as the air pump 24, the air inlet pipe 25, the heat conducting plate 27 and the like, heat is released when chlorine and water react, the water temperature is higher and higher along with the gradual entry of tail gas into the water, and the treatment effect of the tail gas is reduced along with the rise of the water temperature; a temperature sensor and an air pressure sensor are arranged at the bottom of the lower cavity 7, and when the temperature rises, the controller starts to ensure that the air pump 24 blows cold air for a period of time to reduce the water temperature; when the temperature is reduced and the air pressure is increased, in order to avoid the situation that the air pressure in the water treatment tank 2 is too high due to too high air pressure, the air blowing speed of the air pump 24 is slow, the controller closes the air pump in time, and the internal air flows out in an accelerated manner until the air pressure returns to normal; after the air pump 24 is started, the air pump 24 blows outside cold air into the lower cavity 7 of the water treatment tank 5, so that the water temperature in the lower cavity 7 is reduced, the temperature in the water is guided out under the action of the heat conducting plate 27, and the heat on the heat conducting plate 27 is quickly diffused by the heat radiating fins 28 on the heat conducting plate 27, so that the rate of reducing the water temperature is accelerated.
Referring to fig. 1, a conductive block 29 and two second fixing rods 30 are fixedly mounted on the top wall of the lower cavity 7, the two second fixing rods 30 are respectively disposed at two sides of the conductive block 29, a floating ball 31 is slidably mounted between the two second fixing rods 30, an alarm 32 is fixedly mounted at one side of the water treatment tank 2, and the conductive block 29, the floating ball 31 and the alarm 32 are all electrically connected with a power supply through wires.
Through setting up conducting block 29, second dead lever 30, mechanisms such as floater 31, aquatic is along with getting into gradually of tail gas, the concentration of solution is higher and higher, along with the increase of solution concentration, the buoyancy that floater 31 received is bigger and bigger, floater 31 highly risees gradually in solution, when floater 31 and conducting block 29 contact each other, the circuit here is put through, there is the electric current to pass through in the siren 32, siren 32 sends out the police dispatch newspaper, remind the concentration of staff's solution too high, need to change the water of handling tail gas.
Referring to fig. 1, as an embodiment of the present invention, an exhaust pipe 33 is fixedly mounted on the other side of the water treatment tank 2, the end of the exhaust pipe 33 is fixedly mounted on one side of the transition tank 5, an air return pipe 34 is fixedly mounted on the top of the transition tank 5, one end of the air return pipe 34 is fixedly mounted on the other side of the water treatment tank 2, a rotating shaft 35 is rotatably mounted on the inner wall of the transition tank 5, an impeller 36 is fixedly mounted on the rotating shaft 35, the impeller 36 is disposed at the port of the exhaust pipe 33, a worm wheel 37 is fixedly mounted on the rotating shaft 35, a worm 38 is rotatably mounted on the bottom wall of the transition tank 5, and the worm wheel 37 and the worm 38 are engaged with each other.
Through the arrangement of the exhaust pipe 33, the muffler 34, the rotating shaft 35 and other mechanisms, redundant tail gas in the lower cavity 7 after water treatment rises to the upper part of the water surface, redundant tail gas enters the transition box 5 through the exhaust pipe 33, the tail gas in the transition box 5 flows back into the upper cavity 6 again along with air flow to be treated through negative pressure formed in the upper cavity 6, the impeller 36 rotates under the air flow formed by the exhaust pipe 33 and the muffler 34, the rotating shaft 35 rotates under the driving of the impeller 36, the worm wheel 37 on the rotating shaft 35 rotates along with the rotation of the rotating shaft 35, the worm 38 and the worm wheel 37 are meshed with each other, and the worm wheel 37 rotates along with the rotation of the rotating shaft 35 to drive subsequent equipment; after the tail gas circulation treatment reaches the washing treatment standard, a valve in the air return pipe 34 is started, so that the air return pipe 34 is closed, and the tail gas after water treatment flows into a subsequent treatment device through an air outlet pipe on the side wall of the transition box 5 for treatment.
Referring to fig. 1, a reciprocating screw 39 is fixedly mounted at the top end of a worm 38, the top end of the reciprocating screw 39 is rotatably mounted on the top wall of a transition box 5, an annular scraper 40 is movably mounted in the transition box 5, a screw nut 41 is fixedly mounted in the annular scraper 40, and the screw nut 41 is sleeved on the reciprocating screw 39.
Through the arrangement of the reciprocating lead screw 39, the annular scraper 40, the lead screw nut 41 and other mechanisms, the reciprocating lead screw 39 rotates under the driving of the worm 38, the lead screw nut 41 sleeved on the reciprocating lead screw 39 reciprocates, the lead screw nut 41 is fixedly installed inside the annular scraper 40, the limiting rod at the upper end of the annular scraper 40 is clamped with the sliding chute on the inner wall of the transition box 5, the annular scraper 40 is limited when rotating under the interaction of the limiting rod and the sliding chute, so that the annular scraper 40 reciprocates up and down in the transition box 5, tail gas enters the transition box 5 through water with water drops, the annular scraper 40 scrapes off tail gas water drops on the inner wall of the transition box 5, the treatment solution adhered on the inner wall is prevented from volatilizing and diffusing after a long time, and the water drops are collected at the bottom of the transition box 5 below the exhaust pipe 33.
Referring to fig. 1, the material of the air duct 8, the air pipe 10, and the nozzle 11 is aluminum alloy.
The aluminum alloy has the characteristics of oxidation resistance and the like, so that the air duct 8, the air duct 10 and the spray head 11 cannot be corroded due to acidic solution generated by dissolving tail gas in water, and the service lives of the air duct 8, the air duct 10 and the spray head 11 are prolonged.
The working principle is as follows: after the motor 12 is started, the output shaft of the motor 12 drives the driving rod 13 to rotate, the fan blades 14 rotate under the action of the driving rod 13, air flow is formed by the fan blades 14 in the upper cavity 6, negative pressure is formed at a position close to the air inlet 4, tail gas entering from the air inlet 4 flows downwards along with the air flow, the tail gas is accumulated at the collecting groove 15 and is led into the air guide pipe 8 from the air guide port 9 at an accelerated speed, the tail gas enters into the upper cavity 6 from the air inlet 4 and is led into the air guide pipe 8 from the air guide port 9 under the flow guide of the flow guide equipment, the tail gas in the air guide pipe 8 is sprayed into water from the spray head 11 through the air guide pipe 10 at the lower end, the air guide pipe 8 rotates under the action of the driving equipment, the tail gas in the air guide pipe 8 is diffused to the periphery of the water, the air guide pipe 8 rotates under the driving of the driving rod 13, the first crushing blades 16 on the air guide pipe 8 rotate along with the rotation of the air guide pipe 8, and crush tail gas bubbles sprayed from the spray head 11, so that tail gas in bubbles can not be contacted with water due to the isolation of the bubbles, the second crushing blade 18 rotates along with the air duct 8, and the second crushing blade 18 is blown by gas under the action of bottom tail gas bubbles, so that the first spring 19 moves up and down in a reciprocating manner, after chlorine in the air duct 8 reacts with water at the tail end of the air duct 8, water enters the air duct 8 from the tail end of the air duct 8, tail gas quickly enters the air duct 8, so that the whole air duct 8 is filled with chlorine, water possibly flows back to the upper chamber 6, so that the tail gas can not enter water in the lower chamber 7, after the air pump 24 is started, the air pump 24 blows outside cold air into the lower chamber 7 of the water treatment tank 5, so that the water temperature in the lower chamber 7 is reduced, the temperature in the water is guided out under the action of the heat conducting plate 27, and heat on the heat conducting plate 27 is quickly diffused by the heat radiating fins 28 on the heat conducting plate 27, the concentration of the solution is higher and higher along with the gradual entering of tail gas in water, the buoyancy force borne by the floating ball 31 is larger and larger along with the increase of the concentration of the solution, the height of the floating ball 31 in the solution is gradually increased, when the floating ball 31 and the conductive block 29 are contacted with each other, a circuit is connected, current passes through the alarm 32, the alarm 32 gives an alarm, redundant tail gas in the lower cavity 7 after water treatment rises to the upper part of the water surface, the tail gas in the transition box 5 flows back into the upper cavity 6 along with the airflow to be treated by the negative pressure formed in the upper cavity 6, the impeller 36 rotates under the airflow formed by the exhaust pipe 33 and the air return pipe 34, the rotating shaft 35 rotates under the driving of the impeller 36, the worm wheel 37 on the rotating shaft 35 rotates along with the rotation of the rotating shaft 35, the worm 38 and the worm wheel 37 are meshed with each other, the worm wheel 37 rotates along with the rotation of the worm wheel, the reciprocating lead screw 39 rotates under the driving of the worm 38, the lead screw nut 41 sleeved on the reciprocating lead screw 39 reciprocates, the lead screw nut 41 is fixedly installed in the annular scraper 40, the limiting rod on the upper end of the annular scraper 40 and the transition box 5 is acted on the inner wall of the transition box to limit slide groove 40, so that the reciprocating scraper moves up and the transition box 5 up-down, thereby enabling the reciprocating scraper to move up and down.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (10)

1. The utility model provides a tail gas purification processing system of dichlorophenol production, includes base (1), water treatment tank (2) of fixed mounting in base (1) upper end, articulates case lid (3) on water treatment tank (2), sets up air inlet (4) inside case lid (3), its characterized in that: further comprising:
the transition box (5) is fixedly arranged at the upper end of the base (1);
an upper cavity (6) and a lower cavity (7) which are arranged inside the water treatment tank (2);
the air guide mechanism is arranged inside the water treatment tank (2).
2. The system for purifying and treating the tail gas generated in the production of dichlorophenol according to claim 1, characterized in that: air guide mechanism installs air duct (8) on cavity of resorption (7) roof including rotating, set up air guide mouth (9) that two symmetries set up on the lateral wall of air duct (8) upper end, the lower extreme fixed mounting of air duct (8) has air-supply pipe (10) that several symmetries set up, several fixed mounting has a plurality of shower nozzles (11) on the lateral wall of air-supply pipe (10).
3. The system for purifying and treating the tail gas generated in the production of dichlorophenol according to claim 2, characterized in that: the top fixed mounting of case lid (3) has motor (12), the mid-rotation of case lid (3) installs actuating lever (13), the output shaft of motor (12) and the top fixed connection of actuating lever (13), the bottom of actuating lever (13) and the top fixed connection of air duct (8), fixed mounting has flabellum (14) on actuating lever (13), fixed mounting has collection groove (15) on the roof of cavity of resorption (7), the inside of collecting groove (15) is located in air guide port (9).
4. The system for purifying and treating the tail gas generated in the production of dichlorophenol according to claim 2, characterized in that: the middle part fixed mounting of air duct (8) has first broken blade (16), the lower extreme fixed mounting of air duct (8) has two fixed blocks (17), two movable mounting has second broken blade (18) between fixed block (17), two fixed equal fixedly connected with first spring (19) between fixed block (17) and second broken blade (18).
5. The system for purifying and treating the tail gas generated in the production of dichlorophenol according to claim 2, characterized in that: the inside fixed mounting of air duct (8) has first dead lever (20), the upper end fixed mounting of first dead lever (20) has telescopic link (21), the flexible terminal fixed mounting of telescopic link (21) has piston (22), second spring (23) have been cup jointed on telescopic link (21), and the both ends of second spring (23) are fixed connection respectively on first dead lever (20) and piston (22).
6. The system for purifying and treating the tail gas generated in the production of dichlorophenol according to claim 1, characterized in that: the upper end fixed mounting of base (1) has air pump (24), the gas transmission mouth end fixedly connected with intake pipe (25) of air pump (24), the inside fixed mounting of intake pipe (25) has check valve (26), the terminal fixed mounting of gas transmission mouth of intake pipe (25) is on the lateral wall of water treatment case (2), the inside fixed mounting of water treatment case (2) has a plurality of heat-conducting plates (27), and is a plurality of the one end of heat-conducting plate (27) runs through the lateral wall of water treatment case (2) and extends to its outside, and is a plurality of equal fixed mounting has two fin (28) on the lateral wall of heat-conducting plate (27).
7. The system for purifying and treating tail gas generated in dichlorophenol production according to claim 1, wherein: fixed mounting has conducting block (29) and two second dead levers (30) on the roof of cavity of resorption (7), and two second dead levers (30) locate the both sides of conducting block (29) respectively, two slidable mounting has floater (31) between second dead lever (30), one side fixed mounting of water treatment box (2) has siren (32), conducting block (29), floater (31) and siren (32) all pass through wire and power electric connection.
8. The system for purifying and treating the tail gas generated in the production of dichlorophenol according to claim 1, characterized in that: the opposite side fixed mounting of water treatment case (2) has blast pipe (33), the terminal fixed mounting of blast pipe (33) is in one side of transition case (5), the top fixed mounting of transition case (5) has muffler (34), the one end fixed mounting of muffler (34) is at the opposite side of water treatment case (2), rotate on the inner wall of transition case (5) and install pivot (35), fixed mounting has impeller (36) on pivot (35), the port department of blast pipe (33) is located in impeller (36), fixed mounting has worm wheel (37) on pivot (35), rotate on the diapire of transition case (5) and install worm (38), worm wheel (37) and worm (38) intermeshing.
9. The system for purifying and treating the tail gas generated in the production of dichlorophenol according to claim 8, characterized in that: the top fixed mounting of worm (38) has reciprocal lead screw (39), the top of reciprocal lead screw (39) is rotated and is installed on the roof of transition case (5), the inside movable mounting of transition case (5) has annular scraper blade (40), the inside fixed mounting of annular scraper blade (40) has lead screw nut (41), lead screw nut (41) cup joints on reciprocal lead screw (39).
10. The system for purifying and treating the tail gas generated in the production of dichlorophenol according to claim 2, characterized in that: the air duct (8), the air delivery pipe (10) and the spray head (11) are made of aluminum alloy.
CN202210830365.1A 2022-07-14 2022-07-14 Tail gas purification processing system of dichlorophenol production Pending CN115318083A (en)

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Application Number Priority Date Filing Date Title
CN202210830365.1A CN115318083A (en) 2022-07-14 2022-07-14 Tail gas purification processing system of dichlorophenol production

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CN202210830365.1A CN115318083A (en) 2022-07-14 2022-07-14 Tail gas purification processing system of dichlorophenol production

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116371097A (en) * 2023-04-04 2023-07-04 南通爱辰环保科技有限公司 Gas filtering and carbon dioxide collecting device and method for industrial waste gas
CN117679939A (en) * 2024-01-09 2024-03-12 沙湾天山水泥有限责任公司 Dust removing device for bagged cement loading

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116371097A (en) * 2023-04-04 2023-07-04 南通爱辰环保科技有限公司 Gas filtering and carbon dioxide collecting device and method for industrial waste gas
CN117679939A (en) * 2024-01-09 2024-03-12 沙湾天山水泥有限责任公司 Dust removing device for bagged cement loading
CN117679939B (en) * 2024-01-09 2024-05-28 沙湾天山水泥有限责任公司 Dust removing device for bagged cement loading

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