CN115252475B - 润肤洁肤组合物、浴弹及其制备方法 - Google Patents
润肤洁肤组合物、浴弹及其制备方法 Download PDFInfo
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- CN115252475B CN115252475B CN202210909395.1A CN202210909395A CN115252475B CN 115252475 B CN115252475 B CN 115252475B CN 202210909395 A CN202210909395 A CN 202210909395A CN 115252475 B CN115252475 B CN 115252475B
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Abstract
本发明涉及洗护用品领域，公开了一种润肤洁肤组合物、浴弹及其制备方法，该润肤洁肤组合物包括以下重量份数的组分：A组分：碳酸氢钠46～55份；B组分：聚乙二醇‑400 0.5～2份、玫瑰花油2～4份、椰子油0.3～1份、油橄榄果油0.3～1份、葡萄籽油0.3～1份；C组分：氨基酸表面活性剂2～4份；D组分：柠檬酸33～38份；E组分：马齿笕提取物2～4份、鱼腥草提取物0.5～2份。该润肤洁肤组合物泡沫丰富稳定，清洁性好，保湿性好，抗菌消炎性好，能够有效改善皮肤瘙痒和皮肤痘痘。
Description
技术领域
本发明涉及洗护用品领域，特别是涉及一种润肤洁肤组合物、浴弹及其制备方法。
背景技术
随着人们生活水平的提高，对沐浴的追求也越来越来丰富，沐浴用品也得到了很大的发展。沐浴气泡弹，简称浴弹，是沐浴用品的一种，也称为浴盐球。现有的浴弹主要用于满足沐浴趣味性，其护肤功能比较匮乏，并且产生的泡沫比较少，难以满足人们更高层次的沐浴要求。
发明内容
本发明的目的是克服现有技术中的不足之处，提供一种润肤洁肤组合物，泡沫丰富稳定，清洁性好，保湿性好，抗菌消炎性好，能够有效改善皮肤瘙痒和皮肤痘痘。
本发明还提供一种含有上述润肤洁肤组合物的浴弹及其制备方法。
本发明的目的是通过以下技术方案来实现的：
本发明提供一种润肤洁肤组合物，包括以下重量份数的组分：
A组分：碳酸氢钠46～55份；
B组分：聚乙二醇-400 0.5～2份、玫瑰花油2～4份、椰子油0.3～1份、油橄榄果油0.3～1份、葡萄籽油0.3～1份；
C组分：氨基酸表面活性剂2～4份；
D组分：柠檬酸33～38份；
E组分：马齿笕提取物2～4份、鱼腥草提取物0.5～2份。
在其中一种实施方式，所述润肤洁肤组合物包括以下重量份数的组分：
A组分：碳酸氢钠50～52份；
B组分：聚乙二醇-400 1份、玫瑰花油3份、椰子油0.5份、油橄榄果油0.5份、葡萄籽油0.5份；
C组分：氨基酸表面活性剂3份；
D组分：柠檬酸36份；
E组分：马齿笕提取物3份、鱼腥草提取物1份。
需要说明的是，玫瑰(英文名称ROSA RUGOSA)花油，由新鲜玫瑰的花经蒸汽蒸馏而得的一种精油，微黄至淡黄绿色液体，有持久而浓郁的玫瑰香气，主要组分为左旋香茅醇、香叶醇、苯乙醇及橙花醇等。玫瑰花油具有极好的补水保湿作用，并且可以改善皮肤质地，促进血液循环及新陈代谢，还具有极好的抗衰老和止痒作用。
椰子(英文名称COCOS NUCIFERA)油，椰子油别名椰油，是棕榈科植物椰子树的种子精炼制成的非挥发性油。椰子油是一种天然的护肤保湿产品，含有丰富的叶桂酸，还具有很强的抗氧化能力，可以滋润皮肤，改善干燥肤质，消除皱纹；并且具有天然的抗菌能力，可以起到杀死引起疾病的病毒、真菌的作用。
油橄榄(英文名称OLEA EUROPAEA)果油，油橄榄果油是橄榄果经过所有的压榨提取过程后的剩余部分再经过化学溶解处理而得到的，或者是由新鲜的橄榄果实直接冷榨而成的。油橄榄果油富含与皮肤亲和力极佳的鱼鲨烯和人体必需脂肪酸，吸收迅速，有效保持皮肤的弹性和润泽；所含丰富的不饱和脂肪酸、维生素和酚类抗氧化物质，能够消除面部的皱纹，防止肌肤的衰老；假如皮肤受到细菌感染或者有皮肤炎症，适当涂抹油橄榄果油也可以缓解不良症状。
葡萄(英文名称VITIS VINIFERA)籽油，葡萄籽油有两种非常重要的元素，亚麻油酸和原花色素。亚麻油酸可以抵抗自由基，抗老化，帮助吸收维生素C和E，强化循环系统的弹性，降低紫外线的伤害，保护肌肤中的胶原蛋白，改善静脉肿胀与水肿，预防黑色素沉淀。原花色素有保护血管弹性，保护肌肤免于紫外线的荼毒，预防胶原纤维和弹性纤维的破坏，使肌肤保持应有的弹性及张力，避免皮肤下垂及皱纹产生。渗透力强，清爽不油腻，极易被皮肤吸收，任何肤质均适用。
本申请发明人通过研究发现在配方中加入玫瑰花油、椰子油、油橄榄果油、葡萄籽油多种植物精油，不仅具有持久而浓郁的香气，还具有较好的补水保湿滋润皮肤、调节皮肤油脂分泌、改善皮肤屏障功能、抗衰老改善皱纹、抗菌消炎止痒、预防黑色素美白等作用，与聚乙二醇-400、马齿笕提取物、鱼腥草提取物协同作用后，尤其在补水保湿和改善皮肤痘痘方面表现出显著效果；而且能够提高浴弹的肤感，具有温和不刺激、不干涩、不紧绷、不发痒、柔软湿润的浴后肤感。
在其中一种实施方式，所述氨基酸表面活性剂是由重量比为1～2:1的肉豆蔻酰谷氨酸钠和甲基月桂酰基牛磺酸钠复配得到。
需要说明的是，氨基酸型氨基酸表面活性剂是一类可再生生物质来源的新型绿色环保氨基酸表面活性剂，是传统氨基酸表面活性剂的升级换代产品。氨基酸型氨基酸表面活性剂不仅生物质原料来源广泛，毒副作用小，性能温和，刺激性小且生物降解性好，生产工艺绿色化，而且其良好的乳化、润湿、增溶、分散、起泡等性能。氨基酸型氨基酸表面活性剂具有无毒无害，性能温和，无刺激性，去污力佳，各类氨基酸能够渗透进皮肤，保护与改善皮肤屏障。
肉豆蔻酰谷氨酸钠，英文名称是SODIUM MYRISTOYL GLUTAMATE，别名：N-(1-氧代十四烷基)-L-谷氨酸单钠盐。肉豆蔻酰谷氨酸钠是一种阴离子氨基酸表面活性剂，无毒无害，安全温和，有比较温和的清洁去污能力，同时还具有发泡和抑菌功能。
甲基月桂酰基牛磺酸钠(Galapon LT40)又称为月桂酰基甲基牛磺酸钠，是一种阴离子氨基酸表面活性剂，安全无刺激，具有良好的去污力和乳化能力，泡沫性能良好，能赋予毛发和皮肤温和、滋润、清爽、洁净的感觉。
本申请发明人在研究的过程中发现，在配方中加入多种植物精油，不仅具有较好的补水保湿性和抗菌消炎抑制痘痘的作用，还能够使浴弹具有温和不刺激、不干涩、不紧绷、不发痒、柔软湿润的浴后肤感，但是加入一定量的植物精油，会使得浴弹的发泡性能和冲洗效果不佳，但是发明人通过研究发现在配方中加入氨基酸表面活性剂后，不仅能够提高浴弹的去污力和乳化能力，使泡沫更丰富稳定，减少其在皮肤表面的残留，有效提高冲洗效果，还带来温和、滋润、清爽、洁净的肤感；同时氨基酸表面活性剂除了清洁作用，还具有一定的抗菌抑菌功能，与多种植物精油协同改善皮肤痘痘。
在其中一种实施方式，所述马齿笕提取物通过以下方法制备得到：将马齿笕晒干、粉碎，得到马齿笕粉；对所述马齿笕粉进行超临界二氧化碳萃取1～3h，萃取压力为40～50MPa，萃取温度为20～35℃。
需要说明的是，马齿苋，一年生草本，别名马苋、五行草、五方草、长命菜、瓜子菜、麻绳菜、马齿菜等。全草含大量去甲肾上腺素(noradrenaline)和多量钾盐(包括硝酸钾、氯化钾、硫酸钾和其他钾盐)。还含多巴(dopa)，多巴胺(dopamine)，甜菜素(betanidin)，异甜菜素(isobetanidin)，甜菜式(betanin)，异甜菜甙(isobetanin)，草酸(oxalic acid)，苹果酸(malic acid)，柠檬酸(citric acid)，谷氨酸(glutamic acid)，天冬氨酸(asparticacid)，丙氨酸(alanine)以及葡萄糖(glucose)，果糖(fructose)，蔗糖(sucrose)等。
植物多糖和维生素可以营养润滑皮肤和促进上皮细胞的生理功能趋于正常，减少干燥引起的死皮和角质层的生成；氨基酸，可以收缩血管平滑肌，收缩作用兼有的中枢及末梢性，可以舒缓皮肤和抑制干燥引起的皮肤搔痒；黄酮和皂甙可以去自由基和抗氧化、延缓皮肤衰老；生物碱和黄酮可以抗菌及抑制常见致病性皮肤真菌。马齿苋提取物具有在冬季防干燥老化、增加皮肤舒适度以及清除自由基，改善皮肤舒适感等的综合性能。
本申请发明人通过研究发现在配方中加入马齿苋提取物，不仅具有较好的补水保湿性和抗菌消炎性，可以滋润皮肤，调节皮肤油脂分泌，改善皮肤屏障功能，镇静舒缓皮肤，改善皮肤痘痘；还能够使得浴弹的泡沫更加丰富、细腻。稳定。发明人推测可能的原因是马齿苋提取物中含有的植物多糖、氨基酸、皂甙、生物碱等活性组分不仅能够提高溶液的粘度，并且能够增加泡沫的起泡性和稳泡性，同时使得其双电层之间的排斥力减小；同时与聚乙二醇-400、多种植物精油、鱼腥草提取物协同提高补水保湿性和改善皮肤痘痘。
在其中一种实施方式，所述鱼腥草提取物通过以下方法制备得到：将鱼腥草晒干、粉碎，得到鱼腥草粉；对所述鱼腥草粉进行超临界二氧化碳萃取1～3h，萃取压力为40～50MPa，萃取温度为20～35℃。
需要说明的是，鱼腥草(英文名HERBA HOUTTUYNIAE)是中国药典收录的草药。鱼腥草味辛，性寒凉，归肺经。能清热解毒、消肿疗疮、利尿除湿、清热止痢、健胃消食，用治实热、热毒、湿邪、疾热为患的肺痈、疮疡肿毒、痔疮便血、脾胃积热等。现代药理实验表明，本品具有抗菌、抗病毒、提高机体免疫力、利尿等作用。
本申请发明人在研究的过程中发现，在配方中加入马齿苋提取物，不仅具有较好的补水保湿性和抗菌消炎抑制痘痘的作用，还能够提高浴弹的泡沫感；但是加入一定量的马齿苋提取物，会使得浴弹的冲洗效果不佳；但是发明人通过研究发现在配方中加入鱼腥草提取物后，不仅能够有效改善浴弹的冲洗效果，还能进一步提高浴弹的泡沫感，并且具有较好的清热解毒，消炎抗菌，增强皮肤屏障的功效，与聚乙二醇-400、多种植物精油、马齿笕提取物协同改善皮肤痘痘；同时发明人发现在配方中加入鱼腥草提取物后，能够提高浴弹的保湿性。鱼腥草提取物在配方中表现出改善皮肤痘痘的效果，这可能是出于它具有较好的清热解毒，消炎抗菌，增强皮肤屏障的功效；但是现有技术没有公开鱼腥草提取物具有补水保湿和提高泡沫性的作用。发明人推测可能的原因是鱼腥草提取物中活性组分与马齿苋提取物中活性组分相互作用，减少其在皮肤表面的残留量，同时鱼腥草提取物与碳酸氢钠、氨基酸表面活性剂相互作用能够进一步增加浴弹的发泡性和稳泡性，还与聚乙二醇-400、多种植物精油、马齿笕提取物协同作用，有效提高补水保湿和改善皮肤痘痘效果。
本发明还提供一种浴弹，含有上述的润肤洁肤组合物。
在其中一种实施方式，所述浴弹包括以下重量百分数的组分：
A组分：碳酸氢钠46～55份、去离子水0～1％、色素0～0.005％；
B组分：聚乙二醇-400 0.5～2％、玫瑰花油2～4％、椰子油0.3～1％、油橄榄果油0.3～1％、葡萄籽油0.3～1％、香精0～0.5％；
C组分：氨基酸表面活性剂2～4％；
D组分：柠檬酸33～38％；
E组分：马齿笕提取物2～4％、鱼腥草提取物0.5～2％。
在其中一种实施方式，所述浴弹包括以下重量百分数的组分：
A组分：碳酸氢钠50～52％、去离子水0.5％、色素0.002％；
B组分：聚乙二醇-400 1％、玫瑰花油3％、椰子油0.5％、油橄榄果油0.5％、葡萄籽油0.5％、香精0.3％；
C组分：氨基酸表面活性剂3％；
D组分：柠檬酸36％；
E组分：马齿笕提取物3％、鱼腥草提取物1％。
在其中一种实施方式，所述色素为CI 16035。
需要说明的是，本发明提供了一种浴弹完整的配方，碳酸氢钠主要做皮肤调节剂和发泡剂；柠檬酸主要做pH调节剂；氨基酸表面活性剂主要做发泡剂；马齿笕提取物和鱼腥草提取物主要做保湿剂和皮肤调节剂，还具有辅助发泡作用；聚乙二醇-400、玫瑰花油、椰子油、油橄榄果油、葡萄籽油主要做保湿剂和皮肤调节剂；还有芳香剂(即香精)、着色剂(即色素)和溶剂(即去离子水)。
本发明还提供上述浴弹的制备方法，包括以下步骤：
(1)将所述A组分加入到搅拌锅中，高速搅拌均匀；
(2)加入所述B组分到搅拌锅中，高速搅拌均匀；
(3)加入所述C组分搅拌均匀；
(4)加入所述D组分混合均匀，
(5)加入所述E组分混合均匀；
(6)压制成型，干燥得到成品。
与现有技术相比，本发明至少具有以下优点：
本发明提供的润肤洁肤组合物和浴弹通过配方中碳酸氢钠、聚乙二醇-400、玫瑰花油、椰子油、油橄榄果油、葡萄籽油、氨基酸表面活性剂、柠檬酸和马齿笕提取物和鱼腥草提取物的协同作用，使其泡沫丰富细腻稳定，具有温和不刺激、不干涩、不紧绷、不发痒、柔软湿润的浴后肤感；还能够补水保湿滋润皮肤、调节皮肤油脂分泌、改善皮肤屏障功能、抗衰老改善皱纹、抗菌消炎止痒，尤其在泡沫性、补水保湿、改善皮肤瘙痒和改善皮肤痘痘方面表现出显著效果。
具体实施方式
下面结合具体实施例对本发明作进一步详细的描述，但本发明的实施方式不限于此。本发明可以以许多不同的形式来实现，并不限于本文所描述的实施方式。相反地，提供这些实施方式的目的是使对本发明的公开内容理解的更加透彻全面。
实施例中浴弹的各组分用量以重量百分数计，单位％。
实施例1～4浴弹的配方如表1所示。
表1实施例1～4组分表
实施例1～4浴弹的制备方法如下：
(1)将所述A组分加入到搅拌锅中，高速搅拌均匀；
(2)加入所述B组分到搅拌锅中，高速搅拌均匀；
(3)加入所述C组分搅拌均匀；
(4)加入所述D组分混合均匀，
(5)加入所述E组分混合均匀；
(6)压制成型，干燥得到成品。
对比例中浴弹的各组分用量以重量百分数计，单位％。对比例1～8浴弹的配方如表2所示。
表2对比例1～8组分表
对比例1～8浴弹的制备方法同实施例4。
对实施例1～4和对比例1～8的浴弹样品进行以下性能测试。
1.泡沫性能测试
测试方法：参照国家标准GB13173-2008，取各浴弹样品2.5g，分别用150mg/kg硬水溶解，转移到1000mL容量瓶中，并稀释至刻度，摇匀。再将溶液置于(40±0.5)℃恒温水浴中陈化，从加水溶样开始总时间30min，随后用罗氏泡沫仪测定泡沫高度，并计算泡沫稳定性(计算公式：5min后泡沫高度/起始泡沫高度*100％)结果如表3所示。
2.保湿性能测试
测试方法：挑选年龄为20～40岁的测试者120人，男女各半，随机分为12组，每组10人，划定测试区域，测试区域为测试者右手前臂内侧5cm2的位置，取各浴弹样品配制为浓度1％的水溶液进行浸泡洗涤2小时，采用皮肤水分测试仪分别测试洗涤前和洗涤2小时后的皮肤含水量，测试结果取平均值，并计算含水量增加百分率(计算公式：(洗涤后皮肤含水量-洗涤前皮肤含水量)/洗涤前皮肤含水量*100％)，测试结果如表3所示。
3.浴弹使用效果测试
测试方法：挑选年龄为20～40岁的测试者120人，男女各半，随机分为12组，每组10人，测试者按照相同的方法沐浴，每天洗一次，分别对各浴弹样品使用1个月，然后对样品进行评价。评价标准采用5分制，1分表示非常差，2分表示差，3分表示一般，4分表示好，5分表示非常好，统计结果取平均值，测试结果如表4所示。
表3泡沫性能、保湿性能测试表
由表3结果可看出，与对比例1～8相比，本发明实施例1～4的浴弹样品具有较好的泡沫性能和补水保湿效果。
对比例1的浴弹样品与实施例4相比，植物精油含量偏低，表现出泡沫性能无明显变化，补水保湿效果明显下降；对比例2的浴弹样品与实施例4相比，植物精油含量偏高，补水保湿效果无明显变化，泡沫性能明显下降。
对比例3～4的浴弹样品与实施例4相比，采用了与本发明规定不同配比的氨基酸表面活性剂，导致泡沫性能和补水保湿效果均出现下降。
对比例5的浴弹样品与实施例4相比，马齿笕提取物含量偏低，表现出泡沫性能和补水保湿效果均明显下降；对比例6的浴弹样品与实施例4相比，马齿笕提取物含量偏高，导致泡沫性能和补水保湿效果均出现不良影响。
对比例7的浴弹样品与实施例4相比，鱼腥草提取物含量偏低，表现出泡沫性能和补水保湿效果均明显下降；对比例8的浴弹样品与实施例4相比，鱼腥草提取物含量偏高，导致泡沫性能和补水保湿效果均出现不良影响。
实施例1～4和对比例1～8的浴弹样品
表4使用效果测试表
由表4结果可看出，与对比例1～8相比，本发明实施例1～4的浴弹样品在温和性、泡沫性、易冲洗性、清洁性、保湿性、改善皮肤瘙痒和改善皮肤痘痘方面均有很高评价。与实施例4相比，对比例1的浴弹样品中植物精油含量偏低，其保湿性、改善皮肤瘙痒和改善皮肤痘痘的效果明显下降；对比例2的浴弹样品中植物精油含量偏高，其泡沫性、易冲洗性、清洁性、改善皮肤痘痘的效果明显下降。对比例3～4的浴弹样品采用了与本发明规定不同配比的氨基酸表面活性剂，其温和性、泡沫性、易冲洗性、清洁性、保湿性、改善皮肤瘙痒和改善皮肤痘痘的效果均出现下降。对比例5的浴弹样品中马齿笕提取物含量偏低，其泡沫性、保湿性、改善皮肤瘙痒和改善皮肤痘痘的效果均明显下降；对比例6的浴弹样品中马齿笕提取物含量偏高，其易冲洗性明显下降，并且清洁性、改善皮肤瘙痒和改善皮肤痘痘的效果均出现不良影响。对比例7的浴弹样品中鱼腥草提取物含量偏低，其泡沫性、易冲洗性、保湿性、改善皮肤瘙痒和改善皮肤痘痘的效果均明显下降；对比例8的浴弹样品中鱼腥草提取物含量偏高，其泡沫性、清洁性、保湿性、改善皮肤瘙痒和改善皮肤痘痘均出现不良影响。可见本发明浴弹配方中各组分的协同作用，使其在温和性、泡沫性、易冲洗性、清洁性、保湿性、改善皮肤瘙痒和改善皮肤痘痘方面具有良好效果。
以上所述实施例仅表达了本发明的几种实施方式，其描述较为具体和详细，但并不能因此而理解为对发明专利范围的限制。应当指出的是，对于本领域的普通技术人员来说，在不脱离本发明构思的前提下，还可以做出若干变形和改进，这些都属于本发明的保护范围。因此，本发明专利的保护范围应以所附权利要求为准。
Claims (2)
1.一种浴弹，其特征在于，由以下重量百分数的组分组成：
A组分：去离子水0.5％、色素0.002％、碳酸氢钠为余量；
B组分：聚乙二醇-400 1％、玫瑰花油3％、椰子油0.5％、油橄榄果油0.5％、葡萄籽油0.5％、香精0.3％；
C组分：氨基酸表面活性剂3％，所述氨基酸表面活性剂是由重量比为1～2:1的肉豆蔻酰谷氨酸钠和甲基月桂酰基牛磺酸钠复配得到；
D组分：柠檬酸36％；
E组分：马齿苋提取物3％、鱼腥草提取物1％。
2.一种根据权利要求1所述的浴弹的制备方法，其特征在于，包括以下步骤：
(1)将所述A组分加入到搅拌锅中，高速搅拌均匀；
(2)加入所述B组分到搅拌锅中，高速搅拌均匀；
(3)加入所述C组分搅拌均匀；
(4)加入所述D组分混合均匀，
(5)加入所述E组分混合均匀；
(6)压制成型，干燥得到成品。
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| CN112996569A (zh) * | 2018-11-02 | 2021-06-18 | 强生消费者公司 | 可发泡固体清洁剂 |
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