CN115160880A - Diffuse reflection plate spraying material, diffuse reflection plate containing spraying material and preparation method - Google Patents
Diffuse reflection plate spraying material, diffuse reflection plate containing spraying material and preparation method Download PDFInfo
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- CN115160880A CN115160880A CN202210918460.7A CN202210918460A CN115160880A CN 115160880 A CN115160880 A CN 115160880A CN 202210918460 A CN202210918460 A CN 202210918460A CN 115160880 A CN115160880 A CN 115160880A
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- Prior art keywords
- diffuse reflection
- reflection plate
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- oxide
- difference
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- 238000000576 coating method Methods 0.000 claims description 35
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/24—Homopolymers or copolymers of amides or imides
- C09D133/26—Homopolymers or copolymers of acrylamide or methacrylamide
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
- C09D101/284—Alkyl ethers with hydroxylated hydrocarbon radicals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
- C09D101/286—Alkyl ethers substituted with acid radicals
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D105/00—Coating compositions based on polysaccharides or on their derivatives, not provided for in groups C09D101/00 or C09D103/00
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D129/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Coating compositions based on hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Coating compositions based on derivatives of such polymers
- C09D129/02—Homopolymers or copolymers of unsaturated alcohols
- C09D129/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
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- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C09D139/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Coating compositions based on derivatives of such polymers
- C09D139/04—Homopolymers or copolymers of monomers containing heterocyclic rings having nitrogen as ring member
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- C09D171/00—Coating compositions based on polyethers obtained by reactions forming an ether link in the main chain; Coating compositions based on derivatives of such polymers
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
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- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2265—Oxides; Hydroxides of metals of iron
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- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
- C08K2003/3081—Aluminum sulfate
Abstract
The invention relates to the field of spraying materials, and particularly discloses a diffuse reflection plate spraying material, a diffuse reflection plate containing the spraying material and a preparation method. The diffuse reflection plate spraying material comprises the following components in parts by mass: 0-800 parts of iron oxide; 50-600 parts of sulfate; 500-1000 parts of water; 50-150 parts of a water-soluble tackifier. The preparation method of the spray coating material comprises the following steps: and (3) uniformly mixing the components to obtain the diffuse reflection plate spraying material. The diffuse reflection plate containing the diffuse reflection plate spraying material comprises a substrate and the diffuse reflection plate spraying material sprayed on the surface of the substrate. By adopting the spraying material, the reflectivity of the spraying material can be adjusted from 1-97% by only fixing the dosage of other components and adjusting the dosage of the iron oxide, so that the efficiency is extremely high; in addition, the preparation method of the invention also has the advantages of simplicity, convenience and easy industrialization.
Description
Technical Field
The invention relates to the field of spraying materials, in particular to a diffuse reflection plate spraying material, a diffuse reflection plate containing the spraying material and a preparation method.
Background
The spectral calibration is an indispensable step in the spectral instrument measurement, and the diffuse reflection plate is an important optical device in the spectral calibration application, and the reflectivity of the diffuse reflection plate directly affects the accuracy of the spectral instrument measurement, so that the accuracy of the instrument for acquiring data of a measured object is affected.
The current diffuse reflection plate is usually manufactured by spraying coating materials with different reflectance ratios on a substrate, and curing and drying the coating materials. However, the components of the existing spraying materials with different reflectances are very different, and the diffuse reflection plates with different reflectances need to be sprayed by the spraying materials formed by completely different components, so that the preparation of the diffuse reflection plates with different reflectances needs to correspond to various different preparation processes, and the preparation operation of the diffuse reflection plates is extremely complicated and low in efficiency.
Disclosure of Invention
In order to improve the preparation efficiency of diffuse reflection plates with different reflectivity, the application provides a diffuse reflection plate spraying material, a diffuse reflection plate containing the spraying material and a preparation method.
In a first aspect, the present application provides a diffuse reflection plate spray coating material, which adopts the following technical scheme:
a diffuse reflection plate spraying material comprises the following components in parts by mass:
0-800 parts of iron oxide;
50-600 parts of sulfate;
500-1000 parts of water;
50-150 parts of water-soluble tackifier.
Preferably, the water-soluble viscosity increaser comprises one or more of polyethylene glycol, polyvinyl alcohol, polyacrylamide, polyvinylpyrrolidone, carbomer resin, sodium polyacrylate, hydroxypropyl methyl cellulose, sodium carboxymethyl cellulose, hydroxyethyl cellulose and xanthan gum.
Preferably, the water-soluble tackifier comprises one or more of polyethylene glycol, polyvinyl alcohol, polyacrylamide and polyvinylpyrrolidone.
Preferably, the iron oxide comprises one or more of ferrous oxide, ferric oxide and ferroferric oxide.
Preferably, the sulfate includes one or more of calcium sulfate, barium sulfate, copper sulfate, aluminum potassium sulfate, sodium sulfate, and aluminum sulfate.
By adopting the technical scheme, the use amount of other components is fixed, and the adjustment of the reflectivity of the spraying material from 1-97% can be realized by adjusting the use amount of the iron oxide.
When the iron oxide is ferrous oxide, the reflectivity of the diffuse reflection plate can be adjusted to 90-97% by adjusting the using amount of the ferrous oxide to be 0-30 g; the reflectivity of the diffuse reflection plate can be adjusted to 80-89% by adjusting the dosage of the ferrous oxide to 31-60 g; the reflectivity of the diffuse reflection plate can be adjusted to be 70-79% by adjusting the dosage of the ferrous oxide to be 61-80 g; the reflectivity of the diffuse reflection plate can be adjusted to be 60-69% by adjusting the using amount of the ferrous oxide to be 81-120 g; the reflectivity of the diffuse reflection plate can be adjusted to be 50-59% by adjusting the using amount of the ferrous oxide to be 121-200 g; the reflectivity of the diffuse reflection plate can be adjusted to 40-49% by adjusting the using amount of the ferrous oxide to 201-350 g; the reflectivity of the diffuse reflection plate can be adjusted to be 30-39% by adjusting the using amount of the ferrous oxide to be 351-450 g; the reflectivity of the diffuse reflection plate can be adjusted to be 20-29% by adjusting the using amount of the ferrous oxide to be 451-600 g; the reflectivity of the diffuse reflection plate can be adjusted to be 10-19% by adjusting the using amount of the ferrous oxide to be 601-700 g; the reflectivity of the diffuse reflection plate can be adjusted to be 1-9% by adjusting the dosage of the ferrous oxide to be 701-800 g.
When the iron oxide is selected as the iron oxide, the reflectivity of the diffuse reflection plate can be adjusted to be 90-97% by adjusting the using amount of the iron oxide to be 0-15 g; the reflectivity of the diffuse reflection plate can be adjusted to 80-89% by adjusting the using amount of the ferric oxide to 16-30 g; the reflectivity of the diffuse reflection plate can be adjusted to 70-79 percent by adjusting the using amount of the ferric oxide to 31-40 g; the reflectivity of the diffuse reflection plate can be adjusted to be 60-69% by adjusting the using amount of the ferric oxide to be 41-60 g; the reflectivity of the diffuse reflection plate can be adjusted to be 50-59% by adjusting the using amount of the ferric oxide to be 61-100 g; the reflectivity of the diffuse reflection plate can be adjusted to 40-49% by adjusting the using amount of the ferric oxide to be 101-200 g; the reflectivity of the diffuse reflection plate can be adjusted to be 30-39% by adjusting the using amount of the ferric oxide to be 201-300 g; the reflectivity of the diffuse reflection plate can be adjusted to be 20-29% by adjusting the using amount of the ferric oxide to be 301-400 g; the reflectivity of the diffuse reflection plate can be adjusted to be 10-19% by adjusting the using amount of the ferric oxide to be 401-500 g; the reflectivity of the diffuse reflection plate can be adjusted to be 1-9% by adjusting the using amount of the ferric oxide to be 501-600 g.
When the oxide of iron is ferroferric oxide, the reflectivity of the diffuse reflection plate can be adjusted to 90-97% by adjusting the using amount of the ferroferric oxide to 0-10 g; the reflectivity of the diffuse reflection plate can be adjusted to 80-89% by adjusting the dosage of ferroferric oxide to 11-20 g; the reflectivity of the diffuse reflection plate can be adjusted to be 70-79% by adjusting the dosage of ferroferric oxide to be 21-30 g; the reflectivity of the diffuse reflection plate can be adjusted to be 60-69% by adjusting the dosage of ferroferric oxide to be 31-40 g; the reflectivity of the diffuse reflection plate can be adjusted to be 50-59% by adjusting the dosage of the ferroferric oxide to be 41-80 g; the reflectivity of the diffuse reflection plate can be adjusted to 40-49% by adjusting the using amount of ferroferric oxide to 81-100 g; the reflectivity of the diffuse reflection plate can be adjusted to be 30-39% by adjusting the dosage of ferroferric oxide to be 101-200 g; the reflectivity of the diffuse reflection plate can be adjusted to be 20-29% by adjusting the dosage of ferroferric oxide to be 201-300 g; the reflectivity of the diffuse reflection plate can be adjusted to be 10-19% by adjusting the dosage of ferroferric oxide to be 301-400 g; the reflectivity of the diffuse reflection plate can be adjusted to be 1-9% by adjusting the dosage of the ferroferric oxide to be 401-500 g.
In conclusion, the reflectivity can be adjusted from 1-97% by simply adjusting the addition of the iron oxide by compounding the water, the water-soluble tackifier and the sulfate in a specific ratio as fixed components, the operation is simple and convenient, and the efficiency is extremely high.
By preparing a large amount of fixed components for later use, the diffuse reflection plate spraying material can be prepared only by directly mixing iron oxide and the fixed components, so that the production efficiency is greatly improved; even if the diffuse reflection plate spraying material with high reflectivity is difficult to prepare due to excessive addition of iron oxide, the diffuse reflection plate spraying material can be repeatedly used for preparing the diffuse reflection plate spraying material with low reflectivity, so that the fault tolerance of the diffuse reflection plate spraying material can be improved, and the resource waste caused by the fact that the spraying material cannot be continuously applied due to wrong operation can be reduced.
In addition, the substances in the specific proportion are cooperatively compounded to serve as the diffuse reflection plate spraying material, so that the stability of the reflectivity of the diffuse reflection surface formed by the diffuse reflection spraying material is improved, the uncertainty is lower, the reflectivity of the diffuse reflection surface formed by the diffuse reflection plate spraying material tends to be the same regardless of the angle from which the diffuse reflection surface is detected, and the detection accuracy is improved better.
Preferably, the composition comprises the following components in parts by mass:
0-600 parts of ferric oxide;
10-500 parts of calcium sulfate;
500 parts of water;
1-150 parts of polyvinylpyrrolidone.
By compounding the specific substances, the stability of the reflectivity of the diffuse reflection surface formed by the diffuse reflection spraying material is favorably improved, the reflectivity of the diffuse reflection surface formed by the diffuse reflection plate spraying material tends to be the same no matter which angle the diffuse reflection surface is detected from, the uncertainty is lower, and the detection accuracy is favorably improved.
In a second aspect, the present application provides a method for preparing a diffuse reflection plate spray coating material, which adopts the following technical scheme:
a preparation method of the diffuse reflection plate spraying material comprises the step of uniformly mixing all the components at normal temperature to obtain the diffuse reflection plate spraying material.
The diffuse reflection plate spraying material can be prepared by directly and uniformly mixing the components at normal temperature, is simple and convenient to prepare and operate, is easy to realize, is beneficial to improving the production efficiency and is also beneficial to industrial production.
In a third aspect, the present application provides a diffuse reflection plate containing a diffuse reflection plate spray coating material, which adopts the following technical scheme:
a diffuse reflection plate containing the diffuse reflection plate spraying material comprises a substrate and the diffuse reflection plate spraying material sprayed on the surface of the substrate.
By adopting the diffuse reflection plate spraying material to be sprayed on the substrate to serve as the diffuse reflection plate, the diffuse reflection plates with different reflectivities can be prepared only by adjusting the dosage of ferroferric oxide, the operation is simple and convenient, and the production efficiency is favorably improved.
In a fourth aspect, the present application provides a method for preparing the diffuse reflection plate containing the diffuse reflection plate spraying material, which adopts the following technical scheme:
a preparation method of the diffuse reflection plate containing the diffuse reflection plate spraying material comprises the following steps:
step 1, preprocessing a substrate;
step 2, spraying the diffuse reflection plate spraying material according to claim 1 on a substrate;
and 3, curing the diffuse reflection plate spraying material to form a diffuse reflection surface, and thus obtaining the diffuse reflection plate containing the diffuse reflection plate spraying material.
The substrate is pretreated by cleaning, grinding and the like, so that the diffuse reflection plate spraying material is more firmly attached to the surface of the diffuse reflection plate, and the diffuse reflection plate spraying material is easier to spray; in addition, the diffuse reflection plate spraying material can be firmly attached to the surface of the substrate through spraying and curing, and the operation is simple and convenient.
In a fifth aspect, the present application provides an application of the diffuse reflection plate containing the diffuse reflection plate spray coating material, which adopts the following technical scheme:
the diffuse reflection plate containing the diffuse reflection plate spraying material is applied to an unmanned distance test or an identification test or a ring light source uniformity distribution test or a camera uniformity test or a laser target positioning or backlight illumination or an environment test target plate or an optical reflector or a remote sensing target or a simulation target.
The diffuse reflection plate can be applied to multiple fields and has a wide application range; and the reflectivity precision of the diffuse reflection plate is high, and the precision of the test application is improved to a certain extent.
In summary, the present application has the following beneficial effects:
1. the water, the water-soluble tackifier and the sulfate in a specific proportion are compounded to serve as fixed components, so that the reflectivity can be adjusted from 1% -97% by simply adjusting the addition of iron oxide, the operation is simple and convenient, and the efficiency is extremely high.
2. By preparing a large amount of fixed components for standby, the diffuse reflection plate spraying material can be prepared only by directly mixing iron oxide and the fixed components, and the production efficiency is greatly improved.
3. If the addition amount of the iron oxide is too large, the diffuse reflection plate spraying material with high reflectivity is difficult to prepare, and the diffuse reflection plate spraying material can be repeatedly used for preparing the diffuse reflection plate spraying material with low reflectivity, so that the fault tolerance of the diffuse reflection plate spraying material preparation is favorably improved, and the resource waste caused by the fact that the spraying material cannot be continuously applied due to wrong operation is favorably reduced.
4. The diffuse reflection plate spraying material can be prepared by directly and uniformly mixing the components at normal temperature, is simple and convenient to prepare and operate, is easy to realize, is beneficial to improving the production efficiency and is also beneficial to industrial production.
5. The diffuse reflection plate spraying material is sprayed on the substrate to serve as the diffuse reflection plate, so that the diffuse reflection plates with different reflectivity can be prepared only by adjusting the using amount of the iron oxide, the operation is simple and convenient, and the production efficiency is improved.
6. The substrate is pretreated by cleaning, grinding and the like, so that the diffuse reflection plate spraying material is favorably and firmly attached to the surface of the diffuse reflection plate, and the diffuse reflection plate spraying material is easier to spray; in addition, the diffuse reflection plate spraying material can be firmly attached to the surface of the substrate through spraying and curing, and the operation is simple and convenient.
7. The diffuse reflection plate can be applied to multiple fields, and the application range is wide; and the reflectivity precision of the diffuse reflection plate is high, and the precision of the test application is improved to a certain extent.
Detailed Description
The present application will be described in further detail with reference to examples.
In the following examples, all the substances are commercially available, specifically, the molecular weight of polyacrylamide is 800 ten thousand; the polyethylene glycol is polyethylene glycol 6000; the polymerization degree of the polyvinyl alcohol is 800; the CAS number of carbomer resin is 76050-42-5; the CAS number of sodium polyacrylate is 9003-04-7; polyvinylpyrrolidone has a CAS number of 9003-39-8.
Example 1
The embodiment of the application discloses a diffuse reflection plate spraying material which comprises the following components:
0g of ferrous oxide; 50g of sodium sulfate; 500g of water; 50g of polyacrylamide.
The embodiment of the application also discloses a preparation method of the diffuse reflection plate spraying material, which comprises the following specific steps:
step 1, adding polyacrylamide into 250g of water, and stirring and dispersing the polyacrylamide uniformly at the temperature of 60 ℃ to form a mixed solution.
And 2, adding the sodium sulfate solid into the residual 250g, stirring until the sodium sulfate solid is completely dissolved, adding ferrous oxide into the aqueous solution of sodium sulfate, and uniformly stirring and dispersing to form a turbid liquid.
And 3, adding the turbid liquid into the mixed liquid, and treating for 20min by using ultrasonic waves of 25kHz to obtain the diffuse reflection spraying material.
Example 2: the difference from example 1 is that: the amount of added ferrous oxide was 15g.
Example 3: the difference from example 1 is that: the amount of ferrous oxide added was 30g.
Example 4: the difference from example 1 is that: the amount of added ferrous oxide was 31g.
Example 5: the difference from example 1 is that: the amount of ferrous oxide added was 45g.
Example 6: the difference from example 1 is that: the amount of ferrous oxide added was 60g.
Example 7: the difference from example 1 is that: the amount of ferrous oxide added was 61g.
Example 8: the difference from example 1 is that: the amount of ferrous oxide added was 70g.
Example 9: the difference from example 1 is that: the amount of added ferrous oxide was 80g.
Example 10: the difference from example 1 is that: the amount of ferrous oxide added was 81g.
Example 11: the difference from example 1 is that: the amount of ferrous oxide added was 100g.
Example 12: the difference from example 1 is that: the amount of added ferrous oxide was 120g.
Example 13: the difference from example 1 is that: the amount of added ferrous oxide was 121g.
Example 14: the difference from example 1 is that: the amount of added ferrous oxide was 160g.
Example 15: the difference from example 1 is that: the amount of added ferrous oxide was 200g.
Example 16: the difference from example 1 is that: the amount of added ferrous oxide was 201g.
Example 17: the difference from example 1 is that: the amount of added ferrous oxide was 275g.
Example 18: the difference from example 1 is that: the amount of added ferrous oxide was 350g.
Example 19: the difference from example 1 is that: the amount of added ferrous oxide was 351g.
Example 20: the difference from example 1 is that: the amount of added ferrous oxide was 400g.
Example 21: the difference from example 1 is that: the amount of added ferrous oxide was 450g.
Example 22: the difference from example 1 is that: the amount of added ferrous oxide was 451g.
Example 23: the difference from example 1 is that: the amount of added ferrous oxide was 525g.
Example 24: the difference from example 1 is that: the amount of ferrous oxide added was 600g.
Example 25: the difference from example 1 is that: the amount of added ferrous oxide was 601g.
Example 26: the difference from example 1 is that: the amount of added ferrous oxide was 650g.
Example 27: the difference from example 1 is that: the amount of ferrous oxide added was 700g.
Example 28: the difference from example 1 is that: the amount of added ferrous oxide was 701g.
Example 29: the difference from example 1 is that: the amount of added ferrous oxide was 750g.
Example 30: the difference from example 1 is that: the amount of ferrous oxide added was 800g.
Example 31: the difference from example 1 is that: the ferrous oxide was replaced with ferric oxide, and the amount of ferric oxide added was 15g.
Example 32: the difference from example 31 is that: the amount of iron oxide added was 16g.
Example 33: the differences from example 31 are: the amount of iron oxide added was 30g.
Example 34: the difference from example 31 is that: the amount of iron oxide added was 31g.
Example 35: the differences from example 31 are: the amount of iron oxide added was 40g.
Example 36: the differences from example 31 are: the amount of iron oxide added was 41g.
Example 37: the differences from example 31 are: the amount of iron oxide added was 50g.
Example 38: the difference from example 31 is that: the amount of iron oxide added was 60g.
Example 39: the differences from example 31 are: the amount of iron oxide added was 61g.
Example 40: the differences from example 31 are: the amount of iron oxide added was 80g.
Example 41: the difference from example 31 is that: the amount of iron oxide added was 100g.
Example 42: the differences from example 31 are: the amount of iron oxide added was 101g.
Example 43: the differences from example 31 are: the amount of iron oxide added was 150g.
Example 44: the differences from example 31 are: the amount of iron oxide added was 200g.
Example 45: the differences from example 31 are: the amount of iron oxide added was 201g.
Example 46: the differences from example 31 are: the amount of iron oxide added was 250g.
Example 47: the difference from example 31 is that: the amount of iron oxide added was 300g.
Example 48: the difference from example 31 is that: the amount of iron oxide added was 301g.
Example 49: the difference from example 31 is that: the amount of iron oxide added was 350g.
Example 50: the difference from example 31 is that: the amount of iron oxide added was 400g.
Example 51: the differences from example 31 are: the amount of iron oxide added was 401g.
Example 52: the differences from example 31 are: the amount of iron oxide added was 450g.
Example 53: the difference from example 31 is that: the amount of iron oxide added was 500g.
Example 54: the difference from example 31 is that: the amount of iron oxide added was 501g.
Example 55: the differences from example 31 are: the amount of iron oxide added was 550g.
Example 56: the differences from example 31 are: the amount of iron oxide added was 600g.
Example 57: the difference from example 1 is that: the ferrous oxide is replaced by ferroferric oxide, and the addition amount of the ferroferric oxide is 10g.
Example 58: the difference from example 57 is that: the addition amount of ferroferric oxide is 11g.
Example 59: the difference from example 57 is that: the addition amount of ferroferric oxide is 20g.
Example 60: the difference from example 57 is that: the addition amount of ferroferric oxide is 21g.
Example 61: the differences from example 57 are: the addition amount of ferroferric oxide is 30g.
Example 62: the differences from example 57 are: the addition amount of ferroferric oxide is 31g.
Example 63: the differences from example 57 are: the addition amount of the ferroferric oxide is 40g.
Example 64: the differences from example 57 are: the addition amount of ferroferric oxide is 41g.
Example 65: the difference from example 57 is that: the addition amount of ferroferric oxide is 60g.
Example 66: the differences from example 57 are: the addition amount of ferroferric oxide is 80g.
Example 67: the difference from example 57 is that: the addition amount of ferroferric oxide is 81g.
Example 68: the differences from example 57 are: the addition amount of ferroferric oxide is 90g.
Example 69: the differences from example 57 are: the addition amount of ferroferric oxide is 100g.
Example 70: the differences from example 57 are: the addition amount of ferroferric oxide is 101g.
Example 71: the differences from example 57 are: the addition amount of ferroferric oxide is 150g.
Example 72: the difference from example 57 is that: the addition amount of the ferroferric oxide is 200g.
Example 73: the differences from example 57 are: the addition amount of ferroferric oxide is 201g.
Example 74: the difference from example 57 is that: the addition amount of ferroferric oxide is 250g.
Example 75: the difference from example 57 is that: the addition amount of the ferroferric oxide is 300g.
Example 76: the difference from example 57 is that: the addition amount of ferroferric oxide is 301g.
Example 77: the differences from example 57 are: the addition amount of ferroferric oxide is 350g.
Example 78: the difference from example 57 is that: the addition amount of ferroferric oxide is 400g.
Example 79: the differences from example 57 are: the addition amount of ferroferric oxide is 401g.
Example 80: the differences from example 57 are: the addition amount of the ferroferric oxide is 450g.
Example 81: the difference from example 57 is that: the addition amount of ferroferric oxide is 500g.
Example 82: the difference from example 1 is that: the dosage of each component is different, and the specific dosage is as follows:
0g of ferrous oxide; 600g of sodium sulfate; 1000g of water; 150g of polyacrylamide.
Example 83: the differences from example 82 are: the amount of ferrous oxide added was 30g.
Example 84: the differences from example 82 are: the amount of added ferrous oxide was 31g.
Example 85: the differences from example 82 are: the amount of added ferrous oxide was 60g.
Example 86: the difference from example 82 is that: the amount of ferrous oxide added was 61g.
Example 87: the differences from example 82 are: the amount of ferrous oxide added was 80g.
Example 88: the differences from example 82 are: the amount of ferrous oxide added was 81g.
Example 89: the difference from example 82 is that: the amount of added ferrous oxide was 120g.
Example 90: the differences from example 82 are: the amount of added ferrous oxide was 121g.
Example 91: the differences from example 82 are: the amount of added ferrous oxide was 200g.
Example 92: the differences from example 82 are: the amount of added ferrous oxide was 201g.
Example 93: the difference from example 82 is that: the amount of added ferrous oxide was 350g.
Example 94: the difference from example 82 is that: the amount of added ferrous oxide was 351g.
Example 95: the differences from example 82 are: the amount of added ferrous oxide was 450g.
Example 96: the difference from example 82 is that: the amount of added ferrous oxide was 451g.
Example 97: the difference from example 82 is that: the amount of ferrous oxide added was 600g.
Example 98: the difference from example 82 is that: the amount of added ferrous oxide was 601g.
Example 99: the difference from example 82 is that: the amount of ferrous oxide added was 700g.
Example 100: the differences from example 82 are: the amount of added ferrous oxide was 701g.
Example 101: the difference from example 82 is that: the amount of added ferrous oxide was 800g.
Example 102: the difference from example 82 is that: the ferrous oxide was replaced with ferric oxide, and the amount of ferric oxide added was 15g.
Example 103: the difference from the embodiment 102 is that: the amount of iron oxide added was 16g.
Example 104: the difference from the embodiment 102 is that: the amount of iron oxide added was 30g.
Example 105: the difference from the embodiment 102 is that: the amount of iron oxide added was 31g.
Example 106: the difference from the embodiment 102 is that: the amount of iron oxide added was 40g.
Example 107: the difference from the embodiment 102 is that: the amount of iron oxide added was 41g.
Example 108: the difference from the embodiment 102 is that: the amount of iron oxide added was 60g.
Example 109: the difference from the embodiment 102 is that: the amount of iron oxide added was 61g.
Example 110: the difference from the embodiment 102 is that: the amount of iron oxide added was 100g.
Example 111: the difference from the embodiment 102 is that: the amount of iron oxide added was 101g.
Example 112: the difference from the embodiment 102 is that: the amount of iron oxide added was 200g.
Example 113: the difference from the embodiment 102 is that: the amount of iron oxide added was 201g.
Example 114: the difference from the embodiment 102 is that: the amount of iron oxide added was 300g.
Example 115: the difference from the embodiment 102 is that: the amount of iron oxide added was 301g.
Example 116: the difference from the embodiment 102 is that: the amount of iron oxide added was 400g.
Example 117: the difference from the embodiment 102 is that: the amount of iron oxide added was 401g.
Example 118: the difference from the embodiment 102 is that: the amount of iron oxide added was 500g.
Example 119: the difference from the embodiment 102 is that: the amount of iron oxide added was 501g.
Example 120: the difference from the embodiment 102 is that: the amount of iron oxide added was 600g.
Example 121: the differences from example 82 are: the ferrous oxide is replaced by ferroferric oxide, and the addition amount of the ferroferric oxide is 10g.
Example 122: the differences from example 121 are: the addition amount of ferroferric oxide is 11g.
Example 123: the differences from example 121 are: the addition amount of ferroferric oxide is 20g.
Example 124: the differences from example 121 are: the addition amount of ferroferric oxide is 21g.
Example 125: the difference from example 121 is that: the addition amount of ferroferric oxide is 30g.
Example 126: the difference from example 121 is that: the addition amount of ferroferric oxide is 31g.
Example 127: the difference from example 121 is that: the addition amount of ferroferric oxide is 40g.
Example 128: the difference from example 121 is that: the addition amount of ferroferric oxide is 41g.
Example 129: the difference from example 121 is that: the addition amount of ferroferric oxide is 80g.
Example 130: the differences from example 121 are: the addition amount of ferroferric oxide is 81g.
Example 131: the difference from example 121 is that: the addition amount of ferroferric oxide is 100g.
Example 132: the differences from example 121 are: the addition amount of ferroferric oxide is 101g.
Example 133: the differences from example 121 are: the addition amount of ferroferric oxide is 200g.
Example 134: the difference from example 121 is that: the addition amount of ferroferric oxide is 201g.
Example 135: the difference from example 121 is that: the addition amount of the ferroferric oxide is 300g.
Example 136: the differences from example 121 are: the addition amount of ferroferric oxide is 301g.
Example 137: the difference from example 121 is that: the addition amount of ferroferric oxide is 400g.
Example 138: the differences from example 121 are: the addition amount of ferroferric oxide is 401g.
Example 139: the difference from example 121 is that: the addition amount of ferroferric oxide is 500g.
Example 140: the difference from example 82 is that: equal amounts of polyethylene glycol were substituted for polyacrylamide.
Example 141: the differences from example 82 are: equal amounts of polyvinyl alcohol were substituted for polyacrylamide.
Example 142: the difference from example 82 is that: equal amounts of carbomer resin were substituted for polyacrylamide.
Example 143: the difference from example 82 is that: the polyacrylamide was replaced with an equal amount of sodium polyacrylate.
Example 144: the difference from example 82 is that: equal amounts of hydroxypropyl methylcellulose were substituted for polyacrylamide.
Example 145: the difference from example 82 is that: equal amount of sodium carboxymethylcellulose was substituted for polyacrylamide.
Example 146: the difference from example 82 is that: the polyacrylamide was replaced with an equal amount of hydroxyethyl cellulose.
Example 147: the difference from example 82 is that: the polyacrylamide was replaced with an equal amount of xanthan gum.
Example 148: the difference from example 82 is that: equal amounts of barium sulfate were used instead of sodium sulfate.
Example 149: the difference from example 82 is that: equal amounts of copper sulfate were used instead of sodium sulfate.
Example 150: the differences from example 82 are: equal amount of potassium aluminum sulfate was used instead of sodium sulfate.
Example 151: the difference from example 82 is that: equal amount of aluminum sulfate was used instead of sodium sulfate.
Example 152: the difference from example 1 is that: the dosage of each component is different, and the specific dosage is as follows:
0g of iron oxide; 150g of calcium sulfate; 500g of water; 50g of polyvinylpyrrolidone.
Example 153: the difference from example 1 is that: the dosage of each component is different, and the specific dosage is as follows:
300g of iron oxide; 200g of calcium sulfate; 700g of water; 100g of polyvinylpyrrolidone.
Comparative example 1
The application discloses a diffuse reflection coating, which consists of the following components in parts by mass:
31g of barium sulfate; 20g of organic silicon resin; 6g of methyl etherified high imino melamine resin; 10.3g of composite sol; 8g of titanium dioxide; 4g of modified barium sulfate whisker; 0.5g of defoaming agent; 0.2g of fluorine-containing silane coupling agent; 20g of solvent.
In this comparative example, the silicone resin was FJN-9801 self-drying silicone resin; the methyl etherified high imino melamine resin is a product of CYMEL 325 of the American Cyanite company; the model of the defoaming agent is BYK-037; the fluorine-containing silane coupling agent is tridecafluorooctyltrimethylsilane; the solvent is formed by mixing dimethyl nylon acid and ethyl acetate according to the mass ratio of 1.
The preparation method of the composite sol comprises the following steps: adding 5g of 3-aminopropyltriethoxysilane, 25g of absolute ethyl alcohol, 2g of acetic acid and 2.5g of hexadecyl trimethyl ammonium chloride into 50g of deionized water, and uniformly stirring at 60 ℃ to obtain a first mixed solution; adding 18g of metal oxide with reflection performance into 32g of absolute ethyl alcohol, uniformly dispersing, adding 2g of stearic acid and 0.4g of gamma-glycidoxypropyltrimethoxysilane, and uniformly stirring at 75 ℃ to obtain a second mixed solution; and then dropping 1g of the second mixed solution into 3g of the first mixed solution, and carrying out ultrasonic treatment for 40min at 500W to obtain the composite sol.
Wherein the metal oxide with reflection performance is prepared from magnesium oxide and titanium dioxide according to the mass ratio of 1:0.5 is mixed.
The preparation method of the modified barium sulfate whisker comprises the following steps: 20g of barium sulfate whiskers (the barium sulfate whiskers have an average particle size of 100 μm, a compressive strength of 100MPa and a density of 0.25 g/cm) 3 ) 1g of citric acid is added into 79g of 10% sulfuric acid aqueous solution, and the mixture is uniformly dispersed to obtain barium sulfate whisker mixed solution; adding 4g of graphene into the barium sulfate whisker mixed solution, dripping 0.8g of n-octyltriethoxysilane into the mixed solution in a water bath at the temperature of 80 ℃, stirring the mixed solution at the rotating speed of 800rpm for 100min, filtering the mixed solution, taking a filter cake, drying the filter cake, and grinding the filter cake to 2000 meshes to obtain the modified barium sulfate whisker.
The application comparative example also discloses a preparation method of the diffuse reflection coating, which comprises the following specific steps:
31g of barium sulfate; 20g of organic silicon resin; 6g of methyl etherified high imino melamine resin; 10.3g of composite sol; 8g of titanium dioxide; 4g of modified barium sulfate whisker; 0.5g of defoaming agent; 0.2g of fluorine-containing silane coupling agent; 20g of solvent
Adding organic silicon resin, methyl etherified high imino group melamine resin, a composite sol defoaming agent and a fluorine-containing silane coupling agent into a solvent, raising the temperature to 50 ℃, preserving the heat for 90min, stirring and mixing uniformly to form a solution, reducing the temperature of the solution to 30 ℃, adding titanium dioxide, stirring uniformly, continuously adding modified barium sulfate whiskers, stirring uniformly, adding barium sulfate, and stirring uniformly to obtain the diffuse reflection coating.
Comparative example 2: the difference from comparative example 1 is that: the diffuse reflective coating also included 30g of ferrous oxide, with the ferrous oxide added last.
Comparative example 3: the difference from comparative example 1 is that: the diffuse reflective coating also included 60g of ferrous oxide, with the ferrous oxide added last.
Comparative example 4: the difference from comparative example 1 is that: the diffuse reflective coating also included 80g of ferrous oxide, with the ferrous oxide added last.
Comparative example 5: the difference from comparative example 1 is that: the diffuse reflective coating also included 120g of ferrous oxide, with ferrous oxide added last.
Comparative example 6: the difference from comparative example 1 is: the diffuse reflective coating also included 200g of ferrous oxide, with the ferrous oxide added last.
Comparative example 7: the difference from comparative example 1 is: the diffuse reflective coating also included 350g of ferrous oxide, with the ferrous oxide added last.
Comparative example 8: the difference from comparative example 1 is that: the diffuse reflective coating also included 450g of ferrous oxide, with the ferrous oxide added last.
Comparative example 9: the difference from comparative example 1 is that: the diffuse reflective coating also included 600g of ferrous oxide, with the ferrous oxide added last.
Comparative example 10: the difference from comparative example 1 is that: the diffuse reflective coating also included 700g of ferrous oxide, with the ferrous oxide added last.
Comparative example 11: the difference from comparative example 1 is that: the diffuse reflective coating also included 800g of ferrous oxide, with the ferrous oxide added last.
Comparative example 12: the difference from comparative example 1 is that: the diffuse reflective coating also included 15g of iron oxide, with the iron oxide added last.
Comparative example 13: the difference from comparative example 1 is that: the diffuse reflective coating also included 40g of iron oxide, with the iron oxide added last.
Comparative example 14: the difference from comparative example 1 is: the diffuse reflective coating also included 100g of iron oxide, with the iron oxide added last.
Comparative example 15: the difference from comparative example 1 is that: the diffuse reflective coating also included 300g of iron oxide, with the iron oxide added last.
Comparative example 16: the difference from comparative example 1 is: the diffuse reflective coating also included 500g of iron oxide, with the iron oxide added last.
Comparative example 17: the difference from comparative example 1 is that: the diffuse reflection coating also comprises 10g of ferroferric oxide, and the ferroferric oxide is added at the end.
Comparative example 18: the difference from comparative example 1 is that: the diffuse reflection coating also comprises 30g of ferroferric oxide, and the ferroferric oxide is added at the end.
Comparative example 19: the difference from comparative example 1 is that: the diffuse reflection coating also comprises 80g of ferroferric oxide, and the ferroferric oxide is added at the end.
Comparative example 20: the difference from comparative example 1 is that: the diffuse reflection coating also comprises 200g of ferroferric oxide, and the ferroferric oxide is added at the end.
Comparative example 21: the difference from comparative example 1 is: the diffuse reflection coating also comprises 400g of ferroferric oxide, and the ferroferric oxide is added at the end.
Application example 1
The application example of the application discloses a diffuse reflection plate containing a diffuse reflection plate spraying material, which comprises a substrate and the diffuse reflection plate spraying material uniformly sprayed on the surface of the substrate.
In this application example, the substrate was an aluminum plate, and the diffuse reflection plate spray material was the diffuse reflection plate spray material prepared in example 1. In other application examples, the substrate may be other metal plate or alloy metal plate, glass plate, acrylic plate, cloth substrate, or the like.
The application example of the application also discloses a preparation method of the diffuse reflection plate containing the diffuse reflection plate spraying material, which comprises the following steps:
step 1, pre-treating a substrate, specifically as follows:
firstly, cleaning a substrate, and carrying out deoiling treatment on the substrate to ensure that the surface of the substrate is free of oil stains; and then, grinding the surface of the substrate by using a grinding agent to make the surface of the substrate rough.
And 2, loading the corresponding diffuse reflection plate spraying material into a spray gun of the spraying chamber, and uniformly spraying the diffuse reflection plate spraying material on the surface of the substrate by using the spray gun. Controlling the spraying amount of a spray gun at 50-70g/min, after uniformly covering a layer of diffuse reflection plate spraying material on the surface of the substrate, drying the substrate in the air, continuously spraying the diffuse reflection plate spraying material on the dried diffuse reflection surface, drying the substrate in the air, continuously spraying the substrate until the diffuse reflection plate spraying material is sprayed for 7 layers, stopping spraying, and controlling the total spraying thickness of the diffuse reflection spraying material to be 1mm.
And 3, placing the substrate which is subjected to spraying in a ventilation place for natural drying, and curing the diffuse reflection plate spraying material to obtain the diffuse reflection plate containing the diffuse reflection plate spraying material.
Application examples 2 to 153
The difference from application example 1 is that: the diffuse reflection plate coating materials correspond to the diffuse reflection plate coating materials prepared in examples 2 to 153, respectively.
Comparative application examples 1 to 21
The difference from application example 1 is that: the diffuse reflection plate spray coating materials correspond to the diffuse reflection plate spray coating materials prepared in comparative examples 1 to 21, respectively.
Experiment 1
The reflectance (%) of the diffusely reflecting plate prepared in the above application example and comparative application example was measured according to JJG 453-2002 Standard color plate test protocols.
The data from the above experiments are detailed in table 1.
TABLE 1
According to the data comparison of application examples 1-153 in table 1, the sulfate, the tackifier and the water in specific proportions are adopted as fixed components, the dosage range of other components can be fixed, and the adjustment of the reflectivity of the spraying material by 1% -97% can be realized only by adjusting the corresponding addition amount of the iron oxide, so that the operation is simple and convenient, the production efficiency can be greatly improved, and the economic value is great.
According to the comparison of the data of comparative application examples 1 to 21 in table 1, the base material of the spray coating conventionally used at present is compounded with the iron oxide, and the adjustment of the reflectivity cannot be realized by adjusting the dosage of the iron oxide, that is, the fixed components and the adjustment amount corresponding to the iron oxide in the technical scheme of the application both need to be specifically matched to realize the adjustment of the reflectivity.
According to the comparison between the data of the application example 1 and the data of the application examples 152-153 in the table 1, the iron oxide, the calcium sulfate, the water and the polyvinylpyrrolidone in a specific proportion are compounded, so that the adjustment accuracy is improved better, the corresponding relation between the adjustment amount of the iron oxide and the corresponding reflectivity is more accurate and reliable, the reflectivity is adjusted more simply and conveniently, and the production efficiency is higher.
The above embodiments are preferred embodiments of the present application, and the protection scope of the present application is not limited by the above embodiments, so: equivalent changes in structure, shape and principle of the present application shall be covered by the protection scope of the present application.
Claims (10)
1. A diffuse reflection plate spraying material is characterized in that: the composition comprises the following components in parts by mass:
0-800 parts of iron oxide;
50-600 parts of sulfate;
500-1000 parts of water;
50-150 parts of a water-soluble tackifier.
2. A diffuse reflector coating material according to claim 1, wherein: the water-soluble tackifier comprises one or more of polyethylene glycol, polyvinyl alcohol, polyacrylamide, polyvinylpyrrolidone, carbomer resin, sodium polyacrylate, hydroxypropyl methylcellulose, sodium carboxymethylcellulose, hydroxyethyl cellulose and xanthan gum.
3. A diffuse reflector coating material according to claim 2, wherein: the water-soluble tackifier comprises one or more of polyethylene glycol, polyvinyl alcohol, polyacrylamide and polyvinylpyrrolidone.
4. A diffuse reflector coating material according to any of claims 1-3, wherein: the iron oxide comprises one or more of ferrous oxide, ferric oxide and ferroferric oxide.
5. A diffuse reflector coating material according to any of claims 1-3, wherein: the sulfate comprises one or more of calcium sulfate, barium sulfate, copper sulfate, aluminum potassium sulfate, sodium sulfate and aluminum sulfate.
6. A diffuse reflector coating material according to any of claims 1-3, wherein: the composition comprises the following components in parts by mass:
0-600 parts of ferric oxide;
150-200 parts of calcium sulfate;
500-700 parts of water;
50-100 parts of polyvinylpyrrolidone.
7. A method of making a diffusely reflecting plate spray material as in claim 1, further comprising: and (3) uniformly mixing the components at normal temperature to obtain the diffuse reflection plate spraying material.
8. A diffuse reflection plate containing a diffuse reflection plate spraying material is characterized in that: comprising a substrate and a diffusely reflecting plate coating material as claimed in any of claims 1 to 6 applied to a surface of the substrate.
9. A method of making a diffusely reflecting plate including a diffusely reflecting plate coating material as recited in claim, wherein: the method comprises the following steps:
step 1, preprocessing a substrate;
step 2, spraying the diffuse reflection plate spraying material according to claim 1 on a substrate;
and 3, curing the diffuse reflection plate spraying material to form a diffuse reflection surface, and thus obtaining the diffuse reflection plate containing the diffuse reflection plate spraying material.
10. Use of a diffusely reflecting plate comprising a diffusely reflecting plate coating material as claimed in any of the claims 3 to 7, characterized in that: the diffuse reflection plate containing the diffuse reflection plate spraying material is applied to an unmanned distance test, an identification test, a ring light source uniformity distribution test, a camera uniformity test, laser target positioning, backlight illumination, an environment test target plate, an optical reflector, a remote sensing target or a simulation target.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116543050A (en) * | 2023-05-26 | 2023-08-04 | 深圳铭创智能装备有限公司 | Transparent curved surface substrate positioning method, computer equipment and storage medium |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102115625A (en) * | 2009-12-31 | 2011-07-06 | 上海三思电子工程有限公司 | High-reflectivity diffuse reflection coating for LED lamp and preparation method thereof |
| CN103064134A (en) * | 2011-10-20 | 2013-04-24 | 佳能化成株式会社 | Inner surface anti-reflection blacking for optical element |
| CN103140556A (en) * | 2010-09-29 | 2013-06-05 | 日本油漆株式会社 | Aqueous coating composition |
| CN103358638A (en) * | 2012-04-04 | 2013-10-23 | 日本碧化学公司 | A metallic tone plastic and a plastic coating method |
| CN105949827A (en) * | 2016-05-24 | 2016-09-21 | 吉林蓝锐电子科技有限公司 | Diffuse-reflection coating and preparation method thereof |
| CN109143427A (en) * | 2018-09-03 | 2019-01-04 | 广州景颐光电科技有限公司 | A kind of diffusing reflection plate and preparation method thereof |
| CN113492096A (en) * | 2020-03-18 | 2021-10-12 | 关西涂料株式会社 | Method for forming multilayer coating film |
| CN114181618A (en) * | 2021-12-21 | 2022-03-15 | 广州常晖电子科技有限公司 | Laser radar diffuse reflection calibration plate |
| CN114539862A (en) * | 2022-03-24 | 2022-05-27 | 广州常晖电子科技有限公司 | Unmanned calibration plate and preparation method thereof |
-
2022
- 2022-08-01 CN CN202210918460.7A patent/CN115160880A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102115625A (en) * | 2009-12-31 | 2011-07-06 | 上海三思电子工程有限公司 | High-reflectivity diffuse reflection coating for LED lamp and preparation method thereof |
| CN103140556A (en) * | 2010-09-29 | 2013-06-05 | 日本油漆株式会社 | Aqueous coating composition |
| CN103064134A (en) * | 2011-10-20 | 2013-04-24 | 佳能化成株式会社 | Inner surface anti-reflection blacking for optical element |
| CN103358638A (en) * | 2012-04-04 | 2013-10-23 | 日本碧化学公司 | A metallic tone plastic and a plastic coating method |
| CN105949827A (en) * | 2016-05-24 | 2016-09-21 | 吉林蓝锐电子科技有限公司 | Diffuse-reflection coating and preparation method thereof |
| CN109143427A (en) * | 2018-09-03 | 2019-01-04 | 广州景颐光电科技有限公司 | A kind of diffusing reflection plate and preparation method thereof |
| CN113492096A (en) * | 2020-03-18 | 2021-10-12 | 关西涂料株式会社 | Method for forming multilayer coating film |
| CN114181618A (en) * | 2021-12-21 | 2022-03-15 | 广州常晖电子科技有限公司 | Laser radar diffuse reflection calibration plate |
| CN114539862A (en) * | 2022-03-24 | 2022-05-27 | 广州常晖电子科技有限公司 | Unmanned calibration plate and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116543050A (en) * | 2023-05-26 | 2023-08-04 | 深圳铭创智能装备有限公司 | Transparent curved surface substrate positioning method, computer equipment and storage medium |
| CN116543050B (en) * | 2023-05-26 | 2024-03-26 | 深圳铭创智能装备有限公司 | Transparent curved surface substrate positioning method, computer equipment and storage medium |
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