CN115159652A - Electrolyte processing system - Google Patents

Electrolyte processing system Download PDF

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Publication number
CN115159652A
CN115159652A CN202210739796.7A CN202210739796A CN115159652A CN 115159652 A CN115159652 A CN 115159652A CN 202210739796 A CN202210739796 A CN 202210739796A CN 115159652 A CN115159652 A CN 115159652A
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CN
China
Prior art keywords
frame
collecting
blocking
reaction cylinder
electrolyte
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Withdrawn
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CN202210739796.7A
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Chinese (zh)
Inventor
王雨桐
刘大志
施善国
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Anhui Medical College
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Anhui Medical College
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Priority to CN202210739796.7A priority Critical patent/CN115159652A/en
Publication of CN115159652A publication Critical patent/CN115159652A/en
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00—Other mixers; Mixing plants; Combinations of mixers
    • B01F33/40—Mixers using gas or liquid agitation, e.g. with air supply tubes
    • B01F33/402—Mixers using gas or liquid agitation, e.g. with air supply tubes comprising supplementary stirring elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/192—Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements
    • B01F27/1921—Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements comprising helical elements and paddles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/23—Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis
    • B01F27/232—Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis with two or more rotation axes
    • B01F27/2322—Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by the orientation or disposition of the rotor axis with two or more rotation axes with parallel axes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/70—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
    • B01F27/701—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms comprising two or more shafts, e.g. in consecutive mixing chambers
    • B01F27/706—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms comprising two or more shafts, e.g. in consecutive mixing chambers with all the shafts in the same receptacle
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/72—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with helices or sections of helices
    • B01F27/721—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with helices or sections of helices with two or more helices in the same receptacle
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
    • B01F31/44—Mixers with shaking, oscillating, or vibrating mechanisms with stirrers performing an oscillatory, vibratory or shaking movement
    • B01F31/445—Mixers with shaking, oscillating, or vibrating mechanisms with stirrers performing an oscillatory, vibratory or shaking movement performing an oscillatory movement about an axis
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00—Multistage treatment of water, waste water or sewage
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption

Abstract

The invention discloses an electrolyte processing system which comprises a base frame, a settling tank, a supporting plate, a reaction cylinder, a cover plate, a neutralizing mechanism, a collecting mechanism, a liquid discharging mechanism, an air pump and supporting legs, wherein the base frame is provided with a plurality of support plates; the invention solves the problems that the flow exchange rate of the electrolyte between the upper layer, the middle layer and the lower layer of the reaction container and the rate of the slaked lime converted from the accumulation state to the dispersion state are difficult to be improved by the traditional mixing and stirring mode in the electrolyte recycling and processing operation process, so that the neutralization reaction rate is low, the multi-stage uniform filtering and screening of the mixed liquid after the reaction is difficult, the impurities are discharged, the reaction precipitate is difficult to be collected, the separation degree between the clear liquid and the precipitate in the mixed liquid is reduced, the operation intensity of secondary recycling of the collected impurity particles and the precipitate by workers is increased, and the efficiency of the later-stage cleaning and maintenance operation is also reduced.

Description

Electrolyte processing system
Technical Field
The invention relates to the field of electrolyte processing, in particular to an electrolyte processing system.
Background
The electrolyte is a medium used by chemical batteries, electrolytic capacitors and the like, and has large content difference when being used in different industries. The electrolyte in the battery industry is prepared by special sulfuric acid and distilled water according to a certain proportion, the density is generally 1.24-1.30G/cubic centimeter, the specific gravity is 12.75-12.85G/CM3 sulfuric acid and pure water, the sulfuric acid belongs to a strong corrosive chemical reagent, when the battery reaches the service life, the old battery is required to be recycled, the residual electrolyte is further subjected to harmless treatment, components of acid and alkali can be exchanged by neutralization reaction, salt and water are generated, a chemical reaction with the chemical formula of Ca (OH) 2 + H2 4 = CaSO 4 +2H 2O is adopted, the electrolyte can be subjected to harmless treatment, and calcium sulfate in a reaction product can be used as a raw material for manufacturing cement, calcium sulfate hemihydrate and sulfuric acid, and can be used as a raw material for manufacturing a fertilizer for reducing the properties of SOSO 4 +2H 2O, the performances of the calcium sulfate and the soil slake, and the soil slake can be improved, however, the following problems exist in the agricultural chemical fertilizer production process:
(1) In the process of carrying out neutralization reaction of the electrolyte, because impurities are often doped in the electrolyte of the old battery and the hydrated lime is accumulated at the bottom of the reaction container in a granular shape, the traditional mixing and stirring mode is difficult to improve the flow exchange rate of the electrolyte among the upper layer, the middle layer and the lower layer of the reaction container and the rate of the transition of the hydrated lime from the accumulation state to the dispersion state, and the neutralization reaction rate is low.
(2) In the neutralization reaction process of carrying out electrolyte, be difficult to accomplish the multistage even filtration screening of back mixed liquid to the reaction, discharge impurity and collect the processing to the reaction precipitate, reduced the separation degree between clear liquid and the precipitate in the mixed liquid, increased the operating strength that the staff carries out quadratic recycle to the foreign particles and the precipitate of collecting, also reduced the efficiency of later stage washing maintenance operation.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides an electrolyte processing system, which solves the problems in the background art.
The technical scheme adopted by the invention for solving the technical problem is as follows: the utility model provides an electrolyte processing system, includes bed frame, setting tank, backup pad, reaction cylinder, apron, neutralization mechanism, collection mechanism, drainage mechanism, air pump and supporting legs, bed frame lower extreme all install the supporting legs all around, the setting tank is installed to the upper end of bed frame, drainage mechanism is installed to the well lower part of setting tank, collection mechanism is installed on the well upper portion of setting tank, the backup pad is installed to the upper end of setting tank, the backup pad is located the top of collecting the mechanism and the upper end of backup pad is installed reaction cylinder, neutralization mechanism is installed to the lower extreme of reaction cylinder, the lower extreme outer wall fixed mounting of reaction cylinder has the air pump, the air pump is linked together through trachea and neutralization mechanism, the apron is installed to the upper end of reaction cylinder.
The neutralizing mechanism comprises a guide plate, a storage bin, a mixing spray head, a blocking groove, a blocking plate, an electromagnet, a blocking spring, a mixing rotating shaft, a spiral blade and a stirring rod, wherein the guide plate is symmetrically and obliquely arranged at the lower end of a reaction cylinder, the included angle between the guide plates is an obtuse angle, the storage bin is arranged on the reaction cylinder close to the lower end of the guide plate, an incompletely-closed annular cavity is formed between the storage bin and the guide plate, the blocking groove is formed in the lower end of the storage bin, the blocking plate is arranged in the blocking groove in a sliding fit manner, the upper ends of the left side and the right side of the blocking plate are connected with the upper end of the notch of the blocking groove through the blocking spring, the electromagnet is correspondingly arranged in the middle of the blocking plate and the middle of the notch at the upper end of the blocking groove, the middle part of guide plate is radially evenly installed and is mixed the shower nozzle, the input of mixing the shower nozzle is linked together through trachea and air pump, the delivery outlet of mixing the shower nozzle all is towards the direction of hindering the groove, the lower extreme middle part of reaction cylinder installs through the bearing symmetry and mixes the pivot, and mix the pivot and be located between the storage silo of symmetry installation, evenly install helical blade through the mode of key-type connection in the mixing pivot, helical blade all is located the oblique top position department in hindering the groove, it has the multiunit puddler to peg graft along its circumference in the mixing pivot, annular space through guide plate and storage silo formation, can make the spun air current further produce the vortex at the in-process that blows in the mixing shower nozzle, and blow away the accumulational lime slaking and carry out abundant mixing reaction between messenger's and the electrolyte.
Specifically, reaction cylinder lower extreme and the backup pad middle part symmetry adjacent thereto seted up the charging conduit, and the charging conduit of reaction cylinder lower extreme is located between the guide plate, install the closing plate through sliding fit's mode symmetry between the charging conduit at reaction cylinder lower extreme and the charging conduit at backup pad middle part, under the closed condition, closing plate and charging conduit are sealed to be cooperated, the closing plate all is connected with the lower terminal surface of reaction cylinder through sealing spring, the upper end fixed mounting of backup pad has sealed cylinder, and sealed cylinder's output shaft is connected with the closing plate.
The utility model discloses a storage silo, the J font structure of the cross sectional shape handstand of storage silo, the vortex groove has been seted up to the circular-arc upper end of storage silo, the mode fixed mounting through the key-type connection has the vortex pivot in the vortex groove, evenly install the vortex pole through normal running fit's mode in the vortex pivot, and the lower extreme of vortex pole extends to the toroidal cavity middle part that storage silo and guide plate enclose, the flow through air current and electrolyte can make the vortex pole carry out the horizontal hunting in the vortex pivot, promote the hydrated lime by piling up the speed that the state changes to the disperse state, still can increase the production of bubble in the air current through the separation effect of vortex pole to the air current simultaneously.
Specifically, vortex pole and puddler be glass material, promote corrosion-resistant effect.
The utility model discloses a filter, collect the mechanism including collecting the pivot, the spacing ring, the stopper, spacing spring, the follower, collect the frame, filter and stack frame, the middle part left and right sides of setting tank installs through the bearing symmetry and collects the pivot, the outer end tip of collecting the pivot installs the follower through the mode symmetry of key-type connection, the middle part left and right sides outer wall symmetry of setting tank installs the spacing ring, and the center of spacing ring coincides with the axle center of collecting the pivot mutually, the interior anchor symmetry of spacing ring is provided with the stopper, stopper and follower are supported to lean on the contact and stopper and are connected through spacing spring between the follower, the inner cross section of collecting the pivot is the rectangle structure, and collect the mode of installing through the joint between the inner of pivot and collect the frame, collect the frame and all be provided with open-ended rectangle box structure for both ends from top to bottom, the lower extreme open position department of collecting the frame evenly installs the filter, the stack frame is evenly installed to the filter that the stack frame was adjacent interval was arranged, the filter that sets up in the bottom of collecting the frame can carry out preliminary filtration screening to mixed liquid, make the solution part in the mixed liquid pass through and continue to flow downwards, mix in sediment and the reaction remains the granule and the mixed liquid is filtered and is dismantled the activity to the joint and is accomplished the mixed liquid through the quick removal of collecting the formula and is installed.
Specifically, stopper and follow-up piece be vertical distribution in the spacing ring, and the symmetry is provided with the fretwork groove on the ring lateral wall of spacing ring, the follow-up piece is located the notch of fretwork and the follow-up piece can carry out the rotation of certain degree of freedom in the fretwork notch.
Specifically, the stacker upper end be incomplete confined toper structure, the middle part of stacker is provided with the cavity, and the lower extreme of cavity and the up end looks parallel and level of filter, evenly seted up the liquid outlet on the toper lateral wall of stacker, and the lower extreme of liquid outlet is a little higher than the up end of filter, the toper inner chamber of stacker can be convenient for the entering of granule deposit and difficult discharge, the liquid outlet of setting can be convenient for mix solution discharge in the liquid.
Specifically, the backup pad around both ends all install the pressure boost shower nozzle, the input of pressure boost shower nozzle all is linked together through trachea and air pump, the output of pressure boost shower nozzle is located the below of backup pad and the output of pressure boost shower nozzle is located respectively and collects both ends tip top around the frame.
It is specific, the collection frame around both ends tip all be provided with the groove of keeping out the wind, and keep out the wind the groove respectively with the backup pad around the pressure boost shower nozzle on both ends corresponding, set up in the groove of keeping out the wind at collection frame both ends can promote the windage of the air current flow in-process, further the mixed liquid of cooperation flows at the inboard asymmetry of collection frame, the reinforcing is collected the both ends of frame and is blown down the effect that carries out the reciprocal luffing motion of circulation under the intermittent type of air current, promote the flow area of mixed liquid in collection frame bottom, the promotion is to remaining granule and the collection efficiency that blocks that deposits in the mixed liquid.
Specifically, the drainage mechanism comprises a material blocking rod, a material blocking rotating shaft, material blocking blades, adsorption cotton, a torsional spring, a rotating plate, a vibration frame, a stirring frame, a liquid discharging port, a liquid discharging frame and a liquid discharging cylinder, wherein the material blocking rod is uniformly arranged between the side walls of the left side and the right side of the middle lower part of the sedimentation box in a key connection mode, the cross section of the material blocking rod positioned on the inner side of the sedimentation box is of a T-shaped structure, the material blocking rotating shaft is symmetrically arranged on the middle lower part of the material blocking rod in the front and back direction through a bearing, the material blocking blades are arranged on the middle part of the material blocking rotating shaft in the key connection mode, the material blocking blades positioned on two adjacent material blocking rods are in butt fit, the adsorption cotton is arranged in the middle parts of the material blocking blades, one end of the material blocking rotating shaft is exposed on the outer side of the material blocking rod, the rotating plate is arranged on the end part of the material blocking rotating shaft in the key connection mode, and the rotating plate is connected with the side walls of the sedimentation box through the torsional spring, the vibrating frames are symmetrically arranged on the front and back of the side wall of the settling tank close to one side of the rotating plate, the stirring frames are arranged between the vibrating frames in a sliding fit mode, clamping jaws are uniformly arranged at the lower end of each stirring frame, the clamping jaws correspond to the stop rods one by one and are abutted against the upper end face of the rotating plate, liquid discharging ports are symmetrically arranged on the front and back of the bottom of the settling tank and are communicated with the inner cavity of the settling tank, the lower end of the settling tank and the middle part of the base frame adjacent to the lower end of the settling tank are jointly provided with a liquid discharging frame in a sliding fit mode, the upper end of the liquid discharging frame is abutted against the lower end of the stop rods, the middle part of the lower end of the base frame is provided with a liquid discharging cylinder, an output shaft of the liquid discharging cylinder is connected with the liquid discharging frames, and the arranged adsorption cotton can perform secondary blocking on impurities in the sediment, so that the separation degree between the sediment and the mixed liquid is improved, and the secondary recovery and cleaning of collected impurity particles and the sediment are convenient for workers, the efficiency of later stage cleaning maintenance operation is promoted.
The invention has the beneficial effects that:
(1) According to the electrolyte processing system, the annular space formed by the guide plate and the storage bin can further generate vortex in the blowing process of air flow sprayed from the mixing spray head, the accumulated hydrated lime is blown away to enable the accumulated hydrated lime to be fully mixed and reacted with electrolyte, the turbulence rods can swing left and right on the turbulence rotating shafts through the flow of the air flow and the electrolyte, the speed of the hydrated lime changing from the accumulation state to the dispersion state is increased, meanwhile, the generation amount of bubbles in the air flow can be increased through the blocking effect of the turbulence rods on the air flow, the bubbles generated in the air flow flowing process can float upwards under the action of self buoyancy, then flow to the middle upper position of the reaction cylinder from the annular gap position between the guide plate and the storage bin, the flow exchange rate of the electrolyte between the upper layer, the middle layer and the lower layer of the reaction cylinder is increased through the flow of the bubbles, and the continuous rotation of the spiral blades and the stirring rods is matched, so that the uniform degree of mixing of each layer of secondary mixed liquid in the reaction cylinder is further increased, and the neutralization reaction rate is increased.
(2) According to the electrolyte processing system, the filter plate arranged at the bottom of the collecting frame can carry out primary filtering and screening on the mixed liquid, so that the solution in the mixed liquid partially passes through and continuously flows downwards, the residual particles and precipitates doped in the mixed liquid and subjected to neutralization reaction are blocked and left, the conical inner cavity of the stacking frame can facilitate the particles to enter and cannot be discharged easily, the solution in the mixed liquid can be discharged conveniently, the wind blocking grooves arranged at the two ends of the collecting frame can improve the wind resistance in the air flow flowing process, the asymmetric flowing of the mixed liquid at the inner side of the collecting frame is further matched, the effect that the two ends of the collecting frame carry out circular reciprocating up-and-down swinging under the intermittent blowing of the air flow is enhanced, the flowing area of the mixed liquid at the bottom of the collecting frame is improved, the blocking and collecting efficiency on the residual particles and the precipitates in the mixed liquid is improved, the collecting frame mounted in a movable clamping mode can rapidly detach the mixed liquid after the complete filtering of the mixed liquid, the absorbing cotton can carry out secondary blocking on the impurities in the precipitates, the precipitates in the mixed liquid, the separation degree between the clear liquid and the precipitates in the mixed liquid is improved, the secondary cleaning operation of workers and the recovery operation of the collected impurities particles and the precipitates is facilitated, and the post-stage cleaning operation of the workers.
Drawings
The invention is further illustrated with reference to the following figures and examples.
FIG. 1 is a schematic diagram of an overall structure of a preferred embodiment of an electrolyte processing system according to the present invention;
FIG. 2 is a top view of FIG. 1 in accordance with the present invention;
FIG. 3 isbase:Sub>A schematic cross-sectional view taken along line A-A of FIG. 2 in accordance with the present invention;
FIG. 4 is an enlarged view of the area B of FIG. 3 according to the present invention;
FIG. 5 is a schematic cross-sectional view taken along the line C-C of FIG. 2 in accordance with the present invention;
FIG. 6 is a partial perspective sectional view of the neutralizing mechanism, the collecting mechanism and the drainage mechanism of the present invention;
FIG. 7 is a first partial perspective view of the neutralization mechanism of the present invention;
FIG. 8 is a second partial perspective view of the neutralization mechanism of the present invention;
FIG. 9 is a partial perspective view of the sealing plate and the reaction cylinder according to the present invention;
FIG. 10 is a schematic view of a partial perspective view of the collection and drainage mechanisms of the present invention;
FIG. 11 is an enlarged view taken at D of FIG. 10 in accordance with the present invention;
FIG. 12 is an enlarged view of FIG. 10 at E according to the present invention;
FIG. 13 is a schematic view of a partial perspective view of the collection mechanism of the present invention;
in the figure: 1. a base frame; 2. a settling tank; 3. a support plate; 4. a reaction cylinder; 5. a cover plate; 6. a neutralization mechanism; 7. a collection mechanism; 8. a liquid discharge mechanism; 9. an air pump; 10. supporting legs; 61. a baffle; 62. a storage bin; 63. a mixing nozzle; 64. a blocking groove; 65. a damming board; 66. an electromagnet; 67. a blocking spring; 68. a mixing spindle; 69. a helical blade; 610. a stirring rod; 31. a charging chute; 311. a sealing plate; 312. a seal spring; 32. sealing the cylinder; 621. a flow disturbing groove; 6211. a turbulent flow rotating shaft; 6212. a spoiler bar; 71. collecting the rotating shaft; 72. a limiting ring; 73. a limiting block; 74. a limiting spring; 75. a follower block; 76. a collection rack; 77. a filter plate; 78. a stacking rack; 781. a liquid outlet; 33. a pressurized spray head; 761. a wind shield groove; 81. a material blocking rod; 82. a material blocking rotating shaft; 83. a material blocking blade; 84. adsorbing cotton; 85. a torsion spring; 86. rotating the plate; 87. a vibration frame; 88. a toggle frame; 89. a liquid discharge port; 810. a draining rack; 811. liquid drainage cylinder.
Detailed Description
The present invention will be further described with reference to the following detailed description so that the technical means, the creation features, the achievement purposes and the effects of the present invention can be easily understood.
According to the embodiment of the invention, through the electrolyte processing system, the problem that in the process of carrying out neutralization reaction of the electrolyte, impurities are often doped in the electrolyte of an old battery, and hydrated lime is accumulated at the bottom of a reaction container in a granular manner is solved, and the traditional mixing and stirring mode is difficult to improve the flow exchange rate of the electrolyte among the upper layer, the middle layer and the lower layer of the reaction container and the rate of the hydrated lime from the accumulation state to the dispersion state, so that the neutralization reaction rate is low;
and in the neutralization reaction process of the electrolyte, the multi-stage uniform filtering and screening of the mixed liquid after the reaction is finished is difficult to perform, impurities are discharged, and reaction precipitates are collected and processed, so that the separation degree between clear liquid and the precipitates in the mixed liquid is reduced, the operation intensity of secondary recycling of collected impurity particles and the precipitates by workers is increased, and the efficiency of later-stage cleaning and maintenance operation is also reduced.
In order to solve the technical problems, the technical scheme in the embodiment of the invention has the following general idea: according to the invention, through an annular space formed by the guide plate 61 and the storage bin 62, the air flow sprayed out of the mixing spray head can further generate vortex in the blowing process, the accumulated slaked lime is blown away to be subjected to full mixing reaction with the electrolyte, the turbulence bar 6212 can swing left and right on the turbulence rotating shaft 6211 through the flow of the air flow and the electrolyte, the speed of the slaked lime from the accumulation state to the dispersion state is increased, meanwhile, the generation amount of bubbles in the air flow can be increased through the blocking effect of the turbulence bar 6212 on the air flow, the bubbles generated in the air flow flowing process can float upwards under the action of self-buoyancy, then flow to the middle upper position of the reaction cylinder 4 from the annular gap position between the guide plate 61 and the storage bin 62, the flow exchange speed of the electrolyte between the upper layer, the middle layer and the lower layer of the reaction cylinder 4 is increased through the flow of the bubbles, and the continuous rotation of the spiral blade 69 and the stirring rod 610 is matched, and the uniform degree of the mixed liquid among all layers in the reaction cylinder 4 is further increased;
set up filter 77 in collection frame 76 bottom can carry out preliminary filtration screening to mixed liquid, make the solution part in the mixed liquid pass through and continue to flow downwards, dope in mixed liquid and react residual particle and deposit and be blockked and leave, the toper inner chamber of stack frame 78 can be convenient for the entering of granule deposit and difficult discharge, the solution discharge in the mixed liquid can be convenient for to set up liquid outlet 781, set up the wind-break groove 761 at collection frame 76 both ends can promote the windage of air current flow in-process, further cooperate mixed liquid is at the inboard asymmetric flow of collection frame 76, strengthen the both ends of collection frame 76 and carry out the effect of reciprocating luffing motion under the intermittent type of air current blows down, promote the area of flowing through of mixed liquid in collection frame 76 bottom, promote the collection efficiency that blocks of remaining granule and deposit in the mixed liquid, and can dismantle it after mixed liquid complete filtration completion through collection frame 76 of activity joint formula installation, the absorption cotton 84 that sets up can carry out the secondary to the impurity in the deposit and separate the shelves, promote the separation degree between clear liquid and the precipitate, make things convenient for the staff to carry out the impurity particle of collection and deposit and carry out the later maintenance and the later stage cleaning operation of secondary and promote the recovery.
Referring to fig. 1 and 2, an electrolyte processing system comprises a base frame 1, a settling tank 2, a supporting plate 3, a reaction cylinder 4, a cover plate 5, a neutralizing mechanism 6, a collecting mechanism 7, a liquid draining mechanism 8, an air pump 9 and supporting legs 10, wherein the supporting legs 10 are all installed on the periphery of the lower end of the base frame 1, the settling tank 2 is installed at the upper end of the base frame 1, the liquid draining mechanism 8 is installed at the middle lower part of the settling tank 2, the collecting mechanism 7 is installed at the middle upper part of the settling tank 2, the supporting plate 3 is installed at the upper end of the settling tank 2, the reaction cylinder 4 is installed above the collecting mechanism 7 and at the upper end of the supporting plate 3, the neutralizing mechanism 6 is installed at the lower end of the reaction cylinder 4, the air pump 9 is fixedly installed on the outer wall of the lower end of the reaction cylinder 4, the air pump 9 is communicated with the neutralizing mechanism 6 through an air pipe, and the cover plate 5 is installed at the upper end of the reaction cylinder 4;
referring to fig. 3, fig. 8 and fig. 9, the blanking groove 31 has been seted up to reaction cylinder 4 lower extreme and the 3 middle part symmetries of backup pad adjacent to it, and the blanking groove 31 of reaction cylinder 4 lower extreme is located between the guide plate 61, install closing plate 311 through sliding fit's mode symmetry between the blanking groove 31 at reaction cylinder 4 lower extreme and the blanking groove 31 at backup pad 3 middle part, under closed condition, closing plate 311 and blanking groove 31 seal up the cooperation, closing plate 311 all is connected with the lower terminal surface of reaction cylinder 4 through sealing spring 312, the upper end fixed mounting of backup pad 3 has sealed cylinder 32, and the output shaft of sealed cylinder 32 is connected with closing plate 311.
During specific work, firstly, the sealing cylinder 32 is started to work, the sealing plates 311 which are symmetrically installed are enabled to move close to each other in the feeding chute 31 through the sealing cylinder 32 until the sealing plates 311 completely abut against the joint, the sealing operation on the feeding chute 31 is carried out through the joint action between the sealing plates 311, and the sealing operation on the bottom of the reaction cylinder 4 is further realized.
Referring to fig. 3, 4 and 8, the neutralizing mechanism 6 includes a guide plate 61, a storage bin 62, a mixing nozzle 63, a blocking groove 64, a blocking plate 65, an electromagnet 66, a blocking spring 67, a mixing rotating shaft 68, a helical blade 69 and a stirring rod 610, the guide plates 61 are symmetrically and obliquely mounted at the lower end of the reaction cylinder 4, an included angle between the guide plates 61 is an obtuse angle, the storage bin 62 is mounted on the reaction cylinder 4 near the lower end of the guide plate 61, an incompletely closed annular cavity is formed between the storage bin 62 and the guide plate 61, the blocking groove 64 is formed at the lower end of the storage bin 62, the blocking plate 65 is mounted in the blocking groove 64 in a sliding fit manner, the upper ends of the left and right sides of the blocking plate 65 are connected with the upper end of the notch of the blocking groove 64 through the blocking spring 67, the middle portions of the blocking plate 65 and the middle portion of the upper end of the blocking groove 64 are both correspondingly provided with the electromagnet 66, the middle portion of the guide plate 61 is uniformly provided with the mixing nozzle 63 in a radial direction, the input end of the mixing nozzle 63 is communicated with the air pump 9 through an air pipe, the output port of the mixing nozzle 63 faces the direction of the blocking groove 64, the mixing nozzle 68 is mounted at a position symmetrically above the mixing shaft 68, the mixing shaft is mounted on the mixing rod 610, the mixing shaft 68, the mixing rod is mounted at a symmetric position above the mixing shaft 68, and connected with the mixing rod 610;
during the specific operation, firstly, the PH value of the electrolyte to be neutralized is manually measured and weighed, then, through calculation, a proper amount of hydrated lime for neutralization reaction is uniformly put into the annular cavity formed between the storage bin 62 and the guide plate 61 (in the process, the electromagnet 66 is de-energized, the blocking plate 65 is pushed by the elastic force of the blocking spring 67 to tightly abut against the lower half section of the blocking groove 64, and the closing operation of the notch of the blocking groove 64 is carried out), then, the electrolyte to be neutralized is manually poured into the reaction cylinder 4 to carry out the neutralization reaction between the electrolyte and the hydrated lime, and in the process of the neutralization reaction, the air pump 9 is started to work, the air flow generated in the air pump 9 is guided and conveyed by the air pipe to the mixing nozzle 63, and then, the air flow is further blown into the reaction cylinder 4 along the side wall of the guide plate 61 through the operation of the mixing nozzle 63, because the annular space is arranged between the guide plate 61 and the storage bin 62, the air flow further generates vortex in the blowing process and drives the electrolyte in the annular space to synchronously flow, the accumulated slaked lime starts to be gradually dispersed under the co-flow action of the air flow and the electrolyte, the dispersed slaked lime and the electrolyte which is not neutralized are fully contacted and mixed, air bubbles generated in the air flow flowing process can float upwards under the action of self buoyancy, then the air bubbles flow to the middle upper position of the reaction cylinder 4 from the annular gap position between the guide plate 61 and the storage bin 62, the flow exchange rate of the electrolyte among the upper layer, the middle layer and the lower layer of the reaction cylinder 4 is improved through the flow of the air bubbles, and the reaction rate of neutralization reaction is further improved by matching with the dissipation flow of the slaked lime;
after the accumulated hydrated lime is completely dispersed, electrifying the electromagnet 66, generating magnetic force after electrifying the electromagnet 66 and adsorbing and driving the blocking plate 65 to move towards the upper half section of the blocking groove 64, so that the lower half section of the blocking groove 64 is gradually opened, then under the blowing action of air flow, the mixed liquid inside the annular cavity gradually passes through the blocking groove 64 and flows to the middle part of the lower end of the reaction cylinder 4, because the guide plates 61 are obliquely and symmetrically arranged, the mixed liquid flowing in two directions flows upwards along the side wall of the storage bin 62 after being mixed in the middle part of the reaction cylinder 4, the mixed liquid in the upper half part of the reaction cylinder 4 synchronously enters the inner side of the storage bin 62 again from the gap position of the annular cavity, and in the process that the mixed liquid flows out from the blocking groove 64, the spiral blades 69 are synchronously driven to rotate, the mixing rotating shaft 68 is driven to rotate by the spiral blades 69, the mixing shaft 68 is further driven to synchronously rotate the stirring rod 610, and under the continuous rotation action of the stirring rod 610, the mixed liquid in each layer in the reaction cylinder 4 is further promoted to be uniformly mixed.
Referring to fig. 3, fig. 7 and fig. 8, the cross-sectional shape of the storage bin 62 is inverted J-shaped, a turbulent flow groove 621 is provided at the circular arc upper end of the storage bin 62, a turbulent flow rotating shaft 6211 is fixedly installed in the turbulent flow groove 621 through a key connection manner, a turbulent flow rod 6212 made of glass is evenly installed on the turbulent flow rotating shaft 6211 through a rotation fit manner, and the lower end of the turbulent flow rod 6212 extends to the middle of an annular cavity surrounded by the storage bin 62 and the flow guide plate 61.
During specific work, in the process of blowing air flow by the mixing nozzle 63, the air flow and the electrolyte flow to enable the turbulence rod 6212 to swing left and right on the turbulence rotating shaft 6211, the speed of changing the slaked lime from the accumulation state to the dispersion state is improved, meanwhile, the generation amount of bubbles is increased through the obstruction effect of the turbulence rod 6212 on the air flow, the flow exchange speed of the electrolyte is enhanced, and the neutralization reaction speed between the slaked lime and the electrolyte is further improved.
Referring to fig. 3, 6, 10, 11 and 12, the collecting mechanism 7 includes a collecting shaft 71, a limiting ring 72, a limiting block 73, a limiting spring 74, a follower block 75, a collecting frame 76, a filter plate 77 and a stacking frame 78, the collecting shaft 71 is symmetrically installed on the left and right sides of the middle of the settling tank 2 through bearings, the follower block 75 is symmetrically installed on the end of the outer end of the collecting shaft 71 through a key connection manner, the limiting rings 72 are symmetrically installed on the outer walls of the left and right sides of the middle of the settling tank 2, the center of the limiting ring 72 coincides with the axis of the collecting rotating shaft 71, the inner annular surface of the limiting ring 72 is symmetrically provided with limiting blocks 73, the limiting blocks 73 are in abutting contact with the follow-up block 75, the limiting blocks 73 are connected with the follow-up block 75 through limiting springs 74, the limiting blocks 73 and the follow-up block 75 are vertically distributed in the limiting ring 72, and the circular side wall of the limit ring 72 is symmetrically provided with hollow grooves, the follower block 75 is positioned in the hollow groove opening, the follower block 75 can rotate in the hollow groove opening with a certain degree of freedom, the cross section of the inner end of the collecting rotating shaft 71 is of a rectangular structure, and a collecting frame 76 is arranged between the inner ends of the collecting rotating shafts 71 in a clamping manner, the collecting frame 76 is of a rectangular box-shaped structure with openings at the upper end and the lower end, filter plates 77 are uniformly arranged at the opening position of the lower end of the collecting frame 76, stacking frames 78 are uniformly arranged at the opening position of the lower end of the collecting frame 76, the stacking frame 78 and the filter plate 77 are arranged at intervals, the upper end of the stacking frame 78 is in an incompletely closed conical structure, a cavity is arranged in the middle of the stacking frame 78, and the lower extreme of cavity and the up end looks parallel and level of filter 77, evenly seted up liquid outlet 781 on the toper lateral wall of stacker 78, and the lower extreme of liquid outlet 781 is a little higher than the up end of filter 77.
During the specific operation, after the neutralization reaction in the reaction cylinder 4 is completed, the cover plate 5 is manually installed at the upper end of the reaction cylinder 4, so that the inner side of the reaction cylinder 4 is in a closed state, then the sealing cylinder 32 is controlled to perform the reset operation, then the two sealing plates 311 tightly attached to each other under the action of the elastic force of the sealing spring 312 are gradually separated and opened, so that the lower end of the reaction cylinder 4 is in an opened state, then the mixed liquid accumulated in the reaction cylinder 4 gradually passes through the blanking chute 31 and is discharged downwards under the action of gravity and the pushing action of the air pressure in the reaction cylinder 4, and falls onto the collecting frame 76, the filter plate 77 arranged at the bottom of the collecting frame 76 can perform primary filtering and screening on the mixed liquid, so that the solution in the mixed liquid partially passes through and continuously flows downwards, and the neutralization reaction residual particles and precipitates doped in the mixed liquid are blocked and left;
in the process of flowing of the mixed liquid, the particle precipitate gradually enters the inner side space of the material stacking frame 78, the conical inner cavity of the material stacking frame 78 can facilitate the entering of the particle precipitate and is not easy to discharge, the arranged liquid outlet 781 can facilitate the discharge of the solution in the mixed liquid, and in the process of asymmetric flowing of the mixed liquid on the collecting frame 76, the front end and the rear end of the collecting frame 76 are enabled to generate weight change, further the collecting frame 76 and the collecting rotating shaft 71 are enabled to perform reciprocating up-and-down circulating swing on the inner side of the settling tank 2, the mixed liquid falling from the blanking tank 31 can be uniformly dispersed and spread at the bottom of the collecting frame 76, the blocking and collecting efficiency of the residual particles and the precipitate in the mixed liquid is improved, the limiting effect of the limiting ring 72 and the limiting block 73 on the circumferential rotating path of the follow-up block 75 can be avoided, the mixed liquid can be prevented from flowing out from the single side of the collecting frame 76 due to overlarge inclination angle of the collecting shaft 71, the collection effect of the impurity particles and the precipitate can be prevented from affecting the collection effect, the self-elastic force of the limiting spring 74 can provide a certain twisting force in the rotating process of the collecting frame 71, the reciprocating swing effect of the collecting frame 76 and the cleaning of the secondary cleaning of the collected liquid, and the secondary cleaning of the collected particles can be conveniently performed after the cleaning operation of the collected liquid, and the secondary cleaning of the collected liquid, and the collected liquid can be conveniently performed after the secondary cleaning operation of the secondary cleaning of the collected particles, and the collected liquid.
Referring to fig. 3, fig. 6, fig. 9 and fig. 11, backup pad 3 around both ends all install pressure boost shower nozzle 33, pressure boost shower nozzle 33's input all is linked together through trachea and air pump 9, pressure boost shower nozzle 33's output is located backup pad 3's below and pressure boost shower nozzle 33's output is located the front and back both ends tip top of collecting frame 76 respectively, collecting frame 76 around both ends tip all be provided with wind-blocking groove 761, and wind-blocking groove 761 is corresponding with pressure boost shower nozzle 33 on backup pad 3 front and back both ends respectively.
During specific work, when the collection frame 76 filters the mixed liquid, the air flow is conveyed into the pressurizing nozzles 33 through the air pump 9, then the pressurizing nozzles 33 at the front end and the rear end of the support plate 3 are further controlled to perform intermittent circulation air flow ejection operation, the ejected air flow is further blown to the positions of the two ends of the collection frame 76, the wind resistance in the air flow flowing process can be improved through the wind shielding grooves 761 arranged at the two ends of the collection frame 76, the mixed liquid flows inside the collection frame 76 in a further matching mode, the effect that the two ends of the collection frame 76 perform circular reciprocating up-and-down swinging under the intermittent blowing of the air flow is enhanced, the flowing area of the mixed liquid at the bottom of the collection frame 76 is improved, and the blocking efficiency of impurity particles and residues is further improved.
Referring to fig. 3, 6, 10 and 13, the liquid discharge mechanism 8 includes a material blocking rod 81, a material blocking rotating shaft 82, material blocking blades 83, adsorption cotton 84, a torsion spring 85, a rotating plate 86, a vibrating frame 87, a stirring frame 88, a liquid discharge port 89, a liquid discharge frame 810 and a liquid discharge cylinder 811, the material blocking rod 81 is uniformly installed between the left side wall and the right side wall of the middle lower part of the settling box 2 in a key connection mode, the cross section of the material blocking rod 81 positioned inside the settling box 2 is in a T-shaped structure, the material blocking rotating shaft 82 is symmetrically installed at the front and the rear of the middle lower part of the material blocking rod 81 through a bearing, the material blocking blades 83 are installed at the middle part of the material blocking rotating shaft 82 in a key connection mode, the material blocking blades 83 on two adjacent material blocking rods 81 are in abutting fit, the middle parts of the material blocking blades 83 are respectively provided with adsorption cotton 84, one end of each material blocking rotating shaft 82 is exposed outside the material blocking rods 81, the end parts of the material blocking rotating shafts 82 are provided with rotating plates 86 in a key connection mode, the rotating plates 86 are connected with the side walls of the settling box 2 through torsion springs 85, the side walls of the settling box 2 close to one side of each rotating plate 86 are symmetrically provided with vibrating frames 87 in the front-back direction, stirring frames 88 are arranged between the vibrating frames 87 in a sliding fit mode, the lower ends of the stirring frames 88 are uniformly provided with clamping claws, the clamping claws correspond to the material blocking rods 81 one by one and abut against the upper end faces of the rotating plates 86, the bottom of the settling box 2 is symmetrically provided with liquid discharge ports 89 in the front-back direction, and leakage fluid dram 89 is linked together with the inner chamber of setting tank 2, and the lower extreme of setting tank 2 and adjacent 1 middle parts of bed frame with it install drainage frame 810 jointly through sliding fit's mode, and the upper end of drainage frame 810 supports and leans on the lower extreme that keeps off material pole 81, and the lower extreme mid-mounting of bed frame 1 has flowing back cylinder 811, and drainage cylinder 811's output shaft is connected with drainage frame 810.
When the concrete work, under the initial condition, the material blocking rotating shaft 82 is under the torsion action of the torsion spring 85 to drive the material blocking blade 83 to be in a horizontal state all the time, the liquid discharging cylinder 811 is in a working state, the upper end of the liquid discharging frame 810 is jacked upwards by the output shaft of the liquid discharging cylinder 811 and is contacted with the lower end face of the material blocking rod 81, the middle lower part of the sedimentation tank 2 and the middle upper part of the sedimentation tank 2 are in a separated state through the abutting contact of the liquid discharging frame 810 and the inner side wall of the sedimentation tank 2, then the mixed liquid is filtered by the filter plate 77 and then further falls onto the material blocking blade 83 and is gradually stacked from bottom to top, after the mixed liquid completely falls down, proper standing and settling time is set, then, tiny suspended impurities in the mixed liquid are gradually precipitated on the upper layer surface of the material blocking blade 83, when the set standing time is up, the reset work is carried out by controlling the liquid drainage cylinder 811, the liquid drainage cylinder 811 drives the liquid drainage rack 810 to move downwards, the space of the lower layer of the material blocking blade 83 is opened, the accumulated mixed liquid synchronously passes through the adsorption cotton 84 and enters the cavity of the middle-lower part of the settling tank 2, the arranged adsorption cotton 84 can separate the impurities in the precipitate, when the upper end of the liquid drainage rack 810 falls below the hole position of the liquid drainage port 89, the clear liquid accumulated on the middle-lower part of the settling tank 2 gradually flows out from the liquid drainage port 89 under the action of gravity, then the clear liquid is manually recovered, and is discharged after the pH value is detected to be qualified;
at this moment, the precipitate that separates out in the mixed liquid still remains on keeping off material blade 83 and adsorbing cotton 84, afterwards, stir frame 88 and carry out reciprocating sliding on vibration frame 87 through the manual work, stir frame 88 and support between jack catch and the commentaries on classics board 86 and lean on pushing action messenger to keep off material pivot 82 self and produce the rotation in the downstream process, and drive and keep off material blade 83 and adsorb cotton 84 and carry out reciprocating rotation, make and keep off material blade 83 from carrying out the reciprocating switching of circulation between horizontal state and the vertical state, and at the in-process of switching, under the combined action of inertia and self gravity, the precipitate of piling up on adsorbing cotton 84 drops downwards gradually and piles up on flowing back frame 810, after the precipitate drops and accomplishes, scrape off and collect the precipitate of piling up on flowing back frame 810 through the manual work.
When in work:
the first step is as follows: firstly, starting a sealing cylinder 32 to work, enabling sealing plates 311 which are symmetrically installed to mutually approach and move in a charging chute 31 through the sealing cylinder 32 until the sealing plates 311 are completely abutted and attached, sealing the charging chute 31 through the attachment effect between the sealing plates 311, further realizing the sealing operation on the bottom of a reaction cylinder 4, then manually measuring the pH value of electrolyte which is required to be neutralized and weighing the pH value of the electrolyte, then uniformly throwing a proper amount of hydrated lime for neutralization reaction into an annular cavity formed between a storage bin 62 and a guide plate 61 through calculation (in the process, the electromagnet 66 is electrified, the lower blocking plate 65 is pushed by the elasticity of a blocking spring 67 to tightly abut against the lower half section of the blocking groove 64 to seal the notch of the blocking groove 64), and then manually pouring the electrolyte to be neutralized into the reaction cylinder 4 to carry out neutralization reaction between the electrolyte and the hydrated lime;
the second step is that: during the neutralization reaction, starting the air pump 9 to work, leading the air flow generated in the air pump 9 to be conveyed through an air pipe and then to reach the mixing nozzle 63, then further blowing the air flow into the reaction cylinder 4 along the side wall of the guide plate 61 through the work of the mixing nozzle 63, wherein the air flow further generates vortex in the blowing process and drives the electrolyte in the annular space to synchronously flow due to the annular space between the guide plate 61 and the storage bin 62, the accumulated slaked lime starts to be gradually dispersed under the co-flow action of the air flow and the electrolyte, the dispersed slaked lime and the electrolyte which is not neutralized are fully contacted and mixed, bubbles generated in the air flow process float upwards under the action of self-buoyancy, then flow to the middle upper position of the reaction cylinder 4 from the annular gap position between the guide plate 61 and the storage bin 62, the flow exchange rate of the electrolyte among the upper layer, the middle layer and the lower layer of the reaction cylinder 4 is improved through the flow of the bubbles, and the reaction rate of the neutralization reaction is further improved through the cooperation with the dissipation flow of the slaked lime;
the third step: after the accumulated hydrated lime is completely dispersed, electrifying the electromagnet 66, generating magnetic force after electrifying the electromagnet 66, adsorbing and driving the blocking plate 65 to move towards the upper half section of the blocking groove 64, gradually opening the lower half section of the blocking groove 64, then gradually passing the mixed liquid inside the annular cavity through the blocking groove 64 and flowing to the middle part of the lower end of the reaction cylinder 4 under the blowing action of air flow, wherein the guide plates 61 are obliquely and symmetrically arranged, the mixed liquid flowing in two directions flows upwards along the side wall of the storage bin 62 after being mixed in the middle part of the reaction cylinder 4, the mixed liquid in the upper half part of the reaction cylinder 4 synchronously enters the inner side of the storage bin 62 again from the gap position of the annular cavity, synchronously driving the spiral blades 69 to rotate in the process that the mixed liquid flows out from the blocking groove 64, driving the mixing rotating shaft 68 to rotate through the spiral blades 69, further driving the stirring rod 610 to synchronously rotate through the mixing rotating shaft 68, and further improving the uniform degree of the mixed liquid in each layer in the reaction cylinder 4 under the continuous rotation of the stirring rod 610;
the fourth step: in the process of blowing the air flow by the mixing nozzle 63, the air flow and the electrolyte flow to enable the turbulence rod 6212 to swing left and right on the turbulence rotating shaft 6211, so that the speed of the slaked lime converted from the accumulation state to the dispersion state is increased, meanwhile, the generation amount of bubbles is increased through the obstruction effect of the turbulence rod 6212 on the air flow, the flow exchange rate of the electrolyte is enhanced, and the neutralization reaction rate between the slaked lime and the electrolyte is further increased;
the fifth step: after the neutralization reaction in the reaction cylinder 4 is finished, the cover plate 5 is manually installed at the upper end of the reaction cylinder 4, so that the inner side of the reaction cylinder 4 is in a closed state, then the sealing cylinder 32 is controlled to perform reset operation, then the two sealing plates 311 which are tightly attached under the action of the elastic force of the sealing spring 312 are gradually separated and opened, so that the lower end of the reaction cylinder 4 is in an opened state, then the mixed liquid accumulated in the reaction cylinder 4 gradually passes through the blanking chute 31 and is discharged downwards under the action of gravity and the pushing action of the air pressure in the reaction cylinder 4, and falls onto the collecting frame 76, the filter plate 77 arranged at the bottom of the collecting frame 76 can perform primary filtering and screening on the mixed liquid, so that the solution in the mixed liquid partially passes through and continuously flows downwards, and the neutralization reaction residual particles and precipitates doped in the mixed liquid are blocked and left;
and a sixth step: in the process of flowing of the mixed liquid, the particle precipitate gradually enters the inner space of the material stacking frame 78, the conical inner cavity of the material stacking frame 78 can facilitate the entering of the particle precipitate and is not easy to discharge, the arranged liquid outlet 781 can facilitate the discharge of the solution in the mixed liquid, and in the process of asymmetric flowing of the mixed liquid on the collecting frame 76, the front end and the rear end of the collecting frame 76 generate weight change, so that the collecting frame 76 and the collecting rotating shaft 71 can perform reciprocating up-and-down cyclic swinging on the inner side of the settling tank 2, the mixed liquid falling from the blanking groove 31 can be uniformly dispersed and spread at the bottom of the collecting frame 76, the blocking and collecting efficiency of the residual particles and the precipitate in the mixed liquid is improved, through the limiting effect of the limiting ring 72 and the limiting block 73 on the circumferential rotation path of the follow-up block 75, the mixed liquid can be prevented from flowing out from one side of the collecting frame 76 due to the fact that the inclination angle of the collecting rotating shaft 71 is too large, the collecting effect on the impurity particles and the sediments is further influenced, the set limiting spring 74 can provide a certain degree of torsion force for the rotating process of the collecting rotating shaft 71 through self elasticity, the reciprocating swing effect of the collecting frame 76 is enhanced, the collecting frame 76 mounted in a movable clamping mode can rapidly disassemble the mixed liquid after the mixed liquid is completely filtered, secondary recovery and cleaning of the collected impurity particles and the sediments are facilitated for workers, and the efficiency of cleaning and maintenance operation in the later period is improved;
the seventh step: when the collection frame 76 filters the mixed liquid, air flow is conveyed into the pressurizing nozzles 33 through the air pump 9, then the pressurizing nozzles 33 at the front end and the rear end of the support plate 3 are further controlled to perform intermittent circulating air flow spraying operation, the sprayed air flow is further blown to the positions of the two ends of the collection frame 76, and the wind shielding grooves 761 arranged at the two ends of the collection frame 76 can improve wind resistance in the air flow flowing process, the mixed liquid flows inside the collection frame 76 in a further matched mode, the effect that the two ends of the collection frame 76 perform circulating reciprocating up-and-down swinging under the intermittent blowing of the air flow is enhanced, the flowing area of the mixed liquid at the bottom of the collection frame 76 is improved, and the blocking efficiency of impurity particles and residues is further improved;
eighth step: under the initial condition, the material blocking rotating shaft 82 is under the torsion action of a torsion spring 85 to drive the material blocking blade 83 to be in a horizontal placing state all the time, a liquid discharging cylinder 811 is in a working state, an output shaft of the liquid discharging cylinder 811 jacks up the upper end of a liquid discharging frame 810 and contacts with the lower end face of the material blocking rod 81, the middle-lower part of the settling tank 2 and the middle-upper part of the settling tank 2 are in a separated state through the abutting contact of the liquid discharging frame 810 and the inner side wall of the settling tank 2, then the mixed liquid further falls onto the material blocking blade 83 after being filtered by a filter plate 77 and is gradually accumulated from bottom to top, when the mixed liquid completely falls, a proper standing and settling time is set, and then fine suspended impurities in the mixed liquid are gradually settled on the upper layer face of the material blocking blade 83, when the set standing time is up, the reset operation is carried out by controlling the liquid discharge cylinder 811, the liquid discharge cylinder 811 drives the liquid discharge frame 810 to move downwards, the space of the lower layer of the material blocking blade 83 is opened, the accumulated mixed liquid synchronously passes through the adsorption cotton 84 and enters the cavity of the middle-lower part of the settling tank 2, the arranged adsorption cotton 84 can separate impurities in the precipitate, after the upper end of the liquid discharge frame 810 falls below the hole position of the liquid discharge port 89, the clear liquid accumulated at the lower part of the settling tank 2 gradually flows out from the liquid discharge port 89 under the action of gravity, then the clear liquid is manually recovered and is discharged after the PH value is detected to be qualified, and at the moment, the precipitate separated out from the mixed liquid still stays on the material blocking blade 83 and the adsorption cotton 84;
the ninth step: stirring frame 88 is promoted through the manual work and is carried out reciprocating sliding on vibration frame 87, stirring frame 88 makes fender material pivot 82 self produce the rotation through the jack catch and the supporting impetus between the commentaries on classics board 86 in the downward movement in-process, and drive and keep off material blade 83 and adsorb cotton 84 and carry out reciprocating rotation, make and keep off material blade 83 from carrying out the reciprocal switching of circulation between horizontal condition and the vertical state, and at the in-process that switches, under the combined action of inertia and self gravity, it drops and piles up on flowing back frame 810 downwards gradually to pile up the precipitate on adsorbing cotton 84, after the precipitate dropped the completion, scrape and collect the precipitate that will pile up on flowing back frame 810 through the manual work.
The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the embodiments and descriptions given above are only illustrative of the principles of the present invention, and various changes and modifications may be made without departing from the spirit and scope of the invention, which fall within the scope of the claims. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (10)

1. The utility model provides an electrolyte processing system, includes bed frame (1), setting tank (2), backup pad (3), reaction cylinder (4), apron (5), neutralization mechanism (6), collects mechanism (7), drainage mechanism (8), air pump (9) and supporting legs (10), its characterized in that: the device is characterized in that supporting legs (10) are arranged on the periphery of the lower end of the base frame (1), a settling tank (2) is arranged at the upper end of the base frame (1), a liquid drainage mechanism (8) is arranged at the middle lower part of the settling tank (2), a collecting mechanism (7) is arranged at the middle upper part of the settling tank (2), a supporting plate (3) is arranged at the upper end of the settling tank (2), the supporting plate (3) is positioned above the collecting mechanism (7), a reaction cylinder (4) is arranged at the upper end of the supporting plate (3), a neutralizing mechanism (6) is arranged at the lower end of the reaction cylinder (4), an air pump (9) is fixedly arranged on the outer wall of the lower end of the reaction cylinder (4), the air pump (9) is communicated with the neutralizing mechanism (6) through an air pipe, and a cover plate (5) is arranged at the upper end of the reaction cylinder (4);
the neutralizing mechanism (6) comprises a guide plate (61), a storage bin (62), a mixing spray head (63), blocking grooves (64), blocking plates (65), electromagnets (66), blocking springs (67), a mixing rotating shaft (68), helical blades (69) and a stirring rod (610), the guide plates (61) are symmetrically and obliquely arranged at the lower end of a reaction cylinder (4), the included angle between the guide plates (61) is an obtuse angle, the storage bin (62) is arranged on the reaction cylinder (4) close to the lower end of the guide plate (61), an incompletely closed annular cavity is formed between the storage bin (62) and the guide plate (61) together, the blocking grooves (64) are formed at the lower end of the storage bin (62), the blocking plates (65) are arranged in the blocking grooves (64) in a sliding fit manner, the upper ends of the left side and the right side of each blocking plate (65) are connected with the upper ends of notches of the blocking grooves (64) through the blocking springs (67), the electromagnets (66) are correspondingly arranged at the middle parts of the notches of the blocking plates (65) and the upper ends of the notches (64), the middle parts of the left side and the notches of the blocking grooves (61) are uniformly arranged with the upper ends of the mixing spray heads (63) along the radial direction, the mixing spray heads (63) and the mixing spray head (9) are communicated with the output port of the air pump (63), the lower end middle part of reaction cylinder (4) is installed through the bearing symmetry and is mixed pivot (68), and mixes pivot (68) and be located between the symmetrically installed storage silo (62), evenly installs helical blade (69) through the mode of key-type connection on mixing pivot (68), and helical blade (69) all are located the oblique top position department in stopping groove (64), and it has multiunit puddler (610) to peg graft along its circumference on mixing pivot (68).
2. The electrolyte processing system of claim 1, wherein: reaction cylinder (4) lower extreme and backup pad (3) middle part symmetry adjacent to it seted up silo (31), and silo (31) of reaction cylinder (4) lower extreme are located between guide plate (61), install closing plate (311) through sliding fit's mode symmetry between silo (31) of reaction cylinder (4) lower extreme and silo (31) at backup pad (3) middle part, under the closed condition, closing plate (311) and silo (31) are sealed to be cooperated, closing plate (311) all are connected with the lower terminal surface of reaction cylinder (4) through sealing spring (312), the upper end fixed mounting of backup pad (3) has sealed cylinder (32), and the output shaft of sealed cylinder (32) is connected with closing plate (311).
3. The electrolyte processing system of claim 1, wherein: the J font structure of the cross sectional shape handstand of storage silo (62), disturbed flow groove (621) has been seted up to the circular-arc upper end of storage silo (62), there is disturbed flow pivot (6211) through the mode fixed mounting of key-type connection in disturbed flow groove (621), disturbed flow pole (6212) are evenly installed through normal running fit's mode on disturbed flow pivot (6211), and the lower extreme of disturbed flow pole (6212) extends to the annular cavity middle part that storage silo (62) and guide plate (61) enclose.
4. The electrolyte processing system of claim 3, wherein: the turbulence rod (6212) and the stirring rod (610) are made of glass materials.
5. The electrolyte processing system of claim 1, wherein: the collecting mechanism (7) comprises a collecting rotating shaft (71), a limiting ring (72), a limiting block (73), a limiting spring (74), a follow-up block (75), a collecting frame (76), a filter plate (77) and a stacking frame (78), wherein the collecting rotating shaft (71) is symmetrically arranged on the left side and the right side of the middle part of the settling tank (2) through bearings, the follow-up block (75) is symmetrically arranged on the end part of the outer end of the collecting rotating shaft (71) in a key connection mode, the limiting ring (72) is symmetrically arranged on the outer wall of the left side and the right side of the middle part of the settling tank (2), the center of the limiting ring (72) coincides with the axis of the collecting rotating shaft (71), the inner ring surface of the limiting ring (72) is symmetrically provided with limiting blocks (73), the limiting blocks (73) are abutted and contacted with the follow-up block (75), the limiting blocks (73) are connected with the follow-up block (75) through limiting springs (74), the cross section of the inner end of the collecting rotating shaft (71) is of a rectangular structure, a collecting frame (76) is arranged between the inner ends of the collecting rotating shafts (71) in a clamping manner, the collecting frame (76) is of a rectangular box-shaped structure with openings at the upper end and the lower end, filter plates (77) are uniformly arranged at the opening position of the lower end of the collecting frame (76), a stacking frame (78) is uniformly arranged at the opening position of the lower end of the collecting frame (76), and the stacking frame (78) and the filter plate (77) are arranged adjacently at intervals.
6. The electrolyte processing system of claim 5, wherein: the limiting block (73) and the follow-up block (75) are vertically distributed in the limiting ring (72), hollow grooves are symmetrically formed in the circular side wall of the limiting ring (72), the follow-up block (75) is located in the hollow groove opening, and the follow-up block (75) can rotate in the hollow groove opening with a certain degree of freedom.
7. The electrolyte processing system of claim 5, wherein: the stacking frame (78) upper end be incomplete confined toper structure, the middle part of stacking frame (78) is provided with the cavity, and the lower extreme of cavity and the up end looks parallel and level of filter (77), liquid outlet (781) have evenly been seted up on the toper lateral wall of stacking frame (78), and the lower extreme of liquid outlet (781) is a little higher than the up end of filter (77).
8. The electrolyte processing system of claim 5, wherein: backup pad (3) around both ends all install pressure boost shower nozzle (33), the input of pressure boost shower nozzle (33) all is linked together through trachea and air pump (9), the output of pressure boost shower nozzle (33) is located the below of backup pad (3) and the output of pressure boost shower nozzle (33) is located respectively and collects the front and back both ends tip top of frame (76).
9. The electrolyte processing system of claim 8, wherein: the collecting frame (76) is provided with wind shielding grooves (761) at the front end and the rear end, and the wind shielding grooves (761) correspond to the pressurizing nozzles (33) at the front end and the rear end of the supporting plate (3) respectively.
10. The electrolyte processing system of claim 1, wherein: drainage mechanism (8) including striker rod (81), striker spindle (82), striker blade (83), adsorb cotton (84), torsional spring (85), commentaries on classics board (86), vibration frame (87), stir frame (88), leakage fluid dram (89), flowing back frame (810) and flowing back cylinder (811), striker rod (81) are evenly installed through the mode of key-type connection between the well lower part left and right sides lateral wall of setting tank (2), striker rod (81) cross section that is located setting tank (2) inboard is T font structure, striker spindle (82) are installed through symmetry around the bearing to the well lower part of striker rod (81), striker blade (83) are all installed through the mode of key-type connection in the middle part of striker spindle (82), and support between being located between the striker blade (83) on two adjacent striker rod (81) and lean on the cooperation, the middle part of striker blade (83) all is provided with and adsorbs cotton (84), the one end of striker spindle (82) exposes outside and the tip of striker rod (82) and installs through the mode of vibration spindle (86) and stir the lateral wall of key-type connection (86) between the terminal of symmetry spindle (87), the lateral wall (86) and the setting tank (2) and install through the mode of key-type connection between the sliding rack (86) and the lateral wall (85) of sliding rack (2), the lateral wall (85) that sliding rack (86) is connected around the side wall (2), the side wall (87), the side wall (85) is close to the setting tank (2) and the sliding rack (2) of symmetry The utility model discloses a set up the lower extreme of stirring frame (88) and evenly be provided with the jack catch, the jack catch all supports and leans on the up end that changes board (86) with striker rod (81) one-to-one and the jack catch, the symmetry is provided with leakage fluid dram (89) around the bottom of setting tank (2), and leakage fluid dram (89) are linked together with the inner chamber of setting tank (2), drainage frame (810) are installed jointly through sliding fit's mode in the lower extreme of setting tank (2) and adjacent bed frame (1) middle part with it, the upper end of drainage frame (810) supports and leans on the lower extreme at striker rod (81), drainage cylinder (811) are installed at the lower extreme mid-mounting of bed frame (1), the output shaft of drainage cylinder (811) is connected with drainage frame (810).
CN202210739796.7A 2022-06-28 2022-06-28 Electrolyte processing system Withdrawn CN115159652A (en)

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CN202210739796.7A CN115159652A (en) 2022-06-28 2022-06-28 Electrolyte processing system

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Application Number Priority Date Filing Date Title
CN202210739796.7A CN115159652A (en) 2022-06-28 2022-06-28 Electrolyte processing system

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117410608A (en) * 2023-12-11 2024-01-16 天津木华清研科技有限公司 Flow distribution assembly for separating and recycling electrolyte of waste batteries

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117410608A (en) * 2023-12-11 2024-01-16 天津木华清研科技有限公司 Flow distribution assembly for separating and recycling electrolyte of waste batteries
CN117410608B (en) * 2023-12-11 2024-04-12 天津木华清研科技有限公司 Flow distribution assembly for separating and recycling electrolyte of waste batteries

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Application publication date: 20221011