CN115109657A - Preparation method of beer bottle cleaning agent - Google Patents
Preparation method of beer bottle cleaning agent Download PDFInfo
- Publication number
- CN115109657A CN115109657A CN202210764778.4A CN202210764778A CN115109657A CN 115109657 A CN115109657 A CN 115109657A CN 202210764778 A CN202210764778 A CN 202210764778A CN 115109657 A CN115109657 A CN 115109657A
- Authority
- CN
- China
- Prior art keywords
- tank body
- cleaning agent
- tank
- bevel gear
- bottle cleaning
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000012459 cleaning agent Substances 0.000 title claims abstract description 53
- 235000013405 beer Nutrition 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- 229960000892 attapulgite Drugs 0.000 claims abstract description 42
- 229910052625 palygorskite Inorganic materials 0.000 claims abstract description 42
- 239000007788 liquid Substances 0.000 claims abstract description 39
- 238000005192 partition Methods 0.000 claims abstract description 33
- 239000006185 dispersion Substances 0.000 claims abstract description 28
- 238000002156 mixing Methods 0.000 claims abstract description 26
- 230000007246 mechanism Effects 0.000 claims abstract description 13
- 238000007599 discharging Methods 0.000 claims abstract description 5
- 229910000831 Steel Inorganic materials 0.000 claims description 25
- 239000010959 steel Substances 0.000 claims description 25
- 238000003756 stirring Methods 0.000 claims description 19
- 238000005406 washing Methods 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 16
- 239000002994 raw material Substances 0.000 claims description 14
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- AEQDJSLRWYMAQI-UHFFFAOYSA-N 2,3,9,10-tetramethoxy-6,8,13,13a-tetrahydro-5H-isoquinolino[2,1-b]isoquinoline Chemical compound C1CN2CC(C(=C(OC)C=C3)OC)=C3CC2C2=C1C=C(OC)C(OC)=C2 AEQDJSLRWYMAQI-UHFFFAOYSA-N 0.000 claims description 8
- 239000002736 nonionic surfactant Substances 0.000 claims description 8
- 239000000176 sodium gluconate Substances 0.000 claims description 8
- 235000012207 sodium gluconate Nutrition 0.000 claims description 8
- 229940005574 sodium gluconate Drugs 0.000 claims description 8
- KEZYHIPQRGTUDU-UHFFFAOYSA-N 2-[dithiocarboxy(methyl)amino]acetic acid Chemical compound SC(=S)N(C)CC(O)=O KEZYHIPQRGTUDU-UHFFFAOYSA-N 0.000 claims description 7
- 239000008367 deionised water Substances 0.000 claims description 7
- 229910021641 deionized water Inorganic materials 0.000 claims description 7
- BEGBSFPALGFMJI-UHFFFAOYSA-N ethene;sodium Chemical group [Na].C=C BEGBSFPALGFMJI-UHFFFAOYSA-N 0.000 claims description 7
- 239000011259 mixed solution Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 3
- 230000003014 reinforcing effect Effects 0.000 claims description 3
- 239000000661 sodium alginate Substances 0.000 claims description 3
- 235000010413 sodium alginate Nutrition 0.000 claims description 3
- 229940005550 sodium alginate Drugs 0.000 claims description 3
- 238000003466 welding Methods 0.000 claims description 3
- 230000000844 anti-bacterial effect Effects 0.000 claims 1
- 238000005260 corrosion Methods 0.000 abstract description 3
- 230000007797 corrosion Effects 0.000 abstract description 3
- 238000011086 high cleaning Methods 0.000 abstract description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
- -1 methyl taurate Chemical compound 0.000 description 13
- 229940051841 polyoxyethylene ether Drugs 0.000 description 7
- 229920000056 polyoxyethylene ether Polymers 0.000 description 7
- 239000011734 sodium Substances 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- 238000004140 cleaning Methods 0.000 description 6
- 235000019832 sodium triphosphate Nutrition 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 235000014113 dietary fatty acids Nutrition 0.000 description 5
- 239000000194 fatty acid Substances 0.000 description 5
- 229930195729 fatty acid Natural products 0.000 description 5
- 235000019982 sodium hexametaphosphate Nutrition 0.000 description 5
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 5
- 235000011121 sodium hydroxide Nutrition 0.000 description 5
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Polymers [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 5
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 239000000440 bentonite Substances 0.000 description 4
- 229910000278 bentonite Inorganic materials 0.000 description 4
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 4
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 238000005202 decontamination Methods 0.000 description 3
- 230000003588 decontaminative effect Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 150000004665 fatty acids Chemical class 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- LQZZUXJYWNFBMV-UHFFFAOYSA-N 1-dodecanol group Chemical group C(CCCCCCCCCCC)O LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 2
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 2
- 235000013162 Cocos nucifera Nutrition 0.000 description 2
- 244000060011 Cocos nucifera Species 0.000 description 2
- 229940120146 EDTMP Drugs 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 2
- 239000004115 Sodium Silicate Substances 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 239000003945 anionic surfactant Substances 0.000 description 2
- 239000002518 antifoaming agent Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 239000003599 detergent Substances 0.000 description 2
- 239000002270 dispersing agent Substances 0.000 description 2
- NFDRPXJGHKJRLJ-UHFFFAOYSA-N edtmp Chemical compound OP(O)(=O)CN(CP(O)(O)=O)CCN(CP(O)(O)=O)CP(O)(O)=O NFDRPXJGHKJRLJ-UHFFFAOYSA-N 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 150000002191 fatty alcohols Chemical class 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000002455 scale inhibitor Substances 0.000 description 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
- 229910052911 sodium silicate Inorganic materials 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- YDQUROLTIDVHRK-UHFFFAOYSA-N 2-hydroxypropane-1,2,3-tricarboxylic acid;propane-1,2,3-triol Chemical compound OCC(O)CO.OC(=O)CC(O)(C(O)=O)CC(O)=O YDQUROLTIDVHRK-UHFFFAOYSA-N 0.000 description 1
- BMOKHTQIBPRXSL-UHFFFAOYSA-N 2h-benzotriazole;sodium Chemical compound [Na].C1=CC=CC2=NNN=C21 BMOKHTQIBPRXSL-UHFFFAOYSA-N 0.000 description 1
- GODCLGCOHHTLHX-UHFFFAOYSA-N 3,3-diphosphonopropanoic acid Chemical compound OC(=O)CC(P(O)(O)=O)P(O)(O)=O GODCLGCOHHTLHX-UHFFFAOYSA-N 0.000 description 1
- CMGDVUCDZOBDNL-UHFFFAOYSA-N 4-methyl-2h-benzotriazole Chemical compound CC1=CC=CC2=NNN=C12 CMGDVUCDZOBDNL-UHFFFAOYSA-N 0.000 description 1
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- BACYUWVYYTXETD-UHFFFAOYSA-N N-Lauroylsarcosine Chemical compound CCCCCCCCCCCC(=O)N(C)CC(O)=O BACYUWVYYTXETD-UHFFFAOYSA-N 0.000 description 1
- QEOWFDYSNYCPRK-UHFFFAOYSA-N OCC[Na] Chemical compound OCC[Na] QEOWFDYSNYCPRK-UHFFFAOYSA-N 0.000 description 1
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 description 1
- 229920000805 Polyaspartic acid Polymers 0.000 description 1
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
- RRGMJRXKFDEXJY-UQKRIMTDSA-N [Na].CCCCCCCCCCCC(=O)N[C@H](C(O)=O)CCC(N)=O Chemical compound [Na].CCCCCCCCCCCC(=O)N[C@H](C(O)=O)CCC(N)=O RRGMJRXKFDEXJY-UQKRIMTDSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- WGLDZLZWKPBBLK-UHFFFAOYSA-N aminomethyl dimethyl phosphate Chemical group COP(=O)(OC)OCN WGLDZLZWKPBBLK-UHFFFAOYSA-N 0.000 description 1
- BTBJBAZGXNKLQC-UHFFFAOYSA-N ammonium lauryl sulfate Chemical compound [NH4+].CCCCCCCCCCCCOS([O-])(=O)=O BTBJBAZGXNKLQC-UHFFFAOYSA-N 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 238000010009 beating Methods 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000002734 clay mineral Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- GWTCIAGIKURVBJ-UHFFFAOYSA-L dipotassium;dodecyl phosphate Chemical compound [K+].[K+].CCCCCCCCCCCCOP([O-])([O-])=O GWTCIAGIKURVBJ-UHFFFAOYSA-L 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- BSOPSBIGIYEHGT-UHFFFAOYSA-N dodecyl 2-phenylacetate Chemical compound CCCCCCCCCCCCOC(=O)CC1=CC=CC=C1 BSOPSBIGIYEHGT-UHFFFAOYSA-N 0.000 description 1
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 description 1
- TVACALAUIQMRDF-UHFFFAOYSA-N dodecyl dihydrogen phosphate Chemical compound CCCCCCCCCCCCOP(O)(O)=O TVACALAUIQMRDF-UHFFFAOYSA-N 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- RBNPOMFGQQGHHO-UHFFFAOYSA-N glyceric acid Chemical compound OCC(O)C(O)=O RBNPOMFGQQGHHO-UHFFFAOYSA-N 0.000 description 1
- PYIDGJJWBIBVIA-UYTYNIKBSA-N lauryl glucoside Chemical compound CCCCCCCCCCCCO[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O PYIDGJJWBIBVIA-UYTYNIKBSA-N 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229940049964 oleate Drugs 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 108010064470 polyaspartate Proteins 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 108700004121 sarkosyl Proteins 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 235000015424 sodium Nutrition 0.000 description 1
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 description 1
- 235000019795 sodium metasilicate Nutrition 0.000 description 1
- ZNCPFRVNHGOPAG-UHFFFAOYSA-L sodium oxalate Chemical compound [Na+].[Na+].[O-]C(=O)C([O-])=O ZNCPFRVNHGOPAG-UHFFFAOYSA-L 0.000 description 1
- 229940039790 sodium oxalate Drugs 0.000 description 1
- 235000019794 sodium silicate Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 229940104261 taurate Drugs 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
- B01F33/811—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles in two or more consecutive, i.e. successive, mixing receptacles or being consecutively arranged
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents ; Methods for using cleaning compositions
- C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0036—Soil deposition preventing compositions; Antiredeposition agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/08—Silicates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/14—Fillers; Abrasives ; Abrasive compositions; Suspending or absorbing agents not provided for in one single group of C11D3/12; Specific features concerning abrasives, e.g. granulometry or mixtures
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/162—Organic compounds containing Si
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/24—Mixing of ingredients for cleaning compositions
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- C11D2111/18—
Abstract
The invention discloses a preparation method of a beer bottle cleaning agent, and belongs to the technical field of preparation of cleaning agents. The preparation device comprises a mixing tank and a support frame for supporting the mixing tank; the mixing tank comprises a tank body, a feeding hole and a discharging hole, wherein the tank body is internally provided with a hollow cylinder which is transversely arranged on a support frame, a partition plate is arranged inside the tank body, the inside of the tank body is divided into two parts through the partition plate, the two parts are respectively a first tank body and a second tank body, and a plurality of fan-shaped holes are arranged on the partition plate along the circumferential direction; the partition plate is connected with a rotating mechanism in a rotating way. The preparation method comprises the following steps: firstly, preparing attapulgite dispersion liquid in a first tank, then preparing a bottle cleaning agent in a second tank, finally mixing the attapulgite dispersion liquid and the bottle cleaning agent, and adjusting the pH value to obtain the attapulgite bottle cleaning agent. The cleaning agent prepared by the invention has high cleaning efficiency, and greatly reduces the corrosion to beer bottles.
Description
Technical Field
The invention relates to the technical field of preparation of beer cleaning agents, and particularly relates to a preparation method of a beer bottle cleaning agent.
Background
Along with the higher recycling rate of beer bottles, the demand for beer cleaning agents is more and more, most of the beer bottles in the prior art are cleaned by using dilute caustic soda solution at high temperature, and in the washing process, the dilute caustic soda solution can corrode equipment, and labels falling off from the beer bottles can block the washing equipment; and the beer bottle is corroded to different degrees by adopting caustic soda for cleaning at high temperature, so that the beer bottle is further thinned and deformed, and further use of the beer bottle is influenced. Therefore, the related researchers have made improvements to the cleaning agent and the main technical problems of the cleaning equipment in the prior art.
The related research reports in the prior art mainly include:
application No. 201510574081.0 discloses a beer bottle cleaning agent, which is prepared from 1-10 parts by weight of anionic surfactant, 1-10 parts by weight of nonionic surfactant, 15-30 parts by weight of scale inhibitor, 0.5-2 parts by weight of defoaming agent, 35-50 parts by weight of sodium tripolyphosphate, 10-25 parts by weight of sodium gluconate, 1-10 parts by weight of sodium metasilicate, 1-2 parts by weight of solid alkali and 450-550 parts by weight of distilled water; the anionic surfactant is lauryl alcohol polyoxyethylene ether sodium sulfate, lauryl ammonium sulfate, lauryl sodium sulfate, sodium dodecyl benzene sulfonate, secondary alkyl sodium sulfonate, fatty alcohol hydroxyethyl sodium sulfonate, N-lauroyl sarcosine sodium, cocoyl methyl taurate, N-lauroyl glutamine sodium, amide polyoxyethylene ether magnesium sulfate, lauryl alcohol polyoxyethylene ether sodium carboxylate, dodecyl phosphate potassium salt, dodecyl phosphate ester triethanolamine, alpha-alkenyl sodium sulfonate or p-toluene sodium sulfonate; the nonionic surfactant is coconut fatty acid monoethanolamide, coconut fatty acid diethanolamide, fatty acid polyoxyethylene ester, dodecyl glucoside, alkylolamide, high-carbon fatty acid diethanolamide, fatty amine polyoxyethylene ether, carboxyl synthetic alcohol polyoxyethylene ether, alkylphenol polyoxyethylene ether or fatty alcohol polyoxyethylene ether; the scale inhibitor is amino trimethyl phosphoric acid, carboxyl ethylidene diphosphonic acid, ethylene diamine tetra methylene phosphonic acid sodium, ethylene diamine tetra methylene phosphonic acid, carboxyl ethylidene diphosphonic acid tetrasodium, amino trimethyl phosphoric acid tetrasodium, benzotriazole sodium, methyl benzotriazole, polyaspartic acid sodium, sodium tripolyphosphate, sodium hexametaphosphate or polyacrylate; the defoaming agent is higher alcohol, phenethyl alcohol oleate, lauryl phenylacetate, polyoxyethylene, polydimethylsiloxane, polyoxypropylene glycerol ether, polyoxypropylene amine ether, higher alcohol fatty acid ester polymer, polyoxypropylene pentaerythritol ether or emulsified silicone oil.
Application No. 201510251091.0 discloses a special cleaning agent for beer bottles, including: 50-58 parts of glycerol mono-citrate, 15-17 parts of sodium hydroxide, 20-30 parts of alkyl glucoside, 30-33 parts of polyoxyethylene sorbitan monooleate, 8-10 parts of rosin water, 3-5 parts of succinic acid, 3-7 parts of epoxidized soybean oil, 8-10 parts of sodium oxalate, 1-10 parts of thickening agent and 55-65 parts of deionized water.
The prior art improves the formula of the beer bottle cleaning agent to a certain extent, the cleaning efficiency is improved, and the contained sodium hydroxide can further corrode the beer bottle, and the cleaning agent does not mention a related preparation method and a preparation device.
It can be seen that the prior art is subject to further improvement.
Disclosure of Invention
The invention aims to provide a preparation method of a beer bottle cleaning agent, which improves the formula of the cleaning agent and is combined with a device for producing the cleaning agent, so that the prepared cleaning agent has high cleaning efficiency, and the corrosion to beer bottles is greatly reduced.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation method of a beer bottle cleaning agent adopts a preparation device which comprises a mixing tank and a support frame for supporting the mixing tank;
the mixing tank comprises a tank body, a feeding hole and a discharging hole, wherein the tank body is internally provided with a hollow cylinder which is transversely arranged on the supporting frame, a partition plate is arranged inside the tank body, the inside of the tank body is divided into two parts through the partition plate, the two parts are respectively a first tank body and a second tank body, and a plurality of fan-shaped holes are arranged on the partition plate along the circumferential direction; the partition plate is rotatably connected with a rotating mechanism, the rotating mechanism comprises a connecting shaft, a rotating frame and fan-shaped plates positioned in the rotating frame, the connecting shaft is connected with the center of the partition plate, the rotating frame is integrally circular, and a plurality of fan-shaped plates are arranged in the circumferential direction of the rotating frame; the tank comprises a tank body, a sector plate, a bevel gear ring, servo motors, a driving bevel gear, a sector plate and a fan-shaped plate, wherein the sector plate is fixedly connected with the bevel gear ring, the servo motors are arranged on two sides of the tank body, the output shaft of the servo motor is connected with the driving bevel gear, the driving bevel gear is meshed with the bevel gear ring, when the servo motors are started, the driving bevel gear drives the bevel gear ring to rotate, the bevel gear ring drives the sector plate to rotate, the sector plate is used for plugging a plurality of sector holes on a partition plate, and the number and the size of the sector plate are matched with those of the sector holes;
the tank body is symmetrically provided with two flat plate mounting surfaces at left and right, mounting holes are formed in the two flat plate mounting surfaces, rotating pipes are arranged in the mounting holes, the left end and the right end of the tank body are respectively connected with a variable frequency motor, and the variable frequency motors are used for driving the rotating pipes to rotate;
the preparation method comprises the following steps:
a. preparation of an attapulgite dispersion in a first tank
Plugging fan-shaped holes in a partition plate through a rotating mechanism, respectively adding attapulgite and a silane coupling agent into a first tank body for mixing, heating the first tank body at the temperature of 40-80 ℃, starting a variable frequency motor, stirring the mixture through a rotating pipe for 2-6 hours to prepare an attapulgite dispersion liquid, and then cooling and adjusting the pH value of the attapulgite dispersion liquid to 7; wherein the adding amount of the silane coupling agent is 6-10% of the mass of the attapulgite;
b. preparation of bottle wash in the second tank
The bottle cleaning agent comprises the following raw materials in percentage by mass: 10-15% of nonionic surfactant, 5-10% of sodium metasilicate pentahydrate, 6-10% of sodium gluconate, 6-10% of sodium ethylene diamine tetracetate and the balance of deionized water;
sequentially adding the raw materials in percentage by mass into a second tank body, heating the second tank body at the temperature of 40-60 ℃, starting a variable frequency motor, stirring the mixed solution through a rotating pipe for 3-5 hours, and cooling;
c. and (b) starting a rotating mechanism to enable the fan-shaped holes in the partition plate to be in an open state, mixing the attapulgite dispersion liquid prepared in the step a and the bottle cleaning agent prepared in the step b together, continuing to start a variable frequency motor, stirring the mixed liquid through a rotating pipe for 1-3 hours, adding sodium alginate into the mixed liquid, and adjusting the pH value of the mixed liquid to be 8 to obtain the anti-bacterial agent.
In a preferred embodiment of the present invention, the attapulgite has a particle size of 200 mesh.
As another preferable scheme of the present invention, a closed ring is disposed on an inner wall of the tank body, the closed ring is in contact with the bevel gear ring, a stepped groove is disposed on the closed ring, and the driving bevel gear is disposed in the stepped groove on the closed ring.
Preferably, the rotating frame is circular, and the number of the fan-shaped holes and the number of the fan-shaped plates are three.
Preferably, the support frame include two montants and chassis, two montants are fixed connection respectively on the top of chassis, the chassis adopts two to indulge the I-steel and a plurality of horizontal I-steel welding forms, and the mutual welded indulges fixedly connected with reinforcing angle board between I-steel and the horizontal I-steel, two montants are fixed connection respectively and are indulged the top of I-steel two, indulge on the I-steel and all seted up the auxiliary connection hole on the horizontal I-steel, two montants all rotate with the jar body and be connected, and install the drive between a montant in two montants and the jar body and adjust the structure.
Preferably, the driving adjusting structure comprises an electric telescopic rod, a connecting seat is fixedly connected to the electric telescopic rod, the connecting seat is rotatably connected to one end of one of the vertical rods, an end block is fixedly connected to the electric telescopic rod, a connecting lug is rotatably connected to the end block, and the connecting lug is fixedly connected with the tank body.
Preferably, the first tank body and the second tank body are respectively provided with a feeding port and a discharging port, and each feeding port is correspondingly provided with an observation window.
Preferably, the discharge ports of the first tank body and the second tank body are both connected with a liquid discharge pipe, the liquid discharge pipes are both provided with on-off valves, the bottom ends of the two on-off valves are provided with elbows, two ends of the elbow are respectively controlled by the two on-off valves to be in on-off connection with the first tank body and the second tank body, and the bottom ends of the elbows are connected with a collecting pipe.
Compared with the prior art, the invention has the following beneficial technical effects:
(1) the raw material of the beer cleaning agent is added with the attapulgite which is a hydrous magnesium-rich aluminosilicate clay mineral with a layer chain structure, has a special fibrous crystal form and has the characteristics of large surface area and high porosity, so that the attapulgite is used as the raw material of the beer cleaning agent, the beating action of particles in the washing process is increased by utilizing the granular structure of the attapulgite, the washing and decontamination capability can be effectively improved, and in addition, the attapulgite has strong adsorption capability and can also adsorb and remove dirt and fungi in beer bottles. The attapulgite is dispersed by adopting the silane coupling agent, besides chemical bonding, a small amount of silane on the surface of the attapulgite is self-condensed into polysiloxane alcohol to be coated on the surface of the attapulgite to form a flexible interface layer, and the attapulgite particles can strengthen the adsorption capacity and effectively improve the washing and decontamination capacity by introducing the surface modification layer. In addition, the alkaline environment of the bottle cleaning agent can be further reduced by adding the attapulgite.
(2) The porous structure of the attapulgite enables the attapulgite to have certain suspension capacity, and can adsorb dirt, mold and other small molecular substances in the washing process.
(3) The sodium ethylene diamine tetracetate is used as a chelating agent and is matched with the sodium metasilicate pentahydrate, so that dirt precipitates can be prevented from being left on the surface of glass, a synergistic effect is achieved, and the comprehensive performance of the detergent is improved.
(4) Sodium silicate, sodium sulfate and sodium gluconate are used as auxiliaries, so that the surface tension of the solution can be improved, the wetting effect is enhanced, and the effect of auxiliary decontamination can be achieved. The surface tension of the detergent can be reduced and the viscosity of the liquid can be reduced by the cooperation of the three components.
(5) According to the invention, the partition plate is arranged in the tank body, the tank body is divided into two parts by the partition plate, and the fan-shaped holes are formed in the partition plate, so that the first tank body and the second tank body can be kept communicated or blocked according to actual conditions. The first tank body and the second tank body can be quickly communicated, so that the deposition of particles in the attapulgite dispersion liquid can be avoided as much as possible, and the cleaning efficiency of the cleaning agent can be improved.
In conclusion, the preparation device and the preparation method are combined, the attapulgite dispersion liquid and the bottle cleaning agent can be uniformly mixed, the cleaning efficiency of the beer bottle cleaning agent is improved to the maximum extent, and the corrosion of the cleaning agent to beer bottles can be reduced because the pH of the cleaning agent is 8.
Drawings
The invention is further described below with reference to the accompanying drawings:
FIG. 1 is a schematic perspective view, partially in section, of an apparatus used in the present invention;
FIG. 2 is a schematic view of a portion A of FIG. 1;
FIG. 3 is a schematic view of a portion of the enlarged structure at B in FIG. 1;
FIG. 4 is a schematic exploded perspective view of the divider plate, the bevel ring, and the closure ring of the present invention;
FIG. 5 is a partially cross-sectional perspective view of another embodiment of the present invention;
FIG. 6 is an enlarged partial view of the structure at C in FIG. 5;
FIG. 7 is a schematic bottom perspective view of the present invention;
fig. 8 is a partially enlarged schematic view of a portion D in fig. 7.
In the figure: 1. rotating the tube; 2. a mixing tank; 3. a flat plate mounting surface; 4. a partition plate; 5. a first tank; 6. a second tank; 7. a sector hole; 8. a connecting shaft; 9. a sector plate; 10. a conical gear ring; 11. a drive bevel gear; 12. a vertical rod; 13. a liquid discharge pipe; 14. bending the pipe; 15. a header; 16. an observation tube; 17. a bolt; 18. an end plate; 19. quick connection pipes; 20. connecting threads; 21. a connecting seat; 22. an end-block; 23. connecting lugs; 24. longitudinal I-shaped steel; 25. transverse I-shaped steel; 26. auxiliary connecting holes; 27. a closed ring; 28. an arc-shaped protection plate.
Detailed Description
The invention provides a preparation method of a beer bottle cleaning agent, and in order to make the advantages and technical scheme of the invention clearer and clearer, the invention is further explained by combining specific embodiments.
The starting materials described in the present invention are commercially available.
First, referring to FIGS. 1 to 8, the apparatus used in the method for producing a beer bottle cleaning agent of the present invention will be described in detail.
The device for preparing the beer bottle cleaning agent comprises a mixing tank 2 and a support frame for supporting the mixing tank 2;
the mixing tank comprises a tank body, a feeding port and a discharging port, wherein the tank body is internally provided with a hollow cylinder which is transversely arranged on the supporting frame.
As a main improvement point of the invention, a partition plate 4 is arranged in a tank body, the interior of the tank body is divided into two parts by the partition plate, namely a first tank body 5 and a second tank body 6, a plurality of fan-shaped holes 7 are arranged on the partition plate along the circumferential direction, and the fan-shaped holes 7 are used for keeping the first tank body and the second tank body to be closed and communicated; the partition plate is rotatably connected with a rotating mechanism, the sector holes 7 are blocked or opened through the rotation of the rotating mechanism, the rotating mechanism comprises a connecting shaft 8, a rotating frame and sector plates 9 positioned in the rotating frame, the connecting shaft is connected to the center of the partition plate, the rotating frame is integrally circular, and a plurality of sector plates are arranged in the circumferential direction of the rotating frame; the shape of sector plate and the shape phase-match of sector hole, the size of sector plate slightly is greater than the size of sector hole to realize the shutoff to sector hole sector plate on fixedly connected with awl ring gear 10, the jar body both sides install servo motor, servo motor's output shaft on be connected with drive bevel gear 11, drive bevel gear and awl ring gear mesh mutually, when servo motor opened, drive bevel gear drive the awl ring gear rotate, awl ring gear move sector plate and rotate, realize the shutoff or open to sector hole. The first tank body and the second tank body can be converged into a communicated space through the matching of the partition plate and the rotating mechanism, and the first tank body and the second tank body can also be divided into two independent spaces.
The tank body is symmetrically provided with two flat plate mounting surfaces at left and right, mounting holes are formed in the two flat plate mounting surfaces, a rotating pipe 1 is arranged in each mounting hole, the left end and the right end of the tank body are respectively connected with a variable frequency motor, and the variable frequency motors are used for driving the rotating pipes to rotate; through the design of dull and stereotyped installation face 3, supplementary stirring to the cleaner that gets into in the blending tank, the while stirring in-process can also cooperate the rocking of blending tank to go on in step.
Preferably, a closed ring 27 is fixedly connected in the tank body, the closed ring 27 is in contact with the bevel gear ring 10, a stepped groove is formed in the closed ring 27, the driving bevel gear 11 is located in the stepped groove, sealing and protection of the connection position of the driving bevel gear 11 and the bevel gear ring 10 are achieved, and soaking of a cleaning agent on the driving bevel gear 11 and the bevel gear ring 10 is reduced.
Preferably, all be provided with feed inlet and discharge gate on the first jar of body and the second jar of body, still be provided with observation tube 16 on two feed inlets, an viewing aperture has been seted up on the first jar of body and the second jar of body respectively, two observation tubes 16 are fixed connection respectively in two viewing apertures, and two observation tubes 16 keep the intercommunication with the first jar of body and the second jar of body respectively, all be connected with end plate 18 through a plurality of bolts 17 on two observation tubes 16, the liquid feeding hole has all been seted up on two end plates 18, the downthehole equal fixedly connected with of two liquid feeding fast takeover 19, all be provided with connecting thread 20 on two fast takeover 19, the realization is to the putting into of the preparation composition of the cleaner in the first jar of body and the second jar of body, and be convenient for get into the maintenance of the jar body in the hybrid tank.
All be provided with the discharge gate on first jar of body and the second jar of body, a fluid-discharge tube 13 is all connected to every discharge gate, two fluid-discharge tubes 13 communicate with first jar of body and second jar of body respectively, all install the on-off valve on two fluid-discharge tubes 13, elbow 14 is installed to the bottom of two on-off valves, can control the break-make of elbow 14 respectively with the break-make in first district 5 and the break-make in second district 6 through two on-off valves, the bottom intercommunication of elbow 14 has collection pipe 15, when being convenient for first jar of body and the second jar of body use respectively, discharge the cleaner that the two jar internal preparation was good.
The support frame for supporting the mixing tank comprises two vertical rods 12 and a bottom frame, wherein the two vertical rods 12 are fixedly connected to the top end of the bottom frame, the bottom frame is formed by welding two longitudinal I-shaped steels 24 and a plurality of transverse I-shaped steels 25, reinforcing angle plates are fixedly connected between the longitudinal I-shaped steels 24 and the transverse I-shaped steels 25 which are welded with each other, the two vertical rods 12 are respectively and fixedly connected to the top ends of the two longitudinal I-shaped steels 24, a plurality of auxiliary connecting holes 26 are formed in the longitudinal I-shaped steels 24 and the transverse I-shaped steels 25, the longitudinal I-shaped steels 24 and the transverse I-shaped steels 25 are conveniently and respectively fixedly connected with contact surfaces of installation places, the two vertical rods 12 are respectively and rotatably connected with the swinging tank 2, and a driving and adjusting structure is arranged between one vertical rod 12 of the two vertical rods 12 and a tank main body.
The structure is adjusted in the drive includes electric telescopic handle, fixedly connected with connecting seat 21 on the electric telescopic handle, connecting seat 21 rotates the one end that is close to another montant 12 of a montant 12 of connection in two montants 12, fixedly connected with end block 22 on electric telescopic handle's the telescopic link, it is connected with engaging lug 23 to rotate on the end block 22, engaging lug 23 and jar main part fixed connection, design through the support frame, be convenient for the rotation installation and rotation control of jar main part, realize rising and the reduction of the first jar of body and the second jar of body, thereby be convenient for the attapulgite dispersion and the bottle cleaning agent of the preparation of the first jar of body and the second jar of body to mix, prepare alone through the first jar of body and the second jar of body, the cleaner of preparing is derived, do not relate to the transfer step of cleaner, the whole work efficiency is improved.
Preferably, both ends equal fixedly connected with arc guard plate 28 about the blending tank, two arc guard plates 28 realize the protection to two inverter motor respectively.
The method for producing the beer bottle cleaning agent of the present invention will be described in detail below with reference to the above-mentioned production apparatus.
Step one, preparing attapulgite dispersion liquid in a first tank body
Turning on a servo motor, driving a bevel gear connected to an output shaft of the servo motor to drive a bevel gear ring to rotate, driving a sector plate to rotate by the bevel gear ring, turning off the servo motor when the sector plate rotates to a position opposite to a sector hole, so as to plug the sector hole on a partition plate, adding attapulgite and a silane coupling agent into a first tank body respectively to mix, heating the first tank body in an electric heating mode, controlling the heating temperature to be 40-80 ℃, enabling the concave-convex attapulgite to be well dispersed in the silane coupling agent in the temperature range, turning on a variable frequency motor, stirring the mixture through a rotating pipe for 2-6 hours, preparing an attapulgite dispersion liquid, and then cooling and adjusting the pH value of the attapulgite dispersion liquid to be 7; wherein the adding amount of the silane coupling agent is 6-10% of the mass of the attapulgite, and the adding amount is the most suitable adding amount.
Step two, preparing a bottle washing agent in a second tank body
The bottle cleaning agent comprises the following raw materials in percentage by mass: 10-15% of nonionic surfactant, 5-10% of sodium metasilicate pentahydrate, 6-10% of sodium gluconate, 6-10% of sodium ethylene diamine tetracetate and the balance of deionized water;
sequentially adding the raw materials in percentage by mass into a second tank body, heating the second tank body at the temperature of 40-60 ℃, starting a variable frequency motor, stirring the mixed solution through a rotating pipe for 3-5 hours, and cooling;
and step three, opening a servo motor, driving a bevel gear connected to an output shaft of the servo motor to drive a bevel gear ring to rotate, driving a fan-shaped plate to rotate by the bevel gear ring, closing the servo motor when the fan-shaped plate rotates to be staggered with the position of a fan-shaped hole, enabling the fan-shaped hole in the partition plate to be in an open state, mixing the attapulgite dispersion liquid prepared in the step one and the bottle cleaning agent prepared in the step two together, continuing to start the variable frequency motor, stirring the mixed liquid through a rotating pipe, adding sodium alginate into the mixed liquid after stirring for 1-3 hours, and adjusting the pH value to 8 to obtain the finished product.
The invention is further illustrated by the following specific examples:
example 1:
step one, preparing attapulgite dispersion liquid in a first tank body
Weighing a silane coupling agent which accounts for 6 percent of the mass of the attapulgite, adding the silane coupling agent into the attapulgite, controlling the temperature at 60 ℃, stirring for 1000r/min, and stirring for 6h to obtain a diatomite dispersion liquid;
step two, preparing a bottle washing agent in a second tank body
The bottle cleaning agent comprises the following raw materials in percentage by mass: 10-15% of nonionic surfactant, 5-10% of sodium metasilicate pentahydrate, 6-10% of sodium gluconate, 6-10% of sodium ethylene diamine tetracetate and the balance of deionized water;
sequentially adding the raw materials in percentage by mass into a second tank body, heating the second tank body at the temperature of 40-60 ℃, starting a variable frequency motor, stirring the mixed solution through a rotating pipe for 3-5 hours, and cooling;
step three, mixing the attapulgite dispersion liquid and a bottle cleaning agent,
and (3) opening a servo motor, driving a bevel gear connected to an output shaft of the servo motor to drive a bevel gear ring to rotate, driving a fan-shaped plate to rotate by the bevel gear ring, and when the fan-shaped plate rotates to be staggered with the position of a fan-shaped hole, closing the servo motor to enable the fan-shaped hole in the partition plate to be in an open state.
Comparative example 1:
step one, preparing diatomite dispersion liquid in a first tank body, wherein the adopted dispersing agents are sodium polyacrylate, sodium tripolyphosphate and sodium hexametaphosphate, and the preparation method comprises the following steps: adding the sodium polyacrylate dispersion liquid, the sodium tripolyphosphate solution and the sodium hexametaphosphate solution into diatomite, adjusting the pH, and stirring for 1000r/min to obtain the diatomite dispersion liquid;
step two, preparing a bottle washing agent in a second tank body
The bottle washing agent comprises the following raw materials in percentage by mass: 10-15% of nonionic surfactant, 5-10% of sodium metasilicate pentahydrate, 6-10% of sodium gluconate, 6-10% of sodium ethylene diamine tetracetate and the balance of deionized water;
sequentially adding the raw materials in percentage by mass into a second tank body, heating the second tank body at the temperature of 40-60 ℃, starting a variable frequency motor, stirring the mixed solution through a rotating pipe for 3-5 hours, and cooling;
and step three, mixing the diatomite dispersion liquid and the bottle washing agent, and obtaining the product by the same steps as the step three in the example 1.
Comparative example 2:
step one, preparing bentonite dispersion liquid in a first tank body, wherein the adopted dispersing agents are sodium polyacrylate, sodium tripolyphosphate and sodium hexametaphosphate, and the preparation method comprises the following steps: adding sodium polyacrylate dispersion, sodium tripolyphosphate solution and sodium hexametaphosphate solution into bentonite, adjusting pH, and stirring for 1000r/min to obtain bentonite dispersion;
step two, preparing a bottle washing agent in a second tank body
The bottle washing agent comprises the following raw materials in percentage by mass: 10-15% of nonionic surfactant, 5-10% of sodium metasilicate pentahydrate, 6-10% of sodium gluconate, 6-10% of sodium ethylene diamine tetracetate and the balance of deionized water;
sequentially adding the raw materials in percentage by mass into a second tank body, heating the second tank body at the temperature of 40-60 ℃, starting a variable frequency motor, stirring the mixed solution through a rotating pipe for 3-5 hours, and cooling;
and step three, mixing the bentonite dispersion liquid and the bottle washing agent, and obtaining the product by the same steps as the step three of the embodiment 1.
The beer bottle cleaning agents prepared in examples 1, 2 and 3 were evaluated for their detergency, and the change in light transmittance before and after the contamination of the slide glass was reflected by the whiteness value using a slide glass of the same material as that of the beer bottle. The specific evaluation method comprises the following steps:
cleaning the slide, air drying, and reading the contamination with a luminometerWhiteness value a of slide 1 Coating a contaminated slide by a shading pen according to a specified coating and dyeing method, aging at 40 deg.C for 72h, and reading the whiteness value a of the contaminated slide by a whiteness meter 2 Washing with 5% by weight of the above prepared beer bottle cleaning agent, and reading the whiteness value of the washed slide as a 3 Calculating the detergency F according to the whiteness value of the washed slide before washing and the whiteness value of the clean slide
F＝(a 3 -a 2 )/(a 1 -a 2 )
The calculation results are shown in table 1:
TABLE 1
| Formulation of | Value of detergency |
| Example 1 | 90.4 |
| Comparative example 1 | 80.2 |
| Comparative example 2 | 78.3 |
The parts which are not described in the invention can be realized by taking the prior art as reference.
Parts which are not described in the invention can be realized by adopting or referring to the prior art.
It is further understood that the specific embodiments described herein are merely illustrative of the spirit of the invention. Various modifications or additions may be made to the described embodiments or alternatives may be employed by those skilled in the art without departing from the spirit or ambit of the invention as defined in the appended claims.
Claims (8)
1. The preparation method of the beer bottle cleaning agent is characterized in that the adopted preparation device comprises a mixing tank and a support frame for supporting the mixing tank;
the mixing tank comprises a tank body, a feeding hole and a discharging hole, wherein the tank body is internally provided with a hollow cylinder which is transversely arranged on the supporting frame, a partition plate is arranged inside the tank body, the inside of the tank body is divided into two parts through the partition plate, the two parts are respectively a first tank body and a second tank body, and a plurality of fan-shaped holes are arranged on the partition plate along the circumferential direction; the partition plate is rotatably connected with a rotating mechanism, the rotating mechanism comprises a connecting shaft, a rotating frame and fan-shaped plates positioned in the rotating frame, the connecting shaft is connected with the center of the partition plate, the rotating frame is integrally circular, and a plurality of fan-shaped plates are arranged in the circumferential direction of the rotating frame; the tank comprises a tank body, a sector plate, a bevel gear ring, servo motors, a driving bevel gear, a sector plate and a fan-shaped plate, wherein the sector plate is fixedly connected with the bevel gear ring, the servo motors are arranged on two sides of the tank body, the output shaft of the servo motor is connected with the driving bevel gear, the driving bevel gear is meshed with the bevel gear ring, when the servo motors are started, the driving bevel gear drives the bevel gear ring to rotate, the bevel gear ring drives the sector plate to rotate, the sector plate is used for plugging a plurality of sector holes on a partition plate, and the number and the size of the sector plate are matched with those of the sector holes;
the tank body is symmetrically provided with two flat plate mounting surfaces at left and right, mounting holes are formed in the two flat plate mounting surfaces, rotating pipes are arranged in the mounting holes, the left end and the right end of the tank body are respectively connected with a variable frequency motor, and the variable frequency motors are used for driving the rotating pipes to rotate;
the preparation method comprises the following steps:
a. preparation of an attapulgite dispersion in a first tank
Plugging fan-shaped holes in a partition plate through a rotating mechanism, respectively adding attapulgite and a silane coupling agent into a first tank body for mixing, heating the first tank body at the temperature of 40-80 ℃, starting a variable frequency motor, stirring the mixture through a rotating pipe for 2-6 hours to prepare an attapulgite dispersion liquid, and then cooling and adjusting the pH value of the attapulgite dispersion liquid to 7; wherein the adding amount of the silane coupling agent is 6-10% of the mass of the attapulgite;
b. preparation of bottle wash in the second tank
The bottle washing agent comprises the following raw materials in percentage by mass: 10-15% of nonionic surfactant, 5-10% of sodium metasilicate pentahydrate, 6-10% of sodium gluconate, 6-10% of sodium ethylene diamine tetracetate and the balance of deionized water;
sequentially adding the raw materials in percentage by mass into a second tank body, heating the second tank body at 40-60 ℃, starting a variable frequency motor, stirring the mixed solution through a rotating pipe for 3-5 hours, and cooling;
c. and (c) starting a rotating mechanism to enable the fan-shaped holes in the partition plate to be in an open state, mixing the attapulgite dispersion liquid prepared in the step a and the bottle cleaning agent prepared in the step b together, continuing to start a variable frequency motor, stirring the mixed liquid through a rotating pipe for 1-3 hours, adding sodium alginate into the mixed liquid, and adjusting the pH value of the mixed liquid to be 8 to obtain the anti-bacterial bottle cleaning agent.
2. The method for preparing a beer bottle cleaning agent according to claim 1, wherein the method comprises the following steps: the particle size of the attapulgite is 200 meshes.
3. The method for preparing a beer bottle cleaning agent according to claim 1, wherein the method comprises the following steps: the inner wall of jar body be provided with the closed ring, closed ring and bevel gear ring contact the closed ring on be provided with the ladder groove, drive bevel gear be located the ladder inslot on the closed ring.
4. The method for preparing a beer bottle cleaning agent according to claim 1, wherein the method comprises the following steps: the rotating frame is circular, and the number of the fan-shaped holes and the number of the fan-shaped plates are three.
5. The method for preparing a beer bottle cleaning agent according to claim 1, wherein the method comprises the following steps: the support frame include two montants and chassis, two montants are fixed connection respectively on the top of chassis, the chassis adopts two to indulge the I-steel and a plurality of horizontal I-steel welding forms, and the mutual welded indulges fixedly connected with reinforcing angle board between I-steel and the horizontal I-steel, two montants are fixed connection respectively on two tops of indulging the I-steel, indulge on the I-steel and all seted up the auxiliary connection hole on the horizontal I-steel, two montants all are connected with jar body rotation, and install the drive between a montant in two montants and the jar body and adjust the structure.
6. The method for preparing a beer bottle cleaning agent according to claim 5, wherein the method comprises the following steps: the driving adjusting structure comprises an electric telescopic rod, wherein a connecting seat is fixedly connected to the electric telescopic rod, the connecting seat is rotatably connected to one end of one of the vertical rods, an end block is fixedly connected to the electric telescopic rod, a connecting lug is rotatably connected to the end block, and the connecting lug is fixedly connected with the tank body.
7. The method for preparing a beer bottle cleaning agent according to claim 1, wherein the method comprises the following steps: the first jar of body and second jar body on all be provided with feed inlet and discharge gate, correspond in every feed inlet department and be provided with the observation window.
8. The method for preparing a beer bottle cleaning agent according to claim 1, wherein the method comprises the following steps: the discharge ports of the first tank body and the second tank body are both connected with a liquid discharge pipe, the liquid discharge pipes are both provided with on-off valves, the bottom ends of the two on-off valves are provided with elbows, the two ends of the elbow are respectively controlled to be on-off with the first tank body and the second tank body through the two on-off valves, and the bottom ends of the elbows are connected with a collecting pipe.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101613112A (en) * | 2009-07-06 | 2009-12-30 | 江南大学 | A kind of preparation of attapulgite modified by silane coupling agent |
| CN112745989A (en) * | 2020-12-30 | 2021-05-04 | 王晓立 | Quick-acting beer bottle label-removing cleaning additive |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101613112A (en) * | 2009-07-06 | 2009-12-30 | 江南大学 | A kind of preparation of attapulgite modified by silane coupling agent |
| CN112745989A (en) * | 2020-12-30 | 2021-05-04 | 王晓立 | Quick-acting beer bottle label-removing cleaning additive |
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