CN115058287A - Zero-trans-fatty-acid low-toxin corn oil refining process - Google Patents
Zero-trans-fatty-acid low-toxin corn oil refining process Download PDFInfo
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- CN115058287A CN115058287A CN202210520996.3A CN202210520996A CN115058287A CN 115058287 A CN115058287 A CN 115058287A CN 202210520996 A CN202210520996 A CN 202210520996A CN 115058287 A CN115058287 A CN 115058287A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
- C11B3/04—Refining fats or fatty oils by chemical reaction with acids
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/02—Refining fats or fatty oils by chemical reaction
- C11B3/06—Refining fats or fatty oils by chemical reaction with bases
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/16—Refining fats or fatty oils by mechanical means
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Abstract
The invention relates to the technical field of corn oil processing, in particular to a zero trans-fatty acid low-toxin corn oil refining process, which comprises the following steps: (1) adding citric acid into the corn crude oil under the heating condition for reaction, dephosphorizing and degumming; (2) mixing the dephosphorized and degummed corn oil with an alkali liquor for deacidification treatment, wherein the concentration of the alkali liquor is 5-8 degrees Be; (3) pumping the deacidified corn oil into a decoloring tower for decoloring, wherein a secondary decoloring method is adopted for decoloring; (4) dewaxing the decolorized corn oil by crystallization, wherein the dewaxing adopts tubular continuous dewaxing; (5) and deodorizing the dewaxed corn oil by two-stage heating deodorization to obtain the finished oil. The method reduces the damage to the nutrient components such as phytosterol, vitamin E and the like in the corn oil, reduces the content of zearalenone toxin in the corn oil, and prevents the reformation of trans-fatty acid in the refining process.
Description
Technical Field
The invention relates to the technical field of corn oil processing, and particularly relates to a zero trans-fatty acid low-toxin corn oil refining process.
Background
In recent years, as people pay more and more attention to the quality safety of edible oil, the problems of trans-fatty acid, overproof mycotoxin content, the content of nutrient components and the like in the edible oil are concerned more and more, the trans-fatty acid easily causes cardiovascular diseases, easily induces myocardial infarction to increase the occurrence probability of diabetes, and also has adverse effects on infants in the growth and development period and growing teenagers. Mycotoxins are primarily zearalenone which is difficult to remove and, by its nature, is residual and not easily destroyed and also has a toxic effect on humans. If the zearalenone is added to the animal body for a long time, the zearalenone is continuously accumulated in the animal body and deposited in the animal body. It acts like estrogen in animals and causes estrogen overload. Under the condition of acute poisoning, the traditional Chinese medicine has toxic action on nervous system, heart, kidney, liver and lung, and the main mechanism is that the traditional Chinese medicine can cause the nervous system to be excited, and a plurality of bleeding points are caused in organs, so that animals die suddenly. The female sensitivity is higher than that of a male, the fertility is reduced, the behavior is abnormal, meanwhile, the female animals are easy to be infertile, aborted or weakened, and the feminization of the male animals is caused. In addition, the over refining of oil and fat can not only cause the waste of resources and energy sources, but also cause the loss of nutrient elements (such as vitamin E and sterol contents) of the corn oil, CN201210561407.2 discloses a zero trans fatty acid corn oil and a refining process thereof, which produces the corn oil with zero trans fatty acid by proper processing of the corn oil through alkali refining, dewaxing, decoloring, deodorizing, packaging technologies and the like of the corn crude oil, and the prepared corn oil with the zero trans fatty acid has the trans fatty acid content of less than or equal to 0.3 percent, the vitamin E content of more than or equal to 1000mg/kg and the phytosterol content of more than or equal to 10000mg/kg, but has the defects that the zearalenone toxin in the corn oil is not removed, and the corn oil is treated by concentrated alkali liquor of 10 DEG Be-20 DEG Be after the phosphoric acid treatment in the alkali refining process, the nutrient substances of the corn oil are destroyed, and simultaneously, in the deodorizing stage, the temperature rise time is long, trans-fatty acid is easily formed in the corn oil under the conditions of long time, high temperature and the like, and the loss of nutritional ingredients is serious.
Disclosure of Invention
Aiming at the problems of low trans-fatty acid content, zearalenone toxin and the like in the corn oil in the prior art, the invention provides a zero trans-fatty acid low-toxin corn oil refining process, which reduces the damage to the nutrient components such as phytosterol, vitamin E and the like in the corn oil, reduces the content of zearalenone toxin in the corn oil and prevents the reformation of trans-fatty acid in the refining process.
The invention provides a zero trans-fatty acid low-toxin corn oil refining process, which comprises the following steps:
(1) adding citric acid into the corn crude oil under the heating condition for reaction, dephosphorizing and degumming;
(2) mixing the dephosphorized and degummed corn oil with an alkali liquor for deacidification treatment, wherein the concentration of the alkali liquor is 5-8 degrees Be;
(3) pumping the deacidified corn oil into a decoloring tower for decoloring, wherein a secondary decoloring method is adopted for decoloring;
(4) dewaxing the decolorized corn oil by crystallization, wherein the dewaxing adopts tubular continuous dewaxing;
(5) and deodorizing the corn oil after dewaxing, heating and deodorizing the corn oil in two stages, pumping the corn oil into a deodorizing tower for deodorization after heating the corn oil to 180-200 ℃ in the first stage, heating the corn oil to 250-270 ℃ in the second stage for deodorization, wherein the deodorization time in the second stage is less than or equal to 5min, and feeding the corn oil into a finished product tower after deodorization to obtain the finished product oil.
Further, in the step (1), the heating temperature is 51-60 ℃, the mass concentration of citric acid is 20-80%, the dosage of citric acid is 0.1-0.5% of the weight of the crude corn oil, and the reaction time of citric acid is 15-35 min.
Further, the deacidification time of the alkali liquor in the step (2) is 8-13 min.
Further, in the step (3), the secondary decoloring method comprises primary decoloring and secondary decoloring; the primary decolorization process conditions are that the decolorizer adopts active carbon and activated clay, the dosage of the active carbon is 0.5-3% of the weight of the corn oil, the dosage of the activated clay is 0.5-3% of the weight of the corn oil, the decolorization temperature is 95-110 ℃, the decolorization time is 20-30 min, and the pressure of a decolorization tower is 0.010-0.015 MPa; the secondary decolorization process condition is that activated carbon is added into the primarily decolorized corn oil for continuous decolorization, and the use amount of the activated carbon is 0.5-3% of the weight of the corn oil.
Further, in the step (4), the crystallization dewaxing method comprises the steps of pumping the corn oil into a crystallization pipe, sequentially passing through the rest crystallization pipes through an overflow effect, wrapping a condensing coil outside the crystallization pipe for cooling, gradually reducing the oil temperature to 1-7 ℃, preserving the temperature for 24 hours for crystallization and crystal growth, and then keeping the oil temperature at the normal temperature of 20 +/-5 ℃ for filtration.
Further, the second stage deodorization heating in the step (5) is performed in an electric heater having the following structure: the heater comprises a shell, wherein an electric heating pipe is arranged in the shell and is connected with a power supply; the corn oil is positioned in the shell during the deodorization heating in the second stage and is directly contacted with the electric heating pipe for heating, so that the technical effect of quickly heating the corn oil can be achieved; the total deodorization time is 45-60 min.
Furthermore, in the corn oil finished product, the content of trans-fatty acid is less than or equal to 0.3 percent, the content of vitamin E is more than or equal to 1100mg/kg, the content of phytosterol is more than or equal to 11000mg/kg, and the content of gibberellin ketene is less than or equal to 100 ug/kg.
The invention has the beneficial effects that:
(1) the method adopts the dephosphorization and degumming technology of the weak acid citric acid, replaces the food grade phosphoric acid which is conventionally used with the food grade citric acid, has low cost and energy consumption, and saves more energy and reduces consumption;
(2) in the deacidification stage, the low-temperature weak alkali is adopted for deacidification, so that the loss of neutral oil is reduced, the damage of alkali liquor to nutrient substances of the corn oil is reduced, the refining yield is improved, and the energy conservation and consumption reduction are remarkable;
(3) the invention adopts a secondary decolorization method during decolorization, and has the effect of completely adsorbing pigment and mycotoxin in the corn oil. Avoiding the need of prolonging the subsequent deodorization time and increasing the deodorization temperature due to pigments and toxins;
(4) the method adopts a two-temperature double-tower sectional instant heating deodorization technology, adopts rapid heating (less than or equal to 5min) in the second deodorization stage, quickly heats the oil temperature of the corn oil to 250-270 ℃ for deodorization, has high speed, short time and high temperature, and avoids the corn oil from forming trans-fatty acid under the conditions of long time, high temperature and the like.
Detailed Description
In order to make those skilled in the art better understand the technical solutions in the present invention, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
Firstly, heating the corn crude oil to 70 ℃, adding food-grade citric acid with the concentration of 45 percent, wherein the dosage of the food-grade citric acid is 0.1 to 0.5 percent of the total weight of the corn crude oil, carrying out acid treatment for 20min, carrying out neutralization reaction on the mixture subjected to acid treatment and alkali liquor, wherein the concentration of the alkali liquor is 5 Be, and the reaction time is 15min, and carrying out centrifugal separation. Adopting a secondary decolorization method technology, adding activated clay and activated carbon into the deacidified corn oil to perform primary decolorization, removing part of pigments and toxins, then adding activated carbon to perform secondary decolorization, and removing the rest toxins, wherein the primary decolorization process conditions are that an activated carbon and activated clay are adopted as a decolorizer, the using amount of the activated carbon is 1% of the weight of the corn oil, the using amount of the activated clay is 1% of the weight of the corn oil, the decolorization temperature is 100 ℃, the decolorization time is 25min, and the pressure of a decolorization tower is 0.010-0.015 MPa; the secondary decolorization process condition is that activated carbon is added into the primarily decolorized corn oil to continue decolorization, and the use amount of the activated carbon is 1 percent of the weight of the corn oil. Pumping the decolorized corn oil into a dewaxing device for dewaxing at the normal temperature of 20 +/-25 ℃, enabling the corn oil decolorized by adopting a tubular continuous dewaxing technology to enter the next group for continuous dewaxing through a group of pipe groups, pumping the corn oil into a crystallization pipe, sequentially passing through the rest crystallization pipes through the overflow effect, wrapping a condensation coil outside the crystallization pipe for cooling, gradually reducing the oil temperature to 1-7 ℃, preserving the temperature for 24 hours for crystallization and grain growing, and then keeping the oil temperature at the normal temperature of 20 +/-5 ℃ for filtering. Pumping the dewaxed corn oil into a deodorizing tower at 200 deg.C, removing volatile substances such as fatty acid, hydrocarbons, partial pigments and aldehydes, heating the corn oil with an electric heater for 5min to 270 deg.C, and deodorizing for 45min to obtain deodorized oil. Index detection is carried out on the product oil, and the result is as follows: trans fatty acid content 0.19%; the content of vitamin E is 1126 mg/kg; the content of phytosterol is 11186 mg/kg; the content of zearalenone was 85 mg/kg.
Example 2
Firstly, heating the corn crude oil to 55 ℃, adding food-grade citric acid with the concentration of 60 percent, wherein the dosage is 0.1 to 0.5 percent of the total weight of the oil, carrying out acid treatment for 25min, carrying out neutralization reaction on the mixture subjected to acid treatment and alkali liquor, wherein the concentration of the alkali liquor is 7 Be, the reaction time is 12min, and carrying out centrifugal separation. Adopting a secondary decolorization method technology, adding activated clay and activated carbon into the deacidified corn oil to perform primary decolorization, removing partial pigments and toxins, then adding activated carbon to perform secondary decolorization, and removing the residual toxins, wherein the primary decolorization process conditions are that the decolorizer adopts the activated carbon and the activated clay, the using amount of the activated carbon is 0.5% of the weight of the corn oil, the using amount of the activated clay is 0.5% of the weight of the corn oil, the decolorization temperature is 95 ℃, the decolorization time is 20min, and the pressure of a decolorization tower is 0.010-0.015 MPa; the secondary decolorization process condition is that activated carbon is added into the primarily decolorized corn oil to continue decolorization, and the use amount of the activated carbon is 3% of the weight of the corn oil. Pumping the decolorized corn oil into dewaxing equipment for dewaxing at the normal temperature of 20 +/-25 ℃, feeding the decolorized corn oil into the next group of continuous dewaxing equipment through a group of pipe groups by adopting a tubular continuous dewaxing technology, pumping the corn oil into a crystallizing pipe, sequentially passing through the rest crystallizing pipes through an overflow effect, externally wrapping a condensing coil pipe outside the crystallizing pipe for cooling, gradually reducing the oil temperature to 1-7 ℃, preserving the temperature for 24 hours for crystallizing and growing crystals, and then keeping the oil temperature at the normal temperature of 20 +/-5 ℃ for filtering. Pumping the dewaxed corn oil into a deodorizing tower at 200 ℃, removing volatile substances such as fatty acid, hydrocarbons, partial pigments and aldehydes, heating by an electric heater to raise the temperature of the corn oil to 270 ℃ for 45min, and feeding the deodorized oil into a finished product tower. Index detection is carried out on the product oil, and the result is as follows: trans fatty acid content 0.18%; the content of vitamin E is 1123 mg/kg; the content of phytosterol is 11135 mg/kg; the content of zearalenone was 90 mg/kg.
Example 3
Firstly, heating the corn crude oil to 70 ℃, adding food-grade citric acid with the concentration of 60 percent, wherein the dosage is 0.1 to 0.5 percent of the total weight of the oil, carrying out acid treatment for 25min, carrying out neutralization reaction on the mixture subjected to acid treatment and alkali liquor, wherein the concentration of the alkali liquor is 8 Be, the reaction time is 8min, and carrying out centrifugal separation. Adopting a secondary decolorization method technology, adding activated clay and activated carbon into the deacidified corn oil to perform primary decolorization, removing part of pigments and toxins, then adding activated carbon to perform secondary decolorization, and removing the rest toxins, wherein the primary decolorization process conditions are that activated carbon and activated clay are adopted as a decolorizer, the using amount of the activated carbon is 3% of the weight of the corn oil, the using amount of the activated clay is 3% of the weight of the corn oil, the decolorization temperature is 110 ℃, the decolorization time is 30min, and the pressure of a decolorization tower is 0.010-0.015 MPa; the secondary decolorization process condition is that active carbon is added into the primarily decolorized corn oil for continuous decolorization, and the using amount of the active carbon is 0.5 percent of the weight of the corn oil. Pumping the decolorized corn oil into a dewaxing device for dewaxing at the normal temperature of 20 +/-25 ℃, enabling the corn oil decolorized by adopting a tubular continuous dewaxing technology to enter the next group for continuous dewaxing through a group of pipe groups, pumping the corn oil into a crystallization pipe, sequentially passing through the rest crystallization pipes through the overflow effect, wrapping a condensation coil outside the crystallization pipe for cooling, gradually reducing the oil temperature to 1-7 ℃, preserving the temperature for 24 hours for crystallization and grain growing, and then keeping the oil temperature at the normal temperature of 20 +/-5 ℃ for filtering. Pumping the dewaxed corn oil into a deodorizing tower, wherein the temperature of the deodorizing tower is 190 ℃, removing volatile substances such as fatty acid, hydrocarbons, partial pigments and aldehydes, heating by an electric heater, raising the temperature of the corn oil to 260 ℃ for 4min, removing the fatty acid, and leading the whole deodorizing time to be 50min to obtain deodorized oil which enters a finished product tower. Index detection is carried out on the product oil, and the result is as follows: trans fatty acid content 0.20%; the content of vitamin E is 1120 mg/kg; the content of phytosterol is 11140 mg/kg; the zearalenone content was 84 mg/kg.
Although the present invention has been described in detail by way of preferred embodiments, the present invention is not limited thereto. Various equivalent modifications or substitutions can be made on the embodiments of the present invention by those skilled in the art without departing from the spirit and scope of the present invention, and these modifications or substitutions are within the scope of the present invention/any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention.
Claims (7)
1. A refining process of zero trans-fatty acid low-toxin corn oil is characterized by comprising the following steps:
(1) adding citric acid into the corn crude oil under the heating condition for reaction, dephosphorizing and degumming;
(2) mixing the dephosphorized and degummed corn oil with an alkali liquor for deacidification treatment, wherein the concentration of the alkali liquor is 5-8 degrees Be;
(3) pumping the deacidified corn oil into a decoloring tower for decoloring, wherein a secondary decoloring method is adopted for decoloring;
(4) dewaxing the decolorized corn oil by crystallization, wherein the dewaxing adopts tubular continuous dewaxing;
(5) and deodorizing the corn oil after dewaxing, heating and deodorizing the corn oil in two stages, pumping the corn oil into a deodorizing tower for deodorization after heating the corn oil to 180-200 ℃ in the first stage, heating the corn oil to 250-270 ℃ in the second stage for deodorization, wherein the deodorization time in the second stage is less than or equal to 5min, and feeding the corn oil into a finished product tower after deodorization to obtain the finished product oil.
2. The refining process of corn oil with zero trans-fatty acid and low toxin as claimed in claim 1, wherein the heating temperature in step (1) is 51-60 ℃, the mass concentration of citric acid is 20-80%, the amount of citric acid is 0.1-0.5% of the weight of the crude corn oil, and the reaction time of citric acid is 15-35 min.
3. The refining process of zero-trans fatty acid and low-toxin corn oil as claimed in claim 1, wherein the deacidification time of the alkali liquor in the step (2) is 8-13 min, and the temperature is normal temperature.
4. The process for zero trans fatty acid low toxin corn oil refining of claim 1 wherein in step (3), the secondary decolorization process comprises a primary decolorization and a secondary decolorization; the primary decolorization process conditions are that the decolorizer adopts active carbon and activated clay, the dosage of the active carbon is 0.5-3% of the weight of the corn oil, the dosage of the activated clay is 0.5-3% of the weight of the corn oil, the decolorization temperature is 95-110 ℃, the decolorization time is 20-30 min, and the pressure of a decolorization tower is 0.010-0.015 MPa; the secondary decolorization process condition is that activated carbon is added into the primarily decolorized corn oil for continuous decolorization, and the use amount of the activated carbon is 0.5-3% of the weight of the corn oil.
5. The refining process of corn oil with zero trans-fatty acid and low toxin as claimed in claim 1, wherein in the step (4), the crystallization dewaxing method comprises the steps of pumping the corn oil into a crystallization pipe, sequentially passing through the rest crystallization pipes through overflow action, covering a condensing coil outside the crystallization pipe for cooling, gradually reducing the oil temperature to 1-7 ℃, keeping the temperature for 24 hours for crystallization and crystal growing, and then keeping the oil temperature at the normal temperature of 20 +/-5 ℃ for filtration.
6. The zero trans fatty acid low toxin corn oil refining process of claim 1 wherein the second stage deodorizing heating in step (5) is performed in an electric heater having the following structure: the heater comprises a shell, wherein an electric heating pipe is arranged in the shell and is connected with a power supply; the corn oil is directly contacted with an electric heating pipe for heating during the deodorization heating in the second stage; the total deodorization time is 45-60 min.
7. The refining process of corn oil with zero trans-fatty acid and low toxin as claimed in claim 1, wherein the content of trans-fatty acid in the obtained corn oil finished product is less than or equal to 0.3%, the content of vitamin E is greater than or equal to 1100mg/kg, the content of phytosterol is greater than or equal to 11000mg/kg, and the content of gibberellin ketene is less than or equal to 100 ug/kg.
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| CN202210520996.3A CN115058287A (en) | 2022-05-13 | 2022-05-13 | Zero-trans-fatty-acid low-toxin corn oil refining process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116948744A (en) * | 2023-09-20 | 2023-10-27 | 曲阜良友食品有限公司 | Corn oil moderate processing technology |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103005013A (en) * | 2012-12-21 | 2013-04-03 | 山东三星玉米产业科技有限公司 | Zero trans fat acid corn oil and refining process thereof |
| CN104560382A (en) * | 2013-10-18 | 2015-04-29 | 刘俊 | Physical refining process of rice bran oil |
-
2022
- 2022-05-13 CN CN202210520996.3A patent/CN115058287A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103005013A (en) * | 2012-12-21 | 2013-04-03 | 山东三星玉米产业科技有限公司 | Zero trans fat acid corn oil and refining process thereof |
| CN104560382A (en) * | 2013-10-18 | 2015-04-29 | 刘俊 | Physical refining process of rice bran oil |
Non-Patent Citations (2)
| Title |
|---|
| 尚刚等: "精炼加工对玉米油营养指标和风险指标的影响", 中国油脂, vol. 45, no. 2, pages 15 - 20 * |
| 赵雪松等: "玉米毛油中玉米赤霉烯酮脱除技术研究", 粮食与食品工业, vol. 25, no. 3, pages 1 - 3 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116948744A (en) * | 2023-09-20 | 2023-10-27 | 曲阜良友食品有限公司 | Corn oil moderate processing technology |
| CN116948744B (en) * | 2023-09-20 | 2023-12-08 | 曲阜良友食品有限公司 | Corn oil moderate processing technology |
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