CN114958138A - Method for preparing high-viscosity low-resistance seam beautifying agent by using new material - Google Patents

Method for preparing high-viscosity low-resistance seam beautifying agent by using new material Download PDF

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Publication number
CN114958138A
CN114958138A CN202210503078.XA CN202210503078A CN114958138A CN 114958138 A CN114958138 A CN 114958138A CN 202210503078 A CN202210503078 A CN 202210503078A CN 114958138 A CN114958138 A CN 114958138A
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parts
component
agent
epoxy resin
viscosity
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许伟岳
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Chaozhou Mengma Building Materials Technology Co ltd
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Chaozhou Mengma Building Materials Technology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/70Additives characterised by shape, e.g. fibres, flakes or microspheres

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Sealing Material Composition (AREA)

Abstract

The invention discloses a high-viscosity and low-resistance seam beautifying agent prepared from a new material and a preparation method thereof, wherein the seam beautifying agent consists of a component A and a component B, and the component A comprises the following raw materials in parts by weight: 25-35 parts of mammoth elephant aqueous epoxy resin 828; 2-5 parts of benzyl alcohol; 20-27 parts of glass beads; 38-48 parts of calcium powder; 0.2-0.5 part of silane coupling agent; 0.2-0.5 of dispersant; 0.1-0.3 part of defoaming agent; the component B comprises the following raw materials in parts by weight: 4-10 parts of alicyclic amine; 4-10 parts of polyether amine; 3-7 parts of benzyl alcohol; 3-7 parts of mammoth elephant aqueous epoxy resin 828; 38-46 parts of glass beads; 32-40 parts of calcium powder; 1-3 parts of pigment; 0.5-3 parts of thixotropic agent; 0.1-0.3 part of dispersant; 0.1 to 0.3 portion of defoaming agent. The invention is environment-friendly and nontoxic, is simple and convenient to use, and solves the problems of poor binding power and easy falling of the conventional crack sealer in the existing market.

Description

Method for preparing high-viscosity low-resistance seam beautifying agent by using new material
Technical Field
The invention belongs to the technical field of coatings, and particularly relates to a method for preparing a high-viscosity low-resistance crack sealer by using a new material.
Background
The invention relates to the technical field of seam beautifying agents, and provides a seam beautifying agent prepared from a new material and having high viscosity and low resistance and a preparation method thereof. The high-viscosity low-resistance crack sealer comprises a component A and a component B.
Disclosure of Invention
The invention aims to provide a method for preparing a high-viscosity and low-resistance crack sealer by using a new material, and aims to solve the problem of bonding of the crack sealer, increase the bonding force between a ceramic tile and a wall surface or a ground and solve the problem of falling. In order to realize the purpose, the invention adopts the technical scheme that:
a novel material acting material is prepared into a high-viscosity and low-resistance seam beautifying agent, the seam beautifying agent is composed of a component A and a component B, and the component A comprises the following raw materials in parts by weight: 25-35 parts of mammoth elephant aqueous epoxy resin 828; 2-5 parts of benzyl alcohol; 20-27 parts of glass beads; 38-48 parts of calcium powder; 0.2-0.5 part of silane coupling agent; 0.2-0.5 of dispersant; 0.1-0.3 part of defoaming agent;
the component B comprises the following raw materials in parts by weight: 4-10 parts of alicyclic amine; 4-10 parts of polyether amine; 3-7 parts of benzyl alcohol; 3-7 parts of mammoth elephant aqueous epoxy resin 828; 38-46 parts of glass beads; 32-40 parts of calcium powder; 1-3 parts of pigment; 0.5-3 parts of thixotropic agent; 0.1-0.3 part of dispersant; 0.1 to 0.3 portion of defoaming agent.
Preferably, the pigment comprises at least one of pearl powder, glitter powder, copper-gold powder, aluminum paste and titanium dioxide.
Preferably, the weight ratio of the component A to the component B is as follows: 1:1-2.
Preferably, the polyether amine is prepared by reacting at least one of polyoxypropylene diamine, polyoxypropylene triamine and polyoxyethylene diamine with a second liquid epoxy resin and monofunctional glycidyl ether.
Preferably, the thixotropic agent is at least one of hydrogenated castor oil, cellulose, fumed silica and bentonite.
A method for preparing a high-viscosity low-resistance seam beautifying agent by using a new material comprises the following steps:
adding all the mammoth elephant aqueous epoxy resin 828, benzyl alcohol, a silane coupling agent, a dispersing agent, glass beads, calcium powder and a defoaming agent into a horizontal stirrer with a heating device, controlling the temperature to be about 75 ℃, slowly stirring for 30-40 minutes at a constant speed until the mixture is uniform, and vacuumizing to obtain a component A;
the preparation method of the component B comprises the following steps:
adding various alicyclic amines, polyether amines, benzyl alcohol and mammoth aqueous epoxy resin 828 in a certain proportion into a reaction device, stirring and synthesizing, controlling the reaction temperature at 60-90 ℃, controlling the reaction time at 1.5-2 hours, properly cooling by using a water circulation device in the reaction process, avoiding overhigh temperature, and indicating that the synthesis is finished when the reaction temperature does not rise any more;
the synthesized curing agent is a water-based high polymer material with the characteristics of good flexibility, high wear resistance, good adhesion, high water solubility and the like, and the ratio of the water-based high polymer material to the water-based epoxy resin is 1: 2;
then pouring the product into an integrated stirrer with a vacuum device, adding glass beads, calcium powder, pigment, thixotropic agent and defoaming agent at the rotation speed of 100 plus 300 r/min, stirring uniformly for 30-40 min, and vacuumizing to obtain the component B.
The invention has the beneficial effects that: the high-viscosity low-resistance crack sealer and the preparation method thereof are environment-friendly, non-toxic and simple and convenient to use, and solve the problems that the conventional crack sealer on the existing market is poor in bonding force and easy to fall off.
Detailed Description
In order to facilitate an understanding of the invention, reference will now be made to the preferred embodiments of the invention. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used herein in the description of the invention is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
The technical solution of the present patent will be described in further detail with reference to the following embodiments.
The first embodiment is as follows:
a novel material is used for preparing a high-viscosity and low-resistance seam beautifying agent, the seam beautifying agent is composed of a component A and a component B, and the component A comprises the following raw materials in parts by weight: 828 parts of mammoth elephant aqueous epoxy resin; 5 parts of benzyl alcohol; 20 parts of glass beads; 38 parts of calcium powder; 0.2 part of silane coupling agent; 0.2 parts of dispersant; 0.1 part of defoaming agent;
the component B comprises the following raw materials in parts by weight: 10 parts of alicyclic amine; 10 parts of polyether amine; benzyl alcohol, 3 parts; 3 parts of mammoth elephant aqueous epoxy resin 828; 46 parts of glass beads; 40 parts of calcium powder; 1-3 parts of pigment; 3 parts of thixotropic agent; 0.3 part of dispersant; 0.3 part of defoaming agent.
In this embodiment, the pigment includes at least one of pearl powder, glitter powder, bronze powder, aluminum paste, and titanium dioxide.
In this particular example, the weight ratio of the a component to the B component is: 1:1.
In this embodiment, the polyether amine is prepared by reacting at least one of polyoxypropylene diamine, polyoxypropylene triamine and polyoxyethylene diamine with a second liquid epoxy resin and a monofunctional glycidyl ether.
In this particular embodiment, the thixotropic agent is at least one of hydrogenated castor oil, cellulose, fumed silica, bentonite.
Example two:
a novel material is used for preparing a high-viscosity and low-resistance seam beautifying agent, the seam beautifying agent is composed of a component A and a component B, and the component A comprises the following raw materials in parts by weight: 25 parts of mammoth elephant aqueous epoxy resin 828; 5 parts of benzyl alcohol; 27 parts of glass beads; 38 parts of calcium powder; 0.2 part of silane coupling agent; 0.5 parts of dispersing agent; 0.3 part of defoaming agent;
the component B comprises the following raw materials in parts by weight: 10 parts of alicyclic amine; 4 parts of polyether amine; benzyl alcohol, 3 parts; 3 parts of mammoth elephant aqueous epoxy resin 828; 38 parts of glass beads; 32 parts of calcium powder; 3 parts of pigment; 0.5 part of thixotropic agent; 0.1 part of dispersant; 0.1 part of defoaming agent.
In this embodiment, the pigment includes at least one of pearl powder, glitter powder, bronze powder, aluminum paste, and titanium dioxide.
In this particular example, the weight ratio of the a component to the B component is: 1:2.
In this embodiment, the polyether amine is prepared by reacting at least one of polyoxypropylene diamine, polyoxypropylene triamine and polyoxyethylene diamine with a second liquid epoxy resin and a monofunctional glycidyl ether.
In this particular embodiment, the thixotropic agent is at least one of hydrogenated castor oil, cellulose, fumed silica, bentonite.
Example three:
a method for preparing a high-viscosity low-resistance crack sealer by using a new material comprises the following steps:
adding all the mammoth elephant aqueous epoxy resin 828, benzyl alcohol, a silane coupling agent, a dispersing agent, glass beads, calcium powder and a defoaming agent into a horizontal stirrer with a heating device, controlling the temperature to be about 75 ℃, slowly stirring for 30-40 minutes at a constant speed until the mixture is uniform, and vacuumizing to obtain a component A;
the preparation method of the component B comprises the following steps:
adding various alicyclic amines, polyether amines, benzyl alcohol and mammoth aqueous epoxy resin 828 in a certain proportion into a reaction device, stirring and synthesizing, controlling the reaction temperature at 60-90 ℃, controlling the reaction time at 1.5-2 hours, properly cooling by using a water circulation device in the reaction process, avoiding overhigh temperature, and indicating that the synthesis is finished when the reaction temperature does not rise any more;
the synthesized curing agent is a water-based high polymer material with the characteristics of good flexibility, high wear resistance, good adhesion, high water solubility and the like, and the ratio of the water-based high polymer material to the water-based epoxy resin is 1: 2;
then pouring the product into an integrated stirrer with a vacuum device, adding glass beads, calcium powder, pigment, thixotropic agent and defoaming agent, stirring uniformly at the rotation speed of 100-.
Application example:
Figure BDA0003634990370000041
Figure BDA0003634990370000051
in conclusion, the high-viscosity low-resistance crack sealer and the preparation method thereof are environment-friendly, non-toxic, simple and convenient to use, and solve the problems that the conventional crack sealer on the existing market is poor in bonding force and easy to fall off.
The above embodiments are only for illustrating the present invention and not for limiting the present invention, and those skilled in the art can make various changes and modifications without departing from the spirit and scope of the present invention, therefore all equivalent technical solutions also belong to the scope of the present invention, and the protection scope of the present invention should be defined by the claims.

Claims (6)

1. A high-viscosity low-resistance seam beautifying agent prepared from a new material is characterized in that: the crack sealer is composed of a component A and a component B, wherein the component A comprises the following raw materials in parts by weight: 25-35 parts of mammoth elephant aqueous epoxy resin 828; 2-5 parts of benzyl alcohol; 20-27 parts of glass beads; 38-48 parts of calcium powder; 0.2-0.5 part of silane coupling agent; 0.2-0.5 of dispersant; 0.1-0.3 part of defoaming agent;
the component B comprises the following raw materials in parts by weight: 4-10 parts of alicyclic amine; 4-10 parts of polyether amine; 3-7 parts of benzyl alcohol; 3-7 parts of mammoth elephant aqueous epoxy resin 828; 38-46 parts of glass beads; 32-40 parts of calcium powder; 1-3 parts of pigment; 0.5-3 parts of thixotropic agent; 0.1-0.3 part of dispersant; 0.1 to 0.3 portion of defoaming agent.
2. The novel material as claimed in claim 1, which is a high-viscosity and low-resistance crack sealer, characterized in that: the pigment comprises at least one of pearl powder, glitter powder, copper-gold powder, aluminum paste and titanium dioxide.
3. The novel material as claimed in claim 1, which is a high-viscosity and low-resistance crack sealer, characterized in that: the weight ratio of the component A to the component B is as follows: 1:1-2.
4. The novel material as claimed in claim 1, which is a high-viscosity and low-resistance crack sealer, characterized in that: the polyether amine is prepared by reacting at least one of polyoxypropylene diamine, polyoxypropylene triamine and polyoxyethylene diamine with second liquid epoxy resin and monofunctional glycidyl ether.
5. The novel material as claimed in claim 1, which is a high-viscosity and low-resistance crack sealer, characterized in that: the thixotropic agent is at least one of hydrogenated castor oil, cellulose, fumed silica and bentonite.
6. A method for preparing a high-viscosity low-resistance seam beautifying agent by using a new material is characterized by comprising the following steps of: the preparation method of the component A comprises the following steps:
adding all the mammoth elephant aqueous epoxy resin 828, benzyl alcohol, a silane coupling agent, a dispersing agent, glass beads, calcium powder and a defoaming agent into a horizontal stirrer with a heating device, controlling the temperature to be about 75 ℃, slowly stirring for 30-40 minutes at a constant speed until the mixture is uniform, and vacuumizing to obtain a component A;
the preparation method of the component B comprises the following steps:
adding various alicyclic amines, polyether amines, benzyl alcohol and mammoth aqueous epoxy resin 828 in a certain proportion into a reaction device, stirring and synthesizing, controlling the reaction temperature at 60-90 ℃, controlling the reaction time at 1.5-2 hours, properly cooling by using a water circulation device in the reaction process, avoiding overhigh temperature, and indicating that the synthesis is finished when the reaction temperature does not rise any more;
the synthesized curing agent is a water-based high polymer material with the characteristics of good flexibility, high wear resistance, good adhesion, high water solubility and the like, and the ratio of the water-based high polymer material to the water-based epoxy resin is 1: 2;
then pouring the product into an integrated stirrer with a vacuum device, adding glass beads, calcium powder, pigment, thixotropic agent and defoaming agent, stirring uniformly at the rotation speed of 100-.
CN202210503078.XA 2022-05-09 2022-05-09 Method for preparing high-viscosity low-resistance seam beautifying agent by using new material Pending CN114958138A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL7201727A (en) * 1971-06-28 1973-01-02
CN105969046A (en) * 2016-05-13 2016-09-28 苏州久居环保科技有限公司 Disease-suppression antibacterial beautiful sealant and preparation technology thereof
CN107189636A (en) * 2017-07-03 2017-09-22 芜湖市科迪防水节能科技有限公司 A kind of aqueous double-component epoxy joint trimming agent and preparation method thereof
CN110951358A (en) * 2019-11-19 2020-04-03 广东海特高新材料有限公司 Double-component water-based tile crack beautifying agent and preparation method thereof
CN114790357A (en) * 2022-05-17 2022-07-26 潮州市猛犸象建材科技有限公司 Bi-component epoxy crack sealer capable of being used for wet construction and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL7201727A (en) * 1971-06-28 1973-01-02
CN105969046A (en) * 2016-05-13 2016-09-28 苏州久居环保科技有限公司 Disease-suppression antibacterial beautiful sealant and preparation technology thereof
CN107189636A (en) * 2017-07-03 2017-09-22 芜湖市科迪防水节能科技有限公司 A kind of aqueous double-component epoxy joint trimming agent and preparation method thereof
CN110951358A (en) * 2019-11-19 2020-04-03 广东海特高新材料有限公司 Double-component water-based tile crack beautifying agent and preparation method thereof
CN114790357A (en) * 2022-05-17 2022-07-26 潮州市猛犸象建材科技有限公司 Bi-component epoxy crack sealer capable of being used for wet construction and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
吕美华等: "美缝剂性能研究及施工应用", 《广东建材》 *

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