CN114950302A - Fluoride reation kettle temperature control system and temperature control device - Google Patents
Fluoride reation kettle temperature control system and temperature control device Download PDFInfo
- Publication number
- CN114950302A CN114950302A CN202210642170.4A CN202210642170A CN114950302A CN 114950302 A CN114950302 A CN 114950302A CN 202210642170 A CN202210642170 A CN 202210642170A CN 114950302 A CN114950302 A CN 114950302A
- Authority
- CN
- China
- Prior art keywords
- liquid
- reaction kettle
- temperature control
- box
- liquid adding
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
-
- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
- G05D23/00—Control of temperature
- G05D23/19—Control of temperature characterised by the use of electric means
- G05D23/20—Control of temperature characterised by the use of electric means with sensing elements having variation of electric or magnetic properties with change of temperature
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00004—Scale aspects
- B01J2219/00006—Large-scale industrial plants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
Abstract
The invention discloses a fluoride reaction kettle temperature control system and a temperature control device, and relates to the technical field of fluoride reaction. In the invention, through the temperature regulator, the liquid adding device and the adjusting device which are matched with the reaction kettle, the liquid adding sequence of the liquid adding devices is adjusted, and the temperature in the reaction kettle body and the time of the temperature during liquid adding are assisted to be adjusted, so that the large-batch reaction of the fluoride is facilitated.
Description
Technical Field
The invention relates to the technical field of fluoride reaction, in particular to a temperature control system and a temperature control device of a fluoride reaction kettle.
Background
Fluoride refers to organic or inorganic compounds containing fluorine in negative valence. Like other halogens, fluorine generates a single negative ion (fluoride ion F-). In the fluoride reaction, the reaction is often carried out by using a reaction vessel as a vessel.
In order to meet the requirement that reactants in the fluoride can react fully and with high quality, the reaction temperature and the reaction time in the reaction kettle need to be observed and adjusted manually in real time, so that the method is time-consuming, labor-consuming and inconvenient for large-batch reaction of the fluoride.
Disclosure of Invention
The invention aims to solve the problems of the prior art, and provides a temperature control system and a temperature control device for a fluoride reaction kettle.
In order to achieve the purpose, the invention adopts the following technical scheme:
a fluoride reaction kettle temperature control system and a temperature control device comprise a base, a reaction kettle body arranged on the top of the base, a temperature regulator positioned on the right side of the reaction kettle body, a support arranged on the top of the base, a plurality of liquid adding devices arranged on the top of the support and an adjusting device arranged at the bottom of the liquid adding devices, wherein the adjusting device is used for adjusting the liquid adding sequence of the liquid adding devices and assisting in adjusting the temperature and the temperature time in the reaction kettle body during liquid adding;
the liquid adding device comprises a liquid adding box, a piston arranged in the liquid adding box in a sliding manner, a liquid inlet arranged at the right lower part of the liquid adding box, a liquid inlet one-way valve embedded in the liquid inlet and pinched, and a liquid adding pipe arranged on the surface of the liquid adding box and communicated with the liquid inlet, wherein the other end of the liquid adding pipe is communicated with an external liquid storing device, an air hole is formed in the top end of the liquid adding box, a liquid outlet is formed in the bottom of the liquid adding box, and a liquid discharging pipe communicated with the liquid outlet is arranged at the bottom end of the liquid adding box;
adjusting device includes the backplate with leg joint, set up in the cylindric seal box of backplate front side and rotate and set up in the inside commentaries on classics board of cylindric seal box, set up in the catheter of commentaries on classics board front surface, this internal intercommunication of cylindric seal box front end middle part and reation kettle is run through to catheter one end, and is a plurality of the liquid discharge tube is kept away from the one end of liquid feeding box and is communicated with the through-hole of cylindric seal box inner wall, the through-hole slides from the one end of liquid discharge tube and is provided with the opening mechanism who is used for communicateing the catheter, it is provided with the bull stick to change the board rear side, the bull stick passes through first motor drive.
Further, the opening mechanism comprises a sliding cylinder which is arranged in the through hole in an up-and-down sliding manner, the middle part of the sliding cylinder is hollow, one end of the sliding cylinder, which is far away from the liquid guide pipe, is sealed, liquid inlet holes are formed in the front end and the rear end of the sliding cylinder, liquid passing grooves which are communicated with the liquid inlet holes are formed in the inner walls of the left side and the right side of the through hole, the liquid passing grooves are positioned at one end close to the liquid discharge pipe, a limiting block is arranged in one end of the through hole, which is close to the liquid discharge pipe, and a first reset spring is arranged between the sliding cylinder and the limiting block;
the inner wall of cylindric seal box is provided with a plurality of guide holders that rotate with a plurality of slide drums and be connected, slide drum one side sets up and is provided with bellied slide bar, set up in the guide holder with slide bar complex C form spout, C form spout slope sets up.
Further, the liquid guide pipe end part is connected with the surface of the rotating plate through a fixed seat, one side of the fixed seat is provided with a triangular block which is convenient to contact with a plurality of sliding cylinders, and the triangular block is arranged along the rotating direction of the rotating plate.
Furthermore, it is a plurality of opening mechanism and one cross even equidistance of fixing base and distribute in cylindric seal box circumference, and be a plurality of opening mechanism sets up in succession, and one crosses the fixing base and is located a plurality of opening mechanism's end to end department.
Further, the temperature regulator comprises a shell, and a heat medium and a cold medium which are arranged in the shell, wherein the heat medium and the cold medium are respectively conveyed by a first conveying pump and a second conveying pump.
Further, reation kettle body lower part one side is provided with two feed liquor pipes, and two feed liquor pipes communicate with the output of first delivery pump and second delivery pump respectively, reation kettle body upper portion one side is provided with two drain pipes of heat and cold, two drain pipes of heat and cold communicate with hot medium and cold medium respectively, this internal two coiled pipes of heat and cold that are provided with of reation kettle, two coiled pipes of heat and cold communicate with two drain pipes of heat and cold respectively.
Further, opening mechanism one side is provided with the trigger mechanism who is used for opening first delivery pump or second delivery pump, trigger mechanism sets up in the connecting plate on slide surface, sets up ejector pin, the eccentric mounting of connecting plate one side in the movable contact mounting panel on ejector pin surface and the fixed contact mounting panel that is located movable contact mounting panel top including rotating, movable contact mounting panel and fixed contact mounting panel all with guide bar sliding connection, the guide bar is installed in cylindric seal box inner wall, be provided with second reset spring between the inner wall of fixed contact mounting panel top and cylindric seal box, the guide bar surface is located to second reset spring cover.
Further, cylindric seal box surface is provided with a plurality of adjustable timers, and is a plurality of the timer sets up with a plurality of opening mechanism one-to-one, the timer lower part is provided with the start button, the inner wall and the start button contact of cylindric seal box are run through on ejector pin upper portion.
Further, a rotating shaft is rotatably arranged in the reaction kettle body, a plurality of stirring paddles are arranged on the surface of the rotating shaft, the rotating shaft is driven by a second motor, and a discharge opening is formed in the bottom of the reaction kettle body;
the inner wall of the reaction kettle body is sequentially provided with a heat insulation layer, a placing cavity and a heat conduction layer from outside to inside, and the placing cavity is used for placing a coiled pipe.
Furthermore, a plurality of temperature sensors which are uniformly arranged are sequentially arranged on the inner wall of the reaction kettle body from bottom to top, the output ends of the temperature sensors and the counter are electrically connected with the input end of a processor, the processor is respectively electrically connected with a display screen and a keyboard, the output end of the processor is electrically connected with the input end of a relay, and the output end of the relay is respectively electrically connected with a first delivery pump, a first motor of a second delivery pump and a buzzer;
the processor and the relay are embedded inside the control panel, the buzzer, the display screen and the keyboard are embedded on the surface of the control panel, and the control panel is installed on the front surface of the shell.
Compared with the prior art, the invention has the following beneficial effects:
in the invention, through the temperature regulator, the liquid adding device and the adjusting device which are matched with the reaction kettle, the liquid adding sequence of the liquid adding devices is adjusted, and the temperature in the reaction kettle body and the time of the temperature during liquid adding are assisted to be adjusted, so that the large-batch reaction of the fluoride is facilitated.
Drawings
FIG. 1 is a schematic view of the overall structure of a temperature control system and a temperature control device of a fluoride reaction kettle according to the present invention;
FIG. 2 is a schematic structural diagram of a temperature control system of a fluoride reaction kettle and a reaction kettle body in a temperature control device according to the present invention;
FIG. 3 is a schematic structural view of a fluoride reaction kettle temperature control system and a liquid adding device in a temperature control device according to the present invention;
FIG. 4 is a schematic structural diagram of a temperature control system of a fluoride reaction kettle and an adjusting device in a temperature control device according to the present invention;
FIG. 5 is a schematic structural diagram of a temperature control system of a fluoride reaction kettle and an adjusting device in a temperature control device according to the present invention;
FIG. 6 is a schematic structural diagram of an opening mechanism in a temperature control system and a temperature control device of a fluoride reaction kettle according to the present invention;
FIG. 7 is a kinematic diagram of FIG. 6;
FIG. 8 is a schematic structural view of a temperature control system of a fluoride reaction kettle and a structure of a temperature control device in which a top rod is in contact with a start button;
FIG. 9 is a schematic structural view of a fluoride reaction kettle temperature control system and a temperature control device according to the present invention, in which a top rod is separated from a start button;
FIG. 10 is a schematic structural view of a temperature control system of a fluoride reaction vessel and a trigger mechanism in a temperature control device according to the present invention;
FIG. 11 is a kinematic diagram of FIG. 10;
FIG. 12 is a schematic structural view of a guide seat in a temperature control system and a temperature control device of a fluoride reaction kettle according to the present invention;
FIG. 13 is a kinematic diagram of FIG. 12;
fig. 14 is an enlarged view of the temperature control system of the fluoride reaction kettle and the reaction kettle body structure in the temperature control device according to the present invention.
In the figure: 1. a base; 2. a reaction kettle body; 21. a rotating shaft; 22. a stirring paddle; 23. a liquid inlet pipe; 25. a liquid outlet pipe; 26. a serpentine tube; 27. a temperature sensor; 28. a heat conductive layer; 29. a thermal insulation layer; 3. a temperature regulator; 4. a support; 5. a liquid adding device; 51. a liquid adding box; 52. a piston; 53. a liquid feeding pipe; 54. a liquid discharge pipe; 6. an adjustment device; 61. a back plate; 62. a cylindrical seal box; 63. rotating the plate; 64. a catheter; 641. a fixed seat; 65. an opening mechanism; 651. a slide cylinder; 652. a limiting block; 653. a guide seat; 654. a slide bar; 655. a C-shaped chute; 66. a trigger mechanism; 661. a connecting plate; 662. a top rod; 663. a movable contact mounting plate; 664. a fixed contact mounting plate; 665. a guide bar; 67. a timer; 671. the button is actuated.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, are merely for convenience in describing the present invention and simplifying the description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention.
Referring to fig. 1-14, a fluoride reaction kettle temperature control system and a temperature control device comprise a base 1, a reaction kettle body 2 arranged at the top of the base 1, a temperature regulator 3 positioned at the right side of the reaction kettle body 2, a support 4 arranged at the top of the base 1, a plurality of liquid adding devices 5 arranged at the top of the support 4 and an adjusting device 6 arranged at the bottom of the liquid adding devices 5, wherein the adjusting device 6 is used for adjusting the liquid adding sequence of the liquid adding devices 5 and assisting in adjusting the temperature and the temperature time in the reaction kettle body 2 during liquid adding;
the liquid adding device 5 comprises a liquid adding box 51, a piston 52 arranged in the liquid adding box 51 in a sliding manner, a liquid inlet arranged at the right lower part of the liquid adding box 51, a liquid inlet one-way valve embedded between the liquid inlet and a liquid adding pipe 53 arranged on the surface of the liquid adding box 51 and communicated with the liquid inlet, the other end of the liquid adding pipe 53 is communicated with an external liquid storage device, the top end of the liquid adding box 51 is provided with an air hole, the bottom of the liquid adding box 51 is provided with a liquid outlet, and the bottom end of the liquid adding box 51 is provided with a liquid discharging pipe 54 communicated with the liquid outlet;
adjusting device 6 includes backplate 61 of being connected with support 4, set up cylindric seal box 62 and the rotation of backplate 61 front side and set up in the inside commentaries on classics board 63 of cylindric seal box 62, set up in the catheter 64 of commentaries on classics board 63 front surface, intercommunication in cylindric seal box 62 front end middle part and the reation kettle body 2 is run through to catheter 64 one end, the one end that adds liquid box 51 is kept away from to a plurality of fluid-discharge tubes 54 communicates with the through-hole of cylindric seal box 62 inner wall, it is provided with opening mechanism 65 that is used for communicating catheter 64 to slide in the one end that the through-hole leaves fluid-discharge tube 54, commentaries on classics board 63 rear side is provided with the bull stick, the bull stick passes through first motor drive.
Further, the opening mechanism 65 comprises a sliding cylinder 651 arranged in the through hole in a vertically sliding manner, the middle of the sliding cylinder 651 is hollow, one end, away from the liquid guide tube 64, of the sliding cylinder is sealed, liquid inlet holes are formed in the front end and the rear end of the sliding cylinder 651, liquid passing grooves communicated with the liquid inlet holes are formed in the inner walls of the left side and the right side of the through hole, the liquid passing grooves are located at one end close to the liquid discharge tube 54, a limiting block 652 is arranged at one end, close to the liquid discharge tube 54, of the through hole, and a first reset spring is arranged between the sliding cylinder 651 and the limiting block 652;
the inner wall of the cylindrical sealing box 62 is provided with a plurality of guide seats 653 which are rotatably connected with a plurality of sliding cylinders 651, one side of the sliding cylinder 651 is provided with a convex sliding rod 654, a C-shaped sliding groove 655 which is matched with the sliding rod 654 is arranged in the guide seats 653, and the C-shaped sliding groove 655 is obliquely arranged.
Furthermore, the end of the liquid guiding tube 64 is connected to the surface of the rotating plate 63 through a fixing seat 641, and a triangular block which is convenient to contact with the plurality of sliding cylinders 651 is arranged on one side of the fixing seat 641 and is arranged along the rotating direction of the rotating plate 63.
Further, a plurality of opening mechanisms 65 and a fixing seat 641 are uniformly and equidistantly distributed on the circumference of the cylindrical sealing box 62, the plurality of opening mechanisms 65 are continuously arranged, and the fixing seat 641 is located at the end-to-end connection of the plurality of opening mechanisms 65.
Further, the temperature regulator 3 includes a housing, and a heat medium and a cold medium that are provided in the housing, and the heat medium and the cold medium are respectively conveyed by the first conveying pump and the second conveying pump.
Further, 2 lower part one sides of reation kettle body are provided with two feed liquor pipes 23, and two feed liquor pipes 23 communicate with the output of first delivery pump and second delivery pump respectively, and 2 upper portion one sides of reation kettle body are provided with two drain pipes 25 of heat-cold, and two drain pipes 25 of heat-cold communicate with hot medium and cold medium respectively, are provided with two coiled pipes 26 of heat-cold in the reation kettle body 2, and two coiled pipes 26 of heat-cold communicate with two drain pipes 25 of heat-cold respectively.
Further, the opening mechanism 65 is provided with a trigger mechanism 66 for opening the first delivery pump or the second delivery pump on one side, the trigger mechanism 66 includes a connecting plate 661 rotatably disposed on the surface of the sliding barrel 651, a push rod 662 disposed on one side of the connecting plate 661, a movable contact mounting plate 663 eccentrically disposed on the surface of the push rod 662, and a fixed contact mounting plate located at the top of the movable contact mounting plate 663, the movable contact mounting plate 663 and the fixed contact mounting plate 664 are both slidably connected with a guide rod 665, the guide rod 665 is disposed in the inner wall of the cylindrical seal box 62, a second return spring is disposed between the top of the fixed contact mounting plate 664 and the inner wall of the cylindrical seal box 62, and the guide rod 665 is sleeved with the second return spring.
Further, a plurality of adjustable timers 67 are arranged on the surface of the cylindrical sealing box 62, the timers 67 and the opening mechanisms 65 are arranged in a one-to-one correspondence mode, a starting button 671 is arranged on the lower portion of each timer 67, and the upper portion of the ejector rod 662 penetrates through the inner wall of the cylindrical sealing box 62 to be in contact with the starting button 671.
Further, a rotating shaft 21 is rotatably arranged in the reaction kettle body 2, a plurality of stirring paddles 22 are arranged on the surface of the rotating shaft 21, the rotating shaft 21 is driven by a second motor, and a discharge opening is formed in the bottom of the reaction kettle body 2;
the inner wall of the reaction kettle body 2 is provided with a heat insulation layer 29, a placing cavity and a heat conduction layer 28 from outside to inside in sequence, and the placing cavity is used for placing the coiled pipe 26.
Further, a plurality of temperature sensors 27 which are uniformly arranged are sequentially arranged on the inner wall of the reaction kettle body 2 from bottom to top, the output ends of the temperature sensors 27 and the counter are electrically connected with the input end of the processor, the processor is respectively electrically connected with the display screen and the keyboard, the output end of the processor is electrically connected with the input end of the relay, and the output end of the relay is respectively electrically connected with the first delivery pump, the first motor of the second delivery pump and the buzzer;
the processor and the relay are embedded inside the control panel, the buzzer, the display screen and the keyboard are embedded on the surface of the control panel, and the control panel is installed on the front surface of the shell.
The working principle is as follows: when the reaction kettle is used, the sequence and the weight of a plurality of reactants placed in the reaction kettle body 2, the reaction time and the reaction temperature of the two reactants are determined, and the reaction time is correspondingly set in the timer 67;
then, according to the sequence of the reactants and the required weight, the reactants are sequentially introduced into the liquid adding boxes 51 through an external liquid storage device, when the reactants are introduced into the liquid adding boxes 51, the rotating plate 63 in the adjusting device 6 does not rotate, so that the liquid guide pipe 64 is not communicated with any liquid adding box 51, the piston 52 in the liquid adding box 51 is driven to move upwards, and air at the upper part of the liquid adding box 51 is pressed, so that the reactants are temporarily stored in the liquid adding boxes 51, wherein the reactants are sequentially added into the liquid adding boxes 51 from right to left according to the positions in the liquid adding boxes 51 in fig. 1 and the positions of the triangular blocks in fig. 6;
further, the first motor is started, so that the rotating plate 63 is driven to rotate, the triangular block is driven to be in contact with the first sliding cylinder 651, the sliding cylinder 651 is driven to be far away from the rotating plate 63, at the moment, the sliding rod 654 on the surface of the sliding cylinder 651 slides along the obliquely arranged C-shaped sliding groove 655, the sliding cylinder 651 is driven to rotate in the moving process, the sliding cylinder 651 extrudes the first return spring, the liquid inlet hole in the sliding cylinder 651 is communicated with the liquid passing groove, the liquid drainage pipe 54 is communicated with the liquid drainage pipe 64, and then reactants in the liquid adding box 51 flow into the liquid drainage pipe 64 along the liquid drainage pipe 54 and further flow into the reaction kettle body 2;
when the sliding cylinder 651 is far away from the rotating plate 63, the sliding cylinder 651 moves through the connecting plate 661 to drive the ejector rod 662 to move, and further drive the movable contact mounting plate 663 to contact with the fixed contact mounting plate 664, and further start the first conveying pump or the second conveying pump, so that a heat medium or a cold medium enters the coil 26 through the liquid inlet pipe 23 to change the temperature in the reaction kettle body 2, and the temperature in the reaction kettle body 2 is the reaction temperature of the added reactants;
when the top rod 662 moves, one end of the top rod 662 away from the connecting plate 661 is in contact with the start button 671, so that the timer 67 starts to count time;
wherein, the temperature sensor 27 in the reaction kettle body 2 sends the temperature in the reaction kettle body 2 to the processor, and then the processor sends the detection result to the display screen for displaying;
when the time of the timer 67 is up, the processor sends an instruction to the relay to control the first delivery pump or the second delivery pump to be closed, and simultaneously controls the buzzer to sound to remind an operator, and at the moment, the operator can check the temperature data in the reaction kettle body 2 in the display screen;
further, the motor is started to drive the rotating plate 63 to rotate to be separated from the opening mechanism 65 to be contacted with the next opening mechanism 65, and the reaction is repeated;
when the rotating plate 63 rotates to be separated from the opening mechanism 65, the sliding cylinder 651 is reset under the action of the first reset spring, and the trigger mechanism 66 and the opening mechanism 65 are reset;
wherein, the motor is a stepping motor, and the rotation angle of the motor is determined by the number of the plurality of opening mechanisms 65 and the number of the one over-fixing seat 641;
the first delivery pump or the second delivery pump started by the trigger mechanism 66 is specifically determined by the temperature of the last reactant after the reaction and the temperature difference of the reactant;
when the reactants react in the reaction kettle body 2, the second motor is synchronously started to drive the rotating shaft 21 to rotate, and then the reactants are mixed through the stirring paddle 22, so that the reactants are fully contacted;
the final reactant product is directed out through a discharge port.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (10)
1. A fluoride reaction kettle temperature control system and a temperature control device are characterized by comprising a base (1), a reaction kettle body (2) arranged at the top of the base (1), a temperature regulator (3) positioned on the right side of the reaction kettle body (2), a support (4) arranged at the top of the base (1), a plurality of liquid adding devices (5) arranged at the top of the support (4) and an adjusting device (6) arranged at the bottom of the liquid adding devices (5), wherein the adjusting device (6) is used for adjusting the liquid adding sequence of the liquid adding devices (5) and assisting in adjusting the temperature and the temperature time in the reaction kettle body (2) during liquid adding;
the liquid adding device (5) comprises a liquid adding box (51), a piston (52) arranged in the liquid adding box (51) in a sliding mode, a liquid inlet formed in the lower right portion of the liquid adding box (51), a liquid inlet one-way valve embedded in the liquid inlet and pinched, and a liquid adding pipe (53) arranged on the surface of the liquid adding box (51) and communicated with the liquid inlet, wherein the other end of the liquid adding pipe (53) is communicated with an external liquid storage device, an air hole is formed in the top end of the liquid adding box (51), a liquid outlet is formed in the bottom of the liquid adding box (51), and a liquid discharging pipe (54) communicated with the liquid outlet is arranged at the bottom end of the liquid adding box (51);
adjusting device (6) include backplate (61) be connected with support (4), set up in cylindric seal box (62) of backplate (61) front side and rotate set up in cylindric seal box (62) inside commentaries on classics board (63), set up in catheter (64) of changeing board (63) front surface, intercommunication in cylindric seal box (62) front end middle part and reation kettle body (2) is run through to catheter (64) one end, and is a plurality of liquid discharge tube (54) keep away from the one end of adding liquid box (51) and the through-hole intercommunication of cylindric seal box (62) inner wall, the through-hole slides from the one end of liquid discharge tube (54) and is provided with opening mechanism (65) that are used for communicateing catheter (64), it is provided with the bull stick to change board (63) rear side, the bull stick passes through first motor drive.
2. The fluoride reaction kettle temperature control system and device according to claim 1, wherein the opening mechanism (65) comprises a slide cylinder (651) which is slidably arranged in a through hole up and down, the slide cylinder (651) is hollow in the middle, one end far away from the liquid guide tube (64) is sealed, liquid inlet holes are formed in the front end and the rear end of the slide cylinder (651), liquid passing grooves communicated with the liquid inlet holes are formed in the inner walls of the left side and the right side of the through hole, the liquid passing grooves are located at one end close to the liquid discharge tube (54), a limit block (652) is arranged in one end of the through hole close to the liquid discharge tube (54), and a first return spring is arranged between the slide cylinder (651) and the limit block (652);
the inner wall of the cylindrical sealing box (62) is provided with a plurality of guide seats (653) which are rotatably connected with a plurality of sliding cylinders (651), one side of each sliding cylinder (651) is provided with a convex sliding rod (654), a C-shaped sliding groove (655) matched with the sliding rod (654) is formed in each guide seat (653), and the C-shaped sliding groove (655) is obliquely arranged.
3. The fluoride reaction kettle temperature control system and device according to claim 2, wherein the end of the liquid guide tube (64) is connected with the surface of the rotating plate (63) through a fixed seat (641), one side of the fixed seat (641) is provided with a triangular block which is convenient to contact with a plurality of sliding cylinders (651), and the triangular block is arranged along the rotating direction of the rotating plate (63).
4. The fluoride reaction kettle temperature control system and device according to claim 3, wherein the plurality of opening mechanisms (65) and the one passing fixing seat (641) are uniformly and equidistantly distributed on the circumference of the cylindrical sealing box (62), the plurality of opening mechanisms (65) are continuously arranged, and the one passing fixing seat (641) is positioned at the joint of the head and the tail of the plurality of opening mechanisms (65).
5. The fluoride reaction kettle temperature control system and device according to claim 4, wherein the temperature regulator (3) comprises a housing and a heat medium and a cold medium arranged in the housing, and the heat medium and the cold medium are respectively conveyed by a first conveying pump and a second conveying pump.
6. The fluoride reaction kettle temperature control system and device according to claim 5, wherein two liquid inlet pipes (23) are arranged on one side of the lower portion of the reaction kettle body (2), the two liquid inlet pipes (23) are respectively communicated with the output ends of the first delivery pump and the second delivery pump, two hot and cold liquid outlet pipes (25) are arranged on one side of the upper portion of the reaction kettle body (2), the two hot and cold liquid outlet pipes (25) are respectively communicated with the hot medium and the cold medium, two hot and cold coils (26) are arranged in the reaction kettle body (2), and the two hot and cold coils (26) are respectively communicated with the two hot and cold liquid outlet pipes (25).
7. The fluoride reaction kettle temperature control system and the temperature control device according to claim 6, wherein a trigger mechanism (66) for opening the first delivery pump or the second delivery pump is provided at one side of the opening mechanism (65), the trigger mechanism (66) comprises a connecting plate (661) rotatably provided on the surface of the slide cylinder (651), a push rod (662) provided at one side of the connecting plate (661), a movable contact mounting plate (663) eccentrically provided on the surface of the push rod (662), and a fixed contact mounting plate (664) provided at the top of the movable contact mounting plate (663), the movable contact mounting plate (663) and the fixed contact mounting plate (664) are both slidably connected with a guide rod (665), the guide rod (665) is installed in the inner wall of the cylindrical seal box (62), a second return spring is provided between the top of the fixed contact mounting plate (664) and the inner wall of the cylindrical seal box (62), the second return spring is sleeved on the surface of the guide rod (665).
8. The fluoride reaction kettle temperature control system and device according to claim 7, wherein a plurality of adjustable timers (67) are arranged on the surface of the cylindrical sealing box (62), the timers (67) and the opening mechanisms (65) are arranged in a one-to-one correspondence manner, a starting button (671) is arranged on the lower portion of each timer (67), and the upper portion of the ejector rod (662) penetrates through the inner wall of the cylindrical sealing box (62) to be in contact with the starting button (671).
9. The fluoride reaction kettle temperature control system and device according to claim 7, wherein a rotating shaft (21) is rotatably arranged in the reaction kettle body (2), a plurality of stirring paddles (22) are arranged on the surface of the rotating shaft (21), the rotating shaft (21) is driven by a second motor, and a discharge opening is formed in the bottom of the reaction kettle body (2);
the inner wall of the reaction kettle body (2) is sequentially provided with a heat insulation layer (29), a placing cavity and a heat conduction layer (28) from outside to inside, and the placing cavity is used for placing the coiled pipe (26).
10. The fluoride reaction kettle temperature control system and device according to claim 9, wherein a plurality of temperature sensors (27) are arranged on the inner wall of the reaction kettle body (2) from bottom to top, the temperature sensors (27) and the output end of the counter are electrically connected with the input end of a processor, the processor is electrically connected with a display screen and a keyboard, the output end of the processor is electrically connected with the input end of a relay, and the output end of the relay is electrically connected with the first delivery pump, the first motor of the second delivery pump and a buzzer;
the processor and the relay are embedded inside the control panel, the buzzer, the display screen and the keyboard are embedded on the surface of the control panel, and the control panel is installed on the front surface of the shell.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210642170.4A CN114950302A (en) | 2022-06-08 | 2022-06-08 | Fluoride reation kettle temperature control system and temperature control device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210642170.4A CN114950302A (en) | 2022-06-08 | 2022-06-08 | Fluoride reation kettle temperature control system and temperature control device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114950302A true CN114950302A (en) | 2022-08-30 |
Family
ID=82961119
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210642170.4A Pending CN114950302A (en) | 2022-06-08 | 2022-06-08 | Fluoride reation kettle temperature control system and temperature control device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114950302A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116212770A (en) * | 2023-03-13 | 2023-06-06 | 南通太洋高新材料科技有限公司 | Fluoride reation kettle temperature control system and temperature control device |
| CN116826349A (en) * | 2023-08-25 | 2023-09-29 | 中天（江苏）防务装备有限公司 | Ship radar cover ring control liquid cooling source unit |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB767280A (en) * | 1953-10-27 | 1957-01-30 | Standard Toch Chemicals Inc | Liquid dispensing apparatus |
| CN209490820U (en) * | 2018-12-25 | 2019-10-15 | 博爱新开源医疗科技集团股份有限公司 | A kind of high-temperature high-pressure reaction kettle making N- caprolactam |
| CN113274947A (en) * | 2021-05-07 | 2021-08-20 | 浙江德欧化工制造有限公司 | Continuous automatic feeding device for disperse red 3B production bromination |
| CN214553373U (en) * | 2021-04-14 | 2021-11-02 | 抚州市鹤达实业有限公司 | Modified starch processing is with regularly feeding device |
| CN215353442U (en) * | 2021-08-07 | 2021-12-31 | 黑龙江常江化工有限公司 | Reaction kettle with temperature control capability for neutralization in oxadiazine production |
| CN215743310U (en) * | 2021-08-26 | 2022-02-08 | 西谱森新材料(上海)有限公司 | Dispersant processing's processing jar that can adjust carousel rotational speed to control feeding volume |
| CN216024737U (en) * | 2021-08-03 | 2022-03-15 | 四川凯科医药科技有限公司 | Reactor is feeding device regularly |
-
2022
- 2022-06-08 CN CN202210642170.4A patent/CN114950302A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB767280A (en) * | 1953-10-27 | 1957-01-30 | Standard Toch Chemicals Inc | Liquid dispensing apparatus |
| CN209490820U (en) * | 2018-12-25 | 2019-10-15 | 博爱新开源医疗科技集团股份有限公司 | A kind of high-temperature high-pressure reaction kettle making N- caprolactam |
| CN214553373U (en) * | 2021-04-14 | 2021-11-02 | 抚州市鹤达实业有限公司 | Modified starch processing is with regularly feeding device |
| CN113274947A (en) * | 2021-05-07 | 2021-08-20 | 浙江德欧化工制造有限公司 | Continuous automatic feeding device for disperse red 3B production bromination |
| CN216024737U (en) * | 2021-08-03 | 2022-03-15 | 四川凯科医药科技有限公司 | Reactor is feeding device regularly |
| CN215353442U (en) * | 2021-08-07 | 2021-12-31 | 黑龙江常江化工有限公司 | Reaction kettle with temperature control capability for neutralization in oxadiazine production |
| CN215743310U (en) * | 2021-08-26 | 2022-02-08 | 西谱森新材料(上海)有限公司 | Dispersant processing's processing jar that can adjust carousel rotational speed to control feeding volume |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116212770A (en) * | 2023-03-13 | 2023-06-06 | 南通太洋高新材料科技有限公司 | Fluoride reation kettle temperature control system and temperature control device |
| CN116212770B (en) * | 2023-03-13 | 2023-10-27 | 南通太洋高新材料科技有限公司 | Fluoride reation kettle temperature control system and temperature control device |
| CN116826349A (en) * | 2023-08-25 | 2023-09-29 | 中天（江苏）防务装备有限公司 | Ship radar cover ring control liquid cooling source unit |
| CN116826349B (en) * | 2023-08-25 | 2023-11-10 | 中天（江苏）防务装备有限公司 | Ship radar cover ring control liquid cooling source unit |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN114950302A (en) | Fluoride reation kettle temperature control system and temperature control device | |
| CN114028973A (en) | Accurate controlling means of dose is administered in experiment | |
| CN212904949U (en) | Sample feeding detection device for reagent or chemical product | |
| CN111498774B (en) | Filling closing device is used in sirup preparation | |
| CN215602912U (en) | Full-automatic cake stuffing machine | |
| CN211329391U (en) | Biological method outer half-pipe type acrylamide polymerization kettle | |
| US3071907A (en) | Method and apparatus for the production of tetrahedron-shaped packages | |
| CN210814854U (en) | Soap liquid preparation device | |
| CN213467591U (en) | Hospital pharmacy pharmacology analysis experimental apparatus | |
| CN216235993U (en) | Making wine production is with quantitative filling device | |
| CN214233961U (en) | Automatic dosing control device for reaction kettle | |
| CN216415103U (en) | Water and fertilizer integrated sensing device | |
| CN110327815A (en) | A kind of soap lye dispenser | |
| CN210044879U (en) | Centrifugal scraper type film evaporator | |
| CN208742567U (en) | A kind of drug response kettle with sampling Detection function | |
| CN216735295U (en) | Portable intelligent temperature control box for laboratory animal sample storage | |
| CN216856326U (en) | Medicine dissolving device for pharmaceutical analysis | |
| CN217745779U (en) | Fluoroethylene carbonate rectifying tower | |
| CN113624928B (en) | Building material gas emission quality detection device | |
| CN220201805U (en) | Emulsion explosive sensitization machine | |
| CN217674586U (en) | Storage device for circulating heating accelerator | |
| CN116422255B (en) | Ammonia water preparation all-in-one | |
| CN213102175U (en) | Atorvastatin calcium mother nucleus reaction kettle with heating and heat preservation functions | |
| CN212882444U (en) | Device is taken to ration in tetrahydrofuran reaction process | |
| CN213219317U (en) | Feeder is used in hemiplegia patient's nursing |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |