CN114931852B - Carbon dioxide purifying and separating equipment and method - Google Patents
Carbon dioxide purifying and separating equipment and method Download PDFInfo
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- CN114931852B CN114931852B CN202210434916.2A CN202210434916A CN114931852B CN 114931852 B CN114931852 B CN 114931852B CN 202210434916 A CN202210434916 A CN 202210434916A CN 114931852 B CN114931852 B CN 114931852B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/77—Liquid phase processes
- B01D53/78—Liquid phase processes with gas-liquid contact
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2256/00—Main component in the product gas stream after treatment
- B01D2256/22—Carbon dioxide
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/151—Reduction of greenhouse gas [GHG] emissions, e.g. CO2
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Abstract
The invention discloses a carbon dioxide purifying and separating device and a method, and belongs to the field of carbon dioxide preparation. A carbon dioxide purifying and separating device comprises a purifying box body, a reaction cup, a stirring rod, a sliding guide cavity and a reaction quantity control device; the guide sliding cavity is arranged at the top end of the purifying box body, the opening of the guide sliding cavity is upward, and the reaction cup is arranged in the purifying box body in a sliding manner; the reaction cup is used for placing fluid to be reacted, the bottom end of the reaction cup is provided with a measuring component, and the measuring component is used for measuring the weight of the fluid placed in the reaction cup; the reaction quantity control device is arranged in the slide guiding cavity and comprises a liquid calculating element and a gas measuring element, and the liquid calculating element and the gas measuring element are electrically connected with the measuring component; the liquid calculating element and the gas measuring element are arranged in the scheme, and the liquid calculating element and the gas measuring element are arranged in the gas-liquid measuring cup, so that the gas-liquid measuring cup can measure the volume of gas and the weight and volume of liquid.
Description
Technical Field
The invention belongs to the field of carbon dioxide preparation, and particularly relates to carbon dioxide purification and separation equipment and a method.
Background
Carbon dioxide is generally produced by calcining limestone at high temperature or by reacting limestone with dilute hydrochloric acid, and is mainly used for refrigerating perishable foods, as a refrigerant, for producing carbonated soft drinks, as a solvent for homogeneous reactions, and the like. Regarding its toxicity, studies indicate that: the low concentration of carbon dioxide is not toxic.
The existing carbon dioxide preparation equipment generally adopts a traditional method to measure the reaction liquid and the liquid to be reacted independently, then performs fusion stirring and purification, calculates the quantity of the reaction liquid and the quantity of the liquid to be reacted, has complicated and complex whole process, is easy to make mistakes, and is difficult to improve the purification efficiency, so that the carbon dioxide purification and separation equipment which is convenient to use, quick to operate and difficult to make mistakes is required.
Disclosure of Invention
The invention aims to solve the technical problem of providing a carbon dioxide purifying and separating device and a carbon dioxide purifying and separating method, wherein a liquid calculating element and a gas measuring element are arranged, the liquid calculating element and the gas measuring element are both arranged in a gas-liquid measuring cup, the gas-liquid measuring cup can measure the volume of gas and the weight and volume of liquid, and a weight sensor, an electromagnetic valve and a stirring motor are electrically connected, and the electromagnetic valve and the stirring motor can be opened and closed through the weight sensor.
The invention relates to a carbon dioxide purifying and separating device which comprises a purifying box body, a reaction cup, a stirring rod, a sliding guide cavity and a reaction quantity control device, wherein the stirring rod is arranged on the purifying box body;
the guide sliding cavity is arranged at the top end of the purifying box body, the opening of the guide sliding cavity is upward, and the reaction cup is arranged in the purifying box body in a sliding manner; the reaction cup is used for placing fluid to be reacted, the bottom end of the reaction cup is provided with a measuring component, and the measuring component is used for measuring the weight of the fluid placed in the reaction cup;
the reaction quantity control device is arranged in the slide guiding cavity and comprises a liquid calculating element and a gas measuring element, the liquid calculating element and the gas measuring element are electrically connected with the measuring part, a space for containing reaction fluid is arranged in the liquid calculating element, the liquid calculating element is used for calculating the weight of the reaction fluid, the space of the liquid calculating element is arranged on the upper side of the reaction cup, a sealing part is arranged in the liquid calculating element, and the sealing part is used for switching the communication state between the fluid and the reaction cup; the gas measuring element is used for measuring the volume of gas and is arranged in a hidden way;
the purifying box body top is equipped with the inlet, and the inlet is located the one side of leading smooth chamber, and the puddler rotates to locate in the reaction cup, and the puddler rotates round the center pin of reaction cup, and one side of reaction cup is equipped with discharge pipeline.
As a further improvement of the invention, the liquid calculating element comprises a gas-liquid measuring cup, the gas-liquid measuring cup is connected with the inner circular surface of the sliding guide cavity in an up-down sliding way, a measuring cavity with an upward opening is arranged in the gas-liquid measuring cup, the measuring cavity is used for containing fluid, a communicating pipe is fixedly arranged at the bottom end of the gas-liquid measuring cup, an electromagnetic valve cavity which is vertically communicated is arranged in the communicating pipe, the top end of the electromagnetic valve cavity is communicated with the measuring cavity, an electromagnetic valve is fixedly arranged on the inner wall of the electromagnetic valve cavity and used for sealing or communicating the electromagnetic valve cavity, a weight sensor is fixedly arranged on the lower wall of the sliding guide cavity, a measuring spring is fixedly arranged at the top end of the weight sensor, and the top end of the measuring spring is fixedly connected with the bottom end of the gas-liquid measuring cup.
As a further improvement of the invention, the lower side of the sliding guide cavity is communicated with a connecting cavity, the bottom end of the communicating pipe extends into the connecting cavity, the communicating pipe is in sliding connection with the connecting cavity, a sliding cavity is arranged in the purifying box body, and the sliding cavity is positioned at the lower side of the connecting cavity.
As a further improvement of the invention, the gas measuring element comprises an air inlet pipe, the top end of the air inlet pipe extends upwards to the upper side of the gas-liquid measuring cup, the bottom end of the air inlet pipe extends downwards to be communicated with the lower wall of the measuring cavity, a pipeline connecting port is fixedly arranged at the top end of the air inlet pipe, a sealing valve is arranged in the pipeline connecting port and controls the communication and the sealing of the pipeline connecting port, the top end of the air inlet pipe is an air inlet end, the bottom end of the air inlet pipe is an air outlet end, a scale gauge is fixedly arranged on the side wall of the measuring cavity, a measuring plate is arranged on the inner wall of the measuring cavity in a sliding mode, the bottom end of the measuring plate is attached to the lower wall of the measuring cavity, a switching cavity which is vertically communicated is arranged in the measuring plate, and the top end of the measuring plate is hinged with a hinged plate.
As a further improvement of the invention, the liquid inlet comprises a feeding hole, the bottom end of the feeding hole is communicated with a feeding cavity, the lower side of the feeding cavity is communicated with a sliding cavity, the inner wall of the feeding cavity is connected with a sealing plate in a left-right sliding manner, the right end of the sealing plate extends to the outer side of the purifying box body, and the sealing plate is used for communicating or sealing the feeding cavity.
As a further improvement of the invention, the upper wall of the sliding cavity is fixedly provided with a stirring motor, the output shaft at the bottom end of the stirring motor is fixedly provided with a connecting plate, the output shaft of the stirring motor is coaxial with the central shaft of the reaction cup, the reaction cup is internally provided with a reaction cavity, the opening of the reaction cavity is upward, the stirring rod is positioned in the reaction cavity and rotates, and the stirring rod is fixedly arranged at the bottom end of the connecting plate.
As a further improvement of the invention, the bottom end of the sliding cavity is fixedly provided with a weight measuring device, the top end of the weight measuring device is fixedly provided with a connecting spring, the top end of the connecting spring is fixedly connected with the bottom end of the reaction cup, and the weight measuring device is electrically connected with the weight sensor.
As a further improvement of the invention, the outer circular surface of the reaction cup is fixedly provided with a top side guide pipe, the top side guide pipe extends to the outer side of the purification box body, an abdication cavity is arranged in the purification box body, the top side guide pipe is in sliding connection with the abdication cavity, the top side guide pipe is communicated with the reaction cavity, the bottom end of the reaction cup is fixedly provided with a bottom side guide pipe, the bottom side guide pipe extends to the outer side of the purification box body, the bottom side guide pipe is communicated with the reaction cavity, and one ends of the top side guide pipe and the bottom side guide pipe, which are positioned outside the purification box body, are connected with an external suction device.
As a further improvement of the invention, the weight sensor is electrically connected with the electromagnetic valve, the electromagnetic valve is electrically connected with the stirring motor, and the weight measuring device, the stirring motor and the electromagnetic valve are all connected with an external electrical control system.
The carbon dioxide purifying and separating method is used based on carbon dioxide purifying and separating equipment and comprises the following steps:
s1: pouring the liquid to be reacted into the reaction cavity, and measuring the weight of the liquid through the measuring component;
s2: pouring the reaction gas/liquid into the measuring cavity, calculating the volume/weight required by the reaction gas/liquid, opening the electromagnetic valve after the volume/weight is proper, and allowing the reaction gas/liquid to flow into the reaction cavity to react with the liquid to be reacted;
s3, after the electromagnetic valve is opened, the stirring motor is automatically started, and the stirring rod automatically rotates in the reaction cavity for stirring;
and S4, after the reaction and purification, the purified gas or liquid is led out through a bottom side conduit or a top side conduit.
Compared with the prior art, the invention has the advantages that:
(1) This scheme has set up liquid calculation element and gas measurement element, and liquid calculation element and gas measurement element all locate in the gas-liquid measuring cup, and the gas-liquid measuring cup can measure the volume of gas and the weight and the volume of liquid to weight sensor, solenoid valve and agitator motor all pass through electric connection, can open and close solenoid valve and agitator motor through weight sensor.
(2) This scheme has set up and has been equipped with weight induction system at gas-liquid measurement cup bottom side, can measure the liquid weight in the gas-liquid measurement cup through weight induction system to set up the solenoid valve and as sealing device, open the solenoid valve after the weight measurement and can flow liquid downwardly to the reaction cup in.
(3) This scheme is with the top setting of admission line in gas-liquid measurement cup topside to around admission line bottom to gas-liquid measurement cup bottom side, and placed the measurement board, the measurement board can not influence the measurement of liquid, and the measurement board can upwards move and form sealed space when gas measurement, and measure through the scale.
(4) The utility model discloses a sliding is equipped with the closing plate in the feed chamber, and then can seal or communicate the feed chamber by hand, has practiced thrift the cost.
(5) This scheme has set up the puddler of autogiration stirring, has promoted the convenience of use.
Drawings
FIG. 1 is a schematic view of a three-dimensional full section of the present invention;
FIG. 2 is a schematic diagram of the overall structure of the present invention;
FIG. 3 is an enlarged schematic view of the structure of FIG. 2A;
fig. 4 is a flow chart of the present invention.
The reference numerals in the figures illustrate:
11. purifying the box body; 12. a sliding chamber; 13. a reaction cup; 14. a reaction chamber; 15. a weight measuring device; 16. a connecting spring; 17. a bottom side conduit; 18. a topside conduit; 19. a relief cavity; 20. a stirring rod; 21. a connecting plate; 22. a stirring motor; 23. a feed chamber; 24. a closing plate; 25. a feed inlet; 26. a gas-liquid measuring cup; 27. a measurement cavity; 28. a communicating pipe; 29. an electromagnetic valve cavity; 30. a slide guiding cavity; 31. a weight sensor; 32. measuring a spring; 33. an electromagnetic valve; 34. an air inlet pipe; 35. a pipe connection port; 36. a measuring plate; 37. a hinged plate; 38. a switching cavity; 39. a scale; 40. and a connecting cavity.
Detailed Description
First embodiment: referring to fig. 1-4, a carbon dioxide purifying and separating apparatus includes a purifying box 11, a reaction cup 13, a stirring rod 20, a slide guiding cavity 30 and a reaction amount control device;
the slide guiding cavity 30 is arranged at the top end of the purifying box 11, the opening of the slide guiding cavity 30 is upward, and the reaction cup 13 is arranged in the purifying box 11 in a sliding manner; the reaction cup 13 is used for placing fluid to be reacted, the bottom end of the reaction cup 13 is provided with a measuring component, and the measuring component is used for measuring the weight of the fluid placed in the reaction cup 13;
the reaction quantity control device is arranged in the slide guiding cavity 30 and comprises a liquid calculating element and a gas measuring element, wherein the liquid calculating element and the gas measuring element are electrically connected with the measuring part, a space for containing reaction fluid is arranged in the liquid calculating element, the liquid calculating element is used for calculating the weight of the reaction fluid, the space of the liquid calculating element is arranged on the upper side of the reaction cup 13, a sealing part is arranged in the liquid calculating element, and the sealing part is used for switching the communication state between the fluid and the reaction cup 13; the gas measuring element is used for measuring the volume of gas and is arranged in a hidden way;
the top of the purifying box 11 is provided with a liquid inlet which is positioned at one side of the slide guiding cavity 30, the stirring rod 20 is rotationally arranged in the reaction cup 13, the stirring rod 20 rotates around the central shaft of the reaction cup 13, and one side of the reaction cup 13 is provided with a discharge pipeline.
The liquid calculating element comprises a gas-liquid measuring cup 26, the gas-liquid measuring cup 26 is connected with the inner circular surface of a slide guiding cavity 30 in an up-down sliding mode, a measuring cavity 27 with an upward opening is arranged in the gas-liquid measuring cup 26, the measuring cavity 27 is used for containing fluid, a communicating pipe 28 is fixedly arranged at the bottom end of the gas-liquid measuring cup 26, an electromagnetic valve cavity 29 which is vertically communicated is arranged in the communicating pipe 28, the top end of the electromagnetic valve cavity 29 is communicated with the measuring cavity 27, an electromagnetic valve 33 is fixedly arranged on the inner wall of the electromagnetic valve cavity 29, the electromagnetic valve 33 is used for sealing or communicating the electromagnetic valve cavity 29, a weight sensor 31 is fixedly arranged on the lower wall of the slide guiding cavity 30, a measuring spring 32 is fixedly arranged at the top end of the weight sensor 31, and the top end of the measuring spring 32 is fixedly connected with the bottom end of the gas-liquid measuring cup 26.
The lower side of the guide sliding cavity 30 is communicated with a connecting cavity 40, the bottom end of the communicating pipe 28 extends into the connecting cavity 40, the communicating pipe 28 is in sliding connection with the connecting cavity 40, a sliding cavity 12 is arranged in the purifying box 11, and the sliding cavity 12 is positioned at the lower side of the connecting cavity 40.
The feed inlet includes feed inlet 25, and feed inlet 25 bottom intercommunication is equipped with feed chamber 23, feed chamber 23 downside and slip chamber 12 intercommunication, and feed chamber 23 inner wall side-to-side sliding connection has closure plate 24, and the right-hand member of closure plate 24 extends to purification box 11 outside, and closure plate 24 is used for with feed chamber 23 intercommunication or seal.
The upper wall of the sliding cavity 12 is fixedly provided with a stirring motor 22, an output shaft at the bottom end of the stirring motor 22 is fixedly provided with a connecting plate 21, the output shaft of the stirring motor 22 is coaxial with the central shaft of the reaction cup 13, the reaction cup 13 is internally provided with a reaction cavity 14, the opening of the reaction cavity 14 is upward, a stirring rod 20 is positioned in the reaction cavity 14 for rotation, and the stirring rod 20 is fixedly arranged at the bottom end of the connecting plate 21.
The bottom end of the sliding cavity 12 is fixedly provided with a weight measuring device 15, the top end of the weight measuring device 15 is fixedly provided with a connecting spring 16, the top end of the connecting spring 16 is fixedly connected with the bottom end of the reaction cup 13, and the weight measuring device 15 is electrically connected with a weight sensor 31.
The reaction cup 13 outer disc is fixed to be equipped with topside pipe 18, topside pipe 18 extends to purification box 11 outside, be equipped with the chamber of stepping down 19 in the purification box 11, topside pipe 18 and the chamber of stepping down 19 sliding connection, topside pipe 18 and reaction chamber 14 intercommunication, reaction cup 13 bottom end mounting is equipped with bottom side pipe 17, bottom side pipe 17 extends to the purification box 11 outside, bottom side pipe 17 and reaction chamber 14 intercommunication, the one end that topside pipe 18 and bottom side pipe 17 are located the purification box 11 outside is all connected with external suction device, bottom side pipe 17 is used for sucking the liquid in the reaction chamber 14, topside pipe 18 is used for sucking the gas in the reaction chamber 14.
The weight sensor 31 is electrically connected with the electromagnetic valve 33, the electromagnetic valve 33 can be automatically opened or manually opened, the weight sensor 31 controls the opening and closing of the electromagnetic valve 33 through the electrical connection, the electromagnetic valve 33 is electrically connected with the stirring motor 22, and the weight measuring device 15, the stirring motor 22 and the electromagnetic valve 33 are all connected with an external electrical control system.
The carbon dioxide purifying and separating method is used based on carbon dioxide purifying and separating equipment and comprises the following steps:
s1: pouring the liquid to be reacted into the reaction cavity, and measuring the weight of the liquid through the measuring component;
s2: pouring the reaction gas/liquid into the measuring cavity, calculating the volume/weight required by the reaction gas/liquid, opening the electromagnetic valve after the volume/weight is proper, and allowing the reaction gas/liquid to flow into the reaction cavity to react with the liquid to be reacted;
s3, after the electromagnetic valve is opened, the stirring motor is automatically started, and the stirring rod automatically rotates in the reaction cavity for stirring;
and S4, after the reaction and purification, the purified gas or liquid is led out through a bottom side conduit or a top side conduit.
The liquid to be reacted is poured into the feed inlet 25, the closing plate 24 is pulled out manually to enable the feed cavity 23 to be communicated, the liquid in the feed inlet 25 flows into the reaction cavity 14 through the feed cavity 23, the reaction cavity 14 is driven by weight to be compressed by the connecting spring 16, the weight of the reaction cavity 14 is sensed through the weight measuring device 15, the reaction liquid is poured into the measuring cavity 27 at the moment, the hinge plate 37 is in an open state, the switching cavity 38 is in a communicating state, the gas-liquid measuring cup 26 is driven by weight to be compressed by the measuring spring 32, the weight of the reaction liquid in the gas-liquid measuring cup 26 is calculated through the weight sensor 31, meanwhile, the weight of the required reaction liquid is calculated according to the weight of the liquid to be reacted, a threshold value is set for the electromagnetic valve 33, after the weight in the gas-liquid measuring cup 26 reaches the set threshold value, the electromagnetic valve 33 is opened automatically, the reaction liquid in the gas-liquid measuring cup 26 flows downwards into the reaction cavity 14 through the electromagnetic valve cavity 29 to be fused with the liquid to be reacted, the electromagnetic valve 33 is opened, the stirring motor 22 is started automatically, the output shaft is driven to rotate, the connecting plate 21 is driven to rotate through the rotation of the output shaft, the stirring rod 20 is driven to rotate at the bottom of the reaction cavity 14 or the carbon dioxide is purified, the carbon dioxide is guided out of the reaction liquid is purified through the guide tube 14, and the carbon dioxide is purified, the reaction liquid is purified from the side of the reaction cavity is purified through the reaction cavity 14, and the side is purified through the guide tube, and the reaction liquid is purified through the side of the reaction cavity 17.
Specific embodiment II: on the basis of the first embodiment, a carbon dioxide purifying and separating device is provided, the gas measuring element comprises an air inlet pipe 34, the top end of the air inlet pipe 34 extends upwards to the upper side of a gas-liquid measuring cup 26, the bottom end of the air inlet pipe 34 extends downwards to be communicated with the lower wall of a measuring cavity 27, a pipeline connecting port 35 is fixedly arranged at the top end of the air inlet pipe 34, a sealing valve is arranged in the pipeline connecting port 35 and used for controlling the communication and closing of the air inlet pipe 34, the top end of the air inlet pipe 34 is an air inlet end, the bottom end of the air inlet pipe 34 is an air outlet end, a scale 39 is fixedly arranged on the side wall of the measuring cavity 27, a measuring plate 36 is arranged on the inner wall of the measuring cavity 27 in a sliding mode up and down, the measuring plate 36 is in piston connection with the inner wall of the measuring cavity 27, a switching cavity 38 which is vertically communicated is arranged in the measuring plate 36, a hinged plate 37 is hinged to the top end of the switching cavity 38.
When the reactant is gas, the gas is filled into the gas inlet pipe 34 through the pipe connecting port 35 and is filled into the measuring cavity 27 from the bottom side of the measuring cavity 27, at the moment, the hinged plate 37 is in a closed state, the switching cavity 38 is in a closed state, and then the measuring plate 36 is pushed to slide upwards, at the moment, the position of the measuring plate 36 in the measuring cavity 27 is observed through scales on the scale table 39, so that the volume of the gas in the measuring cavity 27 is obtained, when the volume of the reaction gas is enough, the electromagnetic valve 33 is manually opened, at the moment, the gas in the measuring cavity 27 is pushed to flow downwards into the reaction cavity 14 through the weight of the measuring plate 36, and the reaction gas and the liquid to be reacted are reacted and purified through stirring of the stirring rod 20, after the purification is finished, the purified carbon dioxide liquid in the reaction cavity 14 is led out through the bottom side conduit 17, or the purified carbon dioxide gas in the reaction cavity 14 is led out through the top side conduit 18.
Claims (8)
1. The utility model provides a carbon dioxide purification separation equipment which characterized in that: comprises a purifying box body (11), a reaction cup (13), a stirring rod (20), a slide guiding cavity (30) and a reaction quantity control device;
the guide sliding cavity (30) is arranged at the top end of the purifying box body (11), the opening of the guide sliding cavity (30) is upward, and the reaction cup (13) is arranged in the purifying box body (11) in a sliding manner; the reaction cup (13) is used for placing fluid to be reacted, the bottom end of the reaction cup (13) is provided with a measuring component, and the measuring component is used for measuring the weight of the fluid placed in the reaction cup (13);
the reaction quantity control device is arranged in the slide guiding cavity (30), and comprises a liquid calculating element and a gas measuring element, wherein the liquid calculating element and the gas measuring element are electrically connected with the measuring part, a space for containing reaction fluid is arranged in the liquid calculating element, the liquid calculating element is used for calculating the weight of the reaction fluid, the space of the liquid calculating element is arranged on the upper side of the reaction cup (13), and a sealing part is arranged in the liquid calculating element and is used for switching the communication state between the fluid and the reaction cup (13); the gas measuring element is used for measuring the volume of gas and is arranged in a hidden way;
the top end of the purifying box body (11) is provided with a liquid inlet, the liquid inlet is positioned at one side of the slide guiding cavity (30), the stirring rod (20) is rotationally arranged in the reaction cup (13), the stirring rod (20) rotates around the central shaft of the reaction cup (13), and one side of the reaction cup (13) is provided with a discharge pipeline;
the liquid calculating element comprises a gas-liquid measuring cup (26), the gas-liquid measuring cup (26) is connected with the inner circular surface of the sliding guide cavity (30) in an up-down sliding mode, a measuring cavity (27) with an upward opening is arranged in the gas-liquid measuring cup (26), the measuring cavity (27) is used for containing fluid, a communicating pipe (28) is fixedly arranged at the bottom end of the gas-liquid measuring cup (26), an electromagnetic valve cavity (29) which is vertically communicated is arranged in the communicating pipe (28), the top end of the electromagnetic valve cavity (29) is communicated with the measuring cavity (27), an electromagnetic valve (33) is fixedly arranged on the inner wall of the electromagnetic valve cavity (29), the electromagnetic valve (33) is used for sealing or communicating the electromagnetic valve cavity (29), a weight sensor (31) is fixedly arranged on the lower wall of the sliding guide cavity (30), a measuring spring (32) is fixedly arranged at the top end of the weight sensor (31), and the top end of the measuring spring (32) is fixedly connected with the bottom end of the gas-liquid measuring cup (26);
the gas measurement element includes intake pipe (34), the top of intake pipe (34) upwards extends to gas-liquid measurement cup (26) upside, the bottom downwardly extending of intake pipe (34) reaches and measures chamber (27) lower wall intercommunication, be equipped with pipeline connector (35) on intake pipe (34) top is fixed, be equipped with the sealing valve in pipeline connector (35), the intercommunication and the closure of sealing valve control pipeline connector (35), intake pipe (34) top is the inlet end, intake pipe (34) bottom is the end of giving vent to anger, it is equipped with scale (39) to measure chamber (27) lateral wall is fixed, it is equipped with measuring board (36) to slide from top to bottom to measure chamber (27) inner wall, measuring board (36) bottom and measuring chamber (27) lower wall laminating, be equipped with switching chamber (38) that link up from top to bottom in measuring board (36), measuring board (36) top articulates there is hinged joint board (37).
2. The carbon dioxide purifying and separating apparatus of claim 1, wherein: the lower side of the guide sliding cavity (30) is communicated with a connecting cavity (40), the bottom end of the communicating pipe (28) extends into the connecting cavity (40), the communicating pipe (28) is in sliding connection with the connecting cavity (40), a sliding cavity (12) is arranged in the purifying box body (11), and the sliding cavity (12) is located at the lower side of the connecting cavity (40).
3. The carbon dioxide purifying and separating apparatus of claim 1, wherein: the feed liquor mouth includes feed inlet (25), and feed inlet (25) bottom intercommunication is equipped with feed chamber (23), feed chamber (23) downside and slip chamber (12) intercommunication, and sliding connection has closure plate (24) about feed chamber (23) inner wall, and the right-hand member of closure plate (24) extends to purification box (11) outside, and closure plate (24) are used for with feed chamber (23) intercommunication or seal.
4. The carbon dioxide purifying and separating apparatus of claim 1, wherein: the upper wall of the sliding cavity (12) is fixedly provided with a stirring motor (22), an output shaft at the bottom end of the stirring motor (22) is fixedly provided with a connecting plate (21), the output shaft of the stirring motor (22) is coaxial with the central shaft of the reaction cup (13), a reaction cavity (14) is arranged in the reaction cup (13), an opening of the reaction cavity (14) is upward, a stirring rod (20) is positioned in the reaction cavity (14) and rotates, and the stirring rod (20) is fixedly arranged at the bottom end of the connecting plate (21).
5. The carbon dioxide purifying and separating apparatus of claim 1, wherein: the bottom end of the sliding cavity (12) is fixedly provided with a weight measuring device (15), the top end of the weight measuring device (15) is fixedly provided with a connecting spring (16), the top end of the connecting spring (16) is fixedly connected with the bottom end of the reaction cup (13), and the weight measuring device (15) is electrically connected with a weight sensor (31).
6. The carbon dioxide purifying and separating apparatus of claim 1, wherein: the reaction cup (13) outer disc is fixed to be equipped with topside pipe (18), topside pipe (18) extend to purification box (11) outside, be equipped with in the purification box (11) and give way chamber (19), topside pipe (18) and chamber (19) sliding connection give way, topside pipe (18) and reaction chamber (14) intercommunication, reaction cup (13) bottom mounting is equipped with downside pipe (17), underside pipe (17) extend to purification box (11) outside, underside pipe (17) and reaction chamber (14) intercommunication, one end that topside pipe (18) and underside pipe (17) are located outside purification box (11) all is connected with external suction device.
7. The carbon dioxide purifying and separating apparatus of claim 1, wherein: the weight sensor (31) is electrically connected with the electromagnetic valve (33), the electromagnetic valve (33) is electrically connected with the stirring motor (22), and the weight measuring device (15), the stirring motor (22) and the electromagnetic valve (33) are all connected with an external electrical control system.
8. A carbon dioxide purification and separation method, based on the use of a carbon dioxide purification and separation apparatus according to any one of claims 1 to 7, comprising the steps of:
s1: pouring the liquid to be reacted into the reaction cavity, and measuring the weight of the liquid through the measuring component;
s2: pouring the reaction gas/liquid into the measuring cavity, calculating the volume/weight required by the reaction gas/liquid, opening the electromagnetic valve after the volume/weight is proper, and allowing the reaction gas/liquid to flow into the reaction cavity to react with the liquid to be reacted;
s3, after the electromagnetic valve is opened, the stirring motor is automatically started, and the stirring rod automatically rotates in the reaction cavity for stirring;
and S4, after the reaction and purification, the purified gas or liquid is led out through a bottom side conduit or a top side conduit.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202210434916.2A CN114931852B (en) | 2022-04-24 | 2022-04-24 | Carbon dioxide purifying and separating equipment and method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202210434916.2A CN114931852B (en) | 2022-04-24 | 2022-04-24 | Carbon dioxide purifying and separating equipment and method |
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| CN114931852A CN114931852A (en) | 2022-08-23 |
| CN114931852B true CN114931852B (en) | 2023-09-22 |
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| CN111167396A (en) * | 2020-03-04 | 2020-05-19 | 临海永存智能技术有限公司 | Nanoscale calcium carbonate processing device |
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| JPH10267726A (en) * | 1997-03-25 | 1998-10-09 | Kett Electric Lab | Volume-weight measurement device for sample such as grain |
| CN2621692Y (en) * | 2003-05-01 | 2004-06-30 | 陆叙林 | Standless transfusion outfit |
| CN208440342U (en) * | 2018-07-04 | 2019-01-29 | 贵阳学院 | A kind of device for treating waste water with biological pollution |
| CN210833745U (en) * | 2019-11-18 | 2020-06-23 | 泰州润丽工程科技有限公司 | Measuring cylinder with weighing function |
| CN215064809U (en) * | 2021-07-22 | 2021-12-07 | 内蒙古圣圆能源集团有限责任公司 | Belt coal leakage monitoring and weighing alarm system |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111167396A (en) * | 2020-03-04 | 2020-05-19 | 临海永存智能技术有限公司 | Nanoscale calcium carbonate processing device |
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