CN114917838A - Hydrogen peroxide solution control feeding device for synthesizing DATA - Google Patents
Hydrogen peroxide solution control feeding device for synthesizing DATA Download PDFInfo
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- CN114917838A CN114917838A CN202210515185.4A CN202210515185A CN114917838A CN 114917838 A CN114917838 A CN 114917838A CN 202210515185 A CN202210515185 A CN 202210515185A CN 114917838 A CN114917838 A CN 114917838A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/80—Falling particle mixers, e.g. with repeated agitation along a vertical axis
- B01F25/90—Falling particle mixers, e.g. with repeated agitation along a vertical axis with moving or vibrating means, e.g. stirrers, for enhancing the mixing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
- B01J4/007—Feed or outlet devices as such, e.g. feeding tubes provided with moving parts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/2204—Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application
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Abstract
The invention relates to the technical field of DATA synthesis, in particular to a hydrogen peroxide control feeding device for synthesizing DATA, which comprises a fixed support frame, wherein a central fixed sleeve is vertically arranged at the center of the fixed support frame, and the hydrogen peroxide control feeding device further comprises: the central support rod is nested and slidably arranged on the inner side of the central fixing sleeve. The central support rod can drive the submerged distribution disc to be immersed under the liquid level of the materials in the reaction kettle, hydrogen peroxide can be conveyed to the submerged distribution disc to be uniformly conveyed, the central support rod drives the submerged distribution disc to move up and down, the materials pass through the rotary sleeve and drive the rotary sleeve to rotate by the spiral guide plate so as to open and close the conveying opening, so that the hydrogen peroxide can be conveyed into the reaction kettle through the conveying opening when the submerged distribution disc moves up and down, the submerged distribution disc continuously and uniformly releases the hydrogen peroxide while moving up and down so as to be fully mixed with the materials, and the reaction efficiency and the hydrogen peroxide utilization rate are favorably improved.
Description
Technical Field
The invention relates to the technical field of DATA synthesis, in particular to a hydrogen peroxide controlled feeding device for synthesizing DATA.
Background
DATA is a main intermediate of a top-grade organic pigment, namely quinacridone pigment, and the traditional domestic and foreign DATA synthesis process is generally sodium m-nitrobenzenesulfonate oxidation, but the defect of a large amount of solid byproducts exists, so a hydrogen peroxide oxidation process is usually adopted at present, the generation of the solid byproducts can be reduced, water is saved, and the cost is reduced, a hydrogen peroxide dripping mode, namely a mode of contacting with materials also influences the oxidation reaction speed, and the conventional feeding equipment usually adopts direct surface dripping, but the feeding mode and the equipment have poor oxidation effects and low hydrogen peroxide utilization rate.
The patent with the application number of CN201520836920.7 discloses an oxidation reaction kettle with a distributor, which belongs to the technical field of chemical production, wherein an elevated tank is arranged above a kettle body of the reaction kettle, the distributor is arranged in the kettle body, the elevated tank is connected with the distributor through a pipeline, an oxidant in the elevated tank can flow down and divergently contact with substances to be oxidized in the kettle body through uniformly dispersed holes on the distributor, the contact area is increased, so that the contact efficiency between the oxidant and reaction materials can be improved, and the speed and the production efficiency of the whole oxidation reaction are further improved;
but its distributor is fixed reinforced structure, can only react to the material of its surrounding certain extent when feeding in raw material, is difficult to intensive mixing between the material when reinforced, and the material concentration of different positions is different, and reaction efficiency is also different, and whole degree of mixing is lower, needs additionally to set up circulating pump structure circulation material and mixes in order to improve the reaction degree of consistency, and the mixing effect is relatively poor, leads to reacting inadequately easily, and then can lead to reaction efficiency and hydrogen peroxide solution low-usage.
Disclosure of Invention
In view of the above, the present invention aims to provide a hydrogen peroxide controlled feeding device for DATA synthesis, so as to solve the problems that in the current oxidation reaction production, an oxidant distributor is of a fixed feeding structure, only materials in a certain range around the oxidant distributor can be reacted when feeding is performed, the materials are difficult to be fully mixed when feeding is performed, the material concentrations at different positions are different, the reaction efficiency is also different, the overall mixing degree is low, a circulating pump structure needs to be additionally arranged to mix the circulating materials so as to improve the reaction uniformity, the mixing effect is poor, the reaction is easy to be insufficient, and further the reaction efficiency and the hydrogen peroxide utilization rate are low.
Based on the above purpose, the present invention provides a hydrogen peroxide solution controlled feeding device for DATA synthesis, which comprises a fixed support frame, wherein a central fixing sleeve is vertically arranged at the center of the fixed support frame, and the hydrogen peroxide solution controlled feeding device for DATA synthesis is characterized by further comprising:
the central supporting rod is nested and slidably arranged on the inner side of the central fixing sleeve;
the liquid conveying pipe is arranged at the center of the inner side of the central supporting rod, a conveying port is formed in the bottom end of the liquid conveying pipe, a central rotary joint is arranged at the top end of the liquid conveying pipe, and a liquid conveying hose is connected and arranged on the outer side of the central rotary joint;
the submerged distribution disc is arranged at the bottom end of the central support rod and is in sliding connection with the fixed support frame through the central support rod and the central fixing sleeve, a hollow storage barrel is arranged inside the submerged distribution disc, a plurality of umbrella-shaped distribution pipes are uniformly arranged on the outer side of the bottom of the hollow storage barrel in a surrounding manner, the outer ends of the umbrella-shaped distribution pipes are connected with annular distribution pipes, and the liquid material conveying pipe is communicated with the inside of the hollow storage barrel through the conveying port;
the liquid material conveying interlayer is communicated with the inside of the hollow storage barrel through the umbrella-shaped distribution pipes which are correspondingly arranged, all the liquid material conveying interlayers are communicated with each other through the annular distribution pipes, a plurality of conveying openings are formed in the inner side wall of the vertical communication sleeve and are uniformly arranged along the vertical central line direction of the vertical communication sleeve at intervals, the inside of the liquid material conveying interlayer is communicated with the inside of the vertical communication sleeve through the conveying openings, and annular rotary grooves are formed in the upper end and the lower end of the vertical communication sleeve;
the rotary sleeve is nested on the inner side of the vertical communication sleeve, the upper end and the lower end of the rotary sleeve are both provided with rotary connecting rings, the rotary sleeve is rotationally connected with the vertical communication sleeve through the rotary connecting rings and the annular rotary groove, the inner side of the rotary sleeve is provided with spiral guide plates, the spiral guide plates are spirally arranged along the vertical central line direction of the rotary sleeve, the middle of each spiral guide plate is vertically provided with a central connecting column, a plurality of release openings are arranged in the middle of the inner side wall of the rotary sleeve, the release openings are evenly arranged at intervals along the vertical central line direction of the rotary sleeve, the release openings and the conveying openings are arranged in a one-to-one correspondence manner, the outer side wall of the rotary sleeve and the inner side wall of the vertical communication sleeve are mutually attached, and the rotary sleeve drives the release openings to rotate and open the conveying openings when being mutually overlapped, the rotary sleeve drives the release opening to rotate and closes the conveying opening when the release opening and the conveying opening are mutually staggered.
In some optional embodiments, a vertical engaging groove is vertically formed in the middle of the outer side wall of the central support rod, a lifting rack is arranged on the inner side of the vertical engaging groove, a lifting gear is arranged on the outer side of the lifting rack in a meshed manner, a lifting motor is arranged at the shaft end of the lifting gear, a sliding adjusting frame is arranged on the outer side of the lifting motor, and the lifting motor is connected with the fixed support frame through the sliding adjusting frame.
In some optional embodiments, a horizontal guide rod is horizontally arranged in the middle of the fixed support frame, an adjusting sliding sleeve is arranged at the bottom of the sliding adjusting frame, the sliding adjusting frame is connected with the horizontal guide rod in a sliding mode through the adjusting sliding sleeve, a hydraulic telescopic rod is arranged on the rear side of the sliding adjusting frame, and the hydraulic telescopic rod pulls the sliding adjusting frame to horizontally slide along the horizontal guide rod through stretching.
In some optional embodiments, a horizontal sliding sleeve is symmetrically arranged on the inner side of the central fixing sleeve, a magnetic support rod is slidably arranged inside the horizontal sliding sleeve in a nested manner, an arc-shaped thread plate is arranged at the front end of the magnetic support rod, a return spring is arranged on the rear side of the magnetic support rod, and an adjusting electromagnet is arranged at the rear end of the horizontal sliding sleeve.
In some optional embodiments, the outer side surface of the central support rod is provided with a fitting thread, the arc-shaped thread plate and the fitting thread are mutually matched in size, and when the central support rod and the arc-shaped thread plate are mutually connected in a fitting manner through the fitting thread, the central support rod longitudinally slides along the central fixing sleeve and simultaneously rotates in the axial direction.
In some optional embodiments, an air conveying interlayer is further arranged on the inner side of the central support rod and is arranged between the liquid conveying pipe and the inner side of the central support rod, a communication opening is formed in the bottom end of the air conveying interlayer, an interlayer rotary joint is arranged at the top end of the air conveying interlayer, and an air conveying hose is connected and arranged on the outer side of the interlayer rotary joint.
In some optional embodiments, a pressing piston is slidably disposed inside the hollow storage cylinder in a nested manner, a sealing sliding sleeve is disposed in the center of the pressing piston, the sealing sliding sleeve is slidably disposed outside the liquid conveying pipe in a nested manner, and the communication opening is located at the top end of the hollow storage cylinder.
In some optional embodiments, an arc-shaped friction plate is arranged on the inner side of the annular rotary groove, a sealing air bag is arranged on the back surface of the arc-shaped friction plate, the sealing air bag is made of flexible materials and filled with gas, the back surface of the arc-shaped friction plate is connected with the inner side of the annular rotary groove through the sealing air bag, the inner side surface of the arc-shaped friction plate is attached to the outer side annular surface of the rotary connecting ring, and the arc-shaped friction plate is driven to move outwards to be separated from the rotary connecting ring when the sealing air bag is contracted;
the device enables materials to pass through the rotary sleeve by moving the submerged distribution disc up and down, and drives the rotary sleeve to rotate by the spiral guide plate so as to convey hydrogen peroxide, the higher the rotation speed of the rotary sleeve is, the more times of opening the release opening and the conveying opening in coincidence in unit time are, namely, the more hydrogen peroxide is released, the rotary sleeve is rotatably connected with the vertical communication sleeve by the rotary connecting ring and the annular rotary groove, the inner side surface of the arc-shaped friction plate arranged in the annular rotary groove is mutually attached to the outer side ring surface of the rotary connecting ring, the rotation speed of the rotary sleeve can be reduced by friction force, and the arc-shaped friction plate is driven to move outwards when the sealed air bag is contracted so as to be separated from the rotary connecting ring, when the submerged distribution disc is arranged at the lower part of the materials in the reaction kettle, the liquid pressure borne by the sealed air bag is higher, so that the arc-shaped friction plate can be contracted to move outwards, the friction force between the rotary connecting ring and the rotary connecting ring is reduced, so that the rotary speed of the rotary connecting ring can be faster, the quantity of the released and conveyed hydrogen peroxide is increased, and as the submerged distribution disk moves upwards, the liquid pressure on the sealed air bag can be gradually reduced, thereby gradually expanding to enable the arc-shaped friction plate to be close to the rotary connecting ring, gradually increasing the friction force between the arc-shaped friction plate and the rotary connecting ring, enabling the rotary speed of the rotary connecting ring to be slower, further gradually reducing the amount of hydrogen peroxide released and conveyed, and the concentration of the lower part of the materials in the reaction kettle is higher than that of the upper part due to gravity, therefore, the reaction amount of the hydrogen peroxide added at the lower part is higher than that at the upper part, so that through the structure of the sealing air bag and the arc-shaped friction plate, the amount of hydrogen peroxide conveyed can be automatically controlled to match the concentration of materials in the external reaction kettle, so that the reaction efficiency and the hydrogen peroxide utilization rate are improved, and the device is more flexible and convenient to use.
In some optional embodiments, a fixed magnet is disposed in the middle of the annular rotary groove, the fixed magnet and the delivery opening are disposed on the same vertical line, a positioning magnet is disposed in the middle of the rotary connection ring, the positioning magnet and the release opening are disposed on the same vertical line, and adjacent magnetic poles between the fixed magnet and the positioning magnet are the same.
In some optional embodiments, the upper side and the lower side of the submerged distribution disk are both provided with a rotary stirring disk, a central rotating frame is arranged at the center of the rotary stirring disk, the rotary stirring disk is rotatably connected with the submerged distribution disk through the central rotating frame, the axial center line of the central rotating frame and the vertical center line of the submerged distribution disk are located on the same vertical line, a plurality of inclined stirring blades are uniformly arranged on the outer side of the central rotating frame in a surrounding manner, and the inclined directions of the inclined stirring blades arranged on the outer side of the central rotating frame arranged on the upper side and the lower side of the submerged distribution disk are opposite.
From the above, the hydrogen peroxide solution controlled feeding device for the synthetic DATA provided by the invention can drive the submerged distribution disk to be immersed below the liquid level of the materials in the reaction kettle through the central support rod, the hydrogen peroxide solution can be conveyed to the submerged distribution disk to be uniformly conveyed, the submerged distribution disk is provided with a plurality of vertical communication sleeves, the submerged distribution disk can be driven to move up and down through the central support rod, the materials can pass through the submerged distribution disk through the rotary sleeves on the inner sides of the vertical communication sleeves and can be driven to rotate through the spiral guide plates in the process of passing through the rotary sleeves, the rotary sleeves can enable the release openings arranged on the rotary sleeves to be continuously overlapped and staggered with the conveying openings arranged on the vertical communication sleeves to open and close the conveying openings when rotating, so that the hydrogen peroxide solution can be conveyed into the reaction kettle through the conveying openings when the submerged distribution disk moves up and down, the submerged distribution disc continuously and uniformly releases hydrogen peroxide while moving up and down, so that the submerged distribution disc and materials are fully mixed, the overall mixing degree and the mixing effect are improved, and the reaction efficiency and the hydrogen peroxide utilization rate are improved.
Drawings
In order to more clearly illustrate the present invention or the technical solutions in the prior art, the drawings used in the embodiments or the description in the prior art will be briefly described below, it is obvious that the drawings in the following description are only the present invention, and other drawings can be obtained by those skilled in the art without inventive efforts.
FIG. 1 is a schematic diagram of the internal structure of an embodiment of the present invention;
FIG. 2 is a schematic front view of an embodiment of the present invention;
FIG. 3 is a bottom schematic view of an embodiment of the present invention;
FIG. 4 is a schematic structural view of a fixing support according to an embodiment of the present invention;
fig. 5 is a schematic structural view of a center fixing sleeve according to an embodiment of the present invention;
FIG. 6 is a schematic structural view of a submerged distribution tray according to an embodiment of the present invention;
FIG. 7 is a schematic view of the inner side of a submerged distribution tray according to an embodiment of the present invention;
FIG. 8 is a schematic view of the internal structure of the hollow storage cartridge according to the embodiment of the present invention;
FIG. 9 is an outer side schematic view of a vertical communication sleeve according to an embodiment of the present invention;
FIG. 10 is a schematic view of the internal structure of a vertical communication sleeve according to an embodiment of the invention;
FIG. 11 is a schematic structural view of a vertical communication sleeve of an embodiment of the present invention;
fig. 12 is a schematic structural view of a rotating sleeve according to an embodiment of the present invention.
Labeled as:
1. fixing a support frame; 101. a central fixing sleeve; 102. a horizontal guide bar; 103. a sliding adjustment frame; 104. adjusting the sliding sleeve; 105. a hydraulic telescopic rod; 106. a lifting gear; 107. a lifting motor; 2. an arc-shaped thread plate; 201. a magnetic support bar; 202. a horizontal sliding sleeve; 203. adjusting the electromagnet; 204. a return spring; 3. a central support rod; 301. embedding a thread; 302. a vertical tabling groove; 303. a lifting rack; 4. a liquid material conveying pipe; 401. a delivery port; 402. a central swivel joint; 403. a liquid material conveying hose; 5. an air delivery interlayer; 501. a communication opening; 502. an interlayer rotary joint; 503. an air delivery hose; 6. a submerged distribution tray; 601. a hollow storage cylinder; 602. a material pressing piston; 603. sealing the sliding sleeve; 604. an umbrella-shaped distribution pipe; 605. an annular distribution pipe; 7. a vertically communicating sleeve; 701. a liquid material conveying interlayer; 702. a delivery opening; 703. an annular rotating groove; 704. fixing a magnet; 705. an arc-shaped friction plate; 706. sealing the air bag; 8. rotating the sleeve; 801. rotating the connecting ring; 802. a spiral deflector; 803. a central connecting post; 804. a release opening; 805. positioning a magnet; 9. rotating the stirring disc; 901. a central rotating frame; 902. the stirring blades are inclined.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to specific embodiments below.
It is to be noted that technical terms or scientific terms used herein should have the ordinary meaning as understood by those having ordinary skill in the art to which the present invention belongs, unless otherwise defined. The use of "first," "second," and the like, herein does not denote any order, quantity, or importance, but rather the terms "first," "second," and the like are used to distinguish one element from another. The word "comprising" or "comprises", and the like, means that the element or item listed before the word covers the element or item listed after the word and its equivalents, but does not exclude other elements or items. The terms "connected" or "coupled" and the like are not restricted to physical or mechanical connections, but may include electrical connections, whether direct or indirect. "upper", "lower", "left", "right", and the like are used merely to indicate relative positional relationships, and when the absolute position of the object being described is changed, the relative positional relationships may also be changed accordingly.
As shown in fig. 1, fig. 2, fig. 3, fig. 6, fig. 7, fig. 8, fig. 9, fig. 10, fig. 11 and fig. 12, a hydrogen peroxide solution controlled feeding device for synthetic DATA includes a fixed support frame 1, a central fixing sleeve 101 is vertically arranged at the center of the fixed support frame 1, and the hydrogen peroxide solution controlled feeding device further includes:
the central support rod 3 is nested and slidably arranged on the inner side of the central fixing sleeve 101;
the liquid conveying pipe 4 is arranged at the center of the inner side of the central supporting rod 3, a conveying port 401 is arranged at the bottom end of the liquid conveying pipe 4, a central rotary joint 402 is arranged at the top end of the liquid conveying pipe 4, and a liquid conveying hose 403 is connected and arranged on the outer side of the central rotary joint 402;
the submerged distribution disc 6 is arranged at the bottom end of the central support rod 3, the submerged distribution disc 6 is connected with the fixed support frame 1 in a sliding mode through the central support rod 3 and the central fixing sleeve 101, a hollow storage cylinder 601 is arranged inside the submerged distribution disc 6, a plurality of umbrella-shaped distribution pipes 604 are uniformly arranged on the outer side of the bottom of the hollow storage cylinder 601 in a surrounding mode, the outer end of each umbrella-shaped distribution pipe 604 is connected with an annular distribution pipe 605, and the liquid material conveying pipe 4 is communicated with the inside of the hollow storage cylinder 601 through a conveying port 401;
the liquid material conveying device comprises a vertical communicating sleeve 7, the vertical communicating sleeve 7 is circumferentially and uniformly arranged on the outer side of an underwater distribution disc 6 in a surrounding mode, a liquid material conveying interlayer 701 is arranged on the outer side of the vertical communicating sleeve 7, the liquid material conveying interlayer 701 and umbrella-shaped distribution pipes 604 are arranged in a one-to-one correspondence mode, the liquid material conveying interlayer 701 is communicated with the interior of a hollow storage barrel 601 through the correspondingly arranged umbrella-shaped distribution pipes 604, all the liquid material conveying interlayers 701 are communicated with each other through annular distribution pipes 605, a plurality of conveying openings 702 are formed in the inner side wall of the vertical communicating sleeve 7, the conveying openings 702 are uniformly arranged in the vertical central line direction of the vertical communicating sleeve 7 at intervals, the interior of the liquid material conveying interlayer 701 is communicated with the interior of the vertical communicating sleeve 7 through the conveying openings 702, and annular rotating grooves 703 are formed in the upper end and the lower end of the vertical communicating sleeve 7;
the rotary sleeve 8 is nested on the inner side of the vertical communication sleeve 7, the upper end and the lower end of the rotary sleeve 8 are both provided with rotary connecting rings 801, the rotary sleeve 8 is rotatably connected with the vertical communication sleeve 7 through the rotary connecting rings 801 and an annular rotary groove 703, the inner side of the rotary sleeve 8 is provided with spiral guide plates 802, the spiral guide plates 802 are spirally arranged along the vertical central line direction of the rotary sleeve 8, the middle of the spiral guide plates 802 is vertically provided with a central connecting column 803, the middle of the inner side wall of the rotary sleeve 8 is provided with a plurality of release openings 804, the release openings 804 are uniformly arranged along the vertical central line direction of the rotary sleeve 8 at intervals, the release openings 804 and the conveying openings 702 are arranged in a one-to-one correspondence manner, the outer side wall of the rotary sleeve 8 is mutually attached to the inner side wall of the vertical communication sleeve 7, the rotary sleeve 8 drives the release openings 804 to rotate and opens the conveying openings 702 when being mutually overlapped, the rotating sleeve 8 closes the delivery opening 702 when the release opening 804 rotates to interfit with the delivery opening 702.
As shown in fig. 1, fig. 2, fig. 3, fig. 6, fig. 7, fig. 8, fig. 9, fig. 10, fig. 11 and fig. 12, as an embodiment of the present invention, a hydrogen peroxide solution controlled charging device for synthetic DATA includes a fixed support frame 1, a central fixing sleeve 101 is vertically disposed at the center of the fixed support frame 1, and further includes: the central support rod 3 is nested and slidably arranged on the inner side of the central fixing sleeve 101; the liquid conveying pipe 4 is arranged at the center of the inner side of the central support rod 3, a conveying port 401 is arranged at the bottom end of the liquid conveying pipe 4, a central rotary joint 402 is arranged at the top end of the liquid conveying pipe 4, and a liquid conveying hose 403 is connected and arranged on the outer side of the central rotary joint 402; the submerged distribution disc 6 is arranged at the bottom end of the central support rod 3, the submerged distribution disc 6 is connected with the fixed support frame 1 in a sliding mode through the central support rod 3 and the central fixing sleeve 101, a hollow storage cylinder 601 is arranged inside the submerged distribution disc 6, a plurality of umbrella-shaped distribution pipes 604 are uniformly arranged on the outer side of the bottom of the hollow storage cylinder 601 in a surrounding mode, the outer ends of the umbrella-shaped distribution pipes 604 are connected with annular distribution pipes 605, and the liquid material conveying pipe 4 is communicated with the inside of the hollow storage cylinder 601 through a conveying port 401; the liquid material conveying device comprises a vertical communicating sleeve 7, the vertical communicating sleeve 7 is circumferentially and uniformly arranged on the outer side of an underwater distribution disc 6 in a surrounding mode, a liquid material conveying interlayer 701 is arranged on the outer side of the vertical communicating sleeve 7, the liquid material conveying interlayer 701 and umbrella-shaped distribution pipes 604 are arranged in a one-to-one correspondence mode, the liquid material conveying interlayer 701 is communicated with the interior of a hollow storage barrel 601 through the correspondingly arranged umbrella-shaped distribution pipes 604, all the liquid material conveying interlayers 701 are communicated with each other through annular distribution pipes 605, a plurality of conveying openings 702 are formed in the inner side wall of the vertical communicating sleeve 7, the conveying openings 702 are uniformly arranged in the vertical central line direction of the vertical communicating sleeve 7 at intervals, the interior of the liquid material conveying interlayer 701 is communicated with the interior of the vertical communicating sleeve 7 through the conveying openings 702, and annular rotating grooves 703 are formed in the upper end and the lower end of the vertical communicating sleeve 7; the rotary sleeve 8 is nested on the inner side of the vertical communication sleeve 7, the upper end and the lower end of the rotary sleeve 8 are both provided with rotary connecting rings 801, the rotary sleeve 8 is rotatably connected with the vertical communication sleeve 7 through the rotary connecting rings 801 and an annular rotary groove 703, the inner side of the rotary sleeve 8 is provided with spiral guide plates 802, the spiral guide plates 802 are spirally arranged along the vertical central line direction of the rotary sleeve 8, the middle of the spiral guide plates 802 is vertically provided with a central connecting column 803, the middle of the inner side wall of the rotary sleeve 8 is provided with a plurality of release openings 804, the release openings 804 are uniformly arranged along the vertical central line direction of the rotary sleeve 8 at intervals, the release openings 804 and the conveying openings 702 are arranged in a one-to-one correspondence manner, the outer side wall of the rotary sleeve 8 is mutually attached to the inner side wall of the vertical communication sleeve 7, the rotary sleeve 8 drives the release openings 804 to rotate and opens the conveying openings 702 when being mutually overlapped, the rotary sleeve 8 drives the release opening 804 to rotate and closes the conveying opening 702 when being mutually staggered, the device can be installed inside an oxidation reaction kettle through the fixed support frame 1, and the submerged distribution plate 6 is immersed below the liquid level of materials inside the oxidation reaction kettle so as to convey hydrogen peroxide, the hydrogen peroxide can be conveyed into the liquid conveying pipe 4 through the liquid conveying hose 403 and the central rotary joint 402, the liquid conveying pipe 4 can further convey the hydrogen peroxide into the hollow storage barrel 601 through the conveying port 401 for storage, the hollow storage barrel 601 uniformly conveys the hydrogen peroxide to the surrounding liquid conveying interlayer 701 through the umbrella-shaped distribution pipe 604, the central support rod 3 can pull the submerged distribution plate 6 to move up and down in the materials so as to stir the materials, meanwhile, in the moving process of the submerged distribution plate 6, the liquid materials inside the reaction kettle pass through the submerged distribution plate 6 through the rotary sleeve 8 vertically communicated with the inner side of the sleeve 7, and in the process of passing through the rotating sleeve 8, the rotating sleeve 8 is driven to rotate by the spiral guide plate 802 therein, and when the rotating sleeve 8 rotates, the release opening 804 arranged on the rotating sleeve 8 and the conveying opening 702 arranged on the vertical communicating sleeve 7 can be continuously superposed and staggered to open and close the conveying opening 702, so that hydrogen peroxide can be conveyed into the reaction kettle through the conveying opening 702 when the submerged distribution disk 6 moves up and down, the submerged distribution disk 6 continuously and uniformly releases hydrogen peroxide while moving up and down, thereby being convenient for fully mixing between the material and the material, improving the integral mixing degree and mixing effect, further being beneficial to improving the reaction efficiency and the utilization rate of hydrogen peroxide, and the faster the submerged distribution disk 6 moves up and down, the faster the material passes through the rotating sleeve 8, the faster the rotating sleeve 8 is driven to rotate, and the more the coincidence opening times of the release opening 804 and the conveying opening 702 in unit time are increased, that is, the more the amount of the released hydrogen peroxide is, the material amount of the submerged distribution plate 6 is ensured to be in a direct proportion relation with the amount of the released added hydrogen peroxide, and the control of the material adding amount and the material adding uniformity is facilitated.
As shown in fig. 1, 2, 3, 4 and 5, optionally, a vertical tabling groove 302 is vertically arranged in the middle of the outer side wall of the central support rod 3, a lifting rack 303 is arranged inside the vertical tabling groove 302, a lifting gear 106 is meshed with the outer side of the lifting rack 303, a lifting motor 107 is arranged at the shaft end of the lifting gear 106, a sliding adjusting frame 103 is arranged outside the lifting motor 107, the lifting motor 107 is connected with the fixed support frame 1 through the sliding adjusting frame 103, a horizontal guide rod 102 is horizontally arranged in the middle of the fixed support frame 1, an adjusting sliding sleeve 104 is arranged at the bottom of the sliding adjusting frame 103, the sliding adjusting frame 103 is connected with the horizontal guide rod 102 through an adjusting sliding sleeve 104 in a sliding manner, a hydraulic telescopic rod 105 is arranged at the rear side of the sliding adjusting frame 103, the hydraulic telescopic rod 105 horizontally slides along the horizontal guide rod 102 through a telescopic traction sliding adjusting frame 103, and the device releases and adds additive while the underwater distribution plate 6 is pulled to move up and down in the material through the central support rod 3 Hydrogen peroxide, the central support bar 3 slides up and down in the central fixing sleeve 101 to draw the submerged distribution disc 6 to synchronously move up and down, the central support bar 3 is also provided with a lifting rack 303, the lifting rack 303 and a lifting gear 106 on the fixing support frame 1 form a transmission structure, the lifting gear 106 is driven to rotate by a lifting motor 107, so that the lifting rack 303 and the central support bar 3 can be driven to move up and down for uniform material feeding, meanwhile, the lifting motor 107 and the lifting gear 106 are both arranged on a sliding adjusting frame 103, the hydraulic telescopic rod 105 can horizontally slide along a horizontal guide rod 102 by stretching and drawing the sliding adjusting frame 103 to adjust the positions of the lifting motor 107 and the lifting gear 106 on the hydraulic telescopic rod, the lifting gear 106 can be embedded into a vertical embedding groove 302 and the lifting rack 303 to be mutually meshed to drive the central support bar 3 to move up and down, and simultaneously, the lifting gear 106 can be separated from the vertical embedding groove 302 and the lifting rack 303, the central support rod 3 can freely slide and rotate at the moment, so that the position angle of the central support rod 3 and the submerged distribution disc 6 dragged by the central support rod can be conveniently adjusted, and the use is more convenient and flexible.
As shown in fig. 1, 2, 3, 4 and 5, optionally, a horizontal sliding sleeve 202 is symmetrically disposed on the inner side of the central fixing sleeve 101, a magnetic support rod 201 is slidably disposed inside the horizontal sliding sleeve 202 in an embedded manner, an arc-shaped threaded plate 2 is disposed at the front end of the magnetic support rod 201, a return spring 204 is disposed at the rear end of the magnetic support rod 201, an adjusting electromagnet 203 is disposed at the rear end of the horizontal sliding sleeve 202, an embedded thread 301 is disposed on the outer side of the central support rod 3, the size of the arc-shaped threaded plate 2 is matched with that of the embedded thread 301, when the central support rod 3 is connected with the arc-shaped threaded plate 2 in an embedded manner through the embedded thread 301, the central support rod 3 rotates in the axial direction while sliding longitudinally along the central fixing sleeve 101, the device releases and adds hydrogen peroxide while drawing the submerged distribution plate 6 to move up and down in the material through the central support rod 3, the central support rod 3 slides up and down in the central fixing sleeve 101, so as to draw the submerged distribution disk 6 to synchronously move up and down, when the central support rod 3 descends, the central support rod can be driven by the lifting rack 303 and the lifting gear 106 and also can naturally descend by gravity, when the central support rod descends naturally by gravity, the lifting gear 106 can be separated from the vertical tabling groove 302 and the lifting rack 303, so as to save energy, meanwhile, the central support rod 3 can slide and rotate freely, when the central support rod 3 and the submerged distribution disk 6 descend naturally by gravity, the central support rod 3 and the submerged distribution disk 6 are connected with each other by the tabling thread 301 through the power loss of the adjusting electromagnet 203, the arc-shaped thread plates 2 can be pushed by the reset spring 204 to move, the symmetrically arranged arc-shaped thread plates 2 clamp the central support rod 3 therebetween, so that when the central support rod 3 descends naturally by gravity, the central support rod 3 can rotate along the axial direction simultaneously, the submerged distribution disc 6 which is dragged at the bottom end of the submerged distribution disc is driven to synchronously rotate, so that the submerged distribution disc 6 can rotate when moving downwards to release and add hydrogen peroxide, internal materials can be stirred and mixed, and the improvement of the uniformity of adding hydrogen peroxide in the release process is facilitated.
As shown in fig. 1, 2, 3, 5, 6, 7, 8, 9, 10, 11 and 12, optionally, an air conveying interlayer 5 is further disposed inside the central support rod 3, the air conveying interlayer 5 is disposed between the liquid conveying pipe 4 and the inner side of the central support rod 3, a communication opening 501 is disposed at the bottom end of the air conveying interlayer 5, an interlayer rotary joint 502 is disposed at the top end of the air conveying interlayer 5, an air conveying hose 503 is connected to the outer side of the interlayer rotary joint 502, a material pressing piston 602 is slidably disposed inside the hollow material storage cylinder 601 in a nested manner, a sealing sliding sleeve 603 is disposed at the center of the material pressing piston 602, the sealing sliding sleeve 603 is slidably disposed outside the liquid conveying pipe 4 in a nested manner, the communication opening 501 is located at the top end of the hollow material storage cylinder 601, the device pulls the liquid distribution tray 6 to move up and down in the material through the central support rod 3 and releases the added hydrogen peroxide at the same time of moving up and down, while hydrogen peroxide is conveyed to the hollow storage cylinder 601 through the liquid conveying pipe 4 for storage, and then is uniformly distributed and conveyed through the umbrella-shaped distribution pipe 604, and the whole submerged distribution disc 6 and the central support rod 3 are small in overall density and can float above the liquid level of the materials in the reaction kettle under the condition that the hollow storage cylinder 601 is completely unloaded, and after a certain amount of hydrogen peroxide is loaded and stored in the hollow storage cylinder 601, the whole weight of the hollow storage cylinder 601 is increased to sink below the liquid level of the materials, so that the submerged distribution disc 6 can be controlled to be placed at the submerged position by controlling the amount of hydrogen peroxide stored in the hollow storage cylinder 601, and after hydrogen peroxide is loaded in the hollow storage cylinder 601, the submerged distribution disc 6 can sink to the bottom of the materials, and air can be conveyed to the air conveying interlayer 5 through the air conveying hose 503 and the interlayer rotary joint 502 and conveyed to the hollow storage cylinder 601 along the air conveying interlayer 5, air is arranged at the upper part of the hollow storage cylinder 601 to push the material pressing piston 602 to move downwards so as to push hydrogen peroxide on the lower side to be released to the umbrella-shaped distribution pipe 604, and along with the release of the hydrogen peroxide, the amount of the hydrogen peroxide in the hollow storage cylinder 601 is reduced and the air is increased, so that the submerged distribution disc 6 can gradually float upwards and move until the hydrogen peroxide is released, the submerged distribution disc 6 can float to the upper part of the liquid level of the material, and at the moment, the air can be discharged by conveying the hydrogen peroxide to the hollow storage cylinder 601, so that the submerged distribution disc 6 can gradually sink and move downwards, and therefore, through the buoyancy balance structure formed by the hollow storage cylinder 601 and the material pressing piston 602, the hydrogen peroxide and the air are sequentially conveyed, the hydrogen peroxide is conveyed and released while the submerged distribution disc 6 is controlled to continuously move upwards and downwards, the hydrogen peroxide is ensured to be always arranged below the liquid level when the hydrogen peroxide is stored and released in the submerged distribution disc 6, is beneficial to improving the uniformity of adding hydrogen peroxide and the use convenience.
As shown in fig. 1, 2, 8, 9, 10, 11 and 12, optionally, an arc-shaped friction plate 705 is disposed inside the annular rotation groove 703, a sealing air bag 706 is disposed on the back surface of the arc-shaped friction plate 705, the sealing air bag 706 is made of flexible material and filled with air, the back surface of the arc-shaped friction plate 705 is connected to the inside of the annular rotation groove 703 through the sealing air bag 706, the inner side surface of the arc-shaped friction plate 705 is attached to the outer side annular surface of the rotation connection ring 801, the sealing air bag 706 retracts to drive the arc-shaped friction plate 705 to move outward and separate from the rotation connection ring 801, a fixed magnet 704 is disposed in the middle of the annular rotation groove 703, the fixed magnet 704 and the delivery opening 702 are disposed on the same vertical line, a positioning magnet 805 is disposed in the middle of the rotation connection ring 801, the positioning magnet 805 and the release opening 804 are disposed on the same vertical line, adjacent magnetic poles between the fixed magnet 704 and the positioning magnet 805 are the same, the device enables materials to pass through the rotary sleeve 8 by moving the submerged distribution disk 6 up and down, and drives the rotary sleeve 8 to rotate by the spiral guide plate 802 so as to convey hydrogen peroxide, the higher the rotation speed of the rotary sleeve 8 is, the more times of opening the release opening 804 and the conveying opening 702 in coincidence in unit time are, namely, the more the amount of hydrogen peroxide to be released is, the rotary sleeve 8 is rotatably connected with the vertical communication sleeve 7 by the rotary connecting ring 801 and the annular rotary groove 703, the inner side surface of the arc-shaped friction plate 705 arranged in the annular rotary groove 703 is mutually attached to the outer side ring surface of the rotary connecting ring 801, the rotation speed of the rotary sleeve 8 can be reduced by friction force, and the arc-shaped friction plate 705 is driven to move outwards when the sealed air bag 706 is contracted so as to be separated from the rotary connecting ring 801, when the submerged distribution disk 6 is arranged at the lower part of the materials in the reaction kettle, the liquid pressure on the sealed air bag 706 is higher, thereby contracting to move the arc-shaped friction plate 705 outwards, reducing the friction force between the arc-shaped friction plate 705 and the rotary connecting ring 801, enabling the rotating speed of the rotary connecting ring 801 to be faster so as to improve the amount of releasing and conveying hydrogen peroxide, gradually reducing the liquid pressure borne by the sealing air bag 706 along with the upward movement of the submerged distribution disk 6, gradually expanding to enable the arc-shaped friction plate 705 to be close to the rotary connecting ring 801, gradually improving the friction force between the arc-shaped friction plate 705 and the rotary connecting ring 801, enabling the rotating speed of the rotary connecting ring 801 to be slower so as to gradually reduce the amount of releasing and conveying hydrogen peroxide, and because of gravity, the concentration of the lower part of materials in the reaction kettle is higher than that of the upper part, so that the reaction amount of adding hydrogen peroxide in the lower part is higher than that of the upper part, and through the structures of the sealing air bag 706 and the arc-shaped friction plate 705, the amount of conveying hydrogen peroxide can be automatically controlled so as to match the concentration of materials in the external reaction kettle, the reaction efficiency and the hydrogen peroxide utilization rate are improved, the use is more flexible and convenient, the fixed magnets 704 and the positioning magnets 805 are correspondingly arranged between the annular rotary groove 703 and the rotary connecting ring 801 respectively, adjacent magnetic poles between the fixed magnets 704 and the positioning magnets 805 are the same, the stop movement of the submerged distribution disc 6 can be guaranteed through repulsive force between the magnets, when the rotary sleeve 8 stops rotating, the fixed magnets 704 and the positioning magnets 805 are mutually staggered, the conveying openings 702 and the releasing openings 804 correspondingly arranged between the fixed magnets and the positioning magnets are mutually staggered to keep the conveying openings 702 closed, the hydrogen peroxide is prevented from being released and conveyed when the submerged distribution disc 6 stops moving, and the use is more reliable and convenient.
As shown in fig. 1, 2, 3 and 6, optionally, the upper and lower sides of the submerged distribution disk 6 are both provided with a rotating stirring disk 9, the center of the rotating stirring disk 9 is provided with a central rotating frame 901, the rotating stirring disk 9 is rotatably connected with the submerged distribution disk 6 through the central rotating frame 901, the axial center line of the central rotating frame 901 and the vertical center line of the submerged distribution disk 6 are located on the same vertical line, the outer side of the central rotating frame 901 is uniformly provided with a plurality of inclined stirring blades 902 in a surrounding manner, the inclined directions of the inclined stirring blades 902 arranged outside the central rotating frame 901 arranged on the upper and lower sides of the submerged distribution disk 6 are opposite, the device can uniformly convey hydrogen peroxide through the up-down movement of the submerged distribution disk 6, and when the submerged distribution disk 6 moves up and down, the rotating stirring disks 9 on the upper and lower sides can rotate along the central rotating frame 901 through the reverse impact drive of the inclined stirring blades 902, thereby can carry out further mixture through pivoted rotary stirring dish 9 and slope stirring vane 902 to the inside material of reation kettle, with the improvement inside material concentration degree of consistency, and when submerged distribution dish 6 reciprocated because the slope direction of the slope stirring vane 902 that sets up in the center swivel mount 901 outside that the upper and lower both sides of submerged distribution dish 6 set up is opposite, so its direction of rotation also can be opposite, thereby avoid producing the swirl and make inside material receive centrifugal force alternate segregation, be favorable to improving inside material concentration degree of consistency and reaction degree of consistency more, with improvement reaction efficiency and hydrogen peroxide solution utilization ratio.
When in use, the device is integrally installed inside an oxidation reaction kettle, corresponding pipelines are connected, the device is fixedly installed above an opening at the top of the oxidation reaction kettle through a fixed support frame 1, a submerged distribution disc 6 is arranged below the liquid level of a material in the oxidation reaction kettle, the submerged distribution disc 6 can move through gear drive and buoyancy drive during specific work, when the gear drive moves, a sliding adjusting frame 103 needs to be drawn by stretching and contracting of a hydraulic telescopic rod 105 to horizontally slide along a horizontal guide rod 102, the positions of a lifting motor 107 and a lifting gear 106 on the submerged distribution disc are adjusted, the lifting gear 106 is embedded into a vertical embedding groove 302 to be mutually meshed with a lifting rack 303, then the lifting motor 107 drives a central support rod 3 to move up and down through the lifting gear 106 and the lifting rack 303, when the submerged distribution disc 6 moves, hydrogen peroxide is conveyed to a hollow material storage barrel 601 through a liquid conveying hose 403, the liquid material in the reaction kettle passes through the rotary sleeve 8 inside the vertical communication sleeve 7 to pass through the submerged distribution disk 6, and the spiral guide plate 802 drives the rotary sleeve 8 to rotate in the process of passing through the rotary sleeve 8, and when the rotary sleeve 8 rotates, the release opening 804 arranged on the rotary sleeve 8 is continuously overlapped and staggered with the conveying opening 702 arranged on the vertical communication sleeve 7 to open and close the conveying opening 702, so that the hydrogen peroxide can be conveyed into the reaction kettle through the conveying opening 702 when the submerged distribution disk 6 moves up and down, the submerged distribution disk 6 continuously and uniformly releases the hydrogen peroxide while moving up and down, thereby being convenient for the full mixing between the hydrogen peroxide and the material, and when the hydrogen peroxide is driven to move by buoyancy, the lifting gear 106 is separated from the vertical tabling groove 302 and the lifting rack 303 by the traction of the hydraulic telescopic rod 105, and then the hydrogen peroxide is loaded into the material storage cylinder through the liquid material conveying hose 403, the submerged distribution disk 6 is sunk to the bottom of the material, then air can be conveyed to the air conveying interlayer 5 through the air conveying hose 503 and the interlayer rotary joint 502, the air is conveyed to the hollow storage cylinder 601 along the air conveying interlayer 5, the air is placed at the upper part of the hollow storage cylinder 601 to push the material pressing piston 602 to move downwards so as to push hydrogen peroxide on the lower side to the umbrella-shaped distribution pipe 604 for release, along with the release of hydrogen peroxide, the amount of the hydrogen peroxide in the hollow storage cylinder 601 is reduced and the air is increased, the submerged distribution disk 6 gradually floats upwards and moves until the release of the hydrogen peroxide is completed, the submerged distribution disk 6 floats above the liquid level of the material, at the moment, the hydrogen peroxide is conveyed to the hollow storage cylinder 601 to discharge the air, so that the submerged distribution disk 6 gradually sinks and moves downwards, and the hydrogen peroxide and the air are sequentially conveyed to control the continuous up and down movement of the submerged distribution disk 6 and simultaneously convey and release the hydrogen peroxide, and the hydrogen peroxide is ensured to be always placed under the liquid level when the submerged distribution disk 6 stores and releases hydrogen peroxide, and meanwhile, when the submerged distribution disk 6 is placed at the lower part of the material in the reaction kettle, the liquid pressure borne by the sealing air bag 706 is contracted to enable the arc-shaped friction plate 705 to move outwards, the friction force between the arc-shaped friction plate 705 and the rotating connecting ring 801 is reduced, the rotating speed of the rotating connecting ring 801 is higher, the amount of the released and conveyed hydrogen peroxide is increased, along with the upward movement of the submerged distribution disk 6, the liquid pressure borne by the sealing air bag 706 is gradually reduced, the arc-shaped friction plate 705 is gradually expanded to be close to the rotating connecting ring 801, the friction force between the arc-shaped friction plate 705 and the rotating connecting ring 801 is gradually increased, the rotating speed of the rotating connecting ring 801 is slower, the amount of the released and conveyed hydrogen peroxide is gradually reduced, the amount of the conveyed hydrogen peroxide is automatically controlled, and when the submerged distribution disk 6 moves up and down, the rotating stirring disks 9 at the upper side and the lower side are driven to rotate along the central rotating rack 901 through the reverse impact of the inclined stirring blades to rotate And further mixing the materials in the reaction kettle to improve the concentration uniformity of the materials in the reaction kettle.
The hydrogen peroxide solution controlled feeding device for the synthetic DATA provided by the invention can drive the submerged distribution disk 6 through the central support rod 3 to be immersed below the liquid level of the materials in the reaction kettle, the hydrogen peroxide solution can be conveyed to the submerged distribution disk 6 to be uniformly conveyed, the submerged distribution disk 6 is provided with a plurality of vertical communication sleeves 7, the submerged distribution disk 6 can be driven to move up and down through the central support rod 3, the materials can pass through the submerged distribution disk 6 through the rotary sleeve 8 on the inner side of the vertical communication sleeve 7 and can drive the rotary sleeve 8 to rotate through the spiral guide plate 802 in the process of passing through the rotary sleeve 8, when the rotary sleeve 8 rotates, the release opening 804 arranged on the rotary sleeve can be continuously overlapped and staggered with the conveying opening 702 arranged on the vertical communication sleeve 7 to open and close the conveying opening 702, so that the hydrogen peroxide solution can be conveyed into the reaction kettle through the conveying opening 702 when the submerged distribution disk 6 moves up and down, the submerged distribution disk 6 continuously and uniformly releases hydrogen peroxide while moving up and down, so that the submerged distribution disk and materials are fully mixed, the overall mixing degree and the mixing effect are improved, and the reaction efficiency and the hydrogen peroxide utilization rate are improved.
Those of ordinary skill in the art will understand that: the discussion of any embodiment above is meant to be exemplary only, and is not intended to intimate that the scope of the disclosure, including the claims, is limited to these examples; within the idea of the invention, also features in the above embodiments or in different embodiments may be combined, steps may be implemented in any order, and there are many other variations of the different aspects of the invention as described above, which are not provided in detail for the sake of brevity.
The present invention is intended to embrace all such alternatives, modifications and variances which fall within the broad scope of the appended claims. Therefore, any omissions, modifications, substitutions, improvements and the like that may be made without departing from the spirit and principles of the invention are intended to be included within the scope of the invention.
Claims (10)
1. The utility model provides a hydrogen peroxide solution control feeding device for synthetic DATA, including fixed bolster (1), the vertical fixed cover in center (101) that are provided with of center department of fixed bolster (1), its characterized in that still includes:
the central support rod (3) is nested and slidably arranged on the inner side of the central fixing sleeve (101);
the liquid conveying pipe (4) is arranged at the center of the inner side of the central supporting rod (3), a conveying port (401) is formed in the bottom end of the liquid conveying pipe (4), a central rotating joint (402) is arranged at the top end of the liquid conveying pipe (4), and a liquid conveying hose (403) is connected and arranged on the outer side of the central rotating joint (402);
the submerged distribution disc (6) is arranged at the bottom end of the central support rod (3), the submerged distribution disc (6) is connected with the fixed support frame (1) in a sliding mode through the central support rod (3) and the central fixing sleeve (101), a hollow storage cylinder (601) is arranged inside the submerged distribution disc (6), a plurality of umbrella-shaped distribution pipes (604) are uniformly arranged on the outer side of the bottom of the hollow storage cylinder (601) in a surrounding mode, the outer ends of the umbrella-shaped distribution pipes (604) are connected with annular distribution pipes (605), and the liquid conveying pipe (4) is communicated with the inside of the hollow storage cylinder (601) through the conveying port (401);
the liquid material conveying device comprises a vertical communication sleeve (7) which is circumferentially and uniformly arranged outside the submerged distribution disc (6) in a surrounding manner, wherein a liquid material conveying interlayer (701) is arranged outside the vertical communication sleeve (7), the vertical communication sleeve (7) and the liquid material conveying interlayer (701) are arranged in a one-to-one correspondence manner with umbrella-shaped distribution pipes (604), the liquid material conveying interlayer (701) is communicated with the interior of the hollow storage cylinder (601) through the umbrella-shaped distribution pipes (604) which are correspondingly arranged, all the liquid material conveying interlayers (701) are communicated with each other through annular distribution pipes (605), the inner side wall of the vertical communication sleeve (7) is provided with a plurality of conveying openings (702), the conveying openings (702) are uniformly arranged along the vertical central line direction of the vertical communication sleeve (7) at intervals, the interior of the liquid material conveying interlayer (701) is communicated with the inner side of the vertical communication sleeve (7) through the conveying openings (702), the upper end and the lower end of the vertical communication sleeve (7) are provided with annular rotating grooves (703);
the rotary sleeve (8) is nested on the inner side of the vertical communication sleeve (7), the upper end and the lower end of the rotary sleeve (8) are respectively provided with a rotary connecting ring (801), the rotary sleeve (8) is rotationally connected with the vertical communication sleeve (7) through the rotary connecting ring (801) and the annular rotary groove (703), the inner side of the rotary sleeve (8) is provided with a spiral guide plate (802), the spiral guide plate (802) is spirally arranged along the direction of the vertical central line of the rotary sleeve (8), the middle of the spiral guide plate (802) is vertically provided with a central connecting column (803), the middle of the inner side wall of the rotary sleeve (8) is provided with a plurality of release openings (804), the release openings (804) are uniformly arranged at intervals along the direction of the vertical central line of the rotary sleeve (8), and the release openings (804) and the conveying openings (702) are arranged in a one-to-one correspondence manner, the lateral wall of rotatory sleeve (8) with laminate each other between the inside wall of vertical intercommunication sleeve (7), rotatory sleeve (8) drive release opening (804) rotate with carry opening (702) to open when coinciding each other and carry opening (702), rotatory sleeve (8) drive release opening (804) rotate with carry opening (702) to seal when closing each other and carry opening (702).
2. The hydrogen peroxide controlled feeding device for the synthetic DATA as claimed in claim 1, wherein a vertical tabling groove (302) is vertically arranged in the middle of the outer side wall of the central support rod (3), a lifting rack (303) is arranged on the inner side of the vertical tabling groove (302), a lifting gear (106) is arranged on the outer side of the lifting rack (303) in a meshed manner, a lifting motor (107) is arranged at the shaft end of the lifting gear (106), a sliding adjusting frame (103) is arranged on the outer side of the lifting motor (107), and the lifting motor (107) is connected with the fixed support frame (1) through the sliding adjusting frame (103).
3. The hydrogen peroxide solution controlled feeding device for the synthetic DATA as claimed in claim 2, wherein a horizontal guide rod (102) is horizontally arranged in the middle of the fixed support frame (1), an adjusting sliding sleeve (104) is arranged at the bottom of the sliding adjusting frame (103), the sliding adjusting frame (103) is slidably connected with the horizontal guide rod (102) through the adjusting sliding sleeve (104), a hydraulic telescopic rod (105) is arranged at the rear side of the sliding adjusting frame (103), and the hydraulic telescopic rod (105) pulls the sliding adjusting frame (103) to horizontally slide along the horizontal guide rod (102) through extension and retraction.
4. The device for controlling feeding of hydrogen peroxide for synthetic DATA as defined in claim 1, wherein horizontal sliding sleeves (202) are symmetrically arranged inside the central fixing sleeve (101), magnetic supporting rods (201) are slidably arranged inside the horizontal sliding sleeves (202) in a nested manner, an arc-shaped threaded plate (2) is arranged at the front ends of the magnetic supporting rods (201), a return spring (204) is arranged at the rear side of the magnetic supporting rods (201), and an adjusting electromagnet (203) is arranged at the rear end of the horizontal sliding sleeve (202).
5. The device for controlling and feeding hydrogen peroxide solution for DATA synthesis as claimed in claim 4, wherein the outer side surface of the central support rod (3) is provided with an embedded thread (301), the arc-shaped thread plate (2) and the embedded thread (301) are mutually matched in size, and when the central support rod (3) and the arc-shaped thread plate (2) are mutually embedded and connected through the embedded thread (301), the central support rod (3) longitudinally slides along the central fixing sleeve (101) and simultaneously rotates along the axial direction.
6. The device for controlling and feeding hydrogen peroxide for synthetic DATA as claimed in claim 1, wherein an air conveying interlayer (5) is further disposed on the inner side of the central support rod (3), the air conveying interlayer (5) is disposed between the liquid conveying pipe (4) and the inner side of the central support rod (3), a communication opening (501) is disposed at the bottom end of the air conveying interlayer (5), an interlayer rotary joint (502) is disposed at the top end of the air conveying interlayer (5), and an air conveying hose (503) is connected to the outer side of the interlayer rotary joint (502).
7. The hydrogen peroxide controlled feeding device for the synthetic DATA as claimed in claim 6, wherein a material pressing piston (602) is slidably arranged inside the hollow material storage cylinder (601) in a nested manner, a sealing sliding sleeve (603) is arranged in the center of the material pressing piston (602), the sealing sliding sleeve (603) is slidably arranged outside the liquid material conveying pipe (4) in a nested manner, and the communication opening (501) is located at the top end of the hollow material storage cylinder (601).
8. The device for controlling and feeding hydrogen peroxide solution for DATA synthesis according to claim 1, wherein an arc-shaped friction plate (705) is disposed on the inner side of the annular rotating groove (703), a sealing air bag (706) is disposed on the back surface of the arc-shaped friction plate (705), the sealing air bag (706) is made of flexible material and filled with gas, the back surface of the arc-shaped friction plate (705) is connected with the inner side of the annular rotating groove (703) through the sealing air bag (706), the inner side surface of the arc-shaped friction plate (705) is attached to the outer side ring surface of the rotating connecting ring (801), and the sealing air bag (706) drives the arc-shaped friction plate (705) to move outwards to separate from the rotating connecting ring (801) when being contracted.
9. The device for controlling feeding of synthetic DATA with hydrogen peroxide as claimed in claim 1, wherein a fixed magnet (704) is disposed in the middle of said annular rotating groove (703), said fixed magnet (704) and said feeding opening (702) are disposed on the same vertical line, a positioning magnet (805) is disposed in the middle of said rotating connection ring (801), said positioning magnet (805) and said releasing opening (804) are disposed on the same vertical line, and adjacent magnetic poles between said fixed magnet (704) and said positioning magnet (805) are the same.
10. The hydrogen peroxide solution controlled feeding device for the synthetic DATA according to claim 1, wherein the upper side and the lower side of the submerged distribution disc (6) are both provided with a rotary stirring disc (9), the center of the rotary stirring disc (9) is provided with a central rotating frame (901), the rotary stirring disc (9) is rotatably connected with the submerged distribution disc (6) through the central rotating frame (901), the axial center line of the central rotating frame (901) and the vertical center line of the submerged distribution disc (6) are located on the same vertical line, the outer side of the central rotating frame (901) is uniformly provided with a plurality of inclined stirring blades (902) in a surrounding manner, and the inclined directions of the inclined stirring blades (902) arranged on the outer side of the central rotating frame (901) arranged on the upper side and the lower side of the submerged distribution disc (6) are opposite.
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| CN202210515185.4A CN114917838B (en) | 2022-05-11 | 2022-05-11 | Hydrogen peroxide control feeding device for synthesizing DATA |
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| CN202210515185.4A CN114917838B (en) | 2022-05-11 | 2022-05-11 | Hydrogen peroxide control feeding device for synthesizing DATA |
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| CN114917838B CN114917838B (en) | 2023-06-02 |
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| CN118221254B (en) * | 2024-05-22 | 2024-07-16 | 西南石油大学 | Waste liquid treatment device for acidizing and fracturing |
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| CN114917838B (en) | 2023-06-02 |
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