CN114904361A - Adsorption tower device - Google Patents

Adsorption tower device Download PDF

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Publication number
CN114904361A
CN114904361A CN202210523562.9A CN202210523562A CN114904361A CN 114904361 A CN114904361 A CN 114904361A CN 202210523562 A CN202210523562 A CN 202210523562A CN 114904361 A CN114904361 A CN 114904361A
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CN
China
Prior art keywords
adsorption tower
air bag
air outlet
air
compression
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202210523562.9A
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Chinese (zh)
Inventor
徐源泉
张立刚
王延臣
于晓龙
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Weihai Bolin Shengkang Oxygen/air Technology Co ltd
Weihai Dongxing Electronics Co Ltd
Original Assignee
Weihai Bolin Shengkang Oxygen/air Technology Co ltd
Weihai Dongxing Electronics Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Weihai Bolin Shengkang Oxygen/air Technology Co ltd, Weihai Dongxing Electronics Co Ltd filed Critical Weihai Bolin Shengkang Oxygen/air Technology Co ltd
Priority to CN202210523562.9A priority Critical patent/CN114904361A/en
Publication of CN114904361A publication Critical patent/CN114904361A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407Constructional details of adsorbing systems
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407Constructional details of adsorbing systems
    • B01D53/0446Means for feeding or distributing gases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/26Drying gases or vapours
    • B01D53/261Drying gases or vapours by adsorption
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02Preparation of oxygen
    • C01B13/0229Purification or separation processes
    • C01B13/0248Physical processing only
    • C01B13/0259Physical processing only by adsorption on solids
    • C01B13/0262Physical processing only by adsorption on solids characterised by the adsorbent
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/04Purification or separation of nitrogen
    • C01B21/0405Purification or separation processes
    • C01B21/0433Physical processing only
    • C01B21/045Physical processing only by adsorption in solids
    • C01B21/0455Physical processing only by adsorption in solids characterised by the adsorbent
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/106Silica or silicates
    • B01D2253/108Zeolites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/116Molecular sieves other than zeolites
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02CCAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00Capture or disposal of greenhouse gases
    • Y02C20/40Capture or disposal of greenhouse gases of CO2

Abstract

The invention discloses an adsorption tower device which comprises an adsorption tower and a compression air bag, wherein molecular sieve packing is filled in the adsorption tower, an air inlet is formed in the bottom of the adsorption tower, an air outlet is formed in the top of the adsorption tower, an inflation inlet is formed in the compression air bag, gas with set pressure is filled in the compression air bag, and the pressing force of the compression air bag is applied to the uppermost layer of the molecular sieve packing. The invention discloses an air bag compression adsorption tower device, wherein a compression air bag is arranged in an adsorption tower, the compression air bag with elasticity is adopted to compress molecular sieve packing, and the compression air bag can automatically adjust the pressure applied to the molecular sieve packing in real time according to external pressure so as to prevent the molecular sieves from rubbing with each other due to the movement.

Description

Adsorption tower device
Technical Field
The invention relates to the technical field of adsorption towers, in particular to an adsorption tower device.
Background
The adsorption tower is filled with molecular sieve packing such as molecular sieve, so that certain components in gas or liquid entering the tower are adsorbed by the porous structure of the adsorbent, thereby realizing the component separation.
In the prior art, in the working process of an adsorption tower, molecular sieve packing materials such as molecular sieves are scraped when receiving air inlet pressure from the lower part, and the mutual friction generated by scraping of the molecular sieves causes the pulverization problem;
in order to prevent the friction loss caused by the pressure difference of the molecular sieve filler such as the molecular sieve in the adsorption tower, a pressing device (porcelain beads, a cylinder, a spring and the like) is added at the upper part of the adsorption tower, so that the molecular sieve filler such as the molecular sieve filler cannot move when receiving the air inlet pressure from the lower part, and the pulverization problem caused by the mutual friction generated by the scraping of the molecular sieves is prevented.
However, the above-mentioned compressing method still has certain problems:
1) when the porcelain beads are adopted for compaction, the filling is too much or too little or not uniform under the influence of the technical level of designers and constructors. The excessive ceramic beads increase the bearing of the molecular sieve below and occupy the space of the adsorption tower to form the inner space of the ineffective adsorption tower; and too few ceramic beads can not meet the pressing requirement, and rolling wear still occurs.
2) When the air cylinder is adopted for compaction, one or more air cylinders are arranged above the adsorption tower, the air source of the air cylinder is the same as that of the adsorption tower, and the sectional area of the air cylinder is far smaller than that of the adsorption tower, so that the air cylinder cannot be balanced with the air below the adsorption tower, friction caused by the up-and-down movement of the molecular sieve still occurs, and the molecular sieve pulverization is further caused.
3) When the spring is adopted for pressing, the operation is difficult when the upper cover of the adsorption tower is installed, and the molecular sieve is gradually compacted and sunk along with the use of the molecular sieve, so that the pressing force of the spring is reduced, meanwhile, in the service cycle of not less than 10 years, the mechanical strength of the spring is reduced, the spring cannot be pressed, and finally, the pulverization problem still occurs.
In conclusion, the compressing technology cannot meet the requirement of the whole life cycle of the adsorption tower, and the failure of the compressing device can cause the pulverization failure of the molecular sieve, so that a compressing structure of the adsorption tower with long service life and high reliability is urgently needed.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention discloses an adsorption tower device.
In order to realize the purpose, the invention is realized by the following technical scheme:
the invention discloses an adsorption tower device which comprises an adsorption tower and a compression air bag, wherein molecular sieve packing is filled in an adsorption tower body, an air inlet is formed in the bottom of the adsorption tower, an air outlet is formed in the top of the adsorption tower, an inflation inlet is formed in the compression air bag, gas with set pressure is filled in the compression air bag, and the pressing force of the compression air bag is applied to the uppermost layer of the molecular sieve packing.
Preferably, the adsorption tower comprises an adsorption tower body and an arched adsorption tower upper cover, the compression air bag is arranged above the adsorption tower body and positioned in the adsorption tower upper cover, and the upper part of the compression air bag is fixedly connected with the top of the adsorption tower upper cover through a connecting piece.
Preferably, the lower part of the compressing air bag is fixedly arranged on the upper end surface of the air outlet filter core support, the air outlet filter core support is used for supporting the compressing air bag, the air outlet filter core support is fixedly arranged on the upper end surface of the air outlet support, and the lower part of the air outlet support is fixedly connected with an air outlet pressing plate attached to the air outlet support.
Preferably, the adsorption tower body is internally provided with an air outlet filter element, and the air outlet filter element is attached to the lower end face of the air outlet pressing plate and is fixedly connected with the air outlet pressing plate.
Preferably, the compressing air bag is connected with an air bag air inlet pipe arranged outside the adsorption tower, and a pressure gauge and/or a valve are/is arranged on the air bag air inlet pipe.
Preferably, the lower space in the adsorption tower is provided with a pretreatment area communicated with the air inlet, the pretreatment area is separated from the area filled with the molecular sieve filler by a filler partition plate, and the pretreatment area is filled with pretreatment filler at least used for removing water and oil.
Further preferably, the adsorption tower upper cover is fixedly connected with the adsorption tower body through a flange.
The invention also discloses application of the adsorption tower device, and the air bag compression adsorption tower device is at least applied to oxygen generation, nitrogen generation and gas drying.
Compared with the prior art, the invention has at least the following advantages:
the invention discloses an air bag compression adsorption tower device, wherein a compression air bag is arranged in an adsorption tower, the compression air bag with elasticity is adopted to compress molecular sieve packing, and the compression air bag can automatically adjust the pressure applied to the molecular sieve packing in real time according to external pressure so as to prevent the molecular sieves from rubbing with each other due to the movement. When the air is initially fed, the pressure of the air inlet position below the adsorption tower is high, the pressure above the adsorption tower is low, and the external pressure on the compression air bag above the adsorption tower is low, so that a larger downward force is generated to be balanced with the pressure of the air inlet below the compression air bag, and the mutual friction generated by the movement of the molecular sieves is prevented; when the gas in the adsorption tower is gradually balanced, the air pressure around the compressing air bag is approximately the same as the pressure of the air inlet position, the pressure difference between the inside and the outside of the compressing air bag is small, the generated pressure is small, and the high-pressure damage to the molecular sieve packing can be prevented. The pressing mode has long service life and high reliability.
The invention discloses an air bag compression adsorption tower device, which can control the pressure of a compression air bag through an external pressure gauge and a valve and monitor the working state of the compression air bag.
Drawings
In order to more clearly illustrate the technical solutions in the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly introduced below.
Fig. 1 is a schematic structural diagram of an adsorption tower apparatus disclosed in an embodiment of the present invention.
Detailed Description
The present invention will be described in further detail with reference to the following embodiments and the accompanying drawings so that those skilled in the art can implement the invention with reference to the description.
Referring to fig. 1, an embodiment of the present invention discloses an adsorption tower apparatus, including an adsorption tower 1 and a compression air bag 2, the adsorption tower 1 is filled with a molecular sieve filler 3, the bottom of the adsorption tower 1 is provided with an air inlet a, the top of the adsorption tower 1 is provided with an air outlet b, the compression air bag 2 is provided with an inflation inlet, the compression air bag 2 is filled with a gas with a set pressure, and a pressing force of the compression air bag 2 is applied to an uppermost layer of the molecular sieve filler 3.
Preferably, the adsorption tower 1 comprises an adsorption tower body 11 and an arched adsorption tower upper cover 12, the compression air bag 2 is arranged above the adsorption tower body 11 and is positioned in the adsorption tower upper cover 12, and the upper part of the compression air bag 2 is fixedly connected with the top of the adsorption tower upper cover 12 through a connecting piece. The adsorption tower upper cover 12 not only serves the purpose of sealing the adsorption tower body 11, but also can fix and compress the air bag 2.
Preferably, the lower part of the compressing air bag 2 is fixedly arranged on the upper end surface of the air outlet filter element support 5, the air outlet filter element support 5 is used for supporting the compressing air bag 2, and the air outlet filter element support 5 can prevent the molecular sieve filler from being blown to the upper part of the air outlet filter element support in the adsorption process, so that a certain filtering effect is achieved. The air outlet filter core support 5 is fixedly arranged on the upper end surface of the air outlet support 6, and an air outlet pressure plate 7 attached to the air outlet support 6 is fixedly connected below the air outlet support 6.
Preferably, an air outlet filter element 8 is further arranged in the adsorption tower body 11, and the air outlet filter element 8 is attached to the lower end face of the air outlet pressing plate 7 and is fixedly connected with the air outlet pressing plate 7. The air outlet support 6, the air outlet pressing plate 7 and the air outlet filter element 8 can be connected through bolts, and the air outlet support 6, the air outlet pressing plate 7 and the air outlet filter element 8 float on the top of the molecular sieve packing 3. The air outlet filter element 8 serves the purpose of preliminary filtering of the screened gas (oxygen/nitrogen/air, etc.).
Preferably, the pressing air bag 2 is connected with an air bag inlet pipe 21 arranged outside the adsorption tower 1, and a pressure gauge 22 and/or a valve 23 are/is arranged on the air bag inlet pipe 21. The pressure data of the compressed air bag 2 can be seen by the maintenance personnel of the equipment through an external pressure gauge 22, when the pressure of the air bag is low, the air can be filled by opening an external valve 23, and when the pressure of the air bag is too high, a part of air can be discharged.
Preferably, a pretreatment area communicated with the air inlet is formed in the lower space in the adsorption tower 1, the pretreatment area is separated from the area filled with the molecular sieve filler 3 through a filler partition plate 4, and pretreatment filler 9 at least used for removing water and oil is filled in the pretreatment area.
Preferably, the adsorption tower upper cover 12 and the adsorption tower body 11 are fixedly connected through a flange. Through flange fixed connection, convenient and fast.
The embodiment of the invention also discloses application of the adsorption tower device, and the air bag compaction adsorption tower device is at least applied to oxygen generation, nitrogen generation and gas drying. Different molecular sieve fillers are selected according to oxygen production, nitrogen production, air drying and the like.
When the air bag compression adsorption tower device disclosed by the embodiment of the invention works, firstly, compressed air enters a pretreatment area in an adsorption tower 1 from an air inlet to carry out pretreatment (water, oil and the like) and control the uniformity of air flow; then, air enters a molecular sieve filler 3 area in the adsorption tower 1 through a filler partition plate 4 to be sieved; then, the oxygen/nitrogen/air reaches the air outlet filter element 8 again for filtering, then is diffused into the space above through the air outlet pressing plate 7, and then is collected through the air outlet b in a centralized way.
Through the technical scheme, the air bag pressing adsorption tower device disclosed by the embodiment of the invention is characterized in that the pressing air bag 2 is arranged in the adsorption tower 1, the required pressing force is calculated according to the structure of the adsorption tower 1, the pressing air bag 2 with the corresponding area is designed, and the pressing air bag 2 is in an uninflated state when the adsorption tower upper cover 12 is installed, so that the assembly is convenient; after the adsorption tower 1 is assembled, the compression air bag 2 can be inflated through the inflation inlet, appropriate inflation pressure can be obtained according to calculation of pressure and pressure intensity, and the compression state can be checked in real time through the external pressure gauge 22 after inflation.
The compacting air bag 2 can automatically adjust the pressure/pressure applied to the molecular sieve packing 3 in real time according to the pressure change in the adsorption tower in the adsorption process, so as to prevent the mutual friction caused by the scraping of the molecular sieves. When the adsorption tower 1 initially admits air, the pressure of the lower air inlet position in the adsorption tower 1 is high, the upper pressure is low, and the external pressure on the compression air bag 2 above the adsorption tower 1 is low, so that a larger downward force is generated to be balanced with the pressure of the lower air inlet, and the mutual friction generated by the movement of the molecular sieves is prevented;
along with the penetration of gas from bottom to top, when the pressure around the pressing air bag 2 rises, the pressure difference between the inside and the outside of the pressing air bag 2 becomes small, the air pressure around the pressing air bag 2 is close to the pressure of the air inlet position, the pressing force of the air bag is automatically reduced, and the high-pressure damage to the molecular sieve filler 3 can be prevented.
Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (8)

1. An adsorption tower device is characterized in that: the adsorption tower is filled with molecular sieve filler, the bottom of the adsorption tower is provided with an air inlet, the top of the adsorption tower is provided with an air outlet, the compression air bag is provided with an inflation inlet, the compression air bag is filled with gas with set pressure, and the pressing force of the compression air bag is applied to the uppermost layer of the molecular sieve filler.
2. An adsorption column apparatus according to claim 1, wherein: the adsorption tower comprises an adsorption tower body and an arched adsorption tower upper cover, the compression air bag is arranged above the adsorption tower body and is positioned in the adsorption tower upper cover, and the compression air bag is fixedly connected with the top of the adsorption tower upper cover through a connecting piece.
3. An adsorption column apparatus according to claim 2, wherein: the lower part of the compressing air bag is fixedly arranged on the upper end surface of the air outlet filter core support, the air outlet filter core support is used for supporting the compressing air bag, the lower part of the air outlet filter core support is fixedly arranged on the upper end surface of the air outlet support, and the lower part of the air outlet support is fixedly connected with an air outlet pressing plate attached to the air outlet support.
4. An adsorption column apparatus according to claim 3, wherein: the adsorption tower is characterized in that an air outlet filter element is further arranged in the adsorption tower body, and the air outlet filter element is attached to the lower end face of the air outlet pressing plate and fixedly connected with the air outlet pressing plate.
5. An adsorption column apparatus according to claim 1, wherein: the compressing air bag is connected with an air bag air inlet pipe arranged outside the adsorption tower, and a pressure gauge and/or a valve are/is arranged on the air bag air inlet pipe.
6. An adsorption column apparatus according to claim 1, wherein: the lower space in the adsorption tower forms one with the air inlet is mutually communicated with a pretreatment area, the pretreatment area is separated from the area filled with the molecular sieve filler by a filler partition plate, and the pretreatment area is filled with pretreatment filler at least used for removing water and oil.
7. An adsorption column apparatus according to claim 2, wherein: the adsorption tower upper cover and the adsorption tower body are fixedly connected through a flange.
8. The application of the adsorption tower device is characterized in that: the balloon compression adsorption tower apparatus of any of claims 1-7 for use in at least oxygen generation, nitrogen generation, and gas drying.
CN202210523562.9A 2022-05-13 2022-05-13 Adsorption tower device Pending CN114904361A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210523562.9A CN114904361A (en) 2022-05-13 2022-05-13 Adsorption tower device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210523562.9A CN114904361A (en) 2022-05-13 2022-05-13 Adsorption tower device

Publications (1)

Publication Number Publication Date
CN114904361A true CN114904361A (en) 2022-08-16

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Country Status (1)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202942789U (en) * 2012-11-19 2013-05-22 天津利源捷能气体设备有限公司 Novel simple side air outlet device for adsorption towers
CN205907031U (en) * 2016-08-03 2017-01-25 威海东兴电子有限公司 Marine climate is with sub - sieve system of compound system oxygen partial pressure
CN205948604U (en) * 2016-08-30 2017-02-15 四川天采科技有限责任公司 A gasbag closing device for adsorption tower
US20180229212A1 (en) * 2017-02-13 2018-08-16 Won Hi Tech Corp. Adsorption tower for oxygen generating system containing two kinds of adsorbing agents filled therein
CN109052328A (en) * 2018-10-15 2018-12-21 杭州博大净化设备有限公司 A kind of circulation oxygen generating plant
CN214087712U (en) * 2020-11-18 2021-08-31 威海东兴电子有限公司 Oxygen purification and regeneration equipment in multi-tower molecular sieve oxygen generation system
CN215027461U (en) * 2020-11-04 2021-12-07 无锡亚士德机械有限公司 Air bag pressing device for adsorption tower

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202942789U (en) * 2012-11-19 2013-05-22 天津利源捷能气体设备有限公司 Novel simple side air outlet device for adsorption towers
CN205907031U (en) * 2016-08-03 2017-01-25 威海东兴电子有限公司 Marine climate is with sub - sieve system of compound system oxygen partial pressure
CN205948604U (en) * 2016-08-30 2017-02-15 四川天采科技有限责任公司 A gasbag closing device for adsorption tower
US20180229212A1 (en) * 2017-02-13 2018-08-16 Won Hi Tech Corp. Adsorption tower for oxygen generating system containing two kinds of adsorbing agents filled therein
CN109052328A (en) * 2018-10-15 2018-12-21 杭州博大净化设备有限公司 A kind of circulation oxygen generating plant
CN215027461U (en) * 2020-11-04 2021-12-07 无锡亚士德机械有限公司 Air bag pressing device for adsorption tower
CN214087712U (en) * 2020-11-18 2021-08-31 威海东兴电子有限公司 Oxygen purification and regeneration equipment in multi-tower molecular sieve oxygen generation system

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