CN114794093A - Method for dissolving trans-4-phenyl-3-butene-2-ketone in water - Google Patents
Method for dissolving trans-4-phenyl-3-butene-2-ketone in water Download PDFInfo
- Publication number
- CN114794093A CN114794093A CN202210658678.3A CN202210658678A CN114794093A CN 114794093 A CN114794093 A CN 114794093A CN 202210658678 A CN202210658678 A CN 202210658678A CN 114794093 A CN114794093 A CN 114794093A
- Authority
- CN
- China
- Prior art keywords
- phenyl
- trans
- water
- butene
- ketone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 45
- 238000000034 method Methods 0.000 title claims abstract description 19
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims abstract description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 11
- 239000003960 organic solvent Substances 0.000 claims abstract description 11
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims abstract description 11
- 229920000053 polysorbate 80 Polymers 0.000 claims abstract description 11
- 239000004094 surface-active agent Substances 0.000 claims abstract description 11
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 6
- BWHOZHOGCMHOBV-BQYQJAHWSA-N trans-benzylideneacetone Chemical compound CC(=O)\C=C\C1=CC=CC=C1 BWHOZHOGCMHOBV-BQYQJAHWSA-N 0.000 claims description 27
- 229930008408 trans-benzylideneacetone Natural products 0.000 claims description 14
- BWHOZHOGCMHOBV-UHFFFAOYSA-N Benzalacetone Natural products CC(=O)C=CC1=CC=CC=C1 BWHOZHOGCMHOBV-UHFFFAOYSA-N 0.000 claims description 13
- 239000000126 substance Substances 0.000 abstract description 4
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 4
- 230000002401 inhibitory effect Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 244000000005 bacterial plant pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aliphatically bound aldehyde or keto groups, or thio analogues thereof; Derivatives thereof, e.g. acetals
Abstract
The invention discloses a method for dissolving trans-4-phenyl-3-butene-2-ketone in water, wherein the trans-4-phenyl-3-butene-2-ketone is mixed with an organic solvent, a surfactant, an emulsifier and water, the organic solvent adopts one of methanol, ethanol and acetone, the surfactant and the emulsifier adopt Tween 80, and the trans-4-phenyl-3-butene-2-ketone can be quickly dissolved in the water by adopting the substances.
Description
Technical Field
The invention relates to a method for dissolving trans-4-phenyl-3-butene-2-ketone in water, belonging to the technical field of biology.
Background
The trans-4-phenyl-3-butene-2-one is obtained by separating and extracting from plants, and later researches show that the trans-4-phenyl-3-butene-2-one has a certain inhibiting effect on some plant pathogenic bacteria, so that two substances with similar molecular structures are purchased on the market according to the molecular structure diagram of the substance, and the research shows that the substance has the same effect of inhibiting the pathogenic bacteria, so that the trans-4-phenyl-3-butene-2-one needs to be dissolved in water for better developing and utilizing the trans-4-phenyl-3-butene-2-one in biological pesticides.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a traditional Chinese medicine tablet candy capable of reducing urate deposition and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
a method for dissolving trans-4-phenyl-3-buten-2-one in water comprises mixing trans-4-phenyl-3-buten-2-one with organic solvent, surfactant, emulsifier and water.
Further, the trans-4-phenyl-3-buten-2-one is mixed with an organic solvent, then mixed with a surfactant and an emulsifier, and finally mixed with water.
Further, the trans-4-phenyl-3-buten-2-one is mixed with a surfactant and an emulsifier, then mixed with an organic solvent, and finally mixed with water.
Further, the organic solvent is one of methanol, ethanol and acetone.
Further, the surfactant and the emulsifier adopt Tween 80.
Compared with the prior art, the invention has the following beneficial effects:
the invention discloses a method for dissolving trans-4-phenyl-3-butene-2-ketone in water, which can dissolve the trans-4-phenyl-3-butene-2-ketone in the water by mixing the trans-4-phenyl-3-butene-2-ketone with one of methanol, ethanol and propanol, Tween 80 and the water.
Detailed Description
The invention is illustrated by the following specific examples, which are not intended to be limiting.
Example 1
A method for dissolving trans-4-phenyl-3-buten-2-one in water comprises mixing trans-4-phenyl-3-buten-2-one with an organic solvent, a surfactant, an emulsifier and water.
Example 2
A method for dissolving trans-4-phenyl-3-butene-2-one in water comprises mixing 50ul of trans-4-phenyl-3-butene-2-one with 200ul of methanol, adding 50ul of Tween 80, mixing, and adding water to dissolve trans-4-phenyl-3-butene-2-one in water completely.
Example 3
A method for dissolving trans-4-phenyl-3-butene-2-ketone in water comprises mixing 50ul of trans-4-phenyl-3-butene-2-ketone with 200ul of ethanol, adding 50ul of Tween 80, mixing, and adding water to dissolve trans-4-phenyl-3-butene-2-ketone in water completely.
Example 4
A method for dissolving trans-4-phenyl-3-butene-2-ketone in water comprises mixing 50ul of trans-4-phenyl-3-butene-2-ketone with 200ul of propanol, adding 50ul of Tween 80, mixing, and adding water to dissolve trans-4-phenyl-3-butene-2-ketone in water completely.
Example 5
A method for dissolving trans-4-phenyl-3-butene-2-one in water comprises mixing 50ul of trans-4-phenyl-3-butene-2-one with 30ul of methanol, adding 25ul of Tween 80, mixing, and adding water to dissolve trans-4-phenyl-3-butene-2-one in water completely.
Example 6
A method for dissolving trans-4-phenyl-3-butene-2-one in water comprises mixing 50ul of trans-4-phenyl-3-butene-2-one with 30ul of ethanol, adding 25ul of Tween 80, mixing, and adding water to dissolve trans-4-phenyl-3-butene-2-one in water completely.
Example 7
A method for dissolving trans-4-phenyl-3-butene-2-ketone in water comprises mixing 50ul of trans-4-phenyl-3-butene-2-ketone with 30ul of propanol, adding 25ul of Tween 80, mixing, and adding water to dissolve trans-4-phenyl-3-butene-2-ketone in water completely.
The invention relates to a method for dissolving trans-4-phenyl-3-butene-2-ketone in water, which is characterized in that the trans-4-phenyl-3-butene-2-ketone is mixed with one of methanol, ethanol and propanol, Tween 80 and water to dissolve the trans-4-phenyl-3-butene-2-ketone in the water.
Finally, it should be noted that the above embodiments are only used for illustrating and not limiting the technical solutions of the present invention, and although the present invention has been described in detail with reference to the above embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made to the present invention without departing from the spirit and scope of the present invention, and all modifications or partial substitutions should be covered by the scope of the claims of the present invention.
Claims (5)
1. A method for dissolving trans-4-phenyl-3-butene-2-one in water is characterized in that,
trans-4-phenyl-3-buten-2-one is mixed with an organic solvent, a surfactant, an emulsifier and water.
2. The method for dissolving trans-4-phenyl-3-buten-2-one in water according to claim 1, wherein the trans-4-phenyl-3-buten-2-one is mixed with an organic solvent, then mixed with a surfactant and an emulsifier, and finally mixed with water.
3. The method for dissolving trans-4-phenyl-3-buten-2-one in water according to claim 1, wherein the trans-4-phenyl-3-buten-2-one is mixed with a surfactant and an emulsifier, then mixed with an organic solvent, and finally mixed with water.
4. The method for dissolving trans-4-phenyl-3-buten-2-one in water according to any one of claims 1 to 3, wherein the organic solvent is one of methanol, ethanol and acetone.
5. The method for dissolving trans-4-phenyl-3-buten-2-one in water according to any one of claims 1 to 3, wherein Tween 80 is used as the surfactant and the emulsifier.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210658678.3A CN114794093A (en) | 2022-06-12 | 2022-06-12 | Method for dissolving trans-4-phenyl-3-butene-2-ketone in water |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210658678.3A CN114794093A (en) | 2022-06-12 | 2022-06-12 | Method for dissolving trans-4-phenyl-3-butene-2-ketone in water |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114794093A true CN114794093A (en) | 2022-07-29 |
Family
ID=82521710
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210658678.3A Pending CN114794093A (en) | 2022-06-12 | 2022-06-12 | Method for dissolving trans-4-phenyl-3-butene-2-ketone in water |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114794093A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101063220A (en) * | 2007-05-22 | 2007-10-31 | 昆明理工大学 | Zinc and Zn-Fe alloy electroplating brightener |
| CN101063216A (en) * | 2007-05-22 | 2007-10-31 | 昆明理工大学 | Zinc and Zn-Fe alloy electroplating bright technique |
| CN112813442A (en) * | 2020-12-29 | 2021-05-18 | 上海建桥学院 | Environment-friendly special cleaning agent for stainless steel surface and preparation method and application thereof |
-
2022
- 2022-06-12 CN CN202210658678.3A patent/CN114794093A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101063220A (en) * | 2007-05-22 | 2007-10-31 | 昆明理工大学 | Zinc and Zn-Fe alloy electroplating brightener |
| CN101063216A (en) * | 2007-05-22 | 2007-10-31 | 昆明理工大学 | Zinc and Zn-Fe alloy electroplating bright technique |
| CN112813442A (en) * | 2020-12-29 | 2021-05-18 | 上海建桥学院 | Environment-friendly special cleaning agent for stainless steel surface and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Simonetti et al. | In vitro antifungal activity of extracts obtained from Hypericum perforatum adventitious roots cultured in a mist bioreactor against planktonic cells and biofilm of Malassezia furfur | |
| CN104620986B (en) | The induction of Radix Notoginseng adventitious root and method for tissue culture | |
| CN107937453A (en) | A kind of preparation method of II type halogenation polyketides of dichloro substitution and antibacterial activity application | |
| El-Sayed et al. | Molecular characterization and positive impact of brassinosteroids and chitosan on Solidago canadensis cv. Tara characteristics | |
| CN103739638B (en) | A kind of method of fermentable purifying tea saponin | |
| CN114794093A (en) | Method for dissolving trans-4-phenyl-3-butene-2-ketone in water | |
| CN102772477A (en) | Application of caragana korshinskii extract in preparing medicine for treating and preventing skin tinea | |
| CN103773690B (en) | A kind of method of open cultivation microalgae | |
| CN109536561A (en) | A method of using ginseng endophyte, conversion ginsenoside Rb1 is rare ginsenoside | |
| Lu et al. | Lycium barbarum polysaccharides attenuate rat anti-Thy-1 glomerulonephritis through mediating pyruvate dehydrogenase | |
| CN109646447B (en) | Application of rhizoma paridis saponin in resisting malassezia furfur and candida albicans products | |
| CN104059044B (en) | A kind of Xanthone derivative and preparation method thereof and application | |
| Badrhadad et al. | Increase alpha-tocopherol in cell suspension cultures Elaeagnus angustifolia L | |
| CN111494364B (en) | Application of isopentenyl substituted phenol compound in resisting staphylococcus aureus and methicillin-resistant staphylococcus aureus | |
| CN104382911A (en) | Application of tauroursodeoxycholic acid salt used as active ingredient in preparation of drug for treating echinococcosis | |
| CN105274152B (en) | Curcumin biotransformation method, product and application | |
| Yu et al. | Cantharis by photosynthetic bacteria biotransformation: Reduced toxicity and improved antitumor efficacy | |
| Chen et al. | Biotransformation of saponins to astragaloside IV from Radix Astragali by immobilized Aspergillus niger | |
| CN104857116B (en) | Application of the Chinese medicine garden burnet in preparing antifungal medicine synergist | |
| Sheh-Hong et al. | Assessment of anticandidal activity and cytotoxicity of root extract from Curculigo latifolia on pathogenic | |
| CN107954964B (en) | One kind 3,4,6 3 substitution-α-pyrone derivative and its preparation method and application | |
| CN104352505A (en) | Applications of protopanaxatriol and derivatives thereof in preparation of medicines for treating hepatic disease | |
| CN104839153A (en) | Natural insecticide for prevention and treatment of pseudoregma bambusicola | |
| CN106591140B (en) | Aspergillus niger and its cultural method and microbial inoculum and application | |
| CN109463386A (en) | Application of the mangostin in prevention and treatment bacterial wilt |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20220729 |