CN114720372A - An analytical instrument for water content testing of seabed sediments - Google Patents
An analytical instrument for water content testing of seabed sediments Download PDFInfo
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- CN114720372A CN114720372A CN202011525676.4A CN202011525676A CN114720372A CN 114720372 A CN114720372 A CN 114720372A CN 202011525676 A CN202011525676 A CN 202011525676A CN 114720372 A CN114720372 A CN 114720372A
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 239000013049 sediment Substances 0.000 title claims abstract description 17
- 238000012360 testing method Methods 0.000 title claims abstract description 16
- 238000001514 detection method Methods 0.000 claims abstract description 65
- 230000007246 mechanism Effects 0.000 claims abstract description 26
- 238000007789 sealing Methods 0.000 claims 2
- 239000013535 sea water Substances 0.000 abstract description 3
- 238000004140 cleaning Methods 0.000 abstract description 2
- 244000309464 bull Species 0.000 abstract 1
- 238000000926 separation method Methods 0.000 description 8
- 238000000034 method Methods 0.000 description 6
- 230000000903 blocking effect Effects 0.000 description 5
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 238000005119 centrifugation Methods 0.000 description 3
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 229910003480 inorganic solid Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N19/00—Investigating materials by mechanical methods
- G01N19/10—Measuring moisture content, e.g. by measuring change in length of hygroscopic filament; Hygrometers
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A90/00—Technologies having an indirect contribution to adaptation to climate change
- Y02A90/30—Assessment of water resources
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Abstract
Description
技术领域technical field
本发明涉及含水率分析设备,具体地说是一种用于海底沉积物含水率测试的分析仪器。The invention relates to water content analysis equipment, in particular to an analysis instrument used for the water content test of seabed sediments.
背景技术Background technique
能够检测各类有机及无机固体、液体、气体等样品中含水率的仪器叫做水分测定仪,按测定原理可以分类物理测定法和化学测定法两大类。An instrument that can detect the moisture content in various organic and inorganic solids, liquids, gases and other samples is called a moisture analyzer.
物理测定法常用的有失重法、蒸馏分层法和气相色谱分析法等,化学测定方法主要有卡尔费休法和甲苯法等;通过对物体进行水分检测,可得到物体内的水分含量,便于对物体进行水分检测,得到相应的检测数据。但在对含水率测试的分析仪器进行使用时,通常是把检测物体放到仪器内,直接对其检测。在来自海水环境中沉积物的水量过大时,会造成检测数据的不精准;且盛放器皿在设备内固定连接或直接放置在设备内,易造成器皿和设备之间的脱落分离。The commonly used physical measurement methods include weight loss method, distillation stratification method and gas chromatography analysis method, and chemical measurement methods mainly include Karl Fischer method and toluene method. Perform moisture detection on the object to obtain the corresponding detection data. However, when using the analytical instrument for moisture content testing, the detection object is usually placed in the instrument to directly detect it. When the amount of water from the sediment in the seawater environment is too large, the detection data will be inaccurate; and the container is fixedly connected in the equipment or placed directly in the equipment, which may easily cause the utensils and equipment to fall off and separate.
发明内容SUMMARY OF THE INVENTION
为了解决现有对含水率测试存在的上述问题,本发明的目的在于提供一种用于海底沉积物含水率测试的分析仪器。In order to solve the above-mentioned problems existing in the existing water content test, the purpose of the present invention is to provide an analytical instrument for the water content test of seabed sediments.
本发明的目的是通过以下技术方案来实现的:The purpose of this invention is to realize through the following technical solutions:
本发明包括机体、离心机构及固定机构,其中机体包括机板,所述离心机构包括检测槽、放置槽、连接套、马达、该检测槽可拆卸地放置在所述机板内,通过所述机板上设置的固定机构固定,所述放置槽容置于检测槽内,该放置槽的顶部与所述检测槽转动连接,所述放置槽的底部安装有连接套,所述机板内固接有马达,该马达的输出端与转杆的下端相连,所述转杆的上端由机板穿出、并与所述连接套连接;待测试的样品放入所述放置槽中,所述马达通过转杆及连接套带动放置槽在检测槽上旋转。The present invention includes a body, a centrifugal mechanism and a fixing mechanism, wherein the body includes a machine plate, and the centrifugal mechanism includes a detection slot, a placement slot, a connecting sleeve, a motor, and the detection slot is detachably placed in the machine plate, and the The fixing mechanism provided on the machine board is fixed, the placement slot is accommodated in the detection slot, the top of the placement slot is rotatably connected with the detection slot, the bottom of the placement slot is installed with a connecting sleeve, and the machine board is fixed inside. A motor is connected, the output end of the motor is connected with the lower end of the rotating rod, and the upper end of the rotating rod is pierced by the machine board and connected with the connecting sleeve; the sample to be tested is put into the placing slot, the The motor drives the placement slot to rotate on the detection slot through the rotating rod and the connecting sleeve.
其中:所述连接套上设有中心孔,该中心孔的外围沿圆周方向均匀开设有多个卡槽,每个所述卡槽均与中心孔连通;所述转杆插入中心孔内,该转杆的表面沿圆周方向设有与所述卡槽数量相同、且一一对应的卡块,每个所述卡块均容置于所对应的卡槽中。Wherein: the connecting sleeve is provided with a center hole, the periphery of the center hole is evenly provided with a plurality of card slots along the circumferential direction, and each of the card slots is communicated with the center hole; the rotating rod is inserted into the center hole, the The surface of the rotating rod is provided with the same number of clamping blocks and one-to-one correspondence with the clamping grooves along the circumferential direction, and each of the clamping blocks is accommodated in the corresponding clamping groove.
所述放置槽的顶部开设有滑槽,卡杆的下端由所述滑槽穿过、并与所述检测槽的顶部固接,所述卡杆的上端转动连接有挡杆。The top of the placement slot is provided with a chute, the lower end of the clamping rod is passed through the chute and is fixedly connected with the top of the detection slot, and the upper end of the clamping rod is rotatably connected with a blocking rod.
所述放置槽的顶部沿径向向外延伸而形成延伸部,该延伸部上开设有圆环形的滑槽。The top of the placement groove extends radially outward to form an extension portion, and a circular chute is provided on the extension portion.
所述放置槽的底面开设有多个通孔,待测试样品通过离心脱出的水由各所述通孔流入检测槽中。The bottom surface of the placing groove is provided with a plurality of through holes, and the water extracted from the sample to be tested by centrifugation flows into the detection groove through each of the through holes.
所述固定机构包括固定杆、伸缩筒及弹簧,该伸缩筒固接于所述机板内,所述固定杆贯穿于伸缩筒,该固定杆位于所述伸缩筒内的部分套设有弹簧,所述固定杆相对于伸缩筒可沿轴向向外拉出,并通过所述弹簧复位;所述检测槽的下端外边缘设有限位块,所述固定杆靠近检测槽的一端由机板穿出、并压在所述限位块上,进而将所述检测槽固定。The fixing mechanism includes a fixing rod, a telescopic cylinder and a spring, the telescopic cylinder is fixed in the machine board, the fixing rod penetrates the telescopic cylinder, and the part of the fixing rod located in the telescopic cylinder is sleeved with a spring, The fixing rod can be pulled out in the axial direction relative to the telescopic cylinder, and is reset by the spring; the outer edge of the lower end of the detection groove is provided with a limit block, and the end of the fixing rod close to the detection groove is penetrated by the machine board. out, and press it on the limit block, so as to fix the detection slot.
所述固定杆位于伸缩筒内的部分设有限位板,所述弹簧的两端分别与该限位板及伸缩筒抵接,所述伸缩筒远离检测槽一端的开孔处设有对限位板限位的挡板。The part of the fixing rod located in the telescopic cylinder is provided with a limit plate, the two ends of the spring are respectively in contact with the limit plate and the telescopic cylinder, and the opening of the telescopic cylinder at one end away from the detection slot is provided with a pair of limit plates. Plate limit baffle.
所述固定机构为多个,沿圆周方向均匀地安装在所述机板上。There are a plurality of the fixing mechanisms, which are evenly mounted on the machine board along the circumferential direction.
所述机板上可拆卸地连接有封盖,所述检测槽及放置槽被封盖罩于内部。A cover is detachably connected to the board, and the detection slot and the placement slot are covered inside by the cover.
本发明的优点与积极效果为:The advantages and positive effects of the present invention are:
本发明便于对测试样品进行沥水,避免海水环境中物体的水分过大,影响设备对其进行检测的精准性;且盛放物体的器皿在设备内的连接固定,方便对其进行拆卸和清理。具体为:The invention is convenient for draining the test sample, avoids excessive water content of objects in the seawater environment, which affects the accuracy of the device's detection; and the utensils containing the objects are connected and fixed in the device, which is convenient for disassembly and cleaning. Specifically:
1.本发明通过检测槽和放置槽的连接,在卡杆的连接作用下,使放置槽在检测槽上的转动牢固,不会造成放置槽在转动时和检测槽的分离;经马达的转动,使转杆在连接套内转动,进而使放置槽在检测槽内转动,连接套和转杆通过卡槽和卡块的卡合连接,便于对转杆和连接套的连接进行分离,进而方便放置槽和检测槽的分离;卡杆在滑槽内滑动,卡杆表面的挡杆使放置槽在检测槽上固定,在放置槽的转动下,便于对放置槽内的物体进行脱水处理。1. In the present invention, through the connection between the detection slot and the placement slot, under the connection action of the clamping rod, the rotation of the placement slot on the detection slot is firm, and the separation of the placement slot and the detection slot during rotation will not be caused; , make the rotating rod rotate in the connecting sleeve, and then make the placing slot rotate in the detection groove, the connecting sleeve and the rotating rod are connected by the clamping slot and the clamping block, which is convenient for the connection between the rotating rod and the connecting sleeve. Separation of the placement slot and the detection slot; the clamping rod slides in the chute, and the blocking rod on the surface of the clamping rod makes the placement slot fixed on the detection slot, and under the rotation of the placement slot, it is convenient to dehydrate the objects in the placement slot.
2.本发明使固定杆在伸缩筒内伸缩,在弹簧的连接下,使固定杆在伸缩筒内伸缩,经挡板和限位板的连接,使固定杆在伸缩筒内的滑动限定,防止固定杆从伸缩筒内脱离,固定杆对检测槽在机板内的连接固定,便于检测槽和机板的连接分离。2. The present invention makes the fixed rod expand and contract in the telescopic cylinder, and under the connection of the spring, the fixed rod is made to expand and contract in the telescopic cylinder, and the connection between the baffle plate and the limit plate makes the sliding of the fixed rod in the telescopic cylinder limited, preventing the The fixing rod is disengaged from the telescopic cylinder, and the fixing rod is fixed to the connection of the detection slot in the machine board, so as to facilitate the connection and separation of the detection slot and the machine board.
附图说明Description of drawings
图1为本发明的结构主视图;Fig. 1 is the structural front view of the present invention;
图2为图1中连接套和转杆之间连接的结构仰视图;Fig. 2 is the bottom view of the structure connected between the connecting sleeve and the rotating rod in Fig. 1;
图3为图1中放置槽和卡杆之间连接的结构俯视图;Figure 3 is a top view of the structure of the connection between the placement slot and the clamping rod in Figure 1;
图4为图1中A处的局部放大图;Fig. 4 is the partial enlarged view of A place in Fig. 1;
其中:1为机体,11为机板,12为封盖;Among them: 1 is the body, 11 is the machine board, and 12 is the cover;
2为离心机构,21为检测槽,22为放置槽,23为卡杆,24为连接套,25为马达,26为转杆,27为卡槽,28为卡块,29为滑槽;2 is a centrifugal mechanism, 21 is a detection slot, 22 is a placement slot, 23 is a clamping rod, 24 is a connecting sleeve, 25 is a motor, 26 is a rotating rod, 27 is a clamping slot, 28 is a clamping block, and 29 is a chute;
3为固定机构,31为固定杆,32为伸缩筒,33为弹簧,34为挡板,35为限位板;36为挡杆,37为中心孔,38为限位块,39为通孔。3 is a fixing mechanism, 31 is a fixed rod, 32 is a telescopic cylinder, 33 is a spring, 34 is a baffle plate, and 35 is a limit plate; 36 is a stop rod, 37 is a center hole, 38 is a limit block, and 39 is a through hole .
具体实施方式Detailed ways
下面结合附图对本发明作进一步详述。The present invention will be described in further detail below in conjunction with the accompanying drawings.
如图1~4所示,本发明包括机体1、离心机构2及固定机构3,其中机体1包括机板11,该机板11的表面可拆卸地连接有封盖12;离心机构2设置于机板11的内侧,该离心机构2包括检测槽21、放置槽22、连接套24、马达25、该检测槽21可拆卸地放置在机板11内,通过机板11上设置的固定机构3固定,放置槽22容置于检测槽21内,该放置槽22的顶部与检测槽21转动连接,放置槽22的底部安装有连接套24,机板11内固接有马达25,该马达25的输入端通过导线和外部电源的输出端电连接,使马达25转动,马达25的输出端与转杆26的下端相连,转杆26的上端由机板11穿出、并与连接套24连接;待测试的样品放入放置槽22中,马达25通过转杆26及连接套24带动放置槽22在检测槽21上旋转,便于放置槽22对其内部的样品进行离心脱水处理。检测槽21及放置槽22被封盖12罩于内部。As shown in Figures 1-4, the present invention includes a
本实施例的连接套24上设有中心孔37,该中心孔37的外围沿圆周方向均匀开设有多个(本实施例为四个)卡槽27,每个卡槽27均与中心孔37连通;转杆26插入中心孔37内,该转杆26的表面沿圆周方向设有与卡槽27数量相同、且一一对应的卡块28,每个卡块28均容置于所对应的卡槽27中。转杆26和连接套24卡接,通过马达25和转杆26的连接,使转杆26在机板11内转动,连接套24和转杆26卡接,使连接套24带动放置槽22转动,在放置槽22的转动下,对待测样品进行脱水。本实施例的卡槽27呈凹槽形设置在连接套24的表面,卡块28呈凸块状、连接在转杆26的表面,卡槽27和卡块28卡接,通过卡槽27和卡块28的卡接使转杆26带动连接套24转动,在卡槽27和卡块28的连接作用下,便于转杆26和连接套24的分离,进而使放置槽22和检测槽21的连接分离。The connecting
本实施例的放置槽22的顶部沿径向向外延伸而形成延伸部,该延伸部上开设有圆环形的滑槽29,卡杆23的下端由滑槽29穿过、并与检测槽21的顶部固接,卡杆23的上端转动连接有挡杆36。在卡杆23和检测槽21的连接作用下,使卡杆23对放置槽22的连接进行固定,便于放置槽22在检测槽21内的转动。放置槽22的底面开设有多个通孔39,待测试样品通过离心脱出的水由各通孔39流入检测槽21中。The top of the
固定机构3为多个,在检测槽21的外围沿圆周方向均匀地安装在机板11上。本实施例的固定机构3包括固定杆31、伸缩筒32及弹簧33,该伸缩筒32固接于机板11内,固定杆31贯穿于伸缩筒32,该固定杆31位于伸缩筒32内的部分套设有弹簧33,且固定杆31位于伸缩筒32内的部分设有限位板35,弹簧33的两端分别与该限位板35及伸缩筒32抵接,伸缩筒32远离检测槽21一端的开孔边缘沿径向向内延伸、进而形成对限位板35限位的挡板34。固定杆31相对于伸缩筒32可沿轴向向外拉出,并通过弹簧33复位;检测槽21的下端外边缘设有限位块38,固定杆31靠近检测槽21的一端由机板11穿出、并压在限位块38上,进而将检测槽21固定。挡板34和限位板35抵接,在弹簧33的作用下,使固定杆31在伸缩筒32内伸缩,在挡板34和限位板35的作用下,使固定杆31在伸缩筒32内的滑动限定,防止伸缩筒32和固定杆31的分离。There are a plurality of
本发明的工作原理为:The working principle of the present invention is:
使用时,将各固定机构3中的固定杆31向外拉动,使固定杆31在伸缩筒32内伸缩,挡板34和限位板35的抵合连接,使固定杆31在伸缩筒32内的滑动限定,防止固定杆31和伸缩筒32的连接脱落,较为实用。再将检测槽21放入机板11上,松开固定杆31,在弹簧33的作用下复位,进而压在限位块38上,将检测槽21固定。然后,将放置槽22放入检测槽21中,卡杆23由放置槽22上的滑槽29穿出,再旋拧挡杆36,使挡杆36抵接于放置槽22的顶部。将待测试的样品放入放置槽22内。When in use, the fixing
通过马达25的转动,使转杆26在检测槽21内转动,转杆26和连接套24连接,在卡槽27和卡块28的卡接下,使转杆26和连接套24卡合连接,便于连接套24和转杆26的分离,进而方便放置槽22和检测槽21的连接分离,在连接套24的转动作用下,使放置槽22在检测槽21内转动,在卡杆23的连接下,使放置槽22在检测槽21内固定,在卡杆23和滑槽29的连接下,使放置槽22在检测槽21上固定转动。Through the rotation of the
样品通过离心脱出的水,由放置槽22底面的通孔39流入检测槽21中。The water released from the sample by centrifugation flows into the
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Application publication date: 20220708 |