CN114686973B - Reaction cavity structure of semiconductor film growth induction heating type equipment - Google Patents
Reaction cavity structure of semiconductor film growth induction heating type equipment Download PDFInfo
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- CN114686973B CN114686973B CN202210272717.6A CN202210272717A CN114686973B CN 114686973 B CN114686973 B CN 114686973B CN 202210272717 A CN202210272717 A CN 202210272717A CN 114686973 B CN114686973 B CN 114686973B
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- 238000010438 heat treatment Methods 0.000 title claims abstract description 30
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 19
- 239000004065 semiconductor Substances 0.000 title claims abstract description 13
- 230000006698 induction Effects 0.000 title claims abstract description 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 120
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 120
- 239000010439 graphite Substances 0.000 claims abstract description 120
- 229910010271 silicon carbide Inorganic materials 0.000 claims abstract description 25
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000010453 quartz Substances 0.000 claims abstract description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000004321 preservation Methods 0.000 claims abstract description 5
- 239000004020 conductor Substances 0.000 claims 1
- 238000002360 preparation method Methods 0.000 abstract description 2
- 238000009826 distribution Methods 0.000 description 5
- 239000000758 substrate Substances 0.000 description 4
- 230000002500 effect on skin Effects 0.000 description 2
- 230000005674 electromagnetic induction Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 241001272720 Medialuna californiensis Species 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004518 low pressure chemical vapour deposition Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
- C30B25/02—Epitaxial-layer growth
- C30B25/08—Reaction chambers; Selection of materials therefor
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/46—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for heating the substrate
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
- C30B25/02—Epitaxial-layer growth
- C30B25/10—Heating of the reaction chamber or the substrate
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B30/00—Production of single crystals or homogeneous polycrystalline material with defined structure characterised by the action of electric or magnetic fields, wave energy or other specific physical conditions
- C30B30/04—Production of single crystals or homogeneous polycrystalline material with defined structure characterised by the action of electric or magnetic fields, wave energy or other specific physical conditions using magnetic fields
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Mechanical Engineering (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
The invention discloses a reaction cavity structure of semiconductor film growth induction heating type equipment, which belongs to the field of semiconductor preparation and comprises a heating element, a heat preservation layer and a quartz tube wall which are sequentially arranged from inside to outside; the heating piece comprises an upper graphite piece, a lower graphite piece and silicon carbide side walls, wherein the upper graphite piece and the lower graphite piece are hollow, the bottom surface of the upper graphite piece is opposite to the top surface of the lower graphite piece, and two sides of the bottom surface of the upper graphite piece are respectively connected with two sides of the top surface of the lower graphite piece through the silicon carbide side walls; and the two ends of the graphite column are respectively connected with the top wall and the bottom wall of the hollow inner cavity. The invention can not only improve the heating efficiency of the reaction cavity, but also improve the temperature uniformity inside the reaction cavity.
Description
Technical Field
The invention relates to the field of semiconductor preparation, in particular to a reaction cavity structure of semiconductor film growth induction heating type equipment.
Background
In the semiconductor production process, epitaxial film growth is one of the important processes for manufacturing semiconductor devices and chips, and film uniformity of epitaxial film growth is an important index for measuring film quality.
Electromagnetic induction heating equipment such as horizontal LPCVD equipment for preparing semiconductor epitaxial films nowadays, which is used for placing a substrate on a lower graphite base, and externally wrapping a quartz tube wall to ensure vacuum of a cavity, wherein an induction coil is wrapped outside the quartz tube wall, and alternating current can generate an alternating magnetic field in a space when passing through the coil, so that the alternating magnetic field generates eddy current in a graphite piece, and heat is generated. The maximum temperature (or heating efficiency) that the graphite piece in the reaction chamber can reach and the uniformity of the temperature distribution in the reaction chamber have an important effect on the uniformity of the grown film on the substrate, so in order to improve the epitaxial film quality, the reaction chamber of the apparatus needs to achieve the optimal heating efficiency and the optimal substrate temperature distribution.
However, due to the influence of the skin effect, eddy currents generated by the alternating magnetic field are concentrated on the surface of the graphite member, so that the temperature distribution of the graphite base and the substrate is uneven, and the edge temperature is high and the middle temperature is low. Therefore, it is needed to design a novel reaction cavity structure to change the eddy current direction and the heat conduction mode, so as to achieve the purposes of increasing the heating efficiency and improving the temperature uniformity of the graphite base.
Disclosure of Invention
Aiming at the problems of low heating efficiency and uneven temperature distribution of a reaction cavity of electromagnetic induction heating equipment in the prior art, the invention aims to provide a reaction cavity structure of semiconductor film growth induction heating equipment.
In order to achieve the above purpose, the technical scheme of the invention is as follows:
the reaction cavity structure of the semiconductor film growth induction heating type equipment comprises a heating element, a heat preservation layer and a quartz tube wall which are sequentially arranged from inside to outside; the heating piece comprises an upper graphite piece, a lower graphite piece and silicon carbide side walls, wherein the upper graphite piece and the lower graphite piece are hollow, the bottom surface of the upper graphite piece is opposite to the top surface of the lower graphite piece, and two sides of the bottom surface of the upper graphite piece are respectively connected with two sides of the top surface of the lower graphite piece through the silicon carbide side walls; and the two ends of the graphite column are respectively connected with the top wall and the bottom wall of the hollow inner cavity.
Preferably, the bottom surface of the upper graphite member and the top surface of the lower graphite member are parallel to each other.
Preferably, the upper graphite piece and the lower graphite piece are both half-moon shaped.
Preferably, the heating element is of symmetrical construction.
Preferably, the graphite columns are arranged along a perpendicular bisecting plane of the top surface of the lower graphite member.
Preferably, the top surface of the lower graphite piece is provided with a graphite base for placing a graphite tray.
Preferably, the graphite tray is used for placing silicon carbide chips, the diameter of the silicon carbide chips is 150mm, and the width of the graphite column is 20-30mm.
By adopting the technical scheme, the invention has the beneficial effects that:
1. due to the arrangement of the upper graphite piece, the lower graphite piece and the silicon carbide side wall between the upper graphite piece and the lower graphite piece, a main loop which is especially formed can form vortex in an alternating magnetic field environment, so that heat is generated to heat the whole reaction cavity;
2. due to the arrangement of the hollow upper graphite piece and the hollow lower graphite piece, a loop can be formed by the upper graphite piece and the lower graphite piece independently, and vortex can be formed in an alternating magnetic field environment, so that heat is generated to further heat the whole reaction cavity;
3. due to the arrangement of the graphite columns in the lower graphite piece, the hollow inner cavity of the lower graphite piece is divided into two small loops, the two small loops respectively form vortex in an alternating magnetic field environment, the generated heat can not only improve the heating efficiency, but also effectively compensate the temperature of the middle part, so that the temperature of a cavity surrounded by the upper graphite piece, the lower graphite piece and the silicon carbide side wall between the upper graphite piece and the lower graphite piece is more uniform.
Drawings
FIG. 1 is a schematic cross-sectional view of the present invention;
FIG. 2 is a schematic diagram of the structure of the present invention;
FIG. 3 is a schematic view of the temperature at each radial location of the top surface of the lower graphite member;
FIG. 4 is a schematic view of the average and standard deviation of temperature at each radial location of the top surface of the lower graphite member.
In the figure, the heating element is 1-, the upper graphite element is 11-, the lower graphite element is 12-, the side wall of 13-silicon carbide, the graphite column is 14-, the graphite base is 15-, the heat preservation layer is 2-and the wall of 3-quartz tube is 3-.
Detailed Description
The following describes the embodiments of the present invention further with reference to the drawings. The description of these embodiments is provided to assist understanding of the present invention, but is not intended to limit the present invention. In addition, the technical features of the embodiments of the present invention described below may be combined with each other as long as they do not collide with each other.
It should be noted that, in the description of the present invention, the positional or positional relation indicated by the terms such as "upper", "lower", "left", "right", "front", "rear", etc. are merely for convenience of describing the present invention based on the description of the structure of the present invention shown in the drawings, and are not intended to indicate or imply that the apparatus or element to be referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus should not be construed as limiting the present invention.
The terms "first" and "second" in this technical solution are merely references to the same or similar structures, or corresponding structures that perform similar functions, and are not an arrangement of the importance of these structures, nor are they ordered, or are they of a comparative size, or other meaning.
In addition, unless explicitly stated and limited otherwise, the terms "mounted," "connected," and "connected" are to be construed broadly, e.g., the connection may be a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; can be directly connected or indirectly connected through an intermediate medium, and can be communicated with the inside of two structures. It will be apparent to those skilled in the art that the specific meaning of the terms described above in this application may be understood in the light of the general inventive concept in connection with the present application.
The reaction cavity structure of the semiconductor film growth induction heating type equipment is circular in cross section as shown in fig. 1 and 2, and comprises a heating element 1, a heat preservation layer 2 and a quartz tube wall 3 which are sequentially arranged from inside to outside.
The heating element 1 has a vertically and laterally symmetrical structure as a whole, and the heating element 1 specifically includes an upper graphite element 11, a lower graphite element 12, and a silicon carbide sidewall 13. Wherein, the upper graphite member 11 and the lower graphite member 12 are both in a hollow half-moon-shaped structure, and the upper graphite member 11 and the lower graphite member 12 are the same in size, are arranged up and down, and the bottom surface of the upper graphite member 11 is parallel and opposite to the top surface of the lower graphite member 12. The silicon carbide side walls 13 are arranged in two, and two sides of the bottom surface of the upper graphite member 11 are respectively connected with two sides of the top surface of the lower graphite member 12 through the silicon carbide side walls 13, so that the upper graphite member 11, the lower graphite member 12 and the silicon carbide side walls 13 form a main loop, and the upper graphite member 11 and the lower graphite member 12 which are hollow form independent loops. The top surface of the lower graphite member 12 is also provided with a graphite base 15, the graphite base 15 being used for placing a graphite tray, and the graphite tray being used for placing a silicon carbide wafer.
When alternating current is introduced into the induction coil outside the quartz tube wall 3, a main loop is formed by the upper graphite piece 11, the lower graphite piece 12 and the silicon carbide side wall 13, and eddy currents are generated in independent loops formed by the upper graphite piece 11 and the lower graphite piece 12 which are hollow, so that heat is generated, and the heating piece is heated.
However, due to the skin effect and the influence of the eddy current loop, the temperature of the middle position of the lower graphite member 12 is low, and the temperature of the edge position is high, so that the temperature of the lower graphite member 12 is more uniform, in this embodiment, a graphite column 14 is further disposed in the hollow cavity of the lower graphite member 12, and two ends of the graphite column 14 are respectively connected to the top wall and the bottom wall of the hollow cavity, for example, the graphite column 14 is disposed along the perpendicular bisecting plane of the top surface of the lower graphite member 12. By the arrangement, the lower graphite piece 12 is divided into two small loops, namely, the middle position of the lower graphite piece 12 is changed into the edge position of the small loop, so that the temperature of the lower graphite piece 12 is compensated, and the temperature of each position of the top surface of the lower graphite piece 12 is more uniform.
In this embodiment, the silicon carbide wafer is specifically configured to have a diameter of 150mm (i.e., 6 inches), and the graphite susceptor 15 is configured to have a height of 12mm, where the height refers to the distance between the top surface of the graphite susceptor 15 and the top surface of the lower graphite member 12. As shown in FIG. 3, the widths of the graphite columns 14 are respectively 20 mm, 25 mm and 30mm, and the temperature distribution condition of the silicon carbide chip at each position (0-150 mm) along the diameter direction is specifically shown, and the temperature value is obtained through the simulation of COMSOL multiple physical field simulation software (COMSOLMultigics). As can be seen from fig. 3, when the graphite column 14 is arranged, the temperature of the silicon carbide piece at the central position increases significantly, and the temperature of the silicon carbide piece becomes more uniform from the left end to the right end (0 mm coordinates to 150mm coordinates). As shown in fig. 4, which shows the presence or absence of the graphite column 14 and the data of the average temperature and the standard deviation of the temperature (temperature uniformity) of the silicon carbide wafer at each place under different widths of the graphite column 14, it can be seen that the average temperature is raised by 39.6 ℃, the standard deviation of the temperature is reduced by 10.9 ℃, and at the same time, the average temperature is increased and the standard deviation of the temperature is reduced along with the increase of the width of the graphite column 14, thereby achieving the purpose of improving the heating efficiency and the temperature uniformity.
The embodiments of the present invention have been described in detail above with reference to the accompanying drawings, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the invention, and yet fall within the scope of the invention.
Claims (3)
1. The reaction cavity structure of the semiconductor film growth induction heating type equipment is characterized in that: comprises a heating element, a heat preservation layer and a quartz tube wall which are sequentially arranged from inside to outside; the heating piece comprises an upper graphite piece, a lower graphite piece and silicon carbide side walls, wherein the upper graphite piece and the lower graphite piece are hollow, the bottom surface of the upper graphite piece is opposite to the top surface of the lower graphite piece, and two sides of the bottom surface of the upper graphite piece are respectively connected with two sides of the top surface of the lower graphite piece through the silicon carbide side walls; a graphite column is further arranged in the hollow inner cavity of the lower graphite piece, and two ends of the graphite column are respectively connected with the top wall and the bottom wall of the hollow inner cavity; wherein the silicon carbide side wall is a conductor; the bottom surface of the upper graphite piece is parallel to the top surface of the lower graphite piece; the upper graphite piece and the lower graphite piece are both half-moon-shaped; the heating piece is in a symmetrical structure; the graphite posts are disposed along a perpendicular bisector of the top surface of the lower graphite member.
2. The reaction chamber structure of claim 1, wherein: the top surface of lower graphite spare is provided with the graphite base that is used for placing graphite tray.
3. The reaction chamber structure of claim 2, wherein: the graphite tray is used for placing silicon carbide chips, the diameter of the silicon carbide chips is 150mm, and the width of the graphite column is 20-30mm.
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CN202210272717.6A CN114686973B (en) | 2022-03-18 | 2022-03-18 | Reaction cavity structure of semiconductor film growth induction heating type equipment |
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CN202210272717.6A CN114686973B (en) | 2022-03-18 | 2022-03-18 | Reaction cavity structure of semiconductor film growth induction heating type equipment |
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CN114686973B true CN114686973B (en) | 2023-11-14 |
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CN1708602A (en) * | 2002-12-10 | 2005-12-14 | Etc外延技术中心有限公司 | Susceptor system |
CN201706889U (en) * | 2009-10-22 | 2011-01-12 | 赵志强 | Inductive electric heating zinc re-distillation furnace |
CN102231416A (en) * | 2011-06-14 | 2011-11-02 | 泉州市博泰半导体科技有限公司 | Chemical vapor deposition reaction equipment |
CN102783248A (en) * | 2010-02-19 | 2012-11-14 | 新日本制铁株式会社 | Transverse flux induction heating device |
JP2016141612A (en) * | 2015-02-04 | 2016-08-08 | 信越半導体株式会社 | Device and method for manufacturing semiconductor single crystal |
CN109280968A (en) * | 2017-07-21 | 2019-01-29 | 镇江仁德新能源科技有限公司 | A kind of graphite heater and silicon crystal growth oven |
CN210341057U (en) * | 2019-05-06 | 2020-04-17 | 杭州弘晟智能科技有限公司 | Reaction device for epitaxial growth |
CN212019372U (en) * | 2020-03-25 | 2020-11-27 | 湖北天龙石墨碳业有限公司 | Electrical heating graphite melting pot |
CN112831827A (en) * | 2021-02-03 | 2021-05-25 | 路景刚 | Cross arrangement double-loop side heater and crystal silicon ingot furnace |
-
2022
- 2022-03-18 CN CN202210272717.6A patent/CN114686973B/en active Active
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1708602A (en) * | 2002-12-10 | 2005-12-14 | Etc外延技术中心有限公司 | Susceptor system |
CN201706889U (en) * | 2009-10-22 | 2011-01-12 | 赵志强 | Inductive electric heating zinc re-distillation furnace |
CN102783248A (en) * | 2010-02-19 | 2012-11-14 | 新日本制铁株式会社 | Transverse flux induction heating device |
CN102231416A (en) * | 2011-06-14 | 2011-11-02 | 泉州市博泰半导体科技有限公司 | Chemical vapor deposition reaction equipment |
JP2016141612A (en) * | 2015-02-04 | 2016-08-08 | 信越半導体株式会社 | Device and method for manufacturing semiconductor single crystal |
CN109280968A (en) * | 2017-07-21 | 2019-01-29 | 镇江仁德新能源科技有限公司 | A kind of graphite heater and silicon crystal growth oven |
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CN212019372U (en) * | 2020-03-25 | 2020-11-27 | 湖北天龙石墨碳业有限公司 | Electrical heating graphite melting pot |
CN112831827A (en) * | 2021-02-03 | 2021-05-25 | 路景刚 | Cross arrangement double-loop side heater and crystal silicon ingot furnace |
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