CN114558478A - Preparation method of compound based on magnesium alloy three-in-one treatment agent - Google Patents
Preparation method of compound based on magnesium alloy three-in-one treatment agent Download PDFInfo
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- CN114558478A CN114558478A CN202210291160.0A CN202210291160A CN114558478A CN 114558478 A CN114558478 A CN 114558478A CN 202210291160 A CN202210291160 A CN 202210291160A CN 114558478 A CN114558478 A CN 114558478A
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- 229910000861 Mg alloy Inorganic materials 0.000 title claims abstract description 66
- 238000002360 preparation method Methods 0.000 title claims abstract description 50
- 150000001875 compounds Chemical class 0.000 title claims abstract description 40
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 87
- 239000002994 raw material Substances 0.000 claims abstract description 30
- 230000000694 effects Effects 0.000 claims abstract description 27
- 238000012360 testing method Methods 0.000 claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 15
- 239000007787 solid Substances 0.000 claims abstract description 15
- 230000007246 mechanism Effects 0.000 claims description 56
- 230000000670 limiting effect Effects 0.000 claims description 48
- 238000009434 installation Methods 0.000 claims description 39
- 238000003756 stirring Methods 0.000 claims description 34
- 230000005540 biological transmission Effects 0.000 claims description 28
- 238000004140 cleaning Methods 0.000 claims description 25
- 238000007789 sealing Methods 0.000 claims description 21
- 238000003860 storage Methods 0.000 claims description 21
- 238000003825 pressing Methods 0.000 claims description 18
- 238000005498 polishing Methods 0.000 claims description 12
- 238000011010 flushing procedure Methods 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 8
- 239000007921 spray Substances 0.000 claims description 8
- 239000008139 complexing agent Substances 0.000 claims description 6
- 238000004891 communication Methods 0.000 claims description 4
- 150000007522 mineralic acids Chemical class 0.000 claims description 3
- 230000000149 penetrating effect Effects 0.000 claims description 3
- 239000004094 surface-active agent Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 abstract description 2
- 238000009472 formulation Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002585 base Substances 0.000 description 22
- 230000009471 action Effects 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000006260 foam Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 229910000838 Al alloy Inorganic materials 0.000 description 2
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 238000003780 insertion Methods 0.000 description 2
- 230000037431 insertion Effects 0.000 description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000000452 restraining effect Effects 0.000 description 2
- ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 description 1
- QLCAGXDTDCDEGN-UHFFFAOYSA-N 3-sulfanylcarbonylhexanedioic acid Chemical compound OC(=O)CCC(C(O)=S)CC(O)=O QLCAGXDTDCDEGN-UHFFFAOYSA-N 0.000 description 1
- 229910052684 Cerium Inorganic materials 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 229910000914 Mn alloy Inorganic materials 0.000 description 1
- 229910052776 Thorium Inorganic materials 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 229910001093 Zr alloy Inorganic materials 0.000 description 1
- UQCVYEFSQYEJOJ-UHFFFAOYSA-N [Mg].[Zn].[Zr] Chemical compound [Mg].[Zn].[Zr] UQCVYEFSQYEJOJ-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- KBMLJKBBKGNETC-UHFFFAOYSA-N magnesium manganese Chemical compound [Mg].[Mn] KBMLJKBBKGNETC-UHFFFAOYSA-N 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 229940098779 methanesulfonic acid Drugs 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
- C23F3/02—Light metals
- C23F3/03—Light metals with acidic solutions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
Abstract
A preparation method of a compound based on a three-in-one magnesium alloy treating agent belongs to the technical field of magnesium alloy treatment, and aims to solve the problems that during actual preparation, an unintended proportioning condition occurs, corresponding test materials are required to be consumed for testing proportioning effects each time, not only is the cost consumed, but also the labor is consumed, the preparation period is long, and an accurate proportioning effect is difficult to find, and the invention comprises the following steps: s1: preparing a liquid raw material, S2: preparing a solid raw material, S3: preparation of the formulation, S4: experimental observation, S5: by adjusting the water proportion, the invention not only can reduce the cost consumption, but also can save the labor and shorten the preparation period by regularly carrying out proportioning operation, obtain accurate preparation results with high efficiency and is convenient to use.
Description
Technical Field
The invention relates to the technical field of magnesium alloy treatment, in particular to a preparation method of a compound based on a magnesium alloy three-in-one treatment agent.
Background
The magnesium alloy is an alloy formed by adding other elements on the basis of magnesium. The method is characterized in that: the density is small (about 1.8g/cm 3), the strength is high, the elastic modulus is large, the heat dissipation is good, the shock absorption is good, the impact load bearing capacity is larger than that of aluminum alloy, and the corrosion resistance of organic matters and alkali is good. The main alloy elements comprise aluminum, zinc, manganese, cerium, thorium, a small amount of zirconium or cadmium and the like. The most widely used are magnesium-aluminum alloys followed by magnesium-manganese alloys and magnesium-zinc-zirconium alloys. The method is mainly used in aviation, aerospace, transportation, chemical engineering, rocket and other industrial departments. The surface of the magnesium alloy is rusted under the external environmental factors, however, in order to ensure the service performance of the magnesium alloy, a chemical rust removal method is usually used for polishing the magnesium alloy.
The compound of trinity processing agent of present magnesium alloy is when preparing, be difficult to hold the ratio between solid solute and liquid solute and the hydrosolvent usually, when actual preparation, then the diffuse not purposeful ratio condition can appear, and experimental ratio effect at every turn, all need the corresponding experimental material of loss, not only the cost is consumed, also consume the manpower simultaneously, the cycle length is prepared, be difficult to find accurate ratio effect, and magnesium alloy surface after experimental at every turn then can produce more foam cover, generally need the manual work to wash, just can observe polishing effect, it is very inconvenient to operate, promote the cost of labor.
Aiming at the problems, a preparation method of the compound based on the magnesium alloy three-in-one treating agent is provided.
Disclosure of Invention
The invention aims to provide a preparation method of a compound based on a three-in-one magnesium alloy treating agent, which adopts the device to work, thereby solving the problems that when the compound of the three-in-one magnesium alloy treating agent in the background is prepared, the proportion between a solid solute and a liquid solute and an aqueous solvent is difficult to master, and when the compound is actually prepared, the situation of random and unintended proportion can occur, and the proportion effect in each test needs to be lost, so that the consumption cost is low, the manpower is also consumed, the preparation period is long, the accurate proportion effect is difficult to find, and more foam coverage can be generated on the surface of the magnesium alloy after each test, the polishing effect can be observed by manually cleaning, the operation is very inconvenient, and the labor cost is increased.
In order to achieve the purpose, the invention provides the following technical scheme: the preparation method of the compound based on the magnesium alloy three-in-one treating agent is characterized by comprising the following steps:
s1: preparing a liquid raw material: preparing liquid raw materials in corresponding weight parts, respectively pouring the liquid raw materials into the same container, and stirring and mixing the liquid raw materials;
s2: preparing a solid raw material: preparing solid raw materials in corresponding weight parts, respectively pouring the solid raw materials into the same container, and stirring and mixing the solid raw materials;
s3: preparing a compound: preparing 300 parts by weight of water, pouring the water into a proportioning device, and respectively pouring the raw materials prepared in the other two containers into the proportioning device filled with the water;
s4: and (3) test observation: after uniformly stirring, putting the magnesium alloy to be treated into the proportioned solution, and observing the polishing treatment effect of the solution on the surface of the magnesium alloy;
s5: adjusting the water proportion: the proportioning test is carried out by replacing the weight part of the water with 150 parts of the water and repeating the steps, and the proportion of the weight part of the water is reduced by one half or increased by three halves by judging the polishing effect, so that the most accurate proportioning value is obtained.
Further, in S5, the GU-M-025 magnesium alloy three-in-one treating agent is a compound of an inorganic acid agent, an inorganic complexing agent, an organic complexing agent and a surfactant. The weight percentage of the components is as follows:
further, the proportioning device in the S3 includes an installation base and a concave installation frame fixedly installed in the middle of the top surface of the installation base in a communicating manner, a motor is fixedly installed on the outer wall of the upper side of one end of the concave installation frame, a driving shaft is slidably arranged in the inner cavity of the middle of the concave installation frame, a stirring assembly is arranged in the inner cavity of one end of the installation base, a lifting clamping assembly is arranged in the inner cavity of the concave installation frame, the upper end of the lifting clamping assembly is slidably sleeved on the driving shaft, a pneumatic water pressing assembly is installed in the inner cavity of the other end of the concave installation frame, the lower end of the pneumatic water pressing assembly is arranged in the inner cavity of the other end of the installation base, a preparation box is fixedly installed at one end of the top surface of the installation base in an embedded manner, and a cleaning box is fixedly installed at the other end of the top surface of the installation base in an embedded manner;
an L-shaped mounting groove is formed in one end of the top surface of the mounting base, the lower end of the L-shaped mounting groove is arranged below the preparation box, an inner water storage groove is formed in a lower inner cavity of the other end of the mounting base, a communicating inner groove is formed in the lower inner wall of one end of the inner water storage groove, the inner water storage groove is communicated with the cleaning box through the communicating inner groove, a water inlet is formed in the outer wall of one side of the mounting base, and the water inlet is communicated with the inner water storage groove;
a concave through hole is formed in the inner cavity of the concave mounting frame, one end of the concave through hole is communicated with one end of the L-shaped mounting groove, a square through sliding hole is formed in the top surface of the middle of one end of the concave mounting frame, a trapezoidal sliding block is fixedly communicated and arranged on the bottom surface of the middle of the concave mounting frame, and a T-shaped limiting block is fixedly communicated and arranged on the top surface of the middle of the concave mounting frame;
the output tail end of the motor is fixedly provided with a clamping shaft;
the driving shaft comprises a driving limiting mechanism and a driving shaft main body movably arranged at the lower end of the driving limiting mechanism in a penetrating way;
the stirring assembly comprises a gear transmission mechanism and a long transmission shaft movably arranged in the inner cavity of the L-shaped mounting groove, a stirring rod is movably arranged on the top surface of one end of the inner cavity of the L-shaped mounting groove, and the upper end of the stirring rod penetrates through the bottom surface of the preparation box in a sealing manner;
the lifting clamping assembly comprises an H-shaped roller and a reset mechanism movably mounted at one end of the H-shaped roller, a connecting rope is wound on the H-shaped roller, one end of the connecting rope is fixedly connected to the outer wall of the H-shaped roller, and the other end of the connecting rope is fixedly connected to the top surface of the middle part of the clamping mechanism;
the pneumatic water pressing assembly comprises an air pressing mechanism and a connecting pipeline, one end of the connecting pipeline is communicated and installed on the air pressing mechanism, an air inlet pushing mechanism is fixedly installed on the inner wall of one end of the inner cavity of the water storage inner groove in an embedded mode, and the lower end of the connecting pipeline penetrates through the concave through hole and the top surface of the installation base and is communicated and installed with the air inlet pushing mechanism;
the outer wall of one end of the cleaning box is provided with a feeding opening, the inner wall of one side of the lower side of the cleaning box is provided with a water outlet hole, a communicated water flushing inner groove is arranged in an inner cavity of the lower end of the cleaning box, the communicated water flushing inner groove is communicated with the communicated inner groove, the inner wall of the inner cavity of the cleaning box is respectively provided with a spray head, and the spray heads are respectively arranged at openings communicated with the water flushing inner groove;
the inner walls of two sides of the inner cavity of the concave through hole are respectively provided with a side wall sliding groove, the middle part of the trapezoidal sliding block is provided with a square rope threading hole, the middle part of the bottom surface of the T-shaped limiting block is provided with a bottom surface limiting sliding groove, and the inner walls of the upper sides of two sides of the inner cavity of the bottom surface limiting sliding groove are respectively provided with an inclined sliding way.
Further, it includes link block and the insertion slider of fixed mounting respectively on link block both sides middle part outer wall to drive limiting mechanism, the insertion slider slides and sets up in the lateral wall spout, fixed mounting has threaded connection piece on one side outer wall of link block upside, and pass through threaded connection screw knob on the threaded connection piece, link block's lower tip fixed mounting has the connecting sleeve, it includes circular pivot and the joint spout of setting on a circular pivot tip middle part outer wall to drive axle main part, respectively fixed mounting has short restriction slider on the both sides outer wall of circular pivot one end, respectively fixed mounting has long restriction slider on the both sides outer wall of the circular pivot other end, another tip fixed mounting of circular pivot has the restriction disc, the slip setting of joint axle is in the joint spout.
Furthermore, the gear transmission mechanism comprises a hoisting connecting block and a connecting ring fixedly installed at the lower end of the hoisting connecting block, a rotating ring is movably installed on the outer wall of one end of the connecting ring, a clamping gear is fixedly installed on the outer wall of one end of the rotating ring, and a first clamping sliding hole is formed in the middle of the clamping gear.
Further, long transmission shaft includes long transmission shaft main part and the connecting gear of fixed mounting in long transmission shaft main part upper end, the meshing is connected between connecting gear and the joint gear, the lower tip fixed mounting of long transmission shaft main part has first connecting roller, and cup jointed the drive belt on the first connecting roller, the puddler includes the puddler main part and installs the connection bearing on L type mounting groove inner chamber top surface, and puddler main part movable mounting is on connecting the bearing, the lower tip fixed mounting of puddler main part has the second to connect the roller, and be connected through the drive belt between first connecting roller and the second connection roller.
Further, be provided with second joint slide opening on the middle part outer wall of H type roller one end, the one end periphery embedding movable mounting of H type roller has the abrasionproof ring, canceling release mechanical system includes hollow disc and the spring leaf of one end installation on hollow disc inner chamber inner wall, and the other end fixed mounting of spring leaf is on the other end outer wall of H type roller, fixed mounting has the income connecting block on the middle part top surface of hollow disc, and there is flexible piece through extension spring slidable mounting in the inner chamber of income connecting block, and movable mounting has the ball on the both sides outer wall of flexible piece upper end respectively, and the ball sets up in the slope slide.
Further, press from both sides and get mechanism including hoisting installation shell and embedding movable mounting respectively and hoisting the big gyro wheel of installation shell top surface one end both sides department, the other end both sides punishment of hoisting installation shell top surface do not movable mounting have a little gyro wheel, it installs the piece of getting to press from both sides in the inner chamber of installation shell to hoist, it includes that double thread knob and embedding are installed the restriction bearing on hoisting installation shell one side middle part outer wall to press from both sides the piece of getting, it gets the piece to slide to be provided with respectively in the downside inner chamber at hoisting installation shell both ends to press from both sides, and press from both sides the upper end of getting the piece and cup joint output and the output end at double thread knob through the screw thread respectively.
Furthermore, the air compressing mechanism comprises an air compressing shell and an air compressing piston, one end of the air compressing piston is arranged in the inner cavity of the air compressing shell in a sealing sliding mode through an extruding spring, extruding protruding columns are fixedly arranged on the outer walls of the upper side and the lower side of the outer end of the air compressing piston respectively, and a one-way air inlet valve is arranged on the outer wall of the air compressing shell.
Furthermore, the air inlet pushing mechanism comprises a pushing shell and a pushing piston, wherein one end of the pushing piston is arranged in the inner cavity of the pushing shell in a sealing and sliding mode, a pressurized water sealing gasket is fixedly arranged at one end of the pushing piston, the pressurized water sealing gasket is arranged in the water storage inner groove in a sealing and sliding mode, and the other end of the pushing shell is communicated with and provided with an air outlet seal.
Compared with the prior art, the invention has the following beneficial effects:
1. the invention provides a preparation method of a compound based on a magnesium alloy three-in-one treating agent, which comprises the steps of preparing 1-3 parts by weight of isomeric alcohol polyoxyethylene ether and 1-3 parts by weight of EDTA-2Na, respectively pouring the isomeric alcohol polyoxyethylene ether and the EDTA-2Na into the same container, stirring and mixing, respectively pouring 8-12 parts by weight of citric acid, 13-18 parts by weight of sulfamic acid, 23-28 parts by weight of carboxyethylthiosuccinic acid and 7-12 parts by weight of methanesulfonic acid into the same container, stirring and mixing, preparing 100 parts by weight of water, pouring the raw materials prepared in the other two containers into a proportioning device filled with water, uniformly stirring, putting the magnesium alloy to be treated into the proportioned solution, observing the polishing treatment effect of the solution on the surface of the magnesium alloy, replacing 50 parts by weight of water, the steps are repeated again to carry out proportioning test, and the weight of the water is reduced by one half or increased by three halves by judging the polishing effect, so that the most accurate proportioning value is obtained.
2. The invention provides a preparation method of a compound based on a magnesium alloy three-in-one treating agent, which comprises the steps of pushing a connecting slide block to the right side position of a square through slide hole, screwing a threaded knob to fix the connecting slide block, clamping a short limiting slide block into a first clamping slide hole, separating a long limiting slide block from a second clamping slide hole, placing one end of a magnesium alloy to be tested between clamping blocks when an operator needs to test the compound in a proportioning device, screwing a double-threaded knob at the time, relatively moving the clamping blocks under the driving of the double-threaded knob so as to clamp the magnesium alloy, starting a motor by the operator, driving a clamping shaft to rotate by the motor, driving a clamping gear to rotate under the action of the short limiting slide block, driving a connecting gear to rotate by the clamping gear, and realizing the integral rotation of a long transmission shaft, at this moment, under the drive of drive belt, the puddler rotates to can stir the compound in the preparation box, this kind of setting not only operates convenient and fast, uses a motor to accomplish multiple effect simultaneously, and the structure sets up ingeniously, facilitates the use.
3. The invention provides a preparation method of a compound based on a magnesium alloy three-in-one treating agent, which comprises the steps of after the compound is stirred, turning off a motor, pushing a connecting slide block to the left position of a square through slide hole, screwing a threaded knob to fix the connecting slide block, separating a short limiting slide block from a first clamping slide hole, clamping a long limiting slide block into a second clamping slide hole, starting the motor, rotating a clamping shaft to drive a driving shaft main body to rotate, driving an H-shaped roller to rotate under the action of the long limiting slide block, paying off a connecting rope at the moment, continuously compressing a spring piece under the limiting action of a hollow disc, driving the magnesium alloy to move downwards by a clamping mechanism until the magnesium alloy moves into a preparation box, finishing paying off the connecting rope at the moment, turning off the motor, and starting the motor again after the reaction is finished, the motor drives the H-shaped roller to rotate, the connecting rope is reversely wound on the H-shaped roller at the moment, so that the magnesium alloy can be driven to move upwards through the clamping mechanism, the spring piece can be continuously compressed, when the large roller and the small roller are respectively contacted with the bottom surface of the trapezoidal sliding block, the magnesium alloy is taken out from the preparation box, at the moment, the clamping mechanism can slide forwards along the trapezoidal sliding block under the continuous driving of the connecting rope, so that the H-shaped roller can be driven to slide forwards together, until the magnesium alloy enters the cleaning box from the feeding opening, the anti-abrasion circular ring can be contacted with the extrusion convex column, when the H-shaped roller continues to move forwards, the air pressing piston can be driven to move forwards, so that the air in the inner cavity of the air pressing shell can be pressed into the pushing shell through the connecting pipeline, the pushing piston can be driven to move forwards in a reverse direction, the water pressing sealing gasket can extrude the water in the inner cavity of the water storage inner groove, make water accessible intercommunication bath inside groove and intercommunication inside groove spout from the shower nozzle, can realize the clearance to the magnesium alloy, this kind of setting not only makes a motor can accomplish a plurality of effects simultaneously, also makes a drive effect of motor simultaneously, can accomplish the effect of taking out magnesium alloy automatically, automatic shift and self-cleaning, and the structure sets up ingeniously, uses manpower sparingly, has made things convenient for the observation of operator to the test result.
4. According to the preparation method of the compound based on the magnesium alloy three-in-one treatment agent, when the H-shaped roller moves forwards, the ball is driven to move upwards in the inclined slideway, so that the extension spring is extended, after the washing is finished, the output end of the motor loses the limiting effect by turning off the motor, the device can enable the H-shaped roller to rotate reversely and reset under the elastic force action of the extension spring and the spring piece, so that the overall reset of the device can be realized, the structure is skillful, the device can automatically reset on the premise of finishing automatic taking out, automatic shifting and automatic cleaning of magnesium alloy, and the next use is facilitated.
Drawings
FIG. 1 is a flow chart of a preparation method of a compound of a magnesium alloy three-in-one treating agent of the invention;
FIG. 2 is a schematic view of the overall structure of the proportioning device of the present invention;
FIG. 3 is a cross-sectional view of the mounting base of the present invention;
FIG. 4 is a schematic plan view of the long drive shaft of the present invention;
FIG. 5 is a schematic perspective view of the motor of the present invention;
FIG. 6 is a schematic perspective view of a driving shaft according to the present invention;
FIG. 7 is an exploded view of the gear assembly of the present invention;
FIG. 8 is a schematic perspective view of an H-roll of the present invention;
FIG. 9 is a cross-sectional view of the reset mechanism of the present invention;
FIG. 10 is a perspective view of a T-shaped restriction block according to the present invention;
fig. 11 is a schematic perspective view of the gripping mechanism of the present invention;
FIG. 12 is a schematic plan view of a gripping member of the present invention;
FIG. 13 is a schematic perspective view of a trapezoidal slider according to the present invention;
FIG. 14 is a cross-sectional view of the pneumatic water-pressing assembly of the present invention.
In the figure: 1. installing a base; 11. an L-shaped mounting groove; 12. a water storage inner tank; 13. the inner groove is communicated; 14. a water inlet; 2. a concave mounting frame; 21. a concave through hole; 22. a square through sliding hole; 221. a side wall chute; 23. a trapezoidal slider; 231. a square stringing hole; 24. a T-shaped restriction block; 241. a bottom surface limiting chute; 242. inclining the slideway; 3. a motor; 31. clamping the shaft; 4. driving a shaft; 41. driving the limiting mechanism; 411. connecting the sliding block; 412. inserting a slider; 413. a threaded connection block; 414. a threaded knob; 415. a connecting sleeve; 42. a driving shaft main body; 421. a circular rotating shaft; 422. clamping the sliding chute; 423. a short limiting slider; 424. a long limiting slide block; 425. a restraining disk; 5. a stirring assembly; 51. a gear transmission mechanism; 511. connecting the circular rings; 512. hoisting the connecting block; 513. rotating the circular ring; 514. clamping a gear; 515. a first clamping slide hole; 52. a long transmission shaft; 521. a long drive shaft body; 522. a connecting gear; 523. a first connecting roller; 524. a transmission belt; 53. a stirring rod; 531. a stir bar body; 532. connecting a bearing; 533. a second connecting roller; 6. a lifting clamping assembly; 61. an H-shaped roller; 611. a second clamping sliding hole; 612. an anti-abrasion ring; 62. connecting ropes; 63. a reset mechanism; 631. a hollow disc; 632. a spring plate; 633. a connecting block is taken in; 634. a telescopic block; 635. an extension spring; 636. a ball bearing; 64. a gripping mechanism; 641. hoisting the mounting shell; 642. a large roller; 643. a small roller; 644. clamping and taking the workpiece; 6441. a double-threaded knob; 6442. a restraining bearing; 6443. a gripping block; 7. a pneumatic water pressurizing assembly; 71. a gas compressing mechanism; 711. a gas compressing casing; 712. a displacer; 713. extruding the convex column; 714. a one-way intake valve; 72. connecting a pipeline; 73. an air intake pushing mechanism; 731. advancing the housing; 732. air outlet and sealing; 733. a pusher piston; 734. a pressurized water sealing gasket; 8. preparing a box; 9. cleaning the box; 91. a feed opening; 92. a water outlet hole; 93. the flushing inner tank is communicated; 94. and (4) a spray head.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In order to solve the technical problems that not only the cost is consumed, but also the labor is consumed, the preparation period is long, and the accurate proportioning effect is difficult to find in the actual preparation, as shown in fig. 1, the following preferable technical scheme is provided:
the preparation method of the compound based on the magnesium alloy three-in-one treating agent comprises the following steps:
the method comprises the following steps: preparing a liquid raw material: preparing liquid raw materials in corresponding weight parts, respectively pouring the liquid raw materials into the same container, and stirring and mixing the liquid raw materials;
step two: preparing a solid raw material: preparing solid raw materials in corresponding weight parts, respectively pouring the solid raw materials into the same container, and stirring and mixing the solid raw materials;
step three: preparing a compound: preparing 300 parts by weight of water, pouring the water into a proportioning device, and respectively pouring the raw materials prepared in the other two containers into the proportioning device filled with the water;
step four: and (3) test observation: after uniformly stirring, putting the magnesium alloy to be treated into the proportioned solution, and observing the polishing treatment effect of the solution on the surface of the magnesium alloy;
step five: adjusting the water proportion: the proportioning test is carried out by replacing the weight part of the water with 150 parts of the water and repeating the steps, and the proportion of the weight part of the water is reduced by one half or increased by three halves by judging the polishing effect, so that the most accurate proportioning value is obtained.
Specifically, the preparation method can reduce the cost consumption, and meanwhile, the regular proportioning operation can save labor, shorten the preparation period, efficiently obtain an accurate preparation result and facilitate the use.
In the fifth step, the GU-M-025 magnesium alloy three-in-one treating agent is a compound of an inorganic acid agent, an inorganic complexing agent and an organic complexing agent and a surfactant. The weight percentage of the components is as follows:
in order to solve the technical problem of how to realize the stirring of the compound by using the motor 3, as shown in fig. 2-12, the following preferred technical solutions are provided:
proportioning device in S3 includes installation base 1 and the spill mounting bracket 2 of intercommunication fixed mounting at installation base 1 top surface middle part, fixed mounting has motor 3 on the upside outer wall of spill mounting bracket 2 one end, the middle part inner chamber of spill mounting bracket 2 slides and is provided with drive axle 4, be provided with stirring subassembly 5 in the one end inner chamber of installation base 1, it gets subassembly 6 to be provided with the lift clamp in the inner chamber of spill mounting bracket 2, and the lift clamp is got the upper end of subassembly 6 and is slided to cup joint on drive axle 4, install pneumatic pressurized-water subassembly 7 in the other end inner chamber of spill mounting bracket 2, and the lower extreme setting of pneumatic pressurized-water subassembly 7 is in the other end inner chamber of installation base 1, the top surface one end department embedding fixed mounting of installation base 1 has preparation box 8, the top surface other end department embedding fixed mounting of installation base 1 has washing box 9.
An L-shaped mounting groove 11 is arranged at one end of the top surface of the mounting base 1, the lower end part of the L-shaped mounting groove 11 is arranged below the preparation box 8, an inner water storage groove 12 is arranged in the lower inner cavity at the other end of the mounting base 1, a communicating inner groove 13 is arranged on the lower inner wall at one end of the inner cavity of the inner water storage groove 12, the inner water storage groove 12 is communicated with the cleaning box 9 through the communicating inner groove 13, a water inlet 14 is arranged on the outer wall at one side of the mounting base 1, the water inlet 14 is communicated with the inner water storage groove 12, a concave through hole 21 is arranged in the inner cavity of the concave mounting frame 2, one end part of the concave through hole 21 is communicated with one end part of the L-shaped mounting groove 11, a square through sliding hole 22 is arranged on the top surface of the middle part at one end of the concave mounting frame 2, a trapezoidal sliding block 23 is fixedly communicated with the bottom surface of the middle part of the concave mounting frame 2, and a T-shaped limiting block 24 is fixedly arranged on the top surface of the middle part of the concave mounting frame 2, the output end of the motor 3 is fixedly provided with a clamping shaft 31, the driving shaft 4 comprises a driving limiting mechanism 41 and a driving shaft main body 42 movably arranged in the lower end of the driving limiting mechanism 41 in a penetrating way, the stirring assembly 5 comprises a gear transmission mechanism 51 and a long transmission shaft 52 movably arranged in the inner cavity of the L-shaped mounting groove 11, the top surface of one end of the inner cavity of the L-shaped mounting groove 11 is movably provided with a stirring rod 53, the upper end of the stirring rod 53 is arranged in a sealing way and penetrates through the bottom surface of the preparation box 8, the lifting clamping assembly 6 comprises an H-shaped roller 61 and a reset mechanism 63 movably arranged at one end of the H-shaped roller 61, the H-shaped roller 61 is wound with a connecting rope 62, one end of the connecting rope 62 is fixedly connected on the outer wall of the H-shaped roller 61, the other end of the connecting rope 62 is fixedly connected on the top surface of the middle part of the clamping mechanism 64, the pneumatic water pressing assembly 7 comprises an air pressing mechanism 71 and a connecting pipeline 72 with one end communicated and arranged on the air pressing mechanism 71, an air inlet pushing mechanism 73 is fixedly installed on the inner wall of one end of the inner cavity of the water storage inner groove 12 in an embedded mode, the lower end of the connecting pipeline 72 penetrates through the concave through hole 21 and the top surface of the installation base 1 respectively and is communicated with the air inlet pushing mechanism 73 to be installed, a feeding opening 91 is formed in the outer wall of one end of the cleaning box 9, a water outlet hole 92 is formed in the inner wall of one side of the lower side of the cleaning box 9, a communicated water flushing inner groove 93 is formed in the inner cavity of the lower end of the cleaning box 9, the communicated water flushing inner groove 93 is communicated with the communicated inner groove 13, spray heads 94 are arranged on the inner wall of the inner cavity of the cleaning box 9 respectively, and the spray heads 94 are arranged at openings communicated with the water flushing inner groove 93 respectively.
The inner walls of two sides of the inner cavity of the concave through hole 21 are respectively provided with a side wall sliding groove 221, the middle part of the trapezoidal sliding block 23 is provided with a square rope threading hole 231, the middle part of the bottom surface of the T-shaped limiting block 24 is provided with a bottom surface limiting sliding groove 241, and the inner walls of the upper sides of two sides of the inner cavity of the bottom surface limiting sliding groove 241 are respectively provided with an inclined sliding way 242.
Drive limiting mechanism 41 including link block 411 and respectively fixed mounting insert slider 412 on link block 411 both sides middle part outer wall, insert slider 412 and slide and set up in lateral wall spout 221, fixed mounting has threaded connection piece 413 on the one side outer wall of link block 411 upside, and pass through threaded connection screw knob 414 on the threaded connection piece 413, the lower tip fixed mounting of link block 411 has connecting sleeve 415, it includes circular pivot 421 and the joint spout 422 of setting on circular pivot 421 one end middle part outer wall to drive axle main part 42, respectively fixed mounting has short limiting slide 423 on the both sides outer wall of circular pivot 421 one end, respectively fixed mounting has long limiting slide 424 on the both sides outer wall of the circular pivot 421 other end, another tip fixed mounting of circular pivot 421 has restriction disc 425, joint axle 31 slides and sets up in joint spout 422.
The gear transmission mechanism 51 comprises a hoisting connecting block 512 and a connecting ring 511 fixedly installed at the lower end of the hoisting connecting block 512, a rotating ring 513 is movably installed on the outer wall of one end of the connecting ring 511, a clamping gear 514 is fixedly installed on the outer wall of one end of the rotating ring 513, and a first clamping sliding hole 515 is formed in the middle of the clamping gear 514.
The long transmission shaft 52 comprises a long transmission shaft main body 521 and a connecting gear 522 fixedly mounted at the upper end part of the long transmission shaft main body 521, the connecting gear 522 is meshed with the clamping gear 514, a first connecting roller 523 is fixedly mounted at the lower end part of the long transmission shaft main body 521, a transmission belt 524 is sleeved on the first connecting roller 523, the stirring rod 53 comprises a stirring rod main body 531 and a connecting bearing 532 mounted on the top surface of the inner cavity of the L-shaped mounting groove 11, the stirring rod main body 531 is movably mounted on the connecting bearing 532, a second connecting roller 533 is fixedly mounted at the lower end part of the stirring rod main body 531, and the first connecting roller 523 is connected with the second connecting roller 533 through the transmission belt 524.
Specifically, the connecting slider 411 is pushed to the right side of the square through sliding hole 22, and the threaded knob 414 is screwed to fix the connecting slider, at this time, the short limiting slider 423 is clamped into the first clamping sliding hole 515, the long limiting slider 424 is separated from the second clamping sliding hole 611, when an operator needs to test a compound in the proportioning device, one end of the magnesium alloy to be tested can be placed between the clamping blocks 6443, at this time, the double threaded knob 6441 is screwed, the clamping blocks 6443 are moved relatively under the driving of the double threaded knob 6441 to clamp the magnesium alloy, at this time, the operator can start the motor 3, the motor 3 can drive the clamping shaft 31 to rotate, at this time, the clamping gear 514 can be driven to rotate under the action of the short limiting slider 423, the clamping gear 514 can drive the connecting gear 522 to rotate, and thus the whole rotation of the long transmission shaft 52 is realized, at this moment, under the drive of drive belt 524, puddler 53 rotates to can stir the compound in the preparation box 8, this kind of setting not only operates convenient and fast, uses a motor 3 to accomplish multiple effect simultaneously, and the structure sets up ingeniously, facilitates the use.
In order to solve the technical problems that the surface of the magnesium alloy after each test generates more foam coverage, the surface of the magnesium alloy usually needs to be manually cleaned to observe the polishing effect, the operation is very inconvenient, and the labor cost is increased, as shown in fig. 2 to 14, the following preferred technical solutions are provided:
be provided with second joint slide opening 611 on the middle part outer wall of H type roller 61 one end, H type roller 61's one end periphery embedding movable mounting has abrasionproof ring 612, canceling release mechanical system 63 includes hollow disc 631 and spring leaf 632 that one end was installed on hollow disc 631 inner chamber inner wall, and spring leaf 632's the other end fixed mounting is on H type roller 61's other end outer wall, fixed mounting has income connecting block 633 on the middle part top surface of hollow disc 631, and through extension spring 635 slidable mounting have flexible piece 634 in the inner chamber of income connecting block 633, and movable mounting has ball 636 respectively on the both sides outer wall of flexible piece 634 upper end, and ball 636 sets up in inclined slide 242.
The clamping mechanism 64 comprises a hoisting installation shell 641 and large rollers 642 respectively embedded and movably installed at two sides of one end of the top surface of the hoisting installation shell 641, small rollers 643 are respectively movably installed at two sides of the other end of the top surface of the hoisting installation shell 641, a clamping part 644 is installed in an inner cavity of the hoisting installation shell 641, the clamping part 644 comprises a double-thread knob 6441 and a limiting bearing 6442 embedded and installed on the outer wall of the middle part of one side of the hoisting installation shell 641, clamping blocks 6443 are respectively arranged in the inner cavities of the lower sides of two ends of the hoisting installation shell 641 in a sliding mode, and the upper ends of the clamping blocks 6443 are respectively sleeved at the output end and the output end of the double-thread knob 6441 through threads.
The air compressing mechanism 71 comprises an air compressing shell 711 and an air compressing piston 712, one end of the air compressing piston is arranged in the inner cavity of the air compressing shell 711 in a sealing and sliding mode through an extruding spring 714, extruding convex columns 713 are fixedly installed on the outer walls of the upper side and the lower side of the outer end portion of the air compressing piston 712 respectively, and a one-way air inlet valve 714 is arranged on the outer wall of the air compressing shell 711.
The air inlet pushing mechanism 73 comprises a pushing shell 731 and a pushing piston 733 with one end hermetically and slidably arranged in the inner cavity of the pushing shell 731, wherein a pressurized water sealing pad 734 is fixedly arranged at one end of the pushing piston 733, the pressurized water sealing pad 734 is hermetically and slidably arranged in the water storage inner tank 12, and an air outlet sealing opening 732 is communicated with the other end of the pushing shell 731.
Specifically, after the compound is stirred, the motor 3 is turned off, the connecting slider 411 is pushed to the left position of the square through sliding hole 22, the threaded knob 414 is screwed to fix the compound, the short limiting slider 423 is separated from the first clamping sliding hole 515, the long limiting slider 424 is clamped into the second clamping sliding hole 611, the motor 3 is started, the clamping shaft 31 rotates to drive the driving shaft main body 42 to rotate, the H-shaped roller 61 is driven to rotate under the action of the long limiting slider 424, the connecting rope 62 performs paying-off, the spring leaf 632 is continuously compressed under the limiting action of the hollow disc 631, the clamping mechanism 64 drives the magnesium alloy to move downwards until the magnesium alloy moves into the preparation box 8, the connecting rope 62 performs paying-off, the motor 3 is turned off, and after the reaction is finished, the motor 3 is turned on again, the motor 3 drives the H-roller 61 to rotate again, at this time, the connecting rope 62 is reversely wound on the H-roller 61, so that the magnesium alloy can be driven by the clamping mechanism 64 to move upwards, the spring leaf 632 can be continuously compressed, when the large roller 642 and the small roller 643 respectively contact the bottom surface of the trapezoidal sliding block 23, the magnesium alloy is taken out from the preparation box 8, at this time, the clamping mechanism 64 can slide forwards along the trapezoidal sliding block 23 under the continuous driving of the connecting rope 62, so that the H-roller 61 can be driven to slide forwards together until the magnesium alloy enters the cleaning box 9 from the feeding opening 91, at this time, the anti-wear ring 612 can contact the extrusion protrusion 713, when the H-roller 61 continues to move forwards, the air pressing piston 712 can be driven to move forwards, so that the air in the cavity of the air pressing housing 711 can be pressed into the pushing housing 731 through the connecting pipe 72, so that the pushing piston 733 can be driven to move forwards in a reverse direction, the pressurized-water sealed pad 734 can extrude the water in the inner cavity of the water storage inner groove 12, so that the water can be sprayed out from the spray head 94 through the communication flushing inner groove 93 and the communication inner groove 13, the magnesium alloy can be cleaned, the arrangement not only enables one motor 3 to simultaneously complete a plurality of effects, but also enables one driving effect of the motor 3, the magnesium alloy can be automatically taken out, the automatic displacement and automatic cleaning effects are achieved, the structure is ingenious, the labor is saved, and the operator can conveniently observe the test result.
Further, when H type roller 61 moves forward, then can drive ball 636 rebound in slope slide 242, thereby make extension spring 635 stretched, after washing, through closing motor 3, the output of motor 3 loses the limiting displacement, the device can be under extension spring 635 and spring leaf 632's elastic force effect, make H type roller 61 reverse and reset, thereby can realize the whole of device resets, the structure sets up ingeniously, accomplish to take out magnesium alloy is automatic, under automatic shift and self-cleaning's the prerequisite, still can realize the device automatically and reset, be convenient for use next time.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (10)
1. The preparation method of the compound based on the magnesium alloy three-in-one treating agent is characterized by comprising the following steps:
s1: preparing a liquid raw material: preparing liquid raw materials in corresponding weight parts, respectively pouring the liquid raw materials into the same container, and stirring and mixing the liquid raw materials;
s2: preparing a solid raw material: preparing solid raw materials in corresponding weight parts, respectively pouring the solid raw materials into the same container, and stirring and mixing the solid raw materials;
s3: preparing a compound: preparing 300 parts by weight of water, pouring the water into a proportioning device, and respectively pouring the raw materials prepared in the other two containers into the proportioning device filled with the water;
s4: and (3) test observation: after uniformly stirring, putting the magnesium alloy to be treated into the proportioned solution, and observing the polishing treatment effect of the solution on the surface of the magnesium alloy;
s5: adjusting the water proportion: the proportioning test is carried out by replacing the weight part of the water with 150 parts of the water and repeating the steps, and the proportion of the weight part of the water is reduced by one half or increased by three halves by judging the polishing effect, so that the most accurate proportioning value is obtained.
2. The preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 1, is characterized in that: in S5, the GU-M-025 magnesium alloy three-in-one treating agent is a compound of an inorganic acid agent, an inorganic complexing agent and an organic complexing agent and a surfactant. The weight percentage of the components is as follows:
3. the preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 1, is characterized in that: the proportioning device in the S3 comprises a mounting base (1) and a concave mounting frame (2) which is communicated and fixedly mounted in the middle of the top surface of the mounting base (1), wherein a motor (3) is fixedly mounted on the outer wall of the upper side of one end of the concave mounting frame (2), a driving shaft (4) is slidably arranged in the middle inner cavity of the concave mounting frame (2), a stirring assembly (5) is arranged in the inner cavity of one end of the mounting base (1), a lifting clamping assembly (6) is arranged in the inner cavity of the concave mounting frame (2), the upper end of the lifting clamping assembly (6) is slidably sleeved on the driving shaft (4), a pneumatic water pressing assembly (7) is mounted in the inner cavity of the other end of the concave mounting frame (2), the lower end of the pneumatic water pressing assembly (7) is arranged in the inner cavity of the other end of the mounting base (1), and a preparation box (8) is fixedly mounted at one end of the top surface of the mounting base (1) in an embedded mode, a cleaning box (9) is embedded and fixedly arranged at the other end of the top surface of the mounting base (1);
an L-shaped mounting groove (11) is formed in one end of the top surface of the mounting base (1), the lower end of the L-shaped mounting groove (11) is arranged below the preparation box (8), an inner water storage groove (12) is formed in an inner cavity of the lower side of the other end of the mounting base (1), an inner communication groove (13) is formed in the inner wall of the lower side of one end of the inner cavity of the inner water storage groove (12), the inner water storage groove (12) is communicated with the cleaning box (9) through the inner communication groove (13), a water inlet (14) is formed in the outer wall of one side of the mounting base (1), and the water inlet (14) is communicated with the inner water storage groove (12);
a concave through hole (21) is formed in the inner cavity of the concave mounting frame (2), one end of the concave through hole (21) is communicated with one end of the L-shaped mounting groove (11), a square through sliding hole (22) is formed in the top surface of the middle of one end of the concave mounting frame (2), a trapezoidal sliding block (23) is fixedly communicated with the bottom surface of the middle of the concave mounting frame (2), and a T-shaped limiting block (24) is fixedly communicated with the top surface of the middle of the concave mounting frame (2);
the tail end of the output of the motor (3) is fixedly provided with a clamping shaft (31);
the driving shaft (4) comprises a driving limiting mechanism (41) and a driving shaft main body (42) which is movably arranged at the lower end of the driving limiting mechanism (41) in a penetrating way;
the stirring assembly (5) comprises a gear transmission mechanism (51) and a long transmission shaft (52) which is movably arranged in the inner cavity of the L-shaped mounting groove (11), a stirring rod (53) is movably arranged on the top surface of one end of the inner cavity of the L-shaped mounting groove (11), and the upper end of the stirring rod (53) penetrates through the bottom surface of the preparation box (8) in a sealing manner;
the lifting clamping assembly (6) comprises an H-shaped roller (61) and a reset mechanism (63) movably mounted at one end of the H-shaped roller (61), a connecting rope (62) is wound on the H-shaped roller (61), one end of the connecting rope (62) is fixedly connected to the outer wall of the H-shaped roller (61), and the other end of the connecting rope (62) is fixedly connected to the top surface of the middle part of the clamping mechanism (64);
the pneumatic water pressurizing assembly (7) comprises an air compressing mechanism (71) and a connecting pipeline (72) with one end communicated and installed on the air compressing mechanism (71), an air inlet pushing mechanism (73) is embedded and fixedly installed on the inner wall of one end of the inner cavity of the water storage inner groove (12), and the lower end of the connecting pipeline (72) penetrates through the concave through hole (21) and the top surface of the installation base (1) to be communicated and installed with the air inlet pushing mechanism (73);
a feeding opening (91) is formed in the outer wall of one end of the cleaning box (9), a water outlet hole (92) is formed in the inner wall of one side of the lower side of the cleaning box (9), a communicated flushing inner groove (93) is formed in the inner cavity of the lower end of the cleaning box (9), the communicated flushing inner groove (93) is communicated with the communicated inner groove (13), spray heads (94) are respectively arranged on the inner wall of the inner cavity of the cleaning box (9), and the spray heads (94) are respectively arranged at the openings of the communicated flushing inner grooves (93);
the inner walls of two sides of the inner cavity of the concave through hole (21) are respectively provided with a side wall sliding groove (221), the middle part of the trapezoidal sliding block (23) is provided with a square rope threading hole (231), the middle part of the bottom surface of the T-shaped limiting block (24) is provided with a bottom surface limiting sliding groove (241), and the inner walls of the upper sides of two sides of the inner cavity of the bottom surface limiting sliding groove (241) are respectively provided with an inclined sliding way (242).
4. The preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 3, is characterized in that: the driving limiting mechanism (41) comprises a connecting slide block (411) and inserting slide blocks (412) which are respectively and fixedly installed on the outer walls of the middle parts of the two sides of the connecting slide block (411), the inserting slide blocks (412) are arranged in side wall sliding grooves (221) in a sliding mode, a threaded connecting block (413) is fixedly installed on the outer wall of one side of the upper side of the connecting slide block (411), a threaded knob (414) penetrates through the threaded connecting block (413) through threads, a connecting sleeve (415) is fixedly installed at the lower end part of the connecting slide block (411), a driving shaft main body (42) comprises a circular rotating shaft (421) and a clamping sliding groove (422) arranged on the outer wall of the middle part of one end part of the circular rotating shaft (421), short limiting slide blocks (423) are respectively and fixedly installed on the outer walls of the two sides of one end of the circular rotating shaft (421), long limiting slide blocks (424) are respectively and fixedly installed on the outer walls of the two sides of the other end of the circular rotating shaft (421), the other end of the round rotating shaft (421) is fixedly provided with a limiting disc (425), and the clamping shaft (31) is arranged in the clamping sliding groove (422) in a sliding mode.
5. The preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 4, is characterized in that: the gear transmission mechanism (51) comprises a hoisting connecting block (512) and a connecting ring (511) fixedly installed at the lower end of the hoisting connecting block (512), a rotating ring (513) is movably installed on the outer wall of one end of the connecting ring (511), a clamping gear (514) is fixedly installed on the outer wall of one end of the rotating ring (513), and a first clamping sliding hole (515) is formed in the middle of the clamping gear (514).
6. The preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 5, is characterized in that: long transmission shaft (52) include long transmission shaft main part (521) and connection gear (522) of fixed mounting in long transmission shaft main part (521) upper end, it is connected to mesh between connection gear (522) and joint gear (514), the lower tip fixed mounting of long transmission shaft main part (521) has first connecting roller (523), and cup jointed drive belt (524) on first connecting roller (523), puddler (53) include puddler main part (531) and install connection bearing (532) on L type mounting groove (11) inner chamber top surface, and puddler main part (531) movable mounting is on connecting bearing (532), the lower tip fixed mounting of puddler main part (531) has second connecting roller (533), and be connected through drive belt (524) between first connecting roller (523) and the second connecting roller (533).
7. The preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 6, is characterized in that: be provided with second joint slide opening (611) on the middle part outer wall of H type roller (61) one end, the one end periphery embedding movable mounting of H type roller (61) has abrasionproof ring (612), canceling release mechanical system (63) include spring leaf (632) that hollow disc (631) and one end were installed on hollow disc (631) inner chamber inner wall, and the other end fixed mounting of spring leaf (632) is on the other end outer wall of H type roller (61), fixed mounting has income connecting block (633) on the middle part top surface of hollow disc (631), and through extension spring (635) slidable mounting have flexible piece (634) in the inner chamber of income connecting block (633), and movable mounting has ball (636) respectively on the both sides outer wall of flexible piece (634) upper end, and ball (636) set up in slope slide (242).
8. The preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 7, is characterized in that: the clamping mechanism (64) comprises a hoisting installation shell (641) and large rollers (642) which are respectively embedded into two sides of one end of the top surface of the hoisting installation shell (641) in a movable mode, small rollers (643) are respectively and movably installed at two sides of the other end of the top surface of the hoisting installation shell (641), clamping pieces (644) are installed in inner cavities of the hoisting installation shell (641), each clamping piece (644) comprises a double-thread knob (6441) and a limiting bearing (6442) which is embedded into the outer wall of the middle portion of one side of the hoisting installation shell (641), clamping blocks (6443) are respectively arranged in the inner cavities of the lower sides of the two ends of the hoisting installation shell (641) in a sliding mode, and the upper ends of the clamping blocks (6443) are respectively sleeved on the output end and the output end of the double-thread knob (6441) in a sleeved mode.
9. The preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 8, is characterized in that: the air compressing mechanism (71) comprises an air compressing shell (711) and an air compressing piston (712) with one end arranged in the inner cavity of the air compressing shell (711) in a sealing and sliding mode through an extruding spring (714), extruding protruding columns (713) are fixedly arranged on the outer walls of the upper side and the lower side of the outer end of the air compressing piston (712) respectively, and a one-way air inlet valve (714) is arranged on the outer wall of the air compressing shell (711).
10. The preparation method of the compound based on the magnesium alloy three-in-one treatment agent, according to claim 9, is characterized in that: the air inlet pushing mechanism (73) comprises a pushing shell (731) and a pushing piston (733) with one end arranged in the inner cavity of the pushing shell (731) in a sealing and sliding mode, a water pressing sealing gasket (734) is fixedly installed at one end of the pushing piston (733), the water pressing sealing gasket (734) is arranged in the water storage inner groove (12) in a sealing and sliding mode, and an air outlet sealing opening (732) is arranged at the other end of the pushing shell (731) in a communicated mode.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104498967A (en) * | 2014-12-31 | 2015-04-08 | 苏州禾川化学技术服务有限公司 | Multifunctional aluminum material corrosion-inhibition polishing pickling agent |
| CN105233732A (en) * | 2015-11-13 | 2016-01-13 | 重庆索利特涂料有限公司 | Stepless speed change stirring machine |
| CN106198161A (en) * | 2016-06-24 | 2016-12-07 | 北京北冶功能材料有限公司 | A kind of metallographic sample chemical polishing soln and using method thereof |
| CN209663861U (en) * | 2019-03-11 | 2019-11-22 | 兰州兰生血液制品有限公司 | A kind of blood product rubber plug cleaning device |
| CN209810737U (en) * | 2019-03-28 | 2019-12-20 | 嘉兴市丽彩佳五金有限公司 | Combined type automobile accessory cleaning machine |
| WO2020119779A1 (en) * | 2018-12-14 | 2020-06-18 | 大连理工大学 | Semiconductor wafer photoelectrochemical mechanical polishing processing device and processing method |
| CN215877436U (en) * | 2021-08-06 | 2022-02-22 | 上海振戈金属材料有限公司 | Polishing solution mixer for stainless steel processing |
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2022
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| CN104498967A (en) * | 2014-12-31 | 2015-04-08 | 苏州禾川化学技术服务有限公司 | Multifunctional aluminum material corrosion-inhibition polishing pickling agent |
| CN105233732A (en) * | 2015-11-13 | 2016-01-13 | 重庆索利特涂料有限公司 | Stepless speed change stirring machine |
| CN106198161A (en) * | 2016-06-24 | 2016-12-07 | 北京北冶功能材料有限公司 | A kind of metallographic sample chemical polishing soln and using method thereof |
| WO2020119779A1 (en) * | 2018-12-14 | 2020-06-18 | 大连理工大学 | Semiconductor wafer photoelectrochemical mechanical polishing processing device and processing method |
| CN209663861U (en) * | 2019-03-11 | 2019-11-22 | 兰州兰生血液制品有限公司 | A kind of blood product rubber plug cleaning device |
| CN209810737U (en) * | 2019-03-28 | 2019-12-20 | 嘉兴市丽彩佳五金有限公司 | Combined type automobile accessory cleaning machine |
| CN215877436U (en) * | 2021-08-06 | 2022-02-22 | 上海振戈金属材料有限公司 | Polishing solution mixer for stainless steel processing |
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