CN114405279A - Membrane separation lab scale equipment - Google Patents

Membrane separation lab scale equipment Download PDF

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Publication number
CN114405279A
CN114405279A CN202111606184.2A CN202111606184A CN114405279A CN 114405279 A CN114405279 A CN 114405279A CN 202111606184 A CN202111606184 A CN 202111606184A CN 114405279 A CN114405279 A CN 114405279A
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CN
China
Prior art keywords
liquid
membrane separation
filtered
membrane
control valve
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202111606184.2A
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Chinese (zh)
Inventor
李向东
贾赟
吕磊
郑家伟
朗东东
李仅高
孙禹
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guizhou Institute of Technology
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Guizhou Institute of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guizhou Institute of Technology filed Critical Guizhou Institute of Technology
Priority to CN202111606184.2A priority Critical patent/CN114405279A/en
Publication of CN114405279A publication Critical patent/CN114405279A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2311/00Details relating to membrane separation process operations and control
    • B01D2311/16Flow or flux control
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2311/00Details relating to membrane separation process operations and control
    • B01D2311/22Details relating to membrane separation process operations and control characterised by a specific duration or time
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2311/00Details relating to membrane separation process operations and control
    • B01D2311/25Recirculation, recycling or bypass, e.g. recirculation of concentrate into the feed

Abstract

The invention discloses a membrane separation small test device, which relates to the technical field of membrane separation and comprises a case, wherein a pressure pump, a switch and a control valve which are mutually connected through a guide pipe are arranged in the case, the control valve is connected with a control panel, the control valve is connected with a roll-type membrane, the roll-type membrane is connected with the pressure pump, a feed inlet and a discharge outlet are formed in the case, a power supply and a pipeline are connected, the control panel power supply is switched on, a filtration mode and a flow rate are selected on the control panel power supply, the filtration process is that liquid is pumped in by a pump, then the liquid is pumped into the membrane by the pump to be filtered, then the position of the valve is reached, the filtered liquid can be directly filtered or filtered again, the directly filtered liquid directly enters a filtration finished liquid tank, and the liquid filtered again flows into a pump inlet liquid tank.

Description

Membrane separation lab scale equipment
Technical Field
The invention relates to the technical field of membrane separation, in particular to a small-scale membrane separation device.
Background
The membrane separation technology has the functions of separation, concentration, purification and refining, and has the characteristics of high efficiency, energy conservation, environmental protection, simple molecular filtration and filtration process, easy control and the like. Therefore, the membrane separation technology has been widely applied to the fields of food, medicine, biology, environmental protection, chemical industry, metallurgy, energy, petroleum, water treatment, electronics, bionics and the like, generates great economic benefits and social benefits, and becomes one of the most important means in the separation science at present. The membrane separation phenomenon is widely present in nature, particularly in living bodies, but human recognition and research thereof has passed a long and tortuous path. Engineering applications of membrane separation technology were started from desalination of sea water in the 60's of the 20 th century-1960) professor lobbies and sorilagin made the first high flux and high salt rejection cellulose acetate paper membranes with a symmetric structure, from which reverse osmosis was moved from laboratory to industrial use. Then various novel membranes are successively appeared, and in 1967, DuPont company in the United states firstly develops a hollow fiber membrane component taking nylon-66 as a membrane material; in 1970, a Pemiasep B-9 hollow fiber membrane module with aromatic polyamide as a membrane material was developed, and the highest prize of the chemical engineering of CockParteick in 1971 was obtained. From this reverse osmosis technology, there has been a rapid development in the united states and subsequent use throughout the world. Meanwhile, microfiltration and ultrafiltration technologies are also developed correspondingly. The membrane separation technology can be applied to the fields of food, medicine, biology, environmental protection, chemical industry, metallurgy, energy, petroleum, water treatment, electronics, bionics and the like, and particularly, the ultrafiltration ceramic membrane is applied to various industries, such as heavy metal wastewater treatment and recovery. The existing traditional membrane separation technology equipment can cause that the purity cannot meet the requirement when certain fine materials are separated, thereby affecting the quality. Due to state of the art limitations, inorganic membranes are mainly only microfiltration and ultrafiltration grade membranes, mainly ceramic and metal membranes.
Disclosure of Invention
The invention aims to solve the technical problem of providing a membrane separation small test device which has a multifunctional effect by adopting a single chip microcomputer, is simple and convenient to use and has strong practicability in the field of laboratories.
In order to achieve the above purpose, the present invention provides the following technical solutions:
this membrane separation lab scale equipment includes quick-witted case, quick-witted case internally mounted has the force pump through pipe interconnect, a switch, control flap is connected with control panel, control flap is connected with a roll membrane, a roll membrane is connected with the force pump, it has the business turn over material mouth to open on the quick-witted case, connect power and pipe pipeline, open control panel power, select filtration mode and flow on it, the filtration flow is force pump suction liquid, then liquid filters through the force pump suction roll membrane, then reach the control flap position, filterable liquid can directly filter, also can filter once more, the direct entering that the direct filtration was accomplished filters and accomplishes the liquid tank, filterable liquid flow inlet pump liquid tank once more.
Preferably, a flow meter is mounted on the conduit.
Preferably, the control panel is a single chip microcomputer.
The beneficial effect of adopting above technical scheme is:
1. reducing the use amount of a separation filling medium by 50-90%;
2. the yield and the product purity are improved, and the stability of the components and the concentration of the product can be maintained.
3. The dosage of the chemical medicine and the eluent is 30 to 65 percent,
4. the discharge amount of the discharged water is reduced by 30-85%.
5. The system is easy to match with other devices, and is simple and convenient to operate and control. .
Drawings
The following describes embodiments of the present invention in further detail with reference to the accompanying drawings.
FIG. 1 is a schematic diagram of a membrane separation bench of the present invention;
FIG. 2 is a schematic diagram of the structure of a membrane separation chamber of the present invention.
Wherein, 1-case, 2-roll film, 3-control panel, 4-pressure pump, 5-switch, 6-control valve, 7-charging and discharging port.
Detailed Description
Preferred embodiments of the membrane separation chamber of the present invention will be described in detail below with reference to the accompanying drawings.
Figures 1 and 2 show a specific embodiment of the membrane separation pilot plant of the present invention:
as shown in FIG. 2, the membrane separation pilot plant comprises a case 1, a pressure pump 4, a switch 5 and a control valve 6 which are connected with each other through a conduit are arranged in the case 1, and a flow meter is arranged on the conduit. Control valve 6 is connected with control panel 3, and control panel 3 is the singlechip, and the singlechip has: timing filtering, quantitative filtering, real-time real flow, manual mode, automatic mode, single filtering and circulating filtering. The valve can control whether the filtered liquid is filtered again, and the inside of the valve is equivalent to a three-way port. The control valve 6 is connected with the roll-type membrane 2, the roll-type membrane 2 is connected with the pressure pump 4, and the case 1 is provided with a feed inlet and a discharge outlet 7.
As shown in figure 1, when in use, a power supply and a conduit pipeline are connected, a control panel 3 is powered on, a filtering mode and flow can be selected on the power supply, and the selective control can be carried out on timing filtering, quantitative filtering, real-time flow, manual mode, automatic mode, single filtering and circulating filtering. The filtration process is that force pump 4 pumps into liquid, then liquid filters through force pump 4 pump suction spiral-wound membrane 2, then arrives control valve 6 position, and filterable liquid can directly filter, also can filter once more, directly gets into the filtration completion liquid case that directly filters the completion, and the liquid flow that filters once more gets into pump liquid case.
The membrane separation lab scale has a multifunctional effect by adopting the single chip microcomputer, is simple and convenient to use, and has strong practicability in the field of laboratories.
The above is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, many variations and modifications can be made without departing from the inventive concept of the present invention, which falls into the protection scope of the present invention.

Claims (3)

1. A membrane separation bench test device, its characterized in that: the membrane separation small test device comprises a case (1), a pressure pump (4), a switch (5) and a control valve (6) which are connected with each other through a guide pipe are arranged in the case (1), the control valve (6) is connected with a control panel (3), the control valve (6) is connected with a roll-type membrane (2), the roll-type membrane (2) is connected with the pressure pump (4), a feeding and discharging port (7) is arranged on the case (1), a power supply and a guide pipe pipeline are connected, the power supply of the control panel (3) is opened, the filtration mode and the flow rate are selected, the filtration process is that the pressure pump (4) pumps in liquid, then the liquid is pumped into the roll-type membrane (2) by a pressure pump (4) for filtration, and then the position of the control valve (6) is reached, the filtered liquid can be directly filtered or can be filtered again, the directly filtered liquid directly enters a filtering liquid tank, and the re-filtered liquid flows into a pump liquid tank.
2. A membrane separation cartridge according to claim 1, wherein: the conduit is provided with a flow meter.
3. A membrane separation cartridge according to claim 1, wherein: the control panel (3) is a singlechip.
CN202111606184.2A 2021-12-23 2021-12-23 Membrane separation lab scale equipment Pending CN114405279A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111606184.2A CN114405279A (en) 2021-12-23 2021-12-23 Membrane separation lab scale equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111606184.2A CN114405279A (en) 2021-12-23 2021-12-23 Membrane separation lab scale equipment

Publications (1)

Publication Number Publication Date
CN114405279A true CN114405279A (en) 2022-04-29

Family

ID=81269767

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111606184.2A Pending CN114405279A (en) 2021-12-23 2021-12-23 Membrane separation lab scale equipment

Country Status (1)

Country Link
CN (1) CN114405279A (en)

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