CN114380449B - Device is destroyed to sesame essence medicine raffinate based on oxidation incineration method - Google Patents

Device is destroyed to sesame essence medicine raffinate based on oxidation incineration method Download PDF

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Publication number
CN114380449B
CN114380449B CN202210091367.3A CN202210091367A CN114380449B CN 114380449 B CN114380449 B CN 114380449B CN 202210091367 A CN202210091367 A CN 202210091367A CN 114380449 B CN114380449 B CN 114380449B
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pipe
waste gas
liquid
incineration method
residue
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CN114380449A (en
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赵超
张洪平
陈然
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Haining Tianzong Electronic Technology Co ltd
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Haining Tianzong Electronic Technology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/02Treatment of water, waste water, or sewage by heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/10Particle separators, e.g. dust precipitators, using filter plates, sheets or pads having plane surfaces
    • B01D46/12Particle separators, e.g. dust precipitators, using filter plates, sheets or pads having plane surfaces in multiple arrangements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/81Solid phase processes
    • B01D53/82Solid phase processes with stationary reactants
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/72Treatment of water, waste water, or sewage by oxidation
    • C02F1/78Treatment of water, waste water, or sewage by oxidation with ozone
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2251/00Reactants
    • B01D2251/30Alkali metal compounds
    • B01D2251/304Alkali metal compounds of sodium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2251/00Reactants
    • B01D2251/60Inorganic bases or salts
    • B01D2251/604Hydroxides
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/02Non-contaminated water, e.g. for industrial water supply
    • C02F2103/026Treating water for medical or cosmetic purposes

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Water Supply & Treatment (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Hydrology & Water Resources (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Treating Waste Gases (AREA)

Abstract

The invention discloses a device for destroying a residue liquid of a refined sesame seed medicine based on an oxidation incineration method. The device comprises a liquid storage tank, wherein the top of the liquid storage tank is communicated with the outside through a liquid inlet pipe, and the bottom of the liquid storage tank is connected with an atomizer through a liquid delivery pipe. The bottom of the atomizer is connected with the mist feeding pipe. The left side of the fog delivering pipe is connected with the glass cavity, and the bottom is connected with the inlet of the reaction pipe. The bottom of the glass cavity is provided with a fan and an ozone generator, and the ozone generator is arranged at the air outlet of the fan. The reaction tube is internally provided with a heating rod, the outer wall surface of the bottom end is provided with a semiconductor cooling fin, and the outlet is connected with the waste gas absorption chamber I. The first waste gas absorbing chamber is connected with the second waste gas absorbing chamber through a first return pipe, and the second waste gas absorbing chamber is connected with the glass cavity through a second return pipe. The invention adopts the design of a closed loop, ensures that the residual liquid of the refined drugs is completely destroyed in the device, and the generated waste gas is absorbed by the waste gas absorbing chamber without discharging harmful gas, thereby ensuring the safety of surrounding personnel and being applicable to the destruction of the residual liquid of the refined drugs on the indoor site.

Description

Device is destroyed to sesame essence medicine raffinate based on oxidation incineration method
Technical Field
The invention relates to the technical field of medical equipment, in particular to a device for destroying a sesame seed essence medicine residual liquid based on an oxidation incineration method.
Background
The use of the leprosy medicine promotes the development of the medical operation industry to a certain extent, but the powerful dependence and hazard of the leprosy medicine make the national importance of the management and destruction of the leprosy medicine. At present, the method of managing, uniformly recovering and intensively treating the raffinate of the refined drugs in special personnel is mainly adopted for destroying the raffinate of the refined drugs in China. However, this mode has unavoidable vulnerabilities in management due to its lengthy time period and links.
The method has the advantages that the harmless treatment and destruction are carried out on the residue liquid of the refined drugs on site in the drug use site, so that the problems existing in the existing destruction mode can be effectively solved. However, at present, in the aspect of on-site destruction of the residue liquid of the refined drugs in China, an effective harmless treatment method and an effective harmless treatment device are still lacking.
Disclosure of Invention
The invention aims to fill the defect of the existing mechanism for using the refined drugs in a field destruction method, and provides a device for destroying the refined drugs residual liquid based on an oxidation incineration method.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
the device comprises a liquid storage tank, wherein the top of the liquid storage tank is communicated with the outside through a liquid inlet pipe, and the bottom of the liquid storage tank is connected with an atomizer through a liquid conveying pipe. The peristaltic pump is arranged at the middle section of the infusion tube. The bottom of the atomizer is connected with the mist feeding pipe. The left side of the fog delivering pipe is connected with the glass cavity, and the bottom of the fog delivering pipe is connected with the inlet of the reaction pipe. The bottom of the glass cavity is provided with a fan and an ozone generator, and the ozone generator is arranged at the air outlet of the fan. The reaction tube is internally provided with a heating rod, the outer wall surface of the bottom end is provided with a semiconductor cooling fin, and the outlet is connected with the waste gas absorption chamber I. The first waste gas absorption chamber is connected with the second waste gas absorption chamber through a first return pipe, and the second waste gas absorption chamber is connected with the glass cavity through a second return pipe.
Preferably, the inlet of the liquid inlet pipe is funnel-shaped, and a filter screen is arranged in the liquid inlet pipe.
Preferably, the fog delivering pipe adopts a quartz glass pipe, adopts a T-shaped structure, an upper port is connected with the atomizer, a lower port is connected with the reaction pipe, and a left port is connected with the glass cavity. The surface of the mist delivery pipe is subjected to hydrophobic treatment, and micro-nano liquid drops cannot be gathered on the wall surface of the mist delivery pipe.
Preferably, the reaction tube adopts an alloy tube with high strength and high temperature resistance, and adopts an S-shaped structure.
Preferably, the heater adopts PTC ceramic heating rods, is arranged in the reaction tube, and is used for constant-temperature heating.
Preferably, the waste gas absorbing chamber is filled with solid sodium hydroxide.
Preferably, the waste gas absorbing chamber II is filled with active carbon, and a filter screen is arranged at the joint of the waste gas absorbing chamber II and the return pipe I.
Preferably, a temperature thermocouple is arranged in the second return pipe, the temperature thermocouple is connected with a temperature controller, and the temperature of gas in the second return pipe is detected.
Preferably, the temperature controller is connected with the temperature thermocouple and the semiconductor cooling fin, and when the temperature thermocouple detects that the temperature of the gas in the second return pipe is higher than a set value, the temperature controller controls the semiconductor cooling fin to start so as to cool the gas in the reaction pipe.
Compared with the prior art, the invention has the beneficial effects that:
the invention adopts the design of a closed loop, ensures that the residue liquid of the refined drugs is completely destroyed in the device, and the generated waste gas is absorbed by the waste gas absorbing chamber without discharging harmful gas, thereby ensuring the safety of surrounding personnel and being applicable to the destruction of drugs on the indoor site.
According to the invention, the sesame essence medicine residual liquid is atomized into micro-nano liquid drops through the atomizer, and the medicine reaction rate and the treatment efficiency are improved by combining a constant temperature heating technology, so that the quick and effective irreversible destruction of the sesame essence medicine residual liquid is realized.
The temperature controller, the temperature thermocouple and the semiconductor cooling fin maintain the constant temperature in the device, so that damage to an instrument caused by overhigh temperature is prevented, and the safety is high.
Drawings
Fig. 1 is a schematic structural diagram of a destroying device according to the present invention.
Fig. 2 is a cross-sectional view of a tank of the destruction device according to the present invention.
Fig. 3 is a cross-sectional view of the second exhaust gas absorbing chamber of the destruction device according to the present invention.
In the drawings, the list of components represented by the various numbers is as follows:
1. a blower; 2. an ozone generator; 3. a glass chamber; 4. a liquid storage tank; 41. a liquid inlet pipe; 42. a first filter screen; 43. an infusion tube; 5. a peristaltic pump; 6. an atomizer; 7. a spray head; 8. a mist delivery pipe; 9. a reaction tube; 10. a heating rod; 11. a semiconductor cooling fin; 12. a temperature controller; 13. an exhaust gas absorption chamber I; 14. An exhaust gas absorption chamber II; 141. a return pipe II; 142. a temperature thermocouple; 143 a second filter screen; 144. a return pipe I; 15. a housing; 16. and (5) integrating a controller.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments.
Referring to fig. 1-3, a first embodiment of the present invention provides a device for destroying a residue of a refined medicine based on an oxidation incineration method, which comprises a fan 1, an ozone generator 2, a glass chamber 3, a liquid storage tank 4, a peristaltic pump 5, an atomizer 6, an atomizer head 7, a mist feeding pipe 8, a reaction pipe 9, a heating rod 10, a semiconductor cooling fin 11, a temperature controller 12, a first waste gas absorbing chamber 13, a second waste gas absorbing chamber 14, a housing 15 and an integrated controller 16. The device comprises a fan 1, an ozone generator 2, a glass cavity 3, a liquid storage tank 4, a peristaltic pump 5, an atomizer 6, an atomization nozzle 7, a mist delivery pipe 8, a reaction pipe 9, a heating rod 10, a semiconductor cooling fin 11, a temperature controller 12, a waste gas absorption chamber I13, a waste gas absorption chamber II 14 and an integrated controller 16, wherein the fan 1, the ozone generation 3, the peristaltic pump 5, the atomizer 6 and the heating rod 10 temperature controller 12 are all electrically connected with the integrated controller 16, so that automatic control is realized.
The top of the liquid storage tank 4 is communicated with the outside, and the bottom is connected with the atomizer 6 through a liquid delivery pipe 43. The bottom of the atomizer 6 is provided with a spray head 7 and is connected with a mist feeding pipe 8. The left side of the fog delivering pipe 8 is connected with the glass cavity 2, and the bottom is connected with the inlet of the reaction pipe 8. The bottom of the glass cavity 2 is provided with a fan 1 and an ozone generator 3, and the ozone generator 3 is arranged at the air outlet of the fan 1. The reaction tube 9 is internally provided with a heating rod 10, and a semiconductor cooling fin 11 is provided at the bottom end outer wall surface. The outlet of the reaction tube 9 is connected with the first exhaust gas absorbing chamber 13, the first exhaust gas absorbing chamber 13 is connected with the second exhaust gas absorbing chamber 14 through the first return tube 144, and the second exhaust gas absorbing chamber 14 is connected with the glass cavity through the second return tube 141, as shown in fig. 3.
As shown in fig. 2, the upper end of the liquid storage tank 4 is led to the outside through a liquid inlet pipe 41, the mouth of the liquid inlet pipe 41 is funnel-shaped, so that the liquid residue of the hemp extract can enter the device through the liquid inlet, and the liquid residue to be destroyed can enter the device. The liquid inlet pipe 41 is internally provided with a first filter screen 42 for preventing dust in the air from entering. The left end of the liquid storage tank 4 is connected with the atomizer 6 through a liquid delivery pipe 43. The peristaltic pump 5 is connected to the middle section of the infusion tube 43, the peristaltic pump 5 is electrically connected with the integrated controller 16, and the peristaltic pump 5 is regulated by the integrated controller, so that the accurate control of the liquid flow in the infusion tube 43 is realized
The bottom of the atomizer is provided with a spray head 7 and is connected with a mist feeding pipe 8, and the spray head 7 extends into the mist feeding pipe 8. The atomizer is a net type atomizer, can convert the residue liquid of the refined drugs into micro-nano liquid drops, increases the reaction area of the micro-nano liquid drops, and improves the reaction rate and the treatment efficiency of the residue liquid of the refined drugs. The mist feeding pipe 8 is a quartz glass pipe, the surface of the mist feeding pipe is subjected to hydrophobic treatment, a T-shaped structure is adopted, an upper port is connected with the atomizer 6, a lower port is connected with the reaction pipe 9, and a left port is connected with the glass cavity 3. The inside of the glass cavity 3 is provided with a fan 1 and an ozone generator 2, the ozone generator 2 is arranged at the air outlet of the fan 1, and the generated ozone enters the fog feeding pipe 8 through the fan 1. When the device works, the atomizer 6 converts the residue liquid of the refined drugs into micro-nano liquid drops, and the micro-nano liquid drops enter the mist feeding pipe 8 through the spray head 7 and are mixed with ozone to form aerosol, and finally enter the reaction pipe 9 for reaction. The reaction tube 9 is an alloy tube with high strength and high temperature resistance, and adopts an S-shaped structure, so that the reaction time of aerosol in the reaction tube can be greatly prolonged. The ceramic heating rod 10 is arranged in the reaction tube 9, so that the aerosol in the tube can be heated at constant temperature, the aerosol is promoted to undergo an oxidation incineration reaction in the reaction tube 9, and the rapid, effective and irreversible destruction of the residue liquid of the spermatic medicine is realized.
The inside of the device adopts a closed loop design, wherein a glass cavity 3, a mist delivery pipe 8, a reaction pipe 9 and a waste gas absorption chamber I13 are adopted, a return pipe I144, a waste gas absorption chamber II 14 and a return pipe II 141 are mutually connected to form a closed loop, so that micro-nano liquid drops formed after atomization of the residual liquid of the refined drugs can continuously and circularly react in the device under the action of a fan 1, and the residual liquid of the refined drugs is ensured to be completely destroyed in the device.
The waste gas absorbing chamber I13 is filled with a large amount of solid sodium hydroxide for absorbing harmful gases generated in the oxidation incineration reaction. The left side of the first exhaust gas absorbing chamber 13 is connected with the second exhaust gas absorbing chamber 14 through a first return pipe 144. The second filter screen 143 is installed at the joint of the first return pipe 144 and the second exhaust gas absorbing chamber 14 to prevent the solid particles in the second exhaust gas absorbing chamber from falling. The second exhaust gas absorption chamber 14 is internally provided with a large amount of activated carbon for secondarily purifying the gas exhausted from the first exhaust gas absorption chamber 13, so as to ensure that the harmful gas is completely absorbed. Through the waste gas absorption chamber, the device does not discharge harmful gas outwards in the reaction process, and the safety of surrounding personnel is effectively ensured.
The outer wall of the straight line section at the bottom of the reaction tube 9 is provided with a semiconductor cooling fin 11, and the semiconductor cooling fin 11 is connected with a temperature controller 12 and is used for cooling the gas in the reaction tube 9. The second return pipe 141 is internally provided with a temperature thermocouple 142, and the temperature thermocouple 142 is connected with the temperature controller 12 and is used for detecting the temperature of the gas in the pipe. When the temperature of the gas in the tube is higher than the set value, the temperature controller 12 controls the semiconductor cooling fin 11 to be opened to cool the gas in the reaction tube 9, reduce the temperature in the device, prevent the damage to the instrument caused by the overhigh temperature and ensure the safety of the device.

Claims (7)

1. The utility model provides a device is destroyed to sesame seed essence medicine raffinate based on oxidation incineration method which characterized in that: the device comprises a liquid storage tank, wherein the top of the liquid storage tank is communicated with the outside through a liquid inlet pipe, and the bottom of the liquid storage tank is connected with an atomizer through a liquid delivery pipe; a peristaltic pump is arranged at the middle section of the infusion tube; the bottom of the atomizer is connected with the mist feeding pipe;
the left side of the fog conveying pipe is connected with the glass cavity, and the bottom of the fog conveying pipe is connected with the inlet of the reaction pipe; a fan and an ozone generator are arranged at the bottom of the glass cavity, and the ozone generator is arranged at an air outlet of the fan; a heating rod is arranged in the reaction tube, a semiconductor cooling fin is arranged at the outer wall surface of the bottom end, and an outlet is connected with the first waste gas absorption chamber;
the first waste gas absorption chamber is connected with the second waste gas absorption chamber through a first return pipe, and the second waste gas absorption chamber is connected with the glass cavity through a second return pipe;
the fog delivering pipe adopts a quartz glass pipe and adopts a T-shaped structure, an upper port is connected with the atomizer, a lower port is connected with the reaction pipe, and a left port is connected with the glass cavity; the surface of the fog conveying pipe is subjected to hydrophobic treatment;
and a temperature thermocouple is arranged in the second return pipe and is connected with a temperature controller to detect the temperature of the gas in the second return pipe.
2. The device for destroying the residue of the hemp extract medicine based on the oxidation incineration method according to claim 1, wherein the device is characterized in that: the inlet of the liquid inlet pipe is funnel-shaped, and a filter screen is arranged in the liquid inlet pipe.
3. The device for destroying the residue of the hemp extract medicine based on the oxidation incineration method according to claim 1, wherein the device is characterized in that: the reaction tube adopts an alloy tube and adopts an S-shaped structure.
4. The device for destroying the residue of the hemp extract medicine based on the oxidation incineration method according to claim 1, wherein the device is characterized in that: the heater adopts PTC ceramic heating rod, installs in the reaction tube, carries out constant temperature heating.
5. The device for destroying the residue of the hemp extract medicine based on the oxidation incineration method according to claim 1, wherein the device is characterized in that: and the waste gas absorption chamber I is filled with solid sodium hydroxide.
6. The device for destroying the residue of the hemp extract medicine based on the oxidation incineration method according to claim 1, wherein the device is characterized in that: the waste gas absorbing chamber II is filled with active carbon, and a filter screen is arranged at the joint of the return pipe I.
7. The device for destroying the residue of the hemp extract medicine based on the oxidation incineration method according to claim 1, wherein the device is characterized in that: the temperature controller is connected with the temperature thermocouple and the semiconductor cooling fin, and when the temperature thermocouple detects that the temperature of the gas in the second return pipe is higher than a set value, the temperature controller controls the semiconductor cooling fin to start so as to cool the gas in the reaction pipe.
CN202210091367.3A 2022-01-26 2022-01-26 Device is destroyed to sesame essence medicine raffinate based on oxidation incineration method Active CN114380449B (en)

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Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103359875A (en) * 2012-03-27 2013-10-23 三菱电机株式会社 Waste water treatment method and waste water treatment system
CN105451862A (en) * 2013-07-11 2016-03-30 公立大学法人大阪府立大学 Exhaust gas treatment method, and exhaust gas treatment device
CN106276924A (en) * 2016-08-22 2017-01-04 昆明理工大学 A kind of process chlorosilane residual liquid and the method for waste gas simultaneously
CN108285222A (en) * 2018-03-19 2018-07-17 百世杉集团有限公司 A kind of RE waste water exhaust gas environmental protection recycling and processing device
KR102131679B1 (en) * 2020-03-02 2020-07-09 (주)에코이노베이션 Waste fluid treatment apparatus containing salt and method for treating same
CN111423009A (en) * 2020-02-26 2020-07-17 宁波天扬工业新技术有限公司 Intelligent circulation treatment method and device for paint mist spray water
CN112573721A (en) * 2020-12-29 2021-03-30 深圳市同创环保科技有限公司 Efficient low-temperature condensation waste liquid reduction device and method for treating medical waste liquid
CN213193182U (en) * 2020-07-08 2021-05-14 武汉百富环保工程有限公司 Waste gas purification washing tower
CN217323515U (en) * 2022-01-26 2022-08-30 海宁天纵电子科技有限公司 Device is destroyed to smart medicine residual liquid based on oxidation incineration method

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103359875A (en) * 2012-03-27 2013-10-23 三菱电机株式会社 Waste water treatment method and waste water treatment system
CN105451862A (en) * 2013-07-11 2016-03-30 公立大学法人大阪府立大学 Exhaust gas treatment method, and exhaust gas treatment device
CN106276924A (en) * 2016-08-22 2017-01-04 昆明理工大学 A kind of process chlorosilane residual liquid and the method for waste gas simultaneously
CN108285222A (en) * 2018-03-19 2018-07-17 百世杉集团有限公司 A kind of RE waste water exhaust gas environmental protection recycling and processing device
CN111423009A (en) * 2020-02-26 2020-07-17 宁波天扬工业新技术有限公司 Intelligent circulation treatment method and device for paint mist spray water
KR102131679B1 (en) * 2020-03-02 2020-07-09 (주)에코이노베이션 Waste fluid treatment apparatus containing salt and method for treating same
CN213193182U (en) * 2020-07-08 2021-05-14 武汉百富环保工程有限公司 Waste gas purification washing tower
CN112573721A (en) * 2020-12-29 2021-03-30 深圳市同创环保科技有限公司 Efficient low-temperature condensation waste liquid reduction device and method for treating medical waste liquid
CN217323515U (en) * 2022-01-26 2022-08-30 海宁天纵电子科技有限公司 Device is destroyed to smart medicine residual liquid based on oxidation incineration method

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